CN110470522A - A kind of method of prefabricated different water cut saturation degree rock mass of fracture network sample - Google Patents

A kind of method of prefabricated different water cut saturation degree rock mass of fracture network sample Download PDF

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CN110470522A
CN110470522A CN201910886226.9A CN201910886226A CN110470522A CN 110470522 A CN110470522 A CN 110470522A CN 201910886226 A CN201910886226 A CN 201910886226A CN 110470522 A CN110470522 A CN 110470522A
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water
rock mass
mould
sample
slip casting
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CN110470522B (en
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李连崇
牟文强
朱万成
杨天鸿
于庆磊
刘洪磊
张鹏海
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Northeastern University China
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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B28WORKING CEMENT, CLAY, OR STONE
    • B28BSHAPING CLAY OR OTHER CERAMIC COMPOSITIONS; SHAPING SLAG; SHAPING MIXTURES CONTAINING CEMENTITIOUS MATERIAL, e.g. PLASTER
    • B28B1/00Producing shaped prefabricated articles from the material
    • B28B1/26Producing shaped prefabricated articles from the material by slip-casting, i.e. by casting a suspension or dispersion of the material in a liquid-absorbent or porous mould, the liquid being allowed to soak into or pass through the walls of the mould; Moulds therefor ; specially for manufacturing articles starting from a ceramic slip; Moulds therefor
    • B28B1/265Producing shaped prefabricated articles from the material by slip-casting, i.e. by casting a suspension or dispersion of the material in a liquid-absorbent or porous mould, the liquid being allowed to soak into or pass through the walls of the mould; Moulds therefor ; specially for manufacturing articles starting from a ceramic slip; Moulds therefor pressure being applied on the slip in the filled mould or on the moulded article in the mould, e.g. pneumatically, by compressing slip in a closed mould
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B28WORKING CEMENT, CLAY, OR STONE
    • B28BSHAPING CLAY OR OTHER CERAMIC COMPOSITIONS; SHAPING SLAG; SHAPING MIXTURES CONTAINING CEMENTITIOUS MATERIAL, e.g. PLASTER
    • B28B11/00Apparatus or processes for treating or working the shaped or preshaped articles
    • B28B11/24Apparatus or processes for treating or working the shaped or preshaped articles for curing, setting or hardening
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N1/00Sampling; Preparing specimens for investigation
    • G01N1/28Preparing specimens for investigation including physical details of (bio-)chemical methods covered elsewhere, e.g. G01N33/50, C12Q
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N1/00Sampling; Preparing specimens for investigation
    • G01N1/28Preparing specimens for investigation including physical details of (bio-)chemical methods covered elsewhere, e.g. G01N33/50, C12Q
    • G01N1/36Embedding or analogous mounting of samples
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N1/00Sampling; Preparing specimens for investigation
    • G01N1/28Preparing specimens for investigation including physical details of (bio-)chemical methods covered elsewhere, e.g. G01N33/50, C12Q
    • G01N1/36Embedding or analogous mounting of samples
    • G01N2001/366Moulds; Demoulding

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  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Ceramic Engineering (AREA)
  • Analytical Chemistry (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Biochemistry (AREA)
  • General Health & Medical Sciences (AREA)
  • General Physics & Mathematics (AREA)
  • Immunology (AREA)
  • Pathology (AREA)
  • Physics & Mathematics (AREA)
  • Mechanical Engineering (AREA)
  • Health & Medical Sciences (AREA)
  • Structural Engineering (AREA)
  • Dispersion Chemistry (AREA)
  • Manufacturing & Machinery (AREA)
  • Investigation Of Foundation Soil And Reinforcement Of Foundation Soil By Compacting Or Drainage (AREA)
  • Investigating Strength Of Materials By Application Of Mechanical Stress (AREA)

Abstract

The invention discloses a kind of methods of prefabricated different water cut saturation degree rock mass of fracture network sample, belong to aqueous crack rock experimental study application field in geotechnical engineering.The present invention utilizes the slip casting mold made, according to the spatial shape and its water saturation of different rock crannies, the gas of different content is imported before water-setting build-ups ice, there are different cavitys, ice mould of various shapes in being fabricated to, ice mode spacing is placed at the spatial position of slip casting mold setting and is poured proportioned mud materials, carries out High Temperature Curing after extrusion forming;Can be made by later period High Temperature Curing it is ice melting in rock mass sample, to realize the preparation of different water cut saturation degree rock mass of fracture network sample.The present invention can complete the production to non-through different water cut saturation degree crack rock sample, be conducive to all kinds of experimental studies of different water cut saturation degree crack rock, push the development and application of crack rock mechanics.

Description

A kind of method of prefabricated different water cut saturation degree rock mass of fracture network sample
Technical field
The present invention relates in fields such as Grouting Seepage in Rockmass, the infiltration of aqueous crack rock, aqueous crack rock strength tests In, it realizes the rock mass sample of production water saturation Fracture Networks, meets and the mechanical property of crack rock under different condition is surveyed Examination and test requirements document more particularly to a kind of method of prefabricated different water cut saturation degree rock mass of fracture network sample.
Background technique
Mining engineering, Tunnel Engineering, hydraulic engineering etc. are related to the Geological Engineering of rock mass water reinforcement, due to crack in rock mass Presence change the mechanical property of original rock mass, and often containing the water that different water cut saturation degree is presented in rock cranny Point.In view of the importance of the crack rock in key project construction, need to there are the crack rock of different water cut saturation degree into Row experiment of machanics, but influenced by laboratory facilities and the prior art, it tends not to realization and acquires sample in protolith, therefore need The laboratory scale experiment to crack rock is realized using rock mass sample.
And for the construction of the sample of rock mass containing natural fissure, people are often through the addition scraps of paper, 3d printing rock mass mold etc. Means complete the building to single crack rock.Such as a kind of " preparation of the intermittent fracture rock mass sample based on 3D printing technique Method " (ZL201511019619.8) disclose it is a kind of using 3D printing technique make simple mould, realize intermittent fracture rock The preparation of body sample, but constructed using the printing that the mold is only able to achieve single or several discontinuous cracks, and this method is into right Intermittent fracture rock mass is applicable in, and can not achieve the composition of complicated Fracture Networks, and printing shaping forms the precast construction in sample crack Not being pulled out has larger impact to the performance of crack rock, and cannot consider situation aqueous in crack;A kind of " interior Single Fracture Rock sample preparation facilities " (ZL201410052815.4) disclose a kind of preparation method of single crack rock, but cannot The case where considering Fracture Networks, can not consider situation aqueous in crack, can not achieve the reaction in different saturation crack;And And intrinsic fracture is often moisture content, and moisture is very big on the influence of the performance of crack rock, fails to consider aqueous in crack Situation.
Currently lack effective production method and realize that addition constructs Fracture Networks identical with geology rock mass in test specimen, especially Its simple experiment production method for being a lack of the rock mass of fracture network containing different saturation moisture in crack.
Summary of the invention
It the problems of is made for current saturation degree containing different water cut and Fracture Networks crack rock sample, to meeting The preparation method of intrinsic fracture sample proposes a kind of method of prefabricated different water cut saturation degree rock mass of fracture network sample, Purpose, which is to provide, a kind of can be realized to different water cut situation, different cracks form, the staggered crack rock of Fracture Networks Sample production method provides strong technical support and experimental basis for crack rock test, while reducing experimentation cost, makes to try It tests simple, cheap, easy to operate.
To achieve the above object, specific technical solution adopted by the present invention is as follows:
A kind of method of prefabricated different water cut saturation degree rock mass of fracture network sample, method includes the following steps:
The first step measures rock cranny parameter
Measure the geometrical length in crack in the rock mass in engineering site, width, shape, water saturation, crack position, more The interlayer and false relation in crack, so that it is determined that meeting the actual test dimensional parameters of engineering.
Second step prepares ice mould
2.1) meet the Fracture Networks water mould for the test dimensional parameters that the first step determines using wood materials production, water mould is wanted It can be realized and be filled with water and guarantee not generating big deformation in ice conditions;
2.2) all types of water moulds that step 2.1) makes are fixedly placed under refrigerated environment, and it is straight to pour water in Xiang Shuimo To being full of, while the air of different content is filled according to the crack water saturation that the first step determines in water mould;
2.3) freeze ice until after ice cube molding after the water cooling in water mould, remove water mould, be fabricated to inside and contain different skies The ice mould of chamber, to realize the characterization to different water cut saturation degree.
Third step prepares rock mass sample forming device and constructs rock mass sample
3.1) rock mass sample forming device includes pressurization beam 1, hydraulic column 2, connector 3, capping 4 and slip casting mold 7;Pressurization Beam 1 is fixed on floor, and hydraulic column 2 is installed at middle part;Slip casting mold 7 is placed in immediately below hydraulic column 2, slip casting mold 7 pushes up Portion's installation capping 4, and connector 3 is installed covering 4 upper surfaces, it realizes and pressurizes to 7 top plate of slip casting mold;
3.2) according to the crevice space structure of first step measurement and position, second step is made into molding ice mould and is placed on note It starches at spatial position set by mold 7, pours proportioned mud materials into slip casting mold 7 under cryogenic, and Using pressurization beam 1, hydraulic column 2 and connector 3 to the slow pressing formation of capping 4 of slip casting mold 7 at the top of slip casting mold 7, directly To rock mass sample stable molding;
3.3) after rock mass sample preparatory processing molding, slip casting mold 7 is removed, rock mass sample is placed in the high temperature environment Maintenance guarantees that the ice mould inside rock mass sample melts as water and fills internal crack.
Further, in the step 2.2), water mould be have different shape and size inner surface film laying it is removable Wood module is filled, component is required to realize water-filling and can realize complete disassembly;And every group of 8 both ends of water mould or middle part are installed with Stomata 9 (achievable temporary sealing) pours into water to expiring and sealing in water mould 8, by 8 end of water mould or the gas of medium position Hole 9 is to quantitative gas is inputted inside water mould 8, and other end stomata 9 then flows out the water of equal quantities, to guarantee the standard of water saturation True property, then its water saturation is always to be filled with water to subtract after displacement again divided by being always filled with water.
Further, in the step 3.2), other rock mass spaces around the ice mould of crack, purpose should be first poured as early as possible It is that ice mould melts destruction Fracture Networks geometry and distribution character in order to prevent.
Further, the slip casting mold 7 is the square steel plate group component of size 300mm*300mm*300mm.
Further, the pressurization beam 1 is steel " shape of the mouth as one speaks " plate-girder that height is 1000mm.
Beneficial effects of the present invention: the present invention provides effective rock mass sample production methods, can guarantee Fracture Networks The shape of ice mould, size, spatial position keep stablizing without changing.The present invention realizes the production of aqueous crack rock, In particular for the rock mass sample production containing different water cut degree crack, to further studying aqueous crack rock mechanical property Matter, the influence for studying water saturation, study of various test, such as Grouting Seepage in Rockmass, crack rock permeability, crack rock pressure Rip current is dynamic etc. to be of great significance.
Detailed description of the invention
Fig. 1 is a kind of workflow of the method for prefabricated different water cut saturation degree rock mass of fracture network sample of the invention Figure;
Fig. 2 is a kind of device arrangement of the method for prefabricated different water cut saturation degree rock mass of fracture network sample of the invention Figure;
Fig. 3 is a kind of water mould signal of the method for prefabricated different water cut saturation degree rock mass of fracture network sample of the invention Figure;
In figure: 1 pressurization beam;2 hydraulic columns;3 connectors;4 cappings;5 ice moulds;6 air voids;7 slip casting molds;8 water moulds;9 Stomata.
Specific embodiment
A specific embodiment of the invention is described in detail below in conjunction with technical solution and attached drawing.
As shown in Figure 1, a kind of method of prefabricated different water cut saturation degree rock mass of fracture network sample, is specifically divided into three ranks Section: the 1. preparation stage, the stage need the crack rock to be studied comprising fissare geometric parameter, crack position, Network interlocks and all kinds of parameters such as water saturation are determined, so that construction is more in line with the actual crack rock sample of engineering Model;2. constructing ice mould, which mainly makees to contain according to fixed fracture network parameter using wooden water molding The ice mould of specified air content meets the water saturation requirement of rock cranny;3. structural fracture rock mass, by ice mould in the stage According to designed spatial position, proportioned slurry is placed in slip casting mold and poured into, after grouting material stable molding to be added High Temperature Curing forms aqueous (different water cut saturation degree) crack rock.
As shown in Fig. 2, a kind of method of prefabricated different water cut saturation degree rock mass of fracture network sample of the present invention passes through rock mass Sample forming device realizes that the device includes pressurization beam 1, hydraulic column 2, connector 3, capping 4 and slip casting mold 7;Pressurization beam 1 be Hydraulic column 2 is installed at steel " shape of the mouth as one speaks " plate-girder that the height being fixed on floor is 1000mm, middle part;Slip casting mold 7 is size The square steel plate group component of 300mm*300mm*300mm, top is equipped with moveable capping 4, and pacifies covering 4 upper surfaces Load junctor 3;Slip casting mold 7 is placed in immediately below hydraulic column 2, is realized using hydraulic column 2, connector 3 in 1 pair of beam note of pressurization It starches mold 7 and its interior slurry applies pressure.
As shown in figure 3, according to location parameter production water mould 8 and film laying sealing, the both ends or middle part of every group of water mould 8 are equal It stays and sets stomata 9, water is poured into expiring and sealing in water mould 8, the stomata 9 by 8 one end of water mould or medium position is internally defeated Enter quantitative gas, the other end then flows out the water of equal quantities, guarantees the certainty of water saturation, then moves to entire water mould Freezing environment freezes, and surrounding water mould 8 and film are removed after the water freezing in water mould;Ice mould 5 containing air void 6 is placed into In slip casting mold 7, the slurry that proportion is completed is poured into slip casting mold, is added using pressurization beam 1, hydraulic column 2, connector 3, capping 4 It is molded, High Temperature Curing after molding.
Method concrete operations of the present invention are as follows:
The first step measures rock cranny parameter
Measure engineering site in rock mass in crack geometrical length, width, shape, water saturation, more cracks interlayer And false relation, determine test dimensional parameters;
Second step prepares ice mould
(1) meet the Fracture Networks water mould 8 of all types of test dimensional parameters using wood materials production, water mould 8 requires energy Enough realize is filled with water and guarantees not generating big deformation in ice conditions;
(2) all types of water moulds 8 is fixedly placed under refrigerated environment, and poured water into water mould 8 up to being full of, while according to The air of different content is filled in water mould 8 according to determining crack water saturation;
(3) to the water cooling in water mould 8 freeze ice until ice cube form, remove water mould 8, be fabricated in have gas with various gap 6 ice mould 5 of various shapes, to realize the characterization to different water cut saturation degree;
Third step prepares rock mass sample forming device and constructs rock mass sample
(1) according to the crevice space structure of first step measurement and position, ice mould 5 is placed on set by slip casting mold 7 At spatial position, proportioned mud materials are poured under cryogenic, to prevent 5 fast melt of stagnant ice mould;And by pressurization Beam 1 and hydraulic column 2, the capping 4 using connector 3 to slip casting mold 7 slowly applies active force and forms, until rock mass sample forms Stablize;
(2) after rock mass sample preparatory processing molding, slip casting mold 7 is removed, rock mass placement is conserved in the high temperature environment, Ice mould inside guaranteeing melts as water and fills internal crack.
Method equipment making proposed by the invention is simple, and method process is simply easily implemented, low in cost, in laboratory It is easy to accomplish.The present invention can be realized the production of the arbitrarily rock mass sample containing crack, contain in particular for inside is not passed through Water saturation, Fracture Networks crack rock production is conducive to push crack rock mechanics, Flow In Jointed Rock Masses mechanics, split The development of gap rock mass freeze thawing mechanics.

Claims (5)

1. a kind of method of prefabricated different water cut saturation degree rock mass of fracture network sample, which is characterized in that this method includes as follows Step:
The first step measures rock cranny parameter
Measure geometrical length, the width, shape, water saturation, crack position, more cracks in crack in the rock mass in engineering site Interlayer and false relation, so that it is determined that meeting the actual test dimensional parameters of engineering;
Second step prepares ice mould
2.1) meet the Fracture Networks water mould for the test dimensional parameters that the first step determines using wood materials production, water mould is wanted can Realization is filled with water and guarantees not generating big deformation in ice conditions;
2.2) the water mould fixed placement that step 2.1) makes is poured water under refrigerated environment, and in Xiang Shuimo until being full of, simultaneously The crack water saturation determining according to the first step fills the air of different content in water mould;
2.3) freeze ice to the water cooling in water mould until ice cube forms, dismounting water mould is fabricated to the internal ice containing air void Mould, to realize the characterization to different water cut saturation degree;
Third step prepares rock mass sample forming device and constructs rock mass sample
3.1) rock mass sample forming device includes pressurization beam, hydraulic column, connector, capping and slip casting mold;Pressurization beam is fixed on On floor, hydraulic column is installed at middle part;Slip casting mold is placed in immediately below hydraulic column, the installation capping of slip casting die top, and Connector is installed in capping upper surface, realization pressurizes to slurry in slip casting mold;
3.2) according to the crevice space structure of first step measurement and position, second step is made into molding ice mould and is placed on slip casting mould At the set spatial position of tool, proportioned mud materials are poured into slip casting mold under cryogenic, and in slip casting Capping of the die top using pressurization beam, hydraulic column and connector to slip casting mold slowly applies active force and forms, until rock mass Sample stable molding;
3.3) after rock mass sample preparatory processing molding, slip casting mold is removed, the placement of rock mass sample is conserved in the high temperature environment, Guarantee that the ice mould inside rock mass sample melts as water and fills internal crack.
2. a kind of method of prefabricated different water cut saturation degree rock mass of fracture network sample according to claim 1, feature It is, in the step 2.2), water mould is the detachable wooden component of laid inside film;And the both ends or middle part of every group of water mould It is installed with stomata, water is poured into water mould to full and seal, by the stomata of water mould end or medium position into water mould Portion inputs gas, and other end stomata then flows out the water of equivalent, to realize the accurate characterization of water saturation.
3. a kind of method of prefabricated different water cut saturation degree rock mass of fracture network sample according to claim 1 or 2, special Sign is that the slip casting mold is the square steel plate group component of size 300mm*300mm*300mm.
4. a kind of method of prefabricated different water cut saturation degree rock mass of fracture network sample according to claim 1 or 2, special Sign is that the pressurization beam is steel " shape of the mouth as one speaks " plate-girder that height is 1000mm.
5. a kind of method of prefabricated different water cut saturation degree rock mass of fracture network sample according to claim 3, feature It is, the pressurization beam is steel " shape of the mouth as one speaks " plate-girder that height is 1000mm.
CN201910886226.9A 2019-09-19 2019-09-19 Method for prefabricating fracture network rock mass samples with different water saturation degrees Active CN110470522B (en)

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CN111220444A (en) * 2020-01-17 2020-06-02 中国地质大学(武汉) Method for preparing concealed water-containing body
CN111976362A (en) * 2020-08-27 2020-11-24 华南理工大学 Manufacturing method of concrete handicraft with hollow structure
CN113295484A (en) * 2021-04-21 2021-08-24 重庆交通大学 Method for manufacturing concrete test piece for simulating water-containing cavity defect
CN114166613A (en) * 2021-12-16 2022-03-11 广西大学 Device and method for quickly manufacturing fractured rock samples in pressure environment
CN114233380A (en) * 2021-12-27 2022-03-25 徐州格润矿山技术开发有限公司 Method for conducting overburden rock isolation grouting filling on coal-based solid waste
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CN111220444A (en) * 2020-01-17 2020-06-02 中国地质大学(武汉) Method for preparing concealed water-containing body
CN111976362A (en) * 2020-08-27 2020-11-24 华南理工大学 Manufacturing method of concrete handicraft with hollow structure
CN113295484A (en) * 2021-04-21 2021-08-24 重庆交通大学 Method for manufacturing concrete test piece for simulating water-containing cavity defect
CN113295484B (en) * 2021-04-21 2024-01-26 重庆交通大学 Method for manufacturing concrete test piece for simulating water-containing cavity defect
CN114166613A (en) * 2021-12-16 2022-03-11 广西大学 Device and method for quickly manufacturing fractured rock samples in pressure environment
CN114233380A (en) * 2021-12-27 2022-03-25 徐州格润矿山技术开发有限公司 Method for conducting overburden rock isolation grouting filling on coal-based solid waste
CN114233380B (en) * 2021-12-27 2023-12-05 徐州格润矿山技术开发有限公司 Method for isolating, grouting and filling overlying strata by using coal-based solid wastes
CN115078121A (en) * 2022-08-23 2022-09-20 太原理工大学 Indirect visual rock multi-cluster fracturing indoor test device and method
CN115078121B (en) * 2022-08-23 2022-12-09 太原理工大学 Indirect visual rock multi-cluster fracturing indoor test device and method

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Inventor after: Mou Wenqiang

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