CN110404095A - A kind of natural plants deodorant liquid and preparation method thereof - Google Patents
A kind of natural plants deodorant liquid and preparation method thereof Download PDFInfo
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- CN110404095A CN110404095A CN201910767163.5A CN201910767163A CN110404095A CN 110404095 A CN110404095 A CN 110404095A CN 201910767163 A CN201910767163 A CN 201910767163A CN 110404095 A CN110404095 A CN 110404095A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61L—METHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
- A61L9/00—Disinfection, sterilisation or deodorisation of air
- A61L9/01—Deodorant compositions
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61L—METHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
- A61L9/00—Disinfection, sterilisation or deodorisation of air
- A61L9/01—Deodorant compositions
- A61L9/013—Deodorant compositions containing animal or plant extracts, or vegetable material
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61L—METHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
- A61L2209/00—Aspects relating to disinfection, sterilisation or deodorisation of air
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Abstract
The present invention relates to deodorant liquid technical field, it is related to a kind of natural plants deodorant liquid and preparation method thereof.The natural plants deodorant liquid following raw materials according is made according to following mass fractions: 1-50 parts of folium eucalypti extract, 20-30 parts of Cortex cinnamomi japonici (Ramulus Cinnamomi) extract, 15-30 parts of citrene, 1-10 parts of borneol, 1-10 parts of peppermint oil and 1-10 parts of camphor tree oil.Deodorant liquid disclosed in this invention uses natural plants to carry out classification extraction completely, take full advantage of the physical property of plant itself, further simplify extraction step, and its effective ingredient is all extracted from natural plants, it is without any side effects to people and animals, it, can fast deodorization without any secondary pollution, it is a kind of pure natural environment protection deodorising product, it is nontoxic；And deodorization liquid and preparation method thereof disclosed in this invention simplifies preparation process flow, reduces production cost, improves production efficiency, solves the defect that natural plant deodorant preparation cost is high in the prior art, while also improving the efficiency of extraction.
Description
Technical field
The present invention relates to deodorant liquid technical fields, more specifically to a kind of natural plants deodorant liquid and its preparation side
Method.
Background technique
Deodorant liquid is a kind of for removing the reagent of stink, mainly includes plant deodorant, physical deodorization agent, absorption
Property deodorant, masking deodorant, chemical deodorizing agent and salt compounds deodorant.Wherein,
Physical deodorization agent is to carry out deodorization by physical method not change using the physical property of deodorant or foul smell
Odor components as a result, only changing the local concentration of foul smell, or perhaps relative concentration.It common are absorbing and deodorizing agent, cover
Deodorant etc..
Adsorptivity deodorant is to use the intermolecular Van der Waals force of matter utilization with excellent adsorption capacity by malodor molecule
The deodorizing methods being adsorbed in porous material, deodorant specific surface is big, it is empty hold big, it is dense usually to adsorb stench in reduction air
Degree is to achieve the purpose that deodorization.
Masking deodorant is with the substances such as natural aromatic oil, fragrance masking stench.It is smelly mainly for being much difficult to remove
Taste or the more troublesome environment of deodorization, mix several gases for having gas position, in proportion to mitigate stench.
Chemical deodorizing agent is to utilize oxidation, reduction decomposition, neutralization reaction, addition reaction, condensation reaction, ion-exchange reactions
Become odorless substance Deng by the odorant of generation to eliminate foul smell.
The oxidants such as NaClO, chlorine by foul smell organic sulfur and the substances such as organic amine to be oxidized to stink lighter or molten
The higher compound of Xie Du, then acid, Alkali absorption purify.Use salt compounds as deodorant, for example, ferrous ion and
Ascorbic acid inhibits to aoxidize together, reacts with odorants such as ammonia, mercaptan and is allowed to become odorless substance；Ferric iron derivative,
The ligand of metal complex occurs displacement with mercaptan or sulphur and reacts, and converts odorless substance for odorant.
Patent " CN201510973225.X " discloses a kind of preparation method of high-efficiency plant deodorant, it includes extracting solution
The preparation of A, the preparation of extracting solution B, feeding and mixing step；The object of the present invention is to provide a kind of systems of high-efficiency plant deodorant
Preparation Method simplifies the extraction process of plant deodorant, thereby reduces production cost, while substantially increasing effective active again
The content of ingredient, the plant deodorant prepared can fundamentally remove stink by reacting with foul smell molecule.Specially
The preparation method that sharp " CN201010123469.6 " discloses a kind of natural plant deodorant is that the plant leaf that will have been picked is used
Power is 20-60W/g microwave irradiation, and leaf tiles with a thickness of 5-30mm, microwave frequency 2450MHZ, irradiation time 1-3
Minute, it dries in the shade after irradiation；The crushing up leaves that will be dried in the shade, with mass concentration be 20%-80% ethanol water extract, leaf with
The weight ratio of ethanol water is 1: 6-10, and 50-80 DEG C of extraction temperature, extraction time about 10-60 minutes, raw material extracted 2-3
Secondary, merging the filtrate extracted every time is extracting solution；Extracting solution is concentrated under reduced pressure, until it can't detect ethyl alcohol, is filtered, filter
Liquid removes impurity with macroporous adsorbent resin column chromatography, and filtrate with macroporous adsorbent resin column chromatography process is eluted with water first to stream
When liquid is faint yellow out, then with mass concentration it is 40-80% ethanol elution, eluent is detected with hydrochloric acid-magnesium powder method, from
Detection has flavones to start to collect eluent, until detecting without flavones；Recycling ethyl alcohol is concentrated under reduced pressure in the eluent being collected into
And dry powder is made, obtain the dry powder of natural plant deodorant.The present invention has low production cost, simple process, pollution-free, effect
The advantages of fruit is good, easy to use and flexible.Patent " CN201510973225.X " is although disclose a kind of high-efficiency plant deodorant
Preparation method, but this method one side preparation process is complicated, and raw material used in another aspect are numerous, and need using certain
The surfactant lamp raw material of industry of amount, is not fully prepared by natural plants, to increase the natural deodorant
Preparation cost；In addition, patent " CN201010123469.6 " is although also disclose a kind of preparation method of natural plant deodorant,
But the process requirement constantly removes the flavones in filtrate with ethanol elution, so that entire preparation flow needs constantly to repeat Huang
Ketone elution processes seriously affect the preparation efficiency of the natural plant deodorant, and the natural plant deodorant removes ammonia
Smelly efficiency is preferable, and low to other foul smell and pollution sources odor removal efficient.Therefore, it is few, at low cost, high how to prepare a kind of raw material
The natural plant deodorant of efficiency has become current environmental protection industry (epi) urgent problem to be solved.
Summary of the invention
In view of this, the present invention provides a kind of natural plants deodorant liquid and preparation method thereof, to solve in the prior art
The defect of natural plant deodorant preparation cost height and low efficiency.
A kind of natural plants deodorant liquid, including following raw materials according are made according to following mass fractions: folium eucalypti extract 1-50
Part, 20-30 parts of Cortex cinnamomi japonici (Ramulus Cinnamomi) extract, 15-30 parts of citrene, 1-10 parts of borneol, 1-10 parts of peppermint oil and camphor tree oil 1-10
Part.
Preferably, including following raw materials according is made according to following mass fractions: 30-50 parts of folium eucalypti extract, Cortex cinnamomi japonici (Ramulus Cinnamomi) extract
20-30 parts, 15-30 parts of citrene, 4-10 parts of borneol, 4-8 parts of peppermint oil and 1-5 parts of camphor tree oil.
Preferably, including following raw materials according is made according to following mass fractions: 30 parts of folium eucalypti extract, Cortex cinnamomi japonici (Ramulus Cinnamomi) extract 25
Part, 25 parts of citrene, 10 parts of borneol, 5 parts of peppermint oil and 5 parts of camphor tree oil.
In the technical scheme, the main composition of the folium eucalypti extract: 1, 8-Cineole (80% or more), amphene, water
Celery alkene, terpinol, geranyl alcohol, isopentyl aldehyde, citronellal and piperitone etc..Property: colourless or yellowish liquid.In peculiar clear
Cool spine folium eucalypti fragrance simultaneously has peppery mouth refrigerant sense, fragrance is strongly without lasting with a little medicine gas with a few minutes camphor smell.Have certain
The effect of mould proof and sterilization and anticorrosion.It is practically insoluble in water, is dissolved in ethyl alcohol, dehydrated alcohol, in oil & fat.Flash-point is 50 DEG C.
The main component of the Cortex cinnamomi japonici (Ramulus Cinnamomi) extract: cinnamic acid (98.2%), secondly for α-phellandrene, 1,8- cineole,
P-cymene, camphor, linalool, β-carypohyllene, α-Ylangene, alpha-terpineol, geraniol, acid methylester, ethyl cinnamate, cloves
Phenol, cinnamyl alcohol etc..Fragrance: have distinctive pungent strong, the warm sweet tea aroma characteristic of Chinese cinnamon: the time places or is placed in air,
Cinnamon oil, which can be aoxidized gradually, becomes auburn thick liquid.
The citrene is widely present in natural plants essential oil.Wherein mainly there are mandarin orange oil, lemon containing d-isomer
Lemon oil, petit grain oil, light camphor oil etc..There is peppermint oil etc. containing levo form.There are neroli oil, China fir oil and light camphor oil containing raceme
Deng.When manufacturing this product, fractionation is carried out by above-mentioned essential oil respectively and is produced, terpenes can also be extracted from general essential oil, or adding
During work camphorated oil and artificial camphor, it is made as by-product.Gained dipentene can obtain limonene through distilation.With pine
Raw material is made in fuel-economizing, is fractionated, cuts australene, and through isomerization amphene, then fractionation is obtained.The by-product of amphene is double penta
Alkene.In addition, can also by-product dipentene when being hydrated terpinol processed with turpentine oil.
The borneol is colorless and transparent or white translucent the crisp crystallization of sheet；Gas faint scent, it is acrid flavour, cool；Have volatility,
Easily distillation, lights generation dense smoke, and have the flame with light.Borneol is readily soluble in ethyl alcohol, chloroform, gasoline or ether, several in water
It is insoluble.D-Bomeol fusing point is 208 DEG C, and 212 DEG C of boiling point, L-Borneol fusing point is 204 DEG C, 210 DEG C of boiling point.
The peppermint oil is pistachio liquid or flaxen supernatant liquid.It is slightly frozen into solid to the cold.In strong
Peppermint fragrance and refrigerant slight bitter taste.With the passing of time, color gradual change is deep for storage.This product can be mixed arbitrarily with ethyl alcohol, chloroform or ethyl alcohol.Have
The peppermint fragrance of pure fragrance has and strong alters permeability with pungent and refrigerant.There is a large amount of clear crystal to be precipitated when temperature is lower.
With the passing of time then color gradual change is deep for storage, and matter gradual change is viscous.It is soluble easily in water, it can arbitrarily be mixed with alcohol, ether, chloroform etc..
The camphor tree oil main component includes camphor (35%-50%), a- firpene, camphene, phellandrene, terpineol, acetic acid
Geraniol, isopentyl aldehyde, citronellal and piperitone.Its main performance is anti-corrosion, and anti-inflammatory is antiviral, sterilization, resolving sputum, and cough-relieving is excited
Circulation, sweating is rubescent, mosquito repellent.Taste slightly rushes nose, band camphor breath, colourless or yellowish liquid, density 0.890- to be pure and fresh
0.906, evaporation rate is very fast.
Preferably, the preparation flow of the folium eucalypti extract are as follows: first weigh eucalyptus branches and leaves and be placed in extraction kettle, then use revolving speed
Eucalyptus branches and leaves are crushed for the pulverizer of 2000r/min；Then with 70% ethyl alcohol of 60 times of volumes of raw material after co-grinding
The first filtrate and the first filter residue is obtained by filtration after impregnating 20h；Then it is impregnated again with 40% ethyl alcohol of 30 times of volumes of the first filter residue, and
Mixed liquor is stirred with the mixing speed of 200r/min, the second filtrate is obtained after 12h；By the first filtrate and the second filtrate
Mixing, ethyl alcohol therein is recycled by way of distillation, obtains folium eucalypti extract.
In the technical scheme, it since the material is soft for eucalyptus branches and leaves, in crushing process, if crushing excessive velocities, is easy
The molecular structure in eucalyptus branches and leaves is damaged, extract is caused to fail；If crushing excessive velocities, the extract of eucalyptus branches and leaves is caused to extract
Speed is slower, and effective extract can not be extracted by resulting even in, and is found according to experiment, removes powder with the revolving speed of 2000r/min
The crushing effect of broken eucalyptus branches and leaves be it is optimal, eucalyptus branches and leaves can be ground into the pulverized particles of relative ideal；In addition, with ethyl alcohol
Extraction process in, since 1, 8-Cineole is distributed to each corner of eucalyptus branches and leaves, extracted first with the ethyl alcohol of 70% high concentration
To the first filtrate and the first filter residue；Then the second filter residue is extracted again with the ethyl alcohol of concentration in 40% again, and in reextraction mistake
Journey simultaneously needs to be stirred to accelerate rate of extraction mixed liquor with the mixing speed of 200r/min, thus by eucalyptus branches and leaves
The active principles such as 1,8- Cineole extract.In the technical scheme, using two step extractions, using various concentration and not
With the alcohol extraction liquid that stirring requires, both the active principles such as 1, 8-Cineole in eucalyptus branches and leaves can rapidly and efficiently be extracted
Come, reduces extraction time；The usage amount that alcohol extraction liquid can also be reduced achievees the purpose that efficient Rapid Extraction.
Preferably, the preparation flow of the Cortex cinnamomi japonici (Ramulus Cinnamomi) extract are as follows: first weigh cassia bark and be placed in extraction kettle, be then with revolving speed
The pulverizer of 3000r/min crushes eucalyptus branches and leaves；Then it is soaked with 80% ethyl alcohol of 20 times of volumes of raw material after co-grinding
The first filtrate and the first filter residue is obtained by filtration after bubble 30h；Then it is impregnated again with 50% ethyl alcohol of 10 times of volumes of the first filter residue, and with
The mixing speed of 500r/min is stirred mixed liquor, and the second filtrate is obtained after 20h；First filtrate and the second filtrate are mixed
It closes, ethyl alcohol therein is recycled by way of distillation, obtains Cortex cinnamomi japonici (Ramulus Cinnamomi) extract.
In the technical scheme, since the material of cassia bark is harder, in crushing process, if crushing excessive velocities, it is easy damage
Molecular structure in bad cassia bark, causes extract to fail；If crush excessive velocities, cause the extract rate of extraction of cassia bark compared with
Slowly, effective extract can not be extracted by resulting even in, and be found according to experiment, go to crush cassia bark with the revolving speed of 3000r/min
Crushing effect be it is optimal, cassia bark can be ground into the pulverized particles of relative ideal；In addition, in the extraction process with ethyl alcohol
In, since cinnamic acid is distributed to each corner of cassia bark, and extraction difficulty is bigger than the extraction difficulty of folium eucalypti extract, first with 80%
The first filtrate and the first filter residue is obtained by extraction in the ethyl alcohol of high concentration；Then the second filter is extracted again with the ethyl alcohol of concentration in 50% again
Slag, and in reextraction process and need to be stirred to accelerate rate of extraction mixed liquor with the mixing speed of 500r/min,
To which the active principles such as cinnamic acid in cassia bark be extracted.In the technical scheme, using two step extractions, difference is utilized
The alcohol extraction liquid that concentration and different stirring require both can rapidly and efficiently extract the active principles such as cinnamic acid in cassia bark
Come, reduces extraction time；The usage amount that alcohol extraction liquid can also be reduced reaches the mesh of efficient Rapid Extraction Cortex cinnamomi japonici (Ramulus Cinnamomi) extract
's.
Preferably, the preparation flow of the citrene are as follows: first weigh lemonlike citrus leaf and be placed in extraction kettle, be then with revolving speed
The pulverizer of 1000r/min crushes eucalyptus branches and leaves；Then it is soaked with 40% ethyl alcohol of 20 times of volumes of raw material after co-grinding
The first filtrate and the first filter residue is obtained by filtration after bubble 20h；Then it is impregnated again with 20% ethyl alcohol of 10 times of volumes of the first filter residue, and with
The mixing speed of 200r/min is stirred mixed liquor, and the second filtrate is obtained after 12h；First filtrate and the second filtrate are mixed
It closes, ethyl alcohol therein is recycled by way of distillation, obtains citrene liquid.
In the technical scheme, since the material of lemonlike citrus leaf is relatively soft, in crushing process, if crushing excessive velocities, hold
Molecular structure easy to damage, causes extract to fail；If crush excessive velocities, cause the extract rate of extraction of lemonlike citrus leaf compared with
Slowly, effective extract can not be extracted by resulting even in, and be found according to experiment, go to crush cassia bark with the revolving speed of 1000r/min
Crushing effect be it is optimal, lemonlike citrus leaf can be ground into the pulverized particles of relative ideal；In addition, in the extraction with ethyl alcohol
Cheng Zhong, since citrene is distributed to each corner of lemonlike citrus leaf, extraction difficulty is smaller than the extraction difficulty of folium eucalypti extract, first with
The first filtrate and the first filter residue is obtained by extraction in the ethyl alcohol of 40% high concentration；Then is extracted again with the ethyl alcohol of concentration in 20% again
Two filter residues, and in reextraction process and need to be stirred mixed liquor with the mixing speed of 200r/min to accelerate extraction speed
Degree, so that the active principles such as citrene in lemonlike citrus leaf be extracted.In the technical scheme, using two step extractions,
The alcohol extraction liquid required using various concentration and different stirring, both can be fast by active principles such as citrenes in lemonlike citrus leaf
Speed efficiently extracts, and reduces extraction time；The usage amount that alcohol extraction liquid can also be reduced reaches efficient Rapid Extraction lemon
The purpose of terpenes liquid.
Preferably, the preparation flow of the folium eucalypti extract are as follows: first weigh eucalyptus branches and leaves and be placed in extraction kettle, then use revolving speed
Eucalyptus branches and leaves are crushed for the pulverizer of 2000r/min；Then with 70% ethyl alcohol of 60 times of volumes of raw material after co-grinding
The first filtrate and the first filter residue is obtained by filtration after impregnating 20h；Then it is impregnated again with 40% ethyl alcohol of 30 times of volumes of the first filter residue, and
Mixed liquor is stirred with the mixing speed of 200r/min, the second filtrate is obtained after 12h；By the first filtrate and the second filtrate
Mixing, ethyl alcohol therein is recycled by way of distillation, obtains folium eucalypti extract.
In the technical scheme, it since the material is soft for eucalyptus branches and leaves, in crushing process, if crushing excessive velocities, is easy
The molecular structure in eucalyptus branches and leaves is damaged, extract is caused to fail；If crushing excessive velocities, the extract of eucalyptus branches and leaves is caused to extract
Speed is slower, and effective extract can not be extracted by resulting even in, and is found according to experiment, removes powder with the revolving speed of 2000r/min
The crushing effect of broken eucalyptus branches and leaves be it is optimal, eucalyptus branches and leaves can be ground into the pulverized particles of relative ideal；In addition, with ethyl alcohol
Extraction process in, since 1, 8-Cineole is distributed to each corner of eucalyptus branches and leaves, extracted first with the ethyl alcohol of 70% high concentration
To the first filtrate and the first filter residue；Then the second filter residue is extracted again with the ethyl alcohol of concentration in 40% again, and in reextraction mistake
Journey simultaneously needs to be stirred to accelerate rate of extraction mixed liquor with the mixing speed of 200r/min, thus by eucalyptus branches and leaves
The active principles such as 1,8- Cineole extract.In the technical scheme, using two step extractions, using various concentration and not
With the alcohol extraction liquid that stirring requires, both the active principles such as 1, 8-Cineole in eucalyptus branches and leaves can rapidly and efficiently be extracted
Come, reduces extraction time；The usage amount that alcohol extraction liquid can also be reduced achievees the purpose that efficient Rapid Extraction.
Preferably, the preparation flow of the peppermint oil are as follows: first weigh the fresh cauline leaf of peppermint and be placed in extraction kettle, then use and turn
Speed is that the pulverizer of 1000r/min crushes eucalyptus branches and leaves；Then with 40% second of 20 times of volumes of raw material after co-grinding
The first filtrate and the first filter residue is obtained by filtration after impregnating 20h in alcohol；Then it is impregnated again with 20% ethyl alcohol of 10 times of volumes of the first filter residue,
And mixed liquor is stirred with the mixing speed of 200r/min, the second filtrate is obtained after 12h；By the first filtrate and the second filtrate
Mixing, ethyl alcohol therein is recycled by way of distillation, obtains peppermint oil.
In the technical scheme, since the material of the fresh cauline leaf of peppermint is relatively soft, in crushing process, if crushing speed mistake
Fastly, then the molecular structure being easily damaged in the fresh cauline leaf of peppermint, causes extract to fail；If crushing excessive velocities, cause thin
The extract rate of extraction of the fresh cauline leaf of lotus is slower, and effective extract can not be extracted by resulting even in, and is found according to experiment,
With the revolving speed of 1000r/min go the crushing effect for crushing cassia bark be it is optimal, the fresh cauline leaf of peppermint can be ground into opposite reason
The pulverized particles thought；In addition, in the extraction process with ethyl alcohol, due to peppermint oil distribution to each corner of the fresh cauline leaf of peppermint,
It is smaller than the extraction difficulty of folium eucalypti extract to extract difficulty, the first filtrate and first is obtained by extraction first with the ethyl alcohol of 40% high concentration
Filter residue；Then the second filter residue is extracted again with the ethyl alcohol of concentration in 20% again, and in reextraction process and need with 200r/
The mixing speed of min is stirred to accelerate rate of extraction mixed liquor, so that the borneol etc. in the fresh cauline leaf of Blumea balsamifera be had
Effect extracting substances come out.In the technical scheme, using two step extractions, the ethyl alcohol required using various concentration and different stirrings
The active principles such as peppermint oil in the fresh cauline leaf of peppermint both can rapidly and efficiently be extracted, and reduce extraction time by extract liquor；
The usage amount that alcohol extraction liquid can also be reduced achievees the purpose that efficient Rapid Extraction peppermint oil.
Preferably, the preparation flow of the camphor tree oil are as follows: first acquire the fresh branches and leaves of autumn camphor tree, and by the fresh branch of the camphor tree
Leaf is split into wide 1 centimetre, 0.5 centimetre thick, 2 centimetres of length branck of Lignum cinnamomi camphorae thin slice；Then branck of Lignum cinnamomi camphorae thin slice and camphortree leaf are packed into wooden
In steaming kier；Then the wooden steaming kier equipped with branck of Lignum cinnamomi camphorae thin slice and camphortree leaf is placed on copper steamer, and the water in copper steamer
It is separated by 12 centimetres with wooden steaming kier；Then distiller sealing is assembled in copper steamer and starts to distill；Then it will contain camphor tree
The steam of brain and camphor oil enters polycyclic dish type cooler by gas-guide tube, and camphor and oil are kept afloat after condensation, floating on water
The camphor and camphor oil in face are with filtered through gauze up to thick camphor and thick camphor tree oil；Then thick camphor tree oil is put into wooden steaming kier, into
Row second distillation collects 155-200 DEG C of distillate and is known as white oil, crystallized camphor is precipitated after white oil is cooling, then filters, repeatedly
Several times by filtrate distillation, until no camphor is precipitated, remaining is camphor tree oil.
The invention also discloses a kind of preparation method of natural plants deodorant liquid, it is used to prepare a kind of natural plants
Deodorant liquid, comprising the following steps:
S1, folium eucalypti extract, Cortex cinnamomi japonici (Ramulus Cinnamomi) extract, citrene, borneol, peppermint oil and camphor tree oil are first prepared respectively；
S2, measurement Cortex cinnamomi japonici (Ramulus Cinnamomi) extract and camphor tree oil are placed in seal pot, and then under nitrogen protection, constant temperature 40 is Celsius
Degree obtains mixed liquor A after being stirred mixing 0.5h to liquid with the blender of 300r/min；
S3, folium eucalypti extract is measured, the folium eucalypti extract of half volume is first placed in mixed liquor A, then in nitrogen protection
Under, 40 degrees Celsius of constant temperature, mixed liquid B is obtained after being stirred mixing 0.3h to liquid with the blender of 200r/min；Then again
Remaining folium eucalypti extract is placed in mixed liquid B, then under nitrogen protection, 50 degrees Celsius of constant temperature, with the blender of 500r/min
Liquid be quickly stirred after 0.5h and obtains mixed liquor C；
S4, measurement citrene are placed in mixed liquor C, then under nitrogen protection, 40 degrees Celsius of constant temperature, use 300r/min
Blender to liquid be stirred mixing 1h after obtain mixed liquor D；
S5, borneol and peppermint oil are measured, then by the peppermint oil of the borneol of one third volume and 2/3rds volumes
It is mixed to get mixed liquor E, and half an hour is stirred to mixed liquor E with the speed of 50r/min；
S6, on the basis of step S5, mixed liquor E and remaining borneol and peppermint oil are fallen to note simultaneously to mixed liquor
In D, then under nitrogen protection, 40 degrees Celsius of constant temperature, liquid is stirred after mixing 1h i.e. with the blender of 200r/min
Natural plants deodorant liquid finished product can be obtained.
It can be seen from the above technical scheme that the invention has the benefit that
1, deodorant liquid disclosed in this invention uses natural plants to carry out classification extraction completely, takes full advantage of plant itself
Physical property, extraction step is further simplified, and its effective ingredient is all extracted from natural plants, to people and animals without any
Toxic side effect, without any secondary pollution, can fast deodorization, be a kind of pure natural environment protection deodorising product, it is nontoxic, simplify system
Standby process flow, reduces production cost, improves production efficiency, solve natural plant deodorant in the prior art and be prepared into
This high defect, while also improving the efficiency of extraction；
2, deodorant liquid disclosed in this invention contain 1,8- Cineole, cinnamic acid, citrene, borneol, peppermint oil and
Camphor tree oil etc. can absorb the plant extracts for decomposing the foul smell molecules such as sulfur dioxide, ammonia, hydrogen sulfide, benzene, formaldehyde, organic amine,
It reacts with foul smell molecule, is transformed into odorless substance, can fundamentally remove foul smell, environment purification, rather than lead to
It crosses simple cover stink and carrys out deodorization, change the low status of existing market product odor removal efficient, breach industry technology bottleneck.
3, deodorant liquid disclosed in this invention contains the plant flowers fruity of the simple and elegant faint scent such as borneol and peppermint oil, after sprinkling
One pure and fresh pleasant fragrance of thick air, to weaken the stink of foul smell, aroma source changes in natural plant extracts
Existing market product is become and strong scent is mainly generated to cover the status of foul smell by addition compound essence, has been a kind of native annulus
Protect product；
4, deodorization liquid and preparation method thereof disclosed in this invention is impregnated, by the way of filtering and distillation using simple, by plant
Middle deodorization constituents extraction comes out, and extraction process is simple and easy, greatly simplifies the extraction process of existing plant deodorant, reduces
Production cost, solves that natural plant deodorant preparation cost in the prior art is high and the defect of low efficiency, improves production effect
Rate achievees the purpose that rapidly and efficiently to prepare deodorant liquid.
Specific embodiment
Following example is for present invention be described in more detail, but embodiment does not do any type of limit to the present invention
Fixed, except illustrating, reagent that the present invention uses, method and apparatus are the conventional reagent of the art, method and apparatus,
But the invention is not limited in any way.
The invention discloses a kind of natural plants deodorant liquids, including following raw materials according to be made according to following mass fractions: folium eucalypti
1-50 parts of extract, 20-30 parts of Cortex cinnamomi japonici (Ramulus Cinnamomi) extract, 15-30 parts of citrene, 1-10 parts of borneol, 1-10 parts of peppermint oil and camphor tree
Set 1-10 parts of oil.
The invention also discloses a kind of preparation methods of natural plants deodorant liquid:
S1, folium eucalypti extract, Cortex cinnamomi japonici (Ramulus Cinnamomi) extract, citrene, borneol, peppermint oil and camphor tree oil are first prepared respectively；Its
In, the preparation flow of the folium eucalypti extract are as follows: first weigh eucalyptus branches and leaves and be placed in extraction kettle, be then 2000r/min with revolving speed
Pulverizer eucalyptus branches and leaves are crushed；Then with mistake after the 70% ethyl alcohol immersion 20h of 60 times of volumes of raw material after co-grinding
Filter obtains the first filtrate and the first filter residue；Then it is impregnated again with 40% ethyl alcohol of 30 times of volumes of the first filter residue, and with 200r/min
Mixing speed mixed liquor is stirred, the second filtrate is obtained after 12h；First filtrate and the second filtrate are mixed, steaming is passed through
The mode evaporated recycles ethyl alcohol therein, obtains folium eucalypti extract.
The preparation flow of the Cortex cinnamomi japonici (Ramulus Cinnamomi) extract are as follows: first weigh cassia bark and be placed in extraction kettle, be then 3000r/ with revolving speed
The pulverizer of min crushes eucalyptus branches and leaves；Then 30h is impregnated with 80% ethyl alcohol of 20 times of volumes of raw material after co-grinding
After the first filtrate and the first filter residue is obtained by filtration；Then it is impregnated again with 50% ethyl alcohol of 10 times of volumes of the first filter residue, and with 500r/
The mixing speed of min is stirred mixed liquor, and the second filtrate is obtained after 20h；First filtrate and the second filtrate are mixed, passed through
The mode of distillation recycles ethyl alcohol therein, obtains Cortex cinnamomi japonici (Ramulus Cinnamomi) extract.
The preparation flow of the citrene are as follows: first weigh lemonlike citrus leaf and be placed in extraction kettle, be then 1000r/ with revolving speed
The pulverizer of min crushes eucalyptus branches and leaves；Then after impregnating 20h with 40% ethyl alcohol of 20 times of volumes of raw material after co-grinding
The first filtrate and the first filter residue is obtained by filtration；Then it is impregnated again with 20% ethyl alcohol of 10 times of volumes of the first filter residue, and with 200r/
The mixing speed of min is stirred mixed liquor, and the second filtrate is obtained after 12h；First filtrate and the second filtrate are mixed, passed through
The mode of distillation recycles ethyl alcohol therein, obtains citrene liquid.
The preparation flow of the folium eucalypti extract are as follows: first weigh eucalyptus branches and leaves and be placed in extraction kettle, be then with revolving speed
The pulverizer of 2000r/min crushes eucalyptus branches and leaves；Then it is soaked with 70% ethyl alcohol of 60 times of volumes of raw material after co-grinding
The first filtrate and the first filter residue is obtained by filtration after bubble 20h；Then it is impregnated again with 40% ethyl alcohol of 30 times of volumes of the first filter residue, and with
The mixing speed of 200r/min is stirred mixed liquor, and the second filtrate is obtained after 12h；First filtrate and the second filtrate are mixed
It closes, ethyl alcohol therein is recycled by way of distillation, obtains folium eucalypti extract.
The preparation flow of the peppermint oil are as follows: first weigh the fresh cauline leaf of peppermint and be placed in extraction kettle, be then with revolving speed
The pulverizer of 1000r/min crushes eucalyptus branches and leaves；Then it is soaked with 40% ethyl alcohol of 20 times of volumes of raw material after co-grinding
The first filtrate and the first filter residue is obtained by filtration after bubble 20h；Then it is impregnated again with 20% ethyl alcohol of 10 times of volumes of the first filter residue, and
Mixed liquor is stirred with the mixing speed of 200r/min, the second filtrate is obtained after 12h；First filtrate and the second filtrate are mixed
It closes, ethyl alcohol therein is recycled by way of distillation, obtains peppermint oil.
The preparation flow of the camphor tree oil are as follows: first acquire the fresh branches and leaves of autumn camphor tree, and the fresh branches and leaves of the camphor tree are split into
Wide 1 centimetre, 0.5 centimetre thick, 2 centimetres of length branck of Lignum cinnamomi camphorae thin slice；Then branck of Lignum cinnamomi camphorae thin slice and camphortree leaf are packed into wooden steaming kier；
Then the wooden steaming kier equipped with branck of Lignum cinnamomi camphorae thin slice and camphortree leaf is placed on copper steamer, and the water in copper steamer and wooden steaming
Bucket is separated by 12 centimetres；Then distiller sealing is assembled in copper steamer and starts to distill；Then it will contain camphor and camphor oil
Steam, by gas-guide tube enter polycyclic dish type cooler, camphor and oil are kept afloat after condensation, the camphor kept afloat
With camphor oil with filtered through gauze up to thick camphor and thick camphor tree oil；Then thick camphor tree oil is put into wooden steaming kier, carries out secondary steaming
It evaporates, collects 155-200 DEG C of distillate and be known as white oil, crystallized camphor is precipitated after white oil is cooling, then filters, repeatedly steams filtrate
It evaporates several times, until no camphor is precipitated, remaining is camphor tree oil.
S2, measurement Cortex cinnamomi japonici (Ramulus Cinnamomi) extract and camphor tree oil are placed in seal pot, and then under nitrogen protection, constant temperature 40 is Celsius
Degree obtains mixed liquor A after being stirred mixing 0.5h to liquid with the blender of 300r/min；
S3, folium eucalypti extract is measured, the folium eucalypti extract of half volume is first placed in mixed liquor A, then in nitrogen protection
Under, 40 degrees Celsius of constant temperature, mixed liquid B is obtained after being stirred mixing 0.3h to liquid with the blender of 200r/min；Then again
Remaining folium eucalypti extract is placed in mixed liquid B, then under nitrogen protection, 50 degrees Celsius of constant temperature, with the blender of 500r/min
Liquid be quickly stirred after 0.5h and obtains mixed liquor C；
S4, measurement citrene are placed in mixed liquor C, then under nitrogen protection, 40 degrees Celsius of constant temperature, use 300r/min
Blender to liquid be stirred mixing 1h after obtain mixed liquor D；
S5, borneol and peppermint oil are measured, then by the peppermint oil of the borneol of one third volume and 2/3rds volumes
It is mixed to get mixed liquor E, and half an hour is stirred to mixed liquor E with the speed of 50r/min；
S6, on the basis of step S5, mixed liquor E and remaining borneol and peppermint oil are fallen to note simultaneously to mixed liquor
In D, then under nitrogen protection, 40 degrees Celsius of constant temperature, liquid is stirred after mixing 1h i.e. with the blender of 200r/min
Natural plants deodorant liquid finished product can be obtained.
Next, the technical program will be proved its advance in conjunction with specific embodiments.
Embodiment one: a kind of natural plants deodorant liquid, including following raw materials according are made according to following mass fractions: folium eucalypti extracts
1 part of 40 parts of object, 25 parts of Cortex cinnamomi japonici (Ramulus Cinnamomi) extract, 25 parts of citrene, 5 parts of borneol, 4 parts of peppermint oil and camphor tree oil.The natural plants
Deodorant liquid using above-mentioned preparation method by above-mentioned raw materials prepare described in obtain natural plants deodorant liquid A.
Embodiment two: a kind of natural plants deodorant liquid, including following raw materials according are made according to following mass fractions: folium eucalypti extracts
1 part of 40 parts of object, 25 parts of Cortex cinnamomi japonici (Ramulus Cinnamomi) extract, 25 parts of citrene, 5 parts of borneol, 4 parts of peppermint oil and camphor tree oil.The natural plants
Deodorant liquid using above-mentioned preparation method by above-mentioned raw materials prepare described in obtain natural plants deodorant liquid B.
Embodiment three: a kind of natural plants deodorant liquid, including following raw materials according are made according to following mass fractions: folium eucalypti extracts
5 parts of 45 parts of object, 20 parts of Cortex cinnamomi japonici (Ramulus Cinnamomi) extract, 15 parts of citrene, 7 parts of borneol, 8 parts of peppermint oil and camphor tree oil.The natural plants
Deodorant liquid using above-mentioned preparation method by above-mentioned raw materials prepare described in obtain natural plants deodorant liquid C.
Example IV: a kind of natural plants deodorant liquid, including following raw materials according are made according to following mass fractions: folium eucalypti extracts
5 parts of 35 parts of object, 29 parts of Cortex cinnamomi japonici (Ramulus Cinnamomi) extract, 21 parts of citrene, 5 parts of borneol, 5 parts of peppermint oil and camphor tree oil.The natural plants
Deodorant liquid using above-mentioned preparation method by above-mentioned raw materials prepare described in obtain natural plants deodorant liquid D.
Embodiment five: a kind of natural plants deodorant liquid, including following raw materials according are made according to following mass fractions: folium eucalypti extracts
5 parts of 30 parts of object, 25 parts of Cortex cinnamomi japonici (Ramulus Cinnamomi) extract, 25 parts of citrene, 10 parts of borneol, 5 parts of peppermint oil and camphor tree oil.This is naturally planted
Object deodorant liquid using above-mentioned preparation method by above-mentioned raw materials prepare described in obtain natural plants deodorant liquid E.
Comparative example one: the tight standing grain plant deodorant sold by the production of Beijing Yan He Science and Technology Ltd.；
Comparative example two: the vegetation water deodorant sold by the production of Jinan De Lan Chemical Co., Ltd.；
Compliance test result:
The natural plants deodorant liquid that the preparation method of embodiment one to five obtains is diluted with water 40-200 times, with setting by spraying
It is standby to be sprayed on rubbish surface, deodorizing effect is tested, while experiment is compared with comparative example one and two, test result is as follows table:
It can be concluded that, high-efficiency plant deodorant of the invention is relative to existing deodorant, deodorization by testing above
The available significant raising of effect, this is because natural plants deodorant liquid disclosed in this invention contains 1, 8-Cineole, meat
Cinnamic aldehyde, citrene, borneol, peppermint oil and camphor tree oil etc. can absorb decompose sulfur dioxide, ammonia, hydrogen sulfide, benzene, formaldehyde,
The plant extracts of the foul smell molecule such as organic amine, reacts with foul smell molecule, is transformed into odorless substance, can be from basic
Upper removal foul smell, environment purification, rather than existing market product odor removal efficient is changed come deodorization by simple cover stink
Low status breaches industry technology bottleneck；In addition, to contain borneol and peppermint oil etc. simple and elegant for deodorant liquid disclosed in this invention
The plant flowers fruity of faint scent, one pure and fresh pleasant fragrance of thick air after sprinkling, to weaken the stink of foul smell, fragrance
From natural plant extracts, changes existing market product and strong scent is mainly generated by addition compound essence to cover
The status of foul smell is a kind of natural environmental-protective product, solves natural plant deodorant preparation cost height and low efficiency in the prior art
Defect, improve production efficiency, achieve the purpose that rapidly and efficiently to prepare deodorant liquid, while by the embodiment of the present invention one to five
The natural plants deodorant liquid that preparation method obtains is used for public restroom deodorization, can play and dispel stink effect, phase well
It is a significant progress for existing plant deodorant.
Natural plants deodorant liquid disclosed in this invention is atomized by deodorizing device, forms mist, will be presently disclosed
Natural plants deodorant liquid contain the substances mists such as 1,8- Cineole, cinnamic acid, citrene, borneol, peppermint oil and camphor tree oil
Change forms little particle atomized liquid, in radius≤0.04mm of space diffusion drop.Drop has very big specific surface area, has very
Big surface energy, average every mole about tens kilocalories, the energy of this order of magnitude has been the 1/3-1/ of bond energy in many elements
4.Using the substances atomized liquids such as 1,8- Cineole, cinnamic acid, citrene, borneol, peppermint oil and camphor tree oil surface not only
The odor molecules in air can be effectively adsorbed, while also the spatial configuration for the odor molecules being adsorbed can be made to change, are cut
Chemical combination key in weak odor molecules so that the unstability of odor molecules increases, be easy in other molecules and vegetation water
Acidic buffer chemically reacts, and ultimately produces tasteless, nontoxic substance.As hydrogen sulfide reacts life under the action of vegetation water
At sulfate ion and water；Ammonia generates nitrogen and water under the action of vegetation water.It is present in high-temperature (95-100%) air
Or the stench particle in water, it is surrounded by hydrone envelope, deodorization at this time must first destroy hydrone envelope, then will wherein
Stench particle captured.The deodorant is the complex of natural botanical extraction liquid ingredient, is pure natural components.
Natural plants deodorant liquid disclosed in this invention is to spray with different wet process spray applications through dedicated spraying machine
It nebulizes, spreads drop in specific space.Containing with bioactivity, chemistry among effective deodorization molecule in drop
Activity, conjugated double bond isoreactivity group, can have an effect from different peculiar smell.Can not only effectively absorption it is aerial different
Taste molecule, while also the spatial configuration for the odor molecules being adsorbed can be made to change, the chemical combination key in odor molecules is weakened,
So that the unstability of odor molecules increases, it is easy to be chemically reacted with other molecules, thus reach thorough taste removal, deodorization,
Play effective Air purification.
To sum up, natural plants deodorant liquid disclosed in this invention has selective removal effect to smell substance, not with crowd
It is same, it has no effect for life, animal；By eliminating the root of taste in conjunction with smell substance, so, it does not generate new
Stench factor has duration deodorization functions, is a kind of and the entirely different product of general deodorant；For institute's foul smelling, spray
Taste can be removed when spilling immediately, manufactures comfortable environment；For various peculiar smell, has and inhibit, the curative effect of elimination；Not with common product
Together, harmless, even if not had any problems into eye or injured skin yet.
The deodorant liquid effect of natural plants deodorant liquid disclosed in this invention: in conjunction with smell substance；Time deodorization quickly
The high Hydrogen Sulphide odour of intensity；It is non-corrosive, it is decomposed completely using inside rear soil；The strong stench of deodorization is not easy using other
It can remove；Its scope of application are as follows: the deodorization of contaminated air or liquid and clean, purification.Garbage compression station, garbage loading embeading
Field, sewage treatment plant's deodorization.The removal of the deodorization and pollution of washing column.Sewer processing.Drainage plumbing fixture is defeated with other
It send the deodorization of media and cleans.The humidifier supply processing of water.The removal of industry or natural soil and water pollution is handled.It is dirty
Water treatment plant (station) each workplace, sludge room stench are eliminated.
The characteristics of natural plants deodorant liquid disclosed in this invention: not stimulating skin, do not aoxidize, do not have combustibility, is smelly
The first choice being deodorized when air humidity degree > 85%.50-1000 times usually is diluted with water, can effectively be used.Suitable for room temperature, ideal temperature
It is 36 DEG C, high temperature limit is 54 DEG C.Zero degree can be freezed, and not decompose, and effect is not lost after defrosting.Promote oxidation and reaches deodorization, moment
It neutralizes and removes various stinks, effect is lasting.
In addition, may know that from a kind of preparation method of natural plants deodorant liquid disclosed in this invention, it is presently disclosed
Deodorant liquid carry out classification extraction using natural plants, take full advantage of the physical property of plant itself, further simplify and mention
Step is taken, and its effective ingredient is all extracted from natural plants, it is without any side effects to people and animals, without any secondary pollution,
Can fast deodorization, be a kind of pure natural environment protection deodorising product, it is nontoxic, simplify preparation process flow, reduce and be produced into
This, improves production efficiency, solves the defect that natural plant deodorant preparation cost is high in the prior art, also improve simultaneously
The efficiency of extraction.
In a kind of preparation method of natural plants deodorant liquid disclosed in this invention, step S2 needs first extract cassia bark
Object and camphor tree oil are placed in seal pot, and under nitrogen protection, and 40 degrees Celsius of constant temperature, with the blender of 300r/min to liquid
Body obtains mixed liquor A after being stirred mixing 0.5h；This is because Cortex cinnamomi japonici (Ramulus Cinnamomi) extract and camphor tree oil nature are closer to, first will
Cortex cinnamomi japonici (Ramulus Cinnamomi) extract and camphor tree oil mix simultaneously, are then sealed stirring under the protection of nitrogen again, effectively cassia bark can be avoided to mention
Object and camphor tree oil is taken to expose volatilization；And acceleration mixing is carried out to raw material by the mixing speed of 300r/min, do not damaging original
Under the premise of expecting ingredient, more effectively avoids Cortex cinnamomi japonici (Ramulus Cinnamomi) extract and camphor tree oil from exposing volatilization, further improve the natural plants
The preparation efficiency of deodorant liquid.
In addition, step S3 needs first account in a kind of preparation method of natural plants deodorant liquid disclosed in this invention
The half volume of weighed mass/volume or the folium eucalypti extract of half quality are placed in mixed liquor A, then under nitrogen protection,
40 degrees Celsius of constant temperature, mixed liquid B is obtained after being stirred mixing 0.3h to liquid with the blender of 200r/min；Then again will
Remaining folium eucalypti extract is placed in mixed liquid B, then under nitrogen protection, 50 degrees Celsius of constant temperature, with the blender pair of 500r/min
Liquid carries out obtaining mixed liquor C after being quickly stirred 0.5h；In the step, folium eucalypti extract is divided into and is launched twice, a side
Face can cause to be stirred non-uniform defect to avoid disposable launch, and on the other hand can accelerate the mixed of folium eucalypti extract
Close efficiency；Due to be easy to causeing final products if stirring is uneven containing key substances such as 1, 8-Cineoles in folium eucalypti extract
Preparation failure.Mixed liquid B is obtained under the mixing speed of 200r/min and remaining folium eucalypti extract is added, and is then existed again
Mixed liquor C is obtained under the mixing speed of 500r/min, can quickly be mixed the dissolution of folium eucalypti extract into mixed liquor A, further
Improve the preparation efficiency of the natural plants deodorant liquid.
In addition, a kind of preparation method of natural plants deodorant liquid disclosed in the embodiment of the present invention, using folium eucalypti extract,
The different characteristic of this oily five kinds of raw material of Cortex cinnamomi japonici (Ramulus Cinnamomi) extract, citrene, borneol, peppermint oil and camphor tree, during the preparation process
Agitating mode is launched using distribution, by different supply volumes, release time, mixing speed and release sequence, sufficiently
The physical property of plant itself is utilized, further simplifies extraction step, and its effective ingredient is all mentioned from natural plants
Take, reduce production cost, improve production efficiency, solve natural plant deodorant preparation cost in the prior art it is high lack
It falls into, while also improving the efficiency of extraction, achieve the purpose that improve the natural plants deodorant liquid preparation efficiency.
Each embodiment in this specification is described in a progressive manner, the highlights of each of the examples are with other
The difference of embodiment, the same or similar parts in each embodiment cross-reference.
The foregoing description of the disclosed embodiments makes professional and technical personnel in the field can be realized the present invention.To these
A variety of modifications of embodiment will be readily apparent to those skilled in the art, general original as defined herein
Reason can be realized in other embodiments without departing from the spirit or scope of the present invention.Therefore, the present invention will not
Be intended to be limited to the embodiments shown herein, and be to fit to it is consistent with the principles and novel features disclosed in this article most
Wide range.
Claims (9)
1. a kind of natural plants deodorant liquid, which is characterized in that be made including following raw materials according according to following mass fractions: folium eucalypti extracts
1-50 parts of object, 20-30 parts of Cortex cinnamomi japonici (Ramulus Cinnamomi) extract, 15-30 parts of citrene, 1-10 parts of borneol, 1-10 parts of peppermint oil and camphor tree oil
1-10 parts.
2. a kind of natural plants deodorant liquid according to claim 1, which is characterized in that including following raw materials according according to following matter
Amount score is made: 30-50 parts of folium eucalypti extract, 20-30 parts of Cortex cinnamomi japonici (Ramulus Cinnamomi) extract, 15-30 parts of citrene, 4-10 parts of borneol, thin
4-8 parts of lotus oil and 1-5 parts of camphor tree oil.
3. a kind of natural plants deodorant liquid according to claim 1, which is characterized in that including following raw materials according according to following matter
Amount score be made: 30 parts of folium eucalypti extract, 25 parts of Cortex cinnamomi japonici (Ramulus Cinnamomi) extract, 25 parts of citrene, 10 parts of borneol, 5 parts of peppermint oil and
5 parts of camphor tree oil.
4. a kind of natural plants deodorant liquid according to claim 1, which is characterized in that the preparation stream of the folium eucalypti extract
Journey are as follows: first weigh eucalyptus branches and leaves and be placed in extraction kettle, the pulverizer for being then 2000r/min with revolving speed crushes eucalyptus branches and leaves；
Then the first filtrate and the first filter residue is obtained by filtration after impregnating 20h with 70% ethyl alcohol of 60 times of volumes of raw material after co-grinding；
Then it is impregnated with 40% ethyl alcohol of 30 times of volumes of the first filter residue, and mixed liquor is stirred again with the mixing speed of 200r/min
It mixes, the second filtrate is obtained after 12h；First filtrate and the second filtrate are mixed, ethyl alcohol therein is recycled by way of distillation, is obtained
To folium eucalypti extract.
5. a kind of natural plants deodorant liquid according to claim 1, which is characterized in that the preparation stream of the Cortex cinnamomi japonici (Ramulus Cinnamomi) extract
Journey are as follows: first weigh cassia bark and be placed in extraction kettle, the pulverizer for being then 3000r/min with revolving speed crushes eucalyptus branches and leaves；So
The first filtrate and the first filter residue is obtained by filtration after impregnating 30h with 80% ethyl alcohol of 20 times of volumes of raw material after co-grinding afterwards；So
It is impregnated with 50% ethyl alcohol of 10 times of volumes of the first filter residue, and with the mixing speed of 500r/min mixed liquor is stirred again afterwards,
The second filtrate is obtained after 20h；First filtrate and the second filtrate are mixed, ethyl alcohol therein is recycled by way of distillation, is obtained
Cortex cinnamomi japonici (Ramulus Cinnamomi) extract.
6. a kind of natural plants deodorant liquid according to claim 1, which is characterized in that the preparation flow of the borneol are as follows:
It first weighs the fresh cauline leaf of Blumea balsamifera to be placed in extraction kettle, powder then is carried out to eucalyptus branches and leaves with the pulverizer that revolving speed is 1000r/min
It is broken；Then the first filtrate and the first filter are obtained by filtration after impregnating 20h with 40% ethyl alcohol of 20 times of volumes of raw material after co-grinding
Slag；Then it is impregnated with 20% ethyl alcohol of 10 times of volumes of the first filter residue, and mixed liquor is carried out again with the mixing speed of 200r/min
It stirs, obtains the second filtrate after 12h；First filtrate and the second filtrate are mixed, ethyl alcohol therein is recycled by way of distillation,
Obtain borneol liquid.
7. a kind of natural plants deodorant liquid according to claim 1, which is characterized in that the preparation flow of the peppermint oil
Are as follows: it first weighs the fresh cauline leaf of peppermint and is placed in extraction kettle, powder then is carried out to eucalyptus branches and leaves with the pulverizer that revolving speed is 1000r/min
It is broken；Then the first filtrate and the first filter are obtained by filtration after impregnating 20h with 40% ethyl alcohol of 20 times of volumes of raw material after co-grinding
Slag；Then it is impregnated with 20% ethyl alcohol of 10 times of volumes of the first filter residue, and mixed liquor is carried out again with the mixing speed of 200r/min
It stirs, obtains the second filtrate after 12h；First filtrate and the second filtrate are mixed, ethyl alcohol therein is recycled by way of distillation,
Obtain peppermint oil.
8. a kind of natural plants deodorant liquid according to claim 1, which is characterized in that the preparation flow of the camphor tree oil
Are as follows: the fresh branches and leaves of autumn camphor tree are first acquired, and the fresh branches and leaves of the camphor tree are split into wide 1 centimetre, 0.5 centimetre thick, 2 centimetres of length camphor tree
Branch thin slice；Then branck of Lignum cinnamomi camphorae thin slice and camphortree leaf are packed into wooden steaming kier；Then branck of Lignum cinnamomi camphorae thin slice and camphortree leaf will be housed
Wooden steaming kier be placed on copper steamer, and the water in copper steamer and wooden steaming kier are separated by 12 centimetres；Then distiller is close
Envelope is assembled in copper steamer and starts to distill；Then by the steam containing camphor and camphor oil, enter by gas-guide tube polycyclic
Dish type cooler, camphor and oil are kept afloat after condensation, the camphor and camphor oil filtered through gauze kept afloat up to thick camphor
With thick camphor tree oil；Then thick camphor tree oil is put into wooden steaming kier, carries out second distillation, collected 155-200 DEG C of distillate and claim
For white oil, crystallized camphor is precipitated after white oil is cooling, then filters, repeatedly several times by filtrate distillation, until no camphor is precipitated,
Remaining is camphor tree oil.
9. a kind of preparation method of natural plants deodorant liquid, which is characterized in that be used to prepare described in claim 1 a kind of natural
Plant deodorization liquid, comprising the following steps:
S1, folium eucalypti extract, Cortex cinnamomi japonici (Ramulus Cinnamomi) extract, citrene, borneol, peppermint oil and camphor tree oil are first prepared respectively；
S2, measurement Cortex cinnamomi japonici (Ramulus Cinnamomi) extract and camphor tree oil are placed in seal pot, then under nitrogen protection, 40 degrees Celsius of constant temperature, are used
The blender of 300r/min obtains mixed liquor A after being stirred mixing 0.5h to liquid；
S3, folium eucalypti extract is measured, the folium eucalypti extract of half volume is first placed in mixed liquor A, it is then under nitrogen protection, permanent
40 degrees Celsius of temperature obtains mixed liquid B after being stirred mixing 0.3h to liquid with the blender of 200r/min；It then again will be remaining
Folium eucalypti extract is placed in mixed liquid B, then under nitrogen protection, 50 degrees Celsius of constant temperature, with the blender of 500r/min to liquid
It carries out obtaining mixed liquor C after being quickly stirred 0.5h；
S4, measurement citrene are placed in mixed liquor C, then under nitrogen protection, 40 degrees Celsius of constant temperature, with stirring for 300r/min
It mixes after machine is stirred mixing 1h to liquid and obtains mixed liquor D；
S5, borneol and peppermint oil are measured, then mixes the borneol of one third volume with the peppermint oil of 2/3rds volumes
Mixed liquor E is obtained, and half an hour is stirred to mixed liquor E with the speed of 50r/min；
S6, on the basis of step S5, mixed liquor E and remaining borneol and peppermint oil are fallen in note to mixed liquor D simultaneously,
Then under nitrogen protection, 40 degrees Celsius of constant temperature can obtain after being stirred mixing 1h to liquid with the blender of 200r/min
To natural plants deodorant liquid finished product.
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN110882405A (en) * | 2019-12-23 | 2020-03-17 | 广州飞逸生物科技有限公司 | Deodorization fragrance oil for fragrance diffuser and preparation method thereof |
| CN112107715A (en) * | 2019-11-22 | 2020-12-22 | 上海筑程环境工程有限公司 | Plant source compound deodorant |
| CN113750279A (en) * | 2020-06-02 | 2021-12-07 | 苏州工业园区艾舍尔环境技术有限公司 | Oily concentrated air deodorant and preparation method thereof |
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