CN110339120A - A kind of shampoo and preparation method thereof - Google Patents
A kind of shampoo and preparation method thereof Download PDFInfo
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- CN110339120A CN110339120A CN201910771862.7A CN201910771862A CN110339120A CN 110339120 A CN110339120 A CN 110339120A CN 201910771862 A CN201910771862 A CN 201910771862A CN 110339120 A CN110339120 A CN 110339120A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
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- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9728—Fungi, e.g. yeasts
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
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- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9755—Gymnosperms [Coniferophyta]
- A61K8/9761—Cupressaceae [Cypress family], e.g. juniper or cypress
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- A—HUMAN NECESSITIES
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- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9789—Magnoliopsida [dicotyledons]
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- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
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- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9794—Liliopsida [monocotyledons]
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/02—Preparations for cleaning the hair
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/805—Corresponding aspects not provided for by any of codes A61K2800/81 - A61K2800/95
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Abstract
The present invention relates to a kind of shampoo and preparation method thereof, the raw material components of the shampoo include more than 30 raw materials such as water, glycerol, Anjidew NL50, surfactant, solubilizer, Polyquaternium-10, hydrolysis Jojoba esters, Fructus Citri grandis extract.Shampoo cleaning capacity of the present invention is strong, and blistering is fast, and foam is fine and smooth, stablizes, it is easy to rinse after use, usage comfort is high, has preferably wet comb and dry comb property after hair washing, while having the function of stronger black hair strengthen the hair, improving and dry up and prevent hair bifurcated.Shampoo preparation method of the present invention is simple, is easy to be mass produced, stable and controllable for quality, heavy metal free ion and other toxic substances.
Description
Technical field
The invention belongs to daily use chemicals technical fields, and in particular to a kind of shampoo and preparation method thereof.
Background technique
Shampoo is fallen off on the grease, sweat mixed with dirt, scalp of the human secretory being attached on scalp and hair for cleaning
Cell and external dust, microorganism, the residue of approved product and bad smell etc. keep scalp and hair cleaning and head
Send out beautiful product.
Shampoo at present on the market is many kinds of, and function division also increasingly refines, and still, current shampoo is still deposited
In some problems, for example existing shampoo is still weak due to recipe ingredient reasonability, is not made us also in terms of actual efficacy
It is satisfied, and wet comb after washing, dry comb property, still wait improve, in addition, surfactant is the primary raw material of shampoo, additive amount is few
Cleaning force is insufficient, and additive amount is big may to bring skin irritation again, reduces usage comfort, therefore, how rational proportion, thus
Reach the balance of cleaning force and usage comfort, while really realizing additional effect the effect of publicity, is the project for being worth research.
Summary of the invention
In order to solve the above-mentioned problems in the prior art, the present invention provides a kind of shampoo and preparation method thereof.Institute
It is strong to state shampoo cleaning capacity, blistering is fast, and foam is fine and smooth, stablizes, and is easy to rinse after use, and usage comfort is high, has after hair washing
There are preferable wet comb and dry comb property, while having the function of that stronger black hair strengthen the hair, improvement are withered and prevent hair bifurcated.
The technical solution of the present invention is as follows:
A kind of shampoo, raw material components include: water 40-60 parts by weight, glycerol 3-8 parts by weight, Anjidew NL50 1-8 parts by weight, table
Face activating agent 22-60 parts by weight, solubilizer 0.3-1.5 parts by weight, Polyquaternium-10 0.2-1 parts by weight, hydrolysis jojoba ester
Class 0.2-1 parts by weight, Fructus Citri grandis extract 0.2-1 parts by weight, butanediol 0.02-0.2 parts by weight, ginseng root extract 0.01-0.1
Parts by weight, rhizoma anemarrhenae root extract 0.01-0.1 parts by weight, ginger-root extract 0.01-0.1 parts by weight, Angelica roots 0.01-
0.1 parts by weight, Cacumen Platycladi extract 0.01-0.1 parts by weight, fleece-flower root root extract 0.01-0.1 parts by weight, 1,2- pentanediol
0.01-0.1 parts by weight, pungent glycol 0.01-0.1 parts by weight, thickener 0.1-0.8 parts by weight, saccharomycetes to make fermentation Product filtrate
0.1-0.5 parts by weight, -60 0.1-0.6 parts by weight of polysorbate, orange oil 0.1-0.5 parts by weight, pH adjusting agent 0.01-
0.1 parts by weight, preservative 0.08-0.3 parts by weight, dichloroxylenol 0.02-0.04 parts by weight, triclosan 0.006-0.014 weight
Part, dipropylene glycol 0.02-0.1 parts by weight, PEG-50 rilanit special 0.02-0.1 parts by weight, salicylic acid 0.1-0.3 parts by weight,
Chelating agent 0.01-0.1 parts by weight.
Further, the raw material components of the shampoo include: water 45-50 parts by weight, glycerol 4-6 parts by weight, Anjidew NL50 2-
5 parts by weight, surfactant 30-47 parts by weight, solubilizer 0.6-1 parts by weight, Polyquaternium-10 0.4-0.6 parts by weight, water
Solve Jojoba esters 0.4-0.6 parts by weight, Fructus Citri grandis extract 0.4-0.6 parts by weight, butanediol 0.06-0.12 parts by weight, ginseng
Root extract 0.03-0.08 parts by weight, rhizoma anemarrhenae root extract 0.03-0.08 parts by weight, ginger-root extract 0.03-0.08 weight
Part, Angelica roots 0.03-0.08 parts by weight, Cacumen Platycladi extract 0.03-0.08 parts by weight, fleece-flower root root extract
0.03-0.08 parts by weight, 1,2- pentanediol 0.03-0.08 parts by weight, pungent glycol 0.03-0.08 parts by weight, thickener 0.3-0.5
Parts by weight, saccharomycetes to make fermentation Product filtrate 0.2-0.4 parts by weight, -60 0.2-0.4 parts by weight of polysorbate, orange oil 0.2-
0.3 parts by weight, pH adjusting agent 0.03-0.08 parts by weight, preservative 0.14-0.24 parts by weight, dichloroxylenol 0.025-0.035 weight
Measure part, triclosan 0.008-0.012 parts by weight, dipropylene glycol 0.03-0.08 parts by weight, PEG-50 rilanit special 0.03-
0.08 parts by weight, salicylic acid 0.15-0.22 parts by weight, chelating agent 0.03-0.08 parts by weight.
Further, the raw material components of the shampoo include: 48.31 parts by weight of water, 5 parts by weight of glycerol, 3 weight of Anjidew NL50
Measure part, 39 parts by weight of surfactant, 0.8 parts by weight of solubilizer, 0.5 parts by weight of Polyquaternium-10, hydrolysis Jojoba esters
0.5 parts by weight, 0.5 parts by weight of Fructus Citri grandis extract, 0.1 parts by weight of butanediol, 0.05 parts by weight of ginseng root extract, rhizoma anemarrhenae root mention
Take 0.05 parts by weight of object, 0.05 parts by weight of ginger-root extract, 0.05 parts by weight of Angelica roots, 0.05 weight of Cacumen Platycladi extract
Measure part, 0.05 parts by weight of fleece-flower root root extract, 0.05 parts by weight of 1,2- pentanediol, 0.05 parts by weight of pungent glycol, thickener 0.4
Parts by weight, 0.3 parts by weight of saccharomycetes to make fermentation Product filtrate, 0.3 parts by weight of polysorbate -60,0.25 parts by weight of orange oil,
It is 0.05 parts by weight of pH adjusting agent, 0.2 parts by weight of preservative, 0.03 parts by weight of dichloroxylenol, 0.01 parts by weight of triclosan, double third sweet
0.05 parts by weight of alcohol, 0.05 parts by weight of PEG-50 rilanit special, 0.2 parts by weight of salicylic acid, 0.05 parts by weight of chelating agent.
Further, the surfactant is laureth sodium sulfovinate, cocounut oil acyl hydrolysis avenin potassium, cocounut oil
Amido propyl betaine, sodium lauroyl sarcosine, coconut oleoyl amine DEA, sodium cocoamphoacetate, PEG-7 glycerol coconut oil
The mixture of any one or more in ester.
Further, the Fructus Citri grandis extract is prepared with the following method: pomelo peel is isolated from shaddock, to shaddock
The Ca (OH) of 1.5~2wt% of 10~15 times of quality is added in sub- skin2Solution impregnate 6~8h, after filter, discard filtrate,
Obtain filter residue；It after filter residue is dried in vacuo, is placed in supercritical extract tank, is filled with CO2Extraction, isolated Fructus Citri grandis extract.
Further, the temperature of the extraction is 40~45 DEG C, and the pressure of the extraction is 40~55MPa, the extraction
Time be 2~3h.
A method of the shampoo is prepared, is included the following steps:
(1) will water and Polyquaternium-10 mix after first carry out first time homogeneous, after heat, then carry out second
Homogeneous obtains A phase；
(2) glycerol, surfactant, hydrolysis Jojoba esters, thickener, pH adjusting agent, bigcatkin willow are sequentially added into A phase
Acid, chelating agent are stirred to dissolve completely, obtain B phase；
(3) it is heated after mixing solubilizer, polysorbate -60, orange oil, mixture is obtained, by the mixture and B
After mixing, homogeneous cools down later, obtains C phase；
(4) sequentially added into C phase Anjidew NL50, Fructus Citri grandis extract, butanediol, ginseng root extract, rhizoma anemarrhenae root extract,
Ginger-root extract, Angelica roots, Cacumen Platycladi extract, fleece-flower root root extract, 1,2- pentanediol, pungent glycol, saccharomycete
Tunning filtrate, preservative, dichloroxylenol, triclosan, dipropylene glycol, PEG-50 rilanit special, stir evenly to get arriving
The shampoo.
Further, in step (1), the revolving speed of the first time homogeneous is 2000~3000r/min, and the first time is equal
The time of matter is 8~12min, and described to be heated to 75~85 DEG C, the revolving speed of second of homogeneous is 2000~2500r/min,
The time of second of homogeneous is 8~12min.
Further, in step (2), the stirring carries out under 75~85 DEG C of constant temperatures, and the speed of the stirring is
100~600r/min, the time of the stirring are 10~15min.
Further, in step (3), described to be heated to 55~65 DEG C, the revolving speed of the homogeneous is 2000~3000r/
Min, the time of the homogeneous is 1~3min, described to be cooled to 45 DEG C or less.
Fructus Citri grandis extract is extracted from the fruit of shaddock and is obtained, with work that is anti-inflammatory, improving local microcirculation and nutrition supply
With.
Ginseng root extract, has and promotes hair growth, and strong hair follicle reduces the effect of hair loss.It can slowly be inhaled by skin
It receives, there is no any pessimal stimulation to skin, capillary of skin can be expanded, promote skin blood loop, increase skin-nourishing,
Adjust the water and oil balance of skin.
Rhizoma anemarrhenae root extract is extracted from the rhizome of Liliaceae rhizoma anemarrhenae platymiscium rhizoma anemarrhenae and is obtained, and total soap is contained in Asphodeloides Bge Rhizome
Glycosides about 6%, wherein having 1-timosaponin A-1-I, A- II, A- III, A- IV, B- I, B- II, wherein timosaponin A- III is salsa soap
The disaccharide glucoside that glucoside member and timobiose are combined into, timosaponin A- I is salsa sapogenin β-D- galactopyranosyl glucoside.Rhizoma anemarrhenae
Sapogenin in rhizome is mainly salsa sapogenin, the content of Gan Genzhong about 0.5%, and in addition there are markogenins, new
Gitogenin, the also mangiferin containing flavonoids, isomangiferin, the choline of alkaloids, niacinamide, the tan of organic acid
In addition acid, niacin and four kinds of anemarans are gone back the Determination of multiple metal elements such as iron content, zinc, manganese, copper, chromium, nickel and mucilaginous substance, are gone back
Raw sugar etc..
Ginger-root extract, race are the roots for belonging to the ginger (zingiber officinale Roscoe) of zingiberaceous plant.Tool
Play the role of promoting hair growth, sterilization, antipruritic and improvement blood flow, the main component of race, including zingiberone and zingiberene
Etc essential oil and such as zingiberol (such as 6- zingiberol, 8- zingiberol and 10- zingiberol) etc pungent and stimulation component.
Angelica roots can effectively inhibit the biology in skin from the dry root of herbaceos perennial Radix Angelicae Sinensis
One tyrosinase activity of oxidizing ferment, blocks the formation of melanin, is bound directly by itself with tyrosinase, accelerates melanin
It decomposes and drains, so that the deposition of skin pigment is reduced, in addition, there are also the effects of antiphlogistic antibacterial.
Cacumen Platycladi extract, be cupressaceae plant arbor-vitae Platycladus orientalis (L.) Franco branch and
Leaf has cooling blood and hemostasis, growing and blacking hair and other effects.Containing volatile oil, predominantly fenchone (fenchone), camphor, acetic acid borneol
Ester, terpene alcohol；And contain juniperic acid (juniperic acid) Quercetin, poplar luteoxanthin (myricetin), Kaempferide, hinokiflavone
(hinokiflavone), wax etc..In cacumen biotae contain volatile oil 0.26%, oil in main component be α-absinthol, thujene,
Fenchone etc.；It is other still to contain flavones ingredient, such as aromadendrin, Quercetin, myricetin, hinokiflavone；In leaf also
Containing microelements such as potassium, sodium, nitrogen, phosphorus, calcium, magnesium, manganese and zinc.
Fleece-flower root root extract, the dried root of polygonum multiflorum thunb contain anthraquinone analog compound, predominantly rheum emodin
(emodin), Chrysophanol (chrysophanol) and Physcion (physcion), Rhein (rhein) and Chrysophanol
Anthrone (chrysophanol anthrone), has the effects that black beard and hair, anti-aging and antibacterial.
Saccharomycetes to make fermentation Product filtrate is that yeast extracts its protein, nucleic acid, vitamin etc. after broken wall, then through life
The substance of the active skull cap components such as the amino acid rich in small molecule, peptide, nucleotide, vitamin that object digests.And this filtrate is in weak
Acidity, pH value 4.5~5.0 have the effects that inhibit harmful bacteria, anti-infective.
The invention has the benefit that
1, shampoo of the present invention joined including Polyquaternium-10, hydrolysis Jojoba esters, Fructus Citri grandis extract, people
Join root extract, rhizoma anemarrhenae root extract, ginger-root extract, Angelica roots, Cacumen Platycladi extract, fleece-flower root root extract,
A variety of conditioner ingredients including saccharomycetes to make fermentation Product filtrate and orange oil, present inventor have found through a large number of experiments,
These types of ingredient uses simultaneously, and the skin irritation of surfactant can either be greatly reduced, and can be improved wet after hair washing
It combs and does comb property, while making the shampoo of preparation that there is stronger black hair strengthen the hair, improvement to dry up and prevent hair bifurcated
Effect.
2, shampoo cleaning capacity of the present invention is strong, blistering is fast, foam is fine and smooth, stablizes, and is easy to rinse after.
3, shampoo preparation method of the present invention is simple, is easy to be mass produced, stable and controllable for quality, heavy metal free from
Son and other toxic substances.
Specific embodiment
Below by specific embodiment, the invention will be further described.
1g is represented in following embodiment with 1 parts by weight.
Embodiment 1
The present embodiment provides a kind of shampoo, raw material components include:
40 parts by weight of water, 3 parts by weight of glycerol, 8 parts by weight of Anjidew NL50,18 parts by weight of laureth sodium sulfovinate, cocounut oil acyl
4 parts by weight of amine propyl betaine, cocounut oil acyl hydrolyze 10 parts by weight of avenin potassium, 8 parts by weight of sodium lauroyl sarcosine, cocounut oil acyl
1 parts by weight of amine DEA, 0.5 parts by weight of sodium cocoamphoacetate, 1.5 parts by weight of PEG-7 glyceryl cocoate, PEG-40 hydrogen
Change 0.3 parts by weight of castor oil, 1 parts by weight of Polyquaternium-10, hydrolysis 0.2 parts by weight of Jojoba esters, 1 weight of Fructus Citri grandis extract
Part, 0.02 parts by weight of butanediol, 0.1 parts by weight of ginseng root extract, 0.01 parts by weight of rhizoma anemarrhenae root extract, ginger-root extract
0.1 parts by weight, 0.01 parts by weight of Angelica roots, 0.1 parts by weight of Cacumen Platycladi extract, 0.01 weight of fleece-flower root root extract
Part, 0.1 parts by weight of 1,2- pentanediol, 0.01 parts by weight of pungent glycol, 0.8 parts by weight of sodium chloride, saccharomycetes to make fermentation Product filtrate 0.1
Parts by weight, 0.6 parts by weight of polysorbate -60,0.1 parts by weight of orange oil, 0.1 parts by weight of citric acid, DMDM hydantoin
0.03 parts by weight, 0.05 parts by weight of sodium benzoate, 0.04 parts by weight of dichloroxylenol, 0.006 parts by weight of triclosan, dipropylene glycol
0.1 parts by weight, 0.02 parts by weight of PEG-50 rilanit special, 0.3 parts by weight of salicylic acid, 0.1 parts by weight of EDETATE SODIUM；
The Fructus Citri grandis extract is prepared with the following method: isolating pomelo peel from shaddock, adds into pomelo peel
Enter the Ca (OH) of the 1.5wt% of 10 times of quality2Solution impregnate 8h, after filter, discard filtrate, obtain filter residue；Filter residue is true
After sky is dry, it is placed in supercritical extract tank, is filled with CO2Extraction, the temperature of extraction are 40 DEG C, and the pressure of extraction is 55MPa, extraction
The time taken is 3h, isolated Fructus Citri grandis extract.
Further, a kind of method preparing the shampoo is provided, is included the following steps:
(1) first with 2000r/min homogeneous 12min after water and Polyquaternium-10 being mixed, after be heated to 75 DEG C, so
Afterwards with 2000r/min homogeneous 8min, A phase is obtained；
(2) glycerol, laureth sodium sulfovinate, cocounut oil acyl hydrolysis avenin potassium, cocounut oil acyl are sequentially added into A phase
Amine propyl betaine, sodium lauroyl sarcosine, coconut oleoyl amine DEA, sodium cocoamphoacetate, PEG-7 glyceryl cocoate,
Jojoba esters, sodium chloride, citric acid, salicylic acid, EDETATE SODIUM are hydrolyzed, with the stirring of 100r/min under 75 DEG C of constant temperatures
Speed stirs 15min, obtains B phase；
(3) 55 DEG C are heated to after mixing Cremophor RH40, polysorbate -60, orange oil, is mixed
Material with 2000r/min homogeneous 3min, is cooled to 45 DEG C later, obtains C phase after mixing the mixture and B；
(4) sequentially added into C phase Anjidew NL50, Fructus Citri grandis extract, butanediol, ginseng root extract, rhizoma anemarrhenae root extract,
Ginger-root extract, Angelica roots, Cacumen Platycladi extract, fleece-flower root root extract, 1,2- pentanediol, pungent glycol, saccharomycete
Tunning filtrate, DMDM hydantoin, sodium benzoate, dichloroxylenol, triclosan, dipropylene glycol, PEG-50 rilanit special,
It stirs evenly to get the shampoo is arrived.
Embodiment 2
The present embodiment provides a kind of shampoo, raw material components include:
60 parts by weight of water, 8 parts by weight of glycerol, 1 parts by weight of Anjidew NL50,10 parts by weight of laureth sodium sulfovinate, cocounut oil acyl
10 parts by weight of amine propyl betaine, cocounut oil acyl hydrolyze 4 parts by weight of avenin potassium, 3 parts by weight of sodium lauroyl sarcosine, cocounut oil acyl
8 parts by weight of amine DEA, 5 parts by weight of sodium cocoamphoacetate, 0.3 parts by weight of PEG-7 glyceryl cocoate, PEG-40 hydrogenation
1.5 parts by weight of castor oil, 0.2 parts by weight of Polyquaternium-10, hydrolysis 1 parts by weight of Jojoba esters, 0.2 weight of Fructus Citri grandis extract
Part, 0.2 parts by weight of butanediol, 0.01 parts by weight of ginseng root extract, 0.1 parts by weight of rhizoma anemarrhenae root extract, ginger-root extract
0.01 parts by weight, 0.1 parts by weight of Angelica roots, 0.01 parts by weight of Cacumen Platycladi extract, 0.1 weight of fleece-flower root root extract
Part, 0.01 parts by weight of 1,2- pentanediol, 0.1 parts by weight of pungent glycol, 0.1 parts by weight of sodium chloride, saccharomycetes to make fermentation Product filtrate 0.5
Parts by weight, 0.1 parts by weight of polysorbate -60,0.5 parts by weight of orange oil, 0.01 parts by weight of citric acid, DMDM hydantoin
0.15 parts by weight, 0.15 parts by weight of sodium benzoate, 0.02 parts by weight of dichloroxylenol, 0.014 parts by weight of triclosan, dipropylene glycol
0.02 parts by weight, 0.1 parts by weight of PEG-50 rilanit special, 0.1 parts by weight of salicylic acid, 0.01 parts by weight of EDETATE SODIUM；
The Fructus Citri grandis extract is prepared with the following method: isolating pomelo peel from shaddock, adds into pomelo peel
Enter the Ca (OH) of the 2wt% of 15 times of quality2Solution impregnate 6h, after filter, discard filtrate, obtain filter residue；By filter residue vacuum
It after drying, is placed in supercritical extract tank, is filled with CO2Extraction, the temperature of extraction are 45 DEG C, and the pressure of extraction is 40MPa, extraction
Time be 2h, isolated Fructus Citri grandis extract.
Further, a kind of method preparing the shampoo is provided, is included the following steps:
(1) first with 3000r/min homogeneous 8min after water and Polyquaternium-10 being mixed, after be heated to 85 DEG C, then
With 2500r/min homogeneous 12min, A phase is obtained；
(2) glycerol, laureth sodium sulfovinate, cocounut oil acyl hydrolysis avenin potassium, cocounut oil acyl are sequentially added into A phase
Amine propyl betaine, sodium lauroyl sarcosine, coconut oleoyl amine DEA, sodium cocoamphoacetate, PEG-7 glyceryl cocoate,
Jojoba esters, sodium chloride, citric acid, salicylic acid, EDETATE SODIUM are hydrolyzed, with the stirring of 600r/min under 85 DEG C of constant temperatures
Speed stirs 10min, obtains B phase；
(3) 65 DEG C are heated to after mixing Cremophor RH40, polysorbate -60, orange oil, is mixed
Material with 3000r/min homogeneous 1min, is cooled to 40 DEG C later, obtains C phase after mixing the mixture and B；
(4) sequentially added into C phase Anjidew NL50, Fructus Citri grandis extract, butanediol, ginseng root extract, rhizoma anemarrhenae root extract,
Ginger-root extract, Angelica roots, Cacumen Platycladi extract, fleece-flower root root extract, 1,2- pentanediol, pungent glycol, saccharomycete
Tunning filtrate, DMDM hydantoin, sodium benzoate, dichloroxylenol, triclosan, dipropylene glycol, PEG-50 rilanit special,
It stirs evenly to get the shampoo is arrived.
Embodiment 3
The present embodiment provides a kind of shampoo, raw material components include:
45 parts by weight of water, 4 parts by weight of glycerol, 5 parts by weight of Anjidew NL50,16 parts by weight of laureth sodium sulfovinate, cocounut oil acyl
6 parts by weight of amine propyl betaine, cocounut oil acyl hydrolyze 7 parts by weight of avenin potassium, 6 parts by weight of sodium lauroyl sarcosine, cocounut oil acyl
2 parts by weight of amine DEA, 1 parts by weight of sodium cocoamphoacetate, 1.2 parts by weight of PEG-7 glyceryl cocoate, PEG-40 hydrogenation
0.6 parts by weight of castor oil, 0.6 parts by weight of Polyquaternium-10, hydrolysis 0.4 parts by weight of Jojoba esters, 0.6 weight of Fructus Citri grandis extract
Measure part, 0.06 parts by weight of butanediol, 0.08 parts by weight of ginseng root extract, 0.03 parts by weight of rhizoma anemarrhenae root extract, race extraction
0.08 parts by weight of object, 0.03 parts by weight of Angelica roots, 0.08 parts by weight of Cacumen Platycladi extract, fleece-flower root root extract 0.03
Parts by weight, 0.08 parts by weight of 1,2- pentanediol, 0.03 parts by weight of pungent glycol, 0.5 parts by weight of sodium chloride, the filter of saccharomycetes to make fermentation product
0.2 parts by weight of liquid, 0.4 parts by weight of polysorbate -60,0.2 parts by weight of orange oil, 0.08 parts by weight of citric acid, in DMDM second
0.06 parts by weight of uride, 0.08 parts by weight of sodium benzoate, 0.035 parts by weight of dichloroxylenol, 0.008 parts by weight of triclosan, double third
0.08 parts by weight of glycol, 0.03 parts by weight of PEG-50 rilanit special, 0.22 parts by weight of salicylic acid, 0.08 weight of EDETATE SODIUM
Part；
The Fructus Citri grandis extract is prepared with the following method: isolating pomelo peel from shaddock, adds into pomelo peel
Enter the Ca (OH) of the 1.8wt% of 12 times of quality2Solution impregnate 7h, after filter, discard filtrate, obtain filter residue；Filter residue is true
After sky is dry, it is placed in supercritical extract tank, is filled with CO2Extraction, the temperature of extraction are 42 DEG C, and the pressure of extraction is 50MPa, extraction
The time taken is 2.5h, isolated Fructus Citri grandis extract.
Further, a kind of method preparing the shampoo is provided, is included the following steps:
(1) first with 2500r/min homogeneous 8min after water and Polyquaternium-10 being mixed, after be heated to 80 DEG C, then
With 2000r/min homogeneous 10min, A phase is obtained；
(2) glycerol, laureth sodium sulfovinate, cocounut oil acyl hydrolysis avenin potassium, cocounut oil acyl are sequentially added into A phase
Amine propyl betaine, sodium lauroyl sarcosine, coconut oleoyl amine DEA, sodium cocoamphoacetate, PEG-7 glyceryl cocoate,
Jojoba esters, sodium chloride, citric acid, salicylic acid, EDETATE SODIUM are hydrolyzed, with the stirring of 300r/min under 80 DEG C of constant temperatures
Speed stirs 12min, obtains B phase；
(3) 60 DEG C are heated to after mixing Cremophor RH40, polysorbate -60, orange oil, is mixed
Material with 2500r/min homogeneous 2min, is cooled to 40 DEG C later, obtains C phase after mixing the mixture and B；
(4) sequentially added into C phase Anjidew NL50, Fructus Citri grandis extract, butanediol, ginseng root extract, rhizoma anemarrhenae root extract,
Ginger-root extract, Angelica roots, Cacumen Platycladi extract, fleece-flower root root extract, 1,2- pentanediol, pungent glycol, saccharomycete
Tunning filtrate, DMDM hydantoin, sodium benzoate, dichloroxylenol, triclosan, dipropylene glycol, PEG-50 rilanit special,
It stirs evenly to get the shampoo is arrived.
Embodiment 4
The present embodiment provides a kind of shampoo, raw material components include:
50 parts by weight of water, 6 parts by weight of glycerol, 2 parts by weight of Anjidew NL50,12 parts by weight of laureth sodium sulfovinate, cocounut oil acyl
9 parts by weight of amine propyl betaine, cocounut oil acyl hydrolyze 5 parts by weight of avenin potassium, 4 parts by weight of sodium lauroyl sarcosine, cocounut oil acyl
5 parts by weight of amine DEA, 3 parts by weight of sodium cocoamphoacetate, 0.5 parts by weight of PEG-7 glyceryl cocoate, PEG-40 hydrogenation
1 parts by weight of castor oil, 0.4 parts by weight of Polyquaternium-10, hydrolysis 0.6 parts by weight of Jojoba esters, 0.4 weight of Fructus Citri grandis extract
Part, 0.12 parts by weight of butanediol, 0.03 parts by weight of ginseng root extract, 0.08 parts by weight of rhizoma anemarrhenae root extract, ginger-root extract
0.03 parts by weight, 0.08 parts by weight of Angelica roots, 0.03 parts by weight of Cacumen Platycladi extract, 0.08 weight of fleece-flower root root extract
Measure part, 0.03 parts by weight of 1,2- pentanediol, 0.08 parts by weight of pungent glycol, 0.3 parts by weight of sodium chloride, saccharomycetes to make fermentation Product filtrate
0.4 parts by weight, 0.2 parts by weight of polysorbate -60,0.3 parts by weight of orange oil, 0.03 parts by weight of citric acid, acyl in DMDM second
It is 0.12 parts by weight of urea, 0.12 parts by weight of sodium benzoate, 0.025 parts by weight of dichloroxylenol, 0.012 parts by weight of triclosan, double third sweet
0.03 parts by weight of alcohol, 0.08 parts by weight of PEG-50 rilanit special, 0.15 parts by weight of salicylic acid, 0.03 parts by weight of EDETATE SODIUM；
The Fructus Citri grandis extract is prepared with the following method: isolating pomelo peel from shaddock, adds into pomelo peel
Enter the Ca (OH) of the 1.8wt% of 12 times of quality2Solution impregnate 7h, after filter, discard filtrate, obtain filter residue；Filter residue is true
After sky is dry, it is placed in supercritical extract tank, is filled with CO2Extraction, the temperature of extraction are 42 DEG C, and the pressure of extraction is 50MPa, extraction
The time taken is 2.5h, isolated Fructus Citri grandis extract.
Further, a kind of method preparing the shampoo is provided, is included the following steps:
(1) first with 2500r/min homogeneous 8min after water and Polyquaternium-10 being mixed, after be heated to 80 DEG C, then
With 2000r/min homogeneous 10min, A phase is obtained；
(2) glycerol, laureth sodium sulfovinate, cocounut oil acyl hydrolysis avenin potassium, cocounut oil acyl are sequentially added into A phase
Amine propyl betaine, sodium lauroyl sarcosine, coconut oleoyl amine DEA, sodium cocoamphoacetate, PEG-7 glyceryl cocoate,
Jojoba esters, sodium chloride, citric acid, salicylic acid, EDETATE SODIUM are hydrolyzed, with the stirring of 300r/min under 80 DEG C of constant temperatures
Speed stirs 12min, obtains B phase；
(3) 60 DEG C are heated to after mixing Cremophor RH40, polysorbate -60, orange oil, is mixed
Material with 2500r/min homogeneous 2min, is cooled to 40 DEG C later, obtains C phase after mixing the mixture and B；
(4) sequentially added into C phase Anjidew NL50, Fructus Citri grandis extract, butanediol, ginseng root extract, rhizoma anemarrhenae root extract,
Ginger-root extract, Angelica roots, Cacumen Platycladi extract, fleece-flower root root extract, 1,2- pentanediol, pungent glycol, saccharomycete
Tunning filtrate, DMDM hydantoin, sodium benzoate, dichloroxylenol, triclosan, dipropylene glycol, PEG-50 rilanit special,
It stirs evenly to get the shampoo is arrived.
Embodiment 5
The present embodiment provides a kind of shampoo, raw material components include:
48.31 parts by weight of water, 5 parts by weight of glycerol, 3 parts by weight of Anjidew NL50,14 parts by weight of laureth sodium sulfovinate, coconut palm
8 parts by weight of oleamide propyl betaine, cocounut oil acyl hydrolyze 6 parts by weight of avenin potassium, 5 parts by weight of sodium lauroyl sarcosine, coconut palm
3 parts by weight of oleamide DEA, 2 parts by weight of sodium cocoamphoacetate, 1 parts by weight of PEG-7 glyceryl cocoate, PEG-40 hydrogen
Change 0.8 parts by weight of castor oil, 0.5 parts by weight of Polyquaternium-10, hydrolysis 0.5 parts by weight of Jojoba esters, Fructus Citri grandis extract 0.5
Parts by weight, 0.1 parts by weight of butanediol, 0.05 parts by weight of ginseng root extract, 0.05 parts by weight of rhizoma anemarrhenae root extract, race extract
0.05 parts by weight of object, 0.05 parts by weight of Angelica roots, 0.05 parts by weight of Cacumen Platycladi extract, fleece-flower root root extract 0.05
Parts by weight, 0.05 parts by weight of 1,2- pentanediol, 0.05 parts by weight of pungent glycol, 0.4 parts by weight of sodium chloride, the filter of saccharomycetes to make fermentation product
0.3 parts by weight of liquid, 0.3 parts by weight of polysorbate -60,0.25 parts by weight of orange oil, 0.05 parts by weight of citric acid, DMDM second
It is interior 0.1 parts by weight of uride, 0.1 parts by weight of sodium benzoate, 0.03 parts by weight of dichloroxylenol, 0.01 parts by weight of triclosan, double third sweet
0.05 parts by weight of alcohol, 0.05 parts by weight of PEG-50 rilanit special, 0.2 parts by weight of salicylic acid, 0.05 parts by weight of EDETATE SODIUM；
The Fructus Citri grandis extract is prepared with the following method: isolating pomelo peel from shaddock, adds into pomelo peel
Enter the Ca (OH) of the 1.8wt% of 12 times of quality2Solution impregnate 7h, after filter, discard filtrate, obtain filter residue；Filter residue is true
After sky is dry, it is placed in supercritical extract tank, is filled with CO2Extraction, the temperature of extraction are 42 DEG C, and the pressure of extraction is 50MPa, extraction
The time taken is 2.5h, isolated Fructus Citri grandis extract.
Further, a kind of method preparing the shampoo is provided, is included the following steps:
(1) first with 2500r/min homogeneous 8min after water and Polyquaternium-10 being mixed, after be heated to 80 DEG C, then
With 2000r/min homogeneous 10min, A phase is obtained；
(2) glycerol, laureth sodium sulfovinate, cocounut oil acyl hydrolysis avenin potassium, cocounut oil acyl are sequentially added into A phase
Amine propyl betaine, sodium lauroyl sarcosine, coconut oleoyl amine DEA, sodium cocoamphoacetate, PEG-7 glyceryl cocoate,
Jojoba esters, sodium chloride, citric acid, salicylic acid, EDETATE SODIUM are hydrolyzed, with the stirring of 300r/min under 80 DEG C of constant temperatures
Speed stirs 12min, obtains B phase；
(3) 60 DEG C are heated to after mixing Cremophor RH40, polysorbate -60, orange oil, is mixed
Material with 2500r/min homogeneous 2min, is cooled to 40 DEG C later, obtains C phase after mixing the mixture and B；
(4) sequentially added into C phase Anjidew NL50, Fructus Citri grandis extract, butanediol, ginseng root extract, rhizoma anemarrhenae root extract,
Ginger-root extract, Angelica roots, Cacumen Platycladi extract, fleece-flower root root extract, 1,2- pentanediol, pungent glycol, saccharomycete
Tunning filtrate, DMDM hydantoin, sodium benzoate, dichloroxylenol, triclosan, dipropylene glycol, PEG-50 rilanit special,
It stirs evenly to get the shampoo is arrived.
Comparative example 1
Difference with embodiment 5, which is only that, removes hydrolysis Jojoba esters, Fructus Citri grandis extract, saccharomycetes to make fermentation Product filtrate
And orange oil.
Comparative example 2
Difference with embodiment 5, which is only that, removes ginseng root extract, rhizoma anemarrhenae root extract, ginger-root extract, angelica root
Extract, Cacumen Platycladi extract and fleece-flower root root extract.
Experimental example
1, quality testing
Microorganism project and hygienic chemistry item-test have been carried out according to " cosmetics safety technical specification " version in 2015, has been tied
Fruit is shown in Table 1~2:
1 Micro biological Tests result of table
| Inspection project | Testing result | Limit value |
| Total plate count (CFU/g) | <10 | ≤1000 |
| Yeast and mold sum (CFU/g) | <10 | ≤100 |
| Heat-resisting coliform/g | It is not detected | It must not detect |
| Staphylococcus aureus/g | It is not detected | It must not detect |
| Pseudomonas aeruginosa/g | It is not detected | It must not detect |
2 health chemical testing result of table
2, skin patch test
The age is chosen in 20-40 years old 50 people of volunteer as subject, 0.02mL Examples 1 to 5, right will be respectively provided with
The spot tester of 1~2 shampoo of ratio is affixed on the inner forearm of subject with adhesive tape, continues for 24 hours, blank control to be separately arranged.Respectively
In removal 30min after by spot tester, for 24 hours with 48h according to the form below standard sight dermoreaction, and observation is recorded as a result, being shown in Table 3~4.
3 skin patch test dermoreaction classification identification standard of table
4 human skin patch test result of table
As can be seen that Examples 1 to 5 only has suspicious reaction within 2 people to occur in 30min, and for 24 hours and 48h, own
Subject is negative reaction, although and comparative example 1 and comparative example 2 all subjects in 48h are negative reaction,
There is 5 people or more suspicious reaction when 30min, still there is suspicious reaction example for 24 hours, illustrates that the skin irritation of Examples 1 to 5 is obviously low
Illustrate further according to the analysis, irritation is mainly derived from the addition of larger dose surfactant by water in comparative example 1~2
Solve Jojoba esters, Fructus Citri grandis extract, ginseng root extract, rhizoma anemarrhenae root extract, ginger-root extract, Angelica roots, side
CedarLeaves extract, fleece-flower root root extract, saccharomycetes to make fermentation Product filtrate and orange oil these ingredients use simultaneously, Neng Gou great
Width reduces the skin irritation of surfactant, and then improves the whole usage comfort of shampoo.
3, efficacy test
Selecting the age in 20~40 years old 30 people (Dry Hair and oily hair are fifty-fifty) is test object, is randomly divided into 3
Group, every group of 10 people, each group there are no significant in terms of age, hair quality difference.Each group use respectively embodiment 5, comparative example 1 and
The shampoo that comparative example 2 is prepared.Specifically used method are as follows: after drenching hair, take 3g shampoo at the palm of the hand, wait rub
It after blistering, is uniformly applied on hair, then mildly rubs 2~3min from root of hair to the hair tip, rinsed 2 times with clear water later.Each group
A shampoo is used daily, is used continuously 3 months, and the effect after use is collected in the form of questionnaire.Items use effect
In terms of fruit is divided by full marks 10,9-10 points indicate that effects are excellent, and 6-9 points indicate that effects are preferable, and 4-6 points indicate that effects are general, 4 points of following tables
Show that effect is poor, every using effect average situation is as shown in table 5.
5 using effect average situation of table
| Group | Shampoo | Black hair | Anti-hair loss | Moisturizing resists short-tempered | Anti- bifurcated |
| Test group 1 | Embodiment 5 | 6.2 | 7.8 | 9.3 | 6.9 |
| Test group 2 | Comparative example 1 | 4.1 | 4.6 | 5.2 | 3.7 |
| Test group 3 | Comparative example 2 | 4.3 | 5.2 | 5.9 | 3.4 |
The result shows that the usage experience of the embodiment of the present invention 5 is substantially better than comparative example, further according to the analysis, the present invention
By the rational proportion of conditioner ingredient, so that various raw materials act synergistically, thus the shampoo finally prepared is with stronger
Black hair strengthen the hair improves effect that is withered and preventing hair bifurcated.
The above description is merely a specific embodiment, but scope of protection of the present invention is not limited thereto, any
Those familiar with the art in the technical scope disclosed by the present invention, can easily think of the change or the replacement, and should all contain
Lid is within protection scope of the present invention.Therefore, protection scope of the present invention should be based on the protection scope of the described claims.
Claims (10)
1. a kind of shampoo, which is characterized in that raw material components include: water 40-60 parts by weight, glycerol 3-8 parts by weight, Anjidew NL50 1-8
Parts by weight, surfactant 22-60 parts by weight, solubilizer 0.3-1.5 parts by weight, Polyquaternium-10 0.2-1 parts by weight, hydrolysis
Jojoba esters 0.2-1 parts by weight, Fructus Citri grandis extract 0.2-1 parts by weight, butanediol 0.02-0.2 parts by weight, ginseng root extract
0.01-0.1 parts by weight, rhizoma anemarrhenae root extract 0.01-0.1 parts by weight, ginger-root extract 0.01-0.1 parts by weight, angelica root extract
Object 0.01-0.1 parts by weight, Cacumen Platycladi extract 0.01-0.1 parts by weight, fleece-flower root root extract 0.01-0.1 parts by weight, 1,2-
Pentanediol 0.01-0.1 parts by weight, pungent glycol 0.01-0.1 parts by weight, thickener 0.1-0.8 parts by weight, saccharomycetes to make fermentation product
Filtrate 0.1-0.5 parts by weight, -60 0.1-0.6 parts by weight of polysorbate, orange oil 0.1-0.5 parts by weight, pH adjusting agent
0.01-0.1 parts by weight, preservative 0.08-0.3 parts by weight, dichloroxylenol 0.02-0.04 parts by weight, triclosan 0.006-0.014
Parts by weight, dipropylene glycol 0.02-0.1 parts by weight, PEG-50 rilanit special 0.02-0.1 parts by weight, salicylic acid 0.1-0.3 weight
Measure part, chelating agent 0.01-0.1 parts by weight.
2. shampoo according to claim 1, which is characterized in that raw material components include: water 45-50 parts by weight, glycerol 4-6
Parts by weight, Anjidew NL50 2-5 parts by weight, surfactant 30-47 parts by weight, solubilizer 0.6-1 parts by weight, Polyquaternium-10
0.4-0.6 parts by weight, hydrolysis Jojoba esters 0.4-0.6 parts by weight, Fructus Citri grandis extract 0.4-0.6 parts by weight, butanediol 0.06-
0.12 parts by weight, ginseng root extract 0.03-0.08 parts by weight, rhizoma anemarrhenae root extract 0.03-0.08 parts by weight, ginger-root extract
0.03-0.08 parts by weight, Angelica roots 0.03-0.08 parts by weight, Cacumen Platycladi extract 0.03-0.08 parts by weight, He Shou
Black root extract 0.03-0.08 parts by weight, pungent glycol 0.03-0.08 parts by weight, increase 1,2- pentanediol 0.03-0.08 parts by weight
Thick dose of 0.3-0.5 parts by weight, saccharomycetes to make fermentation Product filtrate 0.2-0.4 parts by weight, -60 0.2-0.4 weight of polysorbate
Part, orange oil 0.2-0.3 parts by weight, pH adjusting agent 0.03-0.08 parts by weight, preservative 0.14-0.24 parts by weight, dichloroxylenol
0.025-0.035 parts by weight, triclosan 0.008-0.012 parts by weight, dipropylene glycol 0.03-0.08 parts by weight, PEG-50 hydrogenation
Castor oil 0.03-0.08 parts by weight, salicylic acid 0.15-0.22 parts by weight, chelating agent 0.03-0.08 parts by weight.
3. shampoo according to claim 1, which is characterized in that raw material components include: 48.31 parts by weight of water, 5 weight of glycerol
Measure part, 3 parts by weight of Anjidew NL50,39 parts by weight of surfactant, 0.8 parts by weight of solubilizer, 0.5 parts by weight of Polyquaternium-10, water
Solve 0.5 parts by weight of Jojoba esters, 0.5 parts by weight of Fructus Citri grandis extract, 0.1 parts by weight of butanediol, 0.05 weight of ginseng root extract
Measure part, 0.05 parts by weight of rhizoma anemarrhenae root extract, 0.05 parts by weight of ginger-root extract, 0.05 parts by weight of Angelica roots, arbor-vitae
0.05 parts by weight of leaf extract, 0.05 parts by weight of fleece-flower root root extract, 0.05 parts by weight of 1,2- pentanediol, 0.05 weight of pungent glycol
Measure part, 0.4 parts by weight of thickener, 0.3 parts by weight of saccharomycetes to make fermentation Product filtrate, 0.3 parts by weight of polysorbate -60, sweet orange
Oily 0.25 parts by weight, 0.05 parts by weight of pH adjusting agent, 0.2 parts by weight of preservative, 0.03 parts by weight of dichloroxylenol, triclosan 0.01
Parts by weight, 0.05 parts by weight of dipropylene glycol, 0.05 parts by weight of PEG-50 rilanit special, 0.2 parts by weight of salicylic acid, chelating agent
0.05 parts by weight.
4. shampoo according to claim 1, which is characterized in that the surfactant is laureth sulfuric ester
Sodium, cocounut oil acyl hydrolyze avenin potassium, Cocoamidopropyl betaine, sodium lauroyl sarcosine, coconut oleoyl amine DEA, cocounut oil acyl
The mixture of any one or more in both sexes guanidine-acetic acid sodium, PEG-7 glyceryl cocoate.
5. shampoo according to claim 1, which is characterized in that the Fructus Citri grandis extract is prepared into the following method
To: pomelo peel is isolated from shaddock, and the Ca (OH) of 1.5~2wt% of 10~15 times of quality is added into pomelo peel2Solution leaching
Steep 6~8h, after filter, discard filtrate, obtain filter residue；It after filter residue is dried in vacuo, is placed in supercritical extract tank, is filled with
CO2Extraction, isolated Fructus Citri grandis extract.
6. shampoo according to claim 5, which is characterized in that the temperature of the extraction is 40~45 DEG C, the extraction
Pressure be 40~55MPa, time of the extraction is 2~3h.
7. a kind of method for preparing any one of claim 1-6 shampoo, which comprises the steps of:
(1) will water and Polyquaternium-10 mix after first carry out first time homogeneous, after heat, then carry out second of homogeneous,
Obtain A phase；
(2) sequentially added into A phase glycerol, surfactant, hydrolysis Jojoba esters, thickener, pH adjusting agent, salicylic acid,
Chelating agent is stirred to dissolve completely, obtains B phase；
(3) it is heated after mixing solubilizer, polysorbate -60, orange oil, obtains mixture, the mixture and B phase are mixed
After conjunction, homogeneous cools down later, obtains C phase；
(4) Anjidew NL50, Fructus Citri grandis extract, butanediol, ginseng root extract, rhizoma anemarrhenae root extract, race are sequentially added into C phase
Extract, Angelica roots, Cacumen Platycladi extract, fleece-flower root root extract, 1,2- pentanediol, pungent glycol, saccharomycetes to make fermentation
Product filtrate, preservative, dichloroxylenol, triclosan, dipropylene glycol, PEG-50 rilanit special stir evenly to get described in
Shampoo.
8. the method according to claim 7 for preparing shampoo, which is characterized in that in step (1), the first time homogeneous
Revolving speed be 2000~3000r/min, time of the first time homogeneous is 8~12min, described to be heated to 75~85 DEG C, institute
The revolving speed for stating second of homogeneous is 2000~2500r/min, and the time of second of homogeneous is 8~12min.
9. the method according to claim 7 for preparing shampoo, which is characterized in that in step (2), the stirring 75~
It is carried out under 85 DEG C of constant temperatures, the speed of the stirring is 100~600r/min, and the time of the stirring is 10~15min.
10. the method according to claim 7 for preparing shampoo, which is characterized in that described to be heated to 55 in step (3)
~65 DEG C, the revolving speed of the homogeneous is 2000~3000r/min, and the time of the homogeneous is 1~3min, described to be cooled to 45 DEG C
Below.
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| CN110613627A (en) * | 2019-10-25 | 2019-12-27 | 上海中医药大学 | Cosmetic and preparation method thereof |
| CN110638698A (en) * | 2019-10-29 | 2020-01-03 | 扬州大自然生物科技有限公司 | Male shampoo and production method thereof |
| CN110693789A (en) * | 2019-11-20 | 2020-01-17 | 广东柚通柚美农产品技术研究有限公司 | Natural plant grapefruit essence shampoo and preparation method thereof |
| CN111166703A (en) * | 2019-11-20 | 2020-05-19 | 高林岗 | Shampoo and preparation method thereof |
| CN110974771A (en) * | 2019-12-27 | 2020-04-10 | 广州蜜妆生物科技有限公司 | Scalp care composition and application thereof |
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