CN110339118A - Has effects that the skin whitener of skin whitening, moisturizing - Google Patents
Has effects that the skin whitener of skin whitening, moisturizing Download PDFInfo
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- CN110339118A CN110339118A CN201910764423.3A CN201910764423A CN110339118A CN 110339118 A CN110339118 A CN 110339118A CN 201910764423 A CN201910764423 A CN 201910764423A CN 110339118 A CN110339118 A CN 110339118A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/36—Carboxylic acids; Salts or anhydrides thereof
- A61K8/361—Carboxylic acids having more than seven carbon atoms in an unbroken chain; Salts or anhydrides thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/37—Esters of carboxylic acids
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
- A61K8/44—Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/49—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds
- A61K8/494—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with more than one nitrogen as the only hetero atom
- A61K8/4946—Imidazoles or their condensed derivatives, e.g. benzimidazoles
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
- A61K8/86—Polyethers
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9789—Magnoliopsida [dicotyledons]
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/02—Preparations for care of the skin for chemically bleaching or whitening the skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/59—Mixtures
- A61K2800/592—Mixtures of compounds complementing their respective functions
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/85—Products or compounds obtained by fermentation, e.g. yoghurt, beer, wine
Abstract
The present invention relates to cosmetic field, being difficult to that melanin is inhibited to lead to the problem of, providing a kind of has effects that the skin whitener of skin whitening, moisturizing, including A composition: 3-4 parts of cetostearyl alcohol；7-10 parts of emulsifier；4-6 parts of saualane；5-7 parts of isopropyl myristate；3-6 parts of isononyl isononanoate；1-2 parts of dimethyl silicone polymer；0.3-0.8 parts of vitamin E；0.01-0.2 parts of propyl ester；Composition B: 30-35 parts of water；0.1-0.5 parts of triethanolamine；1.5-2.5 parts of tranexamic acid；0.1-0.2 parts of allantoin；0.1-0.2 parts of methyl esters；4-5 parts of Papain ferment.By using being used in compounding for tranexamic acid, allantoin, methyl esters and Papain ferment, be conducive to inhibit the generation of melanin in skin, so that melanin can be solved on source, simultaneously, be conducive to cutin-softening layer to promote falling off for the dead cell of cuticula, the content of the melanin in skin is advantageously reduced, so that the whitening effect of skin whitener enhances.
Description
Technical field
The present invention relates to cosmetic fields, more specifically, it relates to which a kind of have effects that the skin whitener of skin whitening, moisturizing.
Background technique
The colour of skin is that people examine one of standard of beauty.For Asia women, the pale colour of skin is even more that one kind is generally pursued.Thus,
All kinds of whitening products and method for whitening emerge one after another.
Existing whitening product accelerates cuticula dead generally by the ingredients cutin-softening layer such as tartaric acid, dissolved ceratinase
Cell detachment is died to promote epidermis metabolic, so that into the melanosome in epidermis in the metabolic process with epidermis
It quickly updates and falls off, and then mitigate influence of the melanin to skin color to achieve the effect that whitening.But present whitening
Product can only generally excrete the melanin generated in human body, it is difficult to inhibit the generation of melanin, so that product
Whitening effect always be " palliative ", therefore, still there is improved space.
Summary of the invention
In view of the deficienciess of the prior art, the first object of the present invention is to provide and a kind of has effects that skin whitening, moisturizing
Skin whitener has the advantages that be conducive to that melanin is inhibited to generate.
To achieve the above object, the present invention provides the following technical scheme that
It is a kind of to have effects that the skin whitener of skin whitening, moisturizing, including A composition, composition B, C in combination object, D composition, E group
Close object and F composition；
The A composition includes the component of following mass fraction:
3-4 parts of cetostearyl alcohol；
7-10 parts of emulsifier；
4-6 parts of saualane；
5-7 parts of isopropyl myristate；
3-6 parts of isononyl isononanoate；
1-2 parts of dimethyl silicone polymer；
0.3-0.8 parts of vitamin E；
0.01-0.2 parts of propyl ester；
The composition B includes the component of following mass fraction:
30-35 parts of water；
0.1-0.5 parts of triethanolamine；
1.5-2.5 parts of tranexamic acid；
0.1-0.2 parts of allantoin；
0.1-0.2 parts of methyl esters；
4-5 parts of Papain ferment；
The C in combination object includes the component of following mass fraction:
2-3 parts of niacinamide；
5-6 parts of water；
The D composition includes the component of following mass fraction:
2-3 parts of tussol；
1-2 parts of macromolecular salicylic acid；
3-4 parts of propylene glycol；
5-7 parts of water；
The E composition includes the component of following mass fraction:
1-2 parts of alpha-arbutin；
5-8 parts of water；
The F composition includes the component of following mass fraction:
0.2-0.5 parts of De Minshu；
1-1.5 parts of Chinese herbaceous peony extracting solution；
0.5-1 parts of shea oil.
By adopting the above technical scheme, by using tranexamic acid, allantoin, methyl esters and Papain ferment in composition B
Be used in compounding, be conducive to inhibit skin in melanin generation so that melanin can be solved on source, and then be conducive to
The melanin content in skin is reduced, so that the whitening effect of skin whitener enhances；Meanwhile tranexamic acid, allantoin, methyl esters and wood
Being used in compounding for melon Pepsin also helps falling off for dead cell of the cutin-softening layer to promote cuticula, to be conducive to
Promote the metabolism of epidermis, so that the melanosome for entering to epidermis is easier to separate with skin in the metabolic process,
And then the content of the melanin in skin is advantageously reduced, be conducive to bright color, so that the whitening effect of skin whitener enhances；
Since the cuticula of removal aging is easy so that skin is relatively dry, and dry skin is more prone to produce black
Element is conducive to by using being used in compounding for De Minshu, Chinese herbaceous peony extracting solution and shea oil in F composition as skin
Extra-nutrition and moisture in time, so that the moistening effect of skin improves, so that be conducive to skin is in moisture abundance always
State advantageously reduce the melanin content in skin so that skin is not allowed more to be also easy to produce melanin so that whitening
The whitening effect of frost is more preferable, more longlasting；
To sum up, by composition B and the coordinated of F composition, and A composition, C in combination object, D composition and
Under the facilitation of E composition, be conducive to the generation for inhibiting the melanin in skin, so that the problem of melanin from source
To solve, meanwhile, the removing speed for accelerating melanin is also helped, to advantageously reduce the melanin content in skin, separately
Outside, the moistening effect in skin is also advantageously improved, so that skin is not easy dry feelings occur because removing cuticula
Condition is conducive to solve the problems, such as melanin from the root so that skin is not allowed more to be also easy to produce melanin, so that whitening
It is more preferable, more longlasting that the colour of skin of frost highlights effect, whitening effect and moistening effect.
The present invention is further arranged to: the emulsifier by octadecanoid acid, tristerin/PEG-100 stearate,
Polyoxyethylene -2 (21) tristearin alcohol ether is mixed in the ratio of 3.5:2.5:4.
By adopting the above technical scheme, by by octadecanoid acid, tristerin/PEG-100 stearate, polyoxy second
Alkene -2 (21) tristearin alcohol ether is mixed to form emulsifier in the ratio of 3.5:2.5:4, and each component be conducive in skin whitener is abundant
Emulsification is conducive to the sophistication for improving the lotion of skin whitener so that each component is more easily mutually mixed and is uniformly dispersed, into
And be conducive to improve the stability of skin whitener, so that skin whitener product quality is more stable, and then be conducive to improve skin whitener
Whitening effect and moistening effect.
The present invention is further arranged to: the composition B further includes the component of following mass fraction:
2-2.5 parts of anti-caking agent.
By adopting the above technical scheme, by addition anti-caking agent, be conducive to the degree of scatter for improving skin whitener each component, from
And be conducive to white lotion sophistication of staying pale, so that skin whitener is more not easy during preparing and saving use
Existing caking phenomenon, and then be conducive to improve the stability of skin whitener lotion.
The present invention is further arranged to: the anti-caking agent is glycine betaine.
By adopting the above technical scheme, by using glycine betaine as anti-caking agent, so that skin whitener makes in preparation and preservation
It is not easy to occur the moistening effect for being conducive to improve skin whitener while caking phenomenon during, to be conducive to improve beauty
The stability of bloom product quality, meanwhile, so that skin is not easy dry situation occur because removing cuticula, so that
Skin is not allowed more to be also easy to produce melanin, is conducive to the whitening effect and moistening effect that improve skin whitener.
The present invention is further arranged to: the F composition further includes the component of following mass fraction:
0.2-0.3 parts of preservative.
By adopting the above technical scheme, by the way that preservative is added, it is conducive to extend the pot-life of skin whitener, so that skin whitener
More it is less likely to occur to go bad during preservation.
The present invention is further arranged to: the F composition further includes the component of following mass fraction:
0.01-0.03 parts of essence.
By adopting the above technical scheme, by the way that essence is added, be conducive to skin whitener and distribute pleasant fragrance, to be conducive to increase
The packaging effect of strong skin whitener is conducive to increase economic efficiency so that skin whitener is more suitable for the market demand and society need；Together
When, also advantageously improve the usage experience of user.
In view of the deficienciess of the prior art, the second object of the present invention is to provide and a kind of has effects that skin whitening, moisturizing
The preparation method of skin whitener has the advantages that preparing resulting skin whitener is conducive to that melanin is inhibited to generate.
To achieve the above object, the present invention provides the following technical scheme that
A kind of preparation method with the skin whitener of skin whitening, moisturizing, comprising the following steps:
It is S1, respectively that each component of A composition, composition B, C in combination object, D composition, E composition and F composition is each
It is mixed evenly from by mass parts ratio, obtains A composition, composition B, C in combination object, D composition, E composition and F group
Close object；
S2, in 50 DEG C -55 DEG C of at a temperature of mixing A compositions and composition B, form mixture, and homogenization is mixed
Close object 8-10min；
S3,65 DEG C -70 DEG C at a temperature of C in combination object and D composition are added into mixture, be uniformly mixed,
Form blend；
S4,45 DEG C -50 DEG C at a temperature of E composition and F composition are added into blend, stir evenly, then drop
Low temperature condenses into paste to 33 DEG C -35 DEG C to get having effects that the skin whitener of skin whitening, moisturizing.
By adopting the above technical scheme, it after the completion of by first preparing each composition respectively, then is added at different temperatures not
Same composition is mixed to prepare skin whitener, is conducive to each component and is better dispersed uniformly, to be conducive to each group
Divide and each composition preferably coordinated is to play effect, so that while skin more is not allowed to be also easy to produce melanin
So that the melanin in skin is easier to be removed, be conducive to the whitening effect and moistening effect that improve skin whitener；Meanwhile having
It is preferably fully emulsified conducive to each component, and then be conducive to improve the lotion sophistication for preparing resulting skin whitener, be conducive to mention
The product stability of high skin whitener, and then be conducive to each component in skin whitener and each composition preferably coordinated to send out
The effect of waving is conducive to the removing for inhibiting to be conducive to the melanin in skin while the generation of dermal melanin, so that skin whitener
Whitening effect and moistening effect it is more preferable.
The present invention is further arranged to: in the step S1, the mixing temperature of each component of A composition and composition B
Control is 80 DEG C -90 DEG C, mixing time 20min-30min.
By adopting the above technical scheme, by mixing temperature in mixed process of control A composition and composition B and
Mixing time is conducive to each component in A composition and composition B and is preferably uniformly dispersed mutually, to be conducive to improve A
The stability of composition and composition B so that the stability for preparing resulting skin whitener is more preferable, and then is conducive to skin whitener more
Whitening effect and moistening effect are played well.
The present invention is further arranged to: in the step S2, homogenization operation carries out under vacuum conditions.
By adopting the above technical scheme, it is carried out under vacuum conditions by homogeneous, so that the component in skin whitener is not allowed more
Easily by the dioxygen oxidation in air at other substances, to be conducive to improve the purity of each component in skin whitener, and then be conducive to
Each component in skin whitener preferably cooperates to play synergistic effect, so that the whitening effect and moistening effect of skin whitener are more
It is good.
In conclusion the invention has the following advantages:
1. being conducive to inhibit skin by using being used in compounding for tranexamic acid, allantoin, methyl esters and Papain ferment
The generation of middle melanin, so that melanin can be solved on source, meanwhile, be conducive to cutin-softening layer to promote cuticula
Dead cell falls off, and advantageously reduces the content of the melanin in skin, so that the whitening effect of skin whitener enhances；
2. being conducive to mend in time for skin by De Minshu, Chinese herbaceous peony extracting solution and shea oil coordinated
Nutrition and moisture are filled, so that skin is not allowed more to be also easy to produce melanin, so that the skin whitening, moisturizing effect of skin whitener is more preferable, more holds
Long；
3. by composition B and the coordinated of F composition, and in A composition, C in combination object, D composition and E group
Under the facilitation for closing object, be conducive to the generation for inhibiting the melanin in skin, be conducive to the removing speed for accelerating melanin, also
The moistening effect for being conducive to improve in skin is conducive to solve from the root so that skin is not allowed more to be also easy to produce melanin
The problem of melanin, so as to highlight effect, whitening effect and moistening effect more preferable, more longlasting for the colour of skin of skin whitener；
4. by by octadecanoid acid, tristerin/PEG-100 stearate, the stearic alcohol ether of polyoxyethylene -2 (21)
It is mixed to form emulsifier in the ratio of 3.5:2.5:4, each component be conducive in skin whitener is fully emulsified, is conducive to improve beauty
The sophistication of the lotion of bloom, so that skin whitener product quality is more stable, the whitening effect for being conducive to improve skin whitener is to protect
Wet effect.
Detailed description of the invention
Fig. 1 is to have effects that the process flow chart of the preparation method of the skin whitener of skin whitening, moisturizing in the present invention.
Specific embodiment
With reference to embodiments, invention is further described in detail.
In following embodiment, cetostearyl alcohol uses the cetostearyl alcohol of Nantong Run Feng petrochemical industry Co., Ltd.
In following embodiment, octadecanoid acid uses the octadecane of the model 1801 of Guangzhou to pure Chemical Co., Ltd.
Acid.
In following embodiment, tristerin/PEG-100 stearate creates the limited public affairs of fine chemistry industry using Guangzhou perseverance
The A165 emulsifier of department.
In following embodiment, polyoxyethylene -2 (21) tristearin alcohol ether uses the emulsification of Guangzhou Yi Jin Biotechnology Co., Ltd
Agent 72-721.
In following embodiment, saualane uses the article No. of Kodak Biotechnology Co., Ltd in Xi'an for the angle of ZKD1279
Shark alkane.
In following embodiment, isopropyl myristate uses 887 article No. of model of Jinan Xin Senyuan Chemical Co., Ltd.
For 4548 isopropyl myristate.
In following embodiment, isononyl isononanoate use the article No. of Shaanxi Wen Di Biotechnology Co., Ltd for
The isononyl isononanoate of YiD20190417.
In following embodiment, dimethyl silicone polymer use 202 article No. of model of Jinan Rong Guang Chemical Co., Ltd. for
78455 dimethyl silicone polymer.
In following embodiment, vitamin E uses the vitamin E of Zhengzhou best food additives Co., Ltd.
In following embodiment, propyl ester uses the n-propyl acetate of good Chemical Co., Ltd., Suzhou City nine.
In following embodiment, triethanolamine uses the article No. of Licheng District Li Rui industrial chemicals business department for three ethyl alcohol of TEA
Amine.
In following embodiment, tranexamic acid uses the blood coagulation of the model AM-021 of Guangzhou Pin Ding Chemical Industry Science Co., Ltd
Acid.
In following embodiment, allantoin uses the article No. of Changzhou Rong Ao new chemical materials Co., Ltd for the urine of ra-nns99
Bursin.
In following embodiment, methyl esters uses the fatty acid methyl ester of vast and boundless million Chemical Co., Ltd.s in Guangzhou.
In following embodiment, Papain ferment uses the Papain ferment of Henan Rui Ren bioengineering Co., Ltd.
In following embodiment, glycine betaine use the article No. of Henan Ji Mei Chemical Co., Ltd. for 2109 glycine betaine.
In following embodiment, niacinamide uses the article No. of Guangzhou Xin Ge trade Co., Ltd for the niacinamide of LS00-1.
In following embodiment, tussol uses the tussol of Xi'an Bai Chuan Biotechnology Co., Ltd.
In following embodiment, macromolecular salicylic acid uses the macromolecular salicylic acid of Guangzhou Jia Qi Biotechnology Co., Ltd.
In following embodiment, propylene glycol uses the propylene glycol of Guangzhou Jia Qi Biotechnology Co., Ltd.
In following embodiment, alpha-arbutin uses α-black bearberry of the model yc of Foshan Xin Hang Biotechnology Co., Ltd
Glycosides.
In following embodiment, De Minshu uses the De Minshu of Guangzhou Bao Long International Trading Company Ltd.
In following embodiment, Chinese herbaceous peony extracting solution uses the article No. of Guangzhou omega Biotechnology Co., Ltd for 20180708
Chinese herbaceous peony extracting solution.
In following embodiment, shea oil uses the model bam006 of Zhejiang Ba Shiman Biotechnology Co., Ltd
Organic shea rouge.
In following embodiment, preservative uses the Sang Pujiema A preservative of Guangzhou Jia Qi Biotechnology Co., Ltd.
In following embodiment, essence uses the essence of the easy Chemical Co., Ltd. of new east station of Guangzhou, and the odor type of essence is used according to reality
Border needs to choose, and does not have an impact to essence of the invention.
Embodiment 1
It is a kind of to have effects that the skin whitener of skin whitening, moisturizing, including A composition, composition B, C in combination object, D composition, E group
Close object and F composition；
A composition includes following components:
Cetostearyl alcohol 3kg；Emulsifier 10kg；Saualane 5kg；Isopropyl myristate 5kg；Isononyl isononanoate 6kg；
Dimethyl silicone polymer 1.5kg；Vitamin E 0.3kg；Propyl ester 0.2kg；
Composition B includes following components:
Water 32.5kg；Triethanolamine 0.1kg；Tranexamic acid 2.5kg；Allantoin 0.2kg；Methyl esters 0.2kg；Papain ferment
5kg；
C in combination object includes following components:
Niacinamide 2.5kg；Water 5kg；
D composition includes following components:
Tussol 3kg；Macromolecular salicylic acid 1.5kg；Propylene glycol 3kg；Water 6kg；
E composition includes following components:
Alpha-arbutin 1.5kg；Water 5kg；
F composition includes following components:
De Minshu 0.35kg；Chinese herbaceous peony extracting solution 1.25kg；Shea oil 0.5kg.
In the present embodiment, emulsifier is octadecanoid acid.
Have effects that the skin whitener of skin whitening, moisturizing the preparation method is as follows:
S1, before manufacture, production equipment and apparatus are cleaned up and are sterilized, whale then is added in No. 1 reaction kettle
Wax stearyl alcohol 3kg, emulsifier 10kg, saualane 5kg, isopropyl myristate 5kg, isononyl isononanoate 6kg, poly dimethyl silicon
Oxygen alkane 1.5kg, vitamin E 0.3kg, propyl ester 0.2kg, warming while stirring is to 80 DEG C, and insulated and stirred 30min, stirs evenly,
Form A composition；Water 32.5kg is added in No. 2 reaction kettles；Triethanolamine 0.1kg；Tranexamic acid 2.5kg, allantoin 0.2kg,
Methyl esters 0.2kg, Papain ferment 5kg, warming while stirring is to 90 DEG C, and insulated and stirred 20min, stirs evenly, and forms B group
Close object；Niacinamide 2.5kg, water 5kg are added in No. 3 reaction kettles, stirs evenly, forms C in combination object；Add in No. 4 reaction kettles
Enter tussol 3kg, macromolecular salicylic acid 1.5kg, propylene glycol 3kg, water 6kg, stir evenly, forms D composition；It is reacted at No. 5
Alpha-arbutin 1.5kg, water 5kg are added in kettle, stirs evenly, forms E composition；De Minshu is added in No. 6 reaction kettles
0.35kg, Chinese herbaceous peony extracting solution 1.25kg, shea oil 0.5kg, stir evenly, and form F composition；
S2, vacuum emulsification pot is preheated to 50 DEG C, is added in S1 and prepares resulting composition B, be pumped into S1 while stirring
Resulting A composition is prepared, mixture, and vacuum homogenization mixture 10min are formed；
S3, the temperature of vacuum emulsification pot is adjusted to 65 DEG C, and is successively added in S1 into mixture and prepares resulting C group
Object, D composition are closed, is uniformly mixed, blend is formed；
S4, the temperature of vacuum emulsification pot is down to 45 DEG C, and is successively added in S1 into blend and prepares resulting E combination
Object, F composition, are uniformly mixed, and are cooled to 33 DEG C, condense into paste to get having effects that the skin whitener of skin whitening, moisturizing.
Embodiment 2
It is a kind of to have effects that the skin whitener of skin whitening, moisturizing, including A composition, composition B, C in combination object, D composition, E group
Close object and F composition；
A composition includes following components:
Cetostearyl alcohol 3.5kg；Emulsifier 7kg；Saualane 6kg；Isopropyl myristate 6kg；Isononyl isononanoate
3kg；Dimethyl silicone polymer 2kg；Vitamin E 0.55kg；Propyl ester 0.01kg；
Composition B includes following components:
Water 35kg；Triethanolamine 0.3kg；Tranexamic acid 1.5kg；Allantoin 0.15kg；Methyl esters 0.15kg；Papain ferment
4kg；
C in combination object includes following components:
Niacinamide 3kg；Water 5.5kg；
D composition includes following components:
Tussol 2kg；Macromolecular salicylic acid 2kg；Propylene glycol 3.5kg；Water 5kg；
E composition includes following components:
Alpha-arbutin 2kg；Water 6.5kg；
F composition includes following components:
De Minshu 0.2kg；Chinese herbaceous peony extracting solution 1.5kg；Shea oil 0.75kg.
In the present embodiment, emulsifier is octadecanoid acid.
Have effects that the skin whitener of skin whitening, moisturizing the preparation method is as follows:
S1, before manufacture, production equipment and apparatus are cleaned up and are sterilized, whale then is added in No. 1 reaction kettle
Wax stearyl alcohol 3.5kg, emulsifier 7kg, saualane 6kg, isopropyl myristate 6kg, isononyl isononanoate 3kg, poly dimethyl
Siloxanes 2kg, vitamin E 0.55kg, propyl ester 0.01kg, warming while stirring is to 80 DEG C, and insulated and stirred 30min, and stirring is equal
It is even, form A composition；Water 35kg is added in No. 2 reaction kettles；Triethanolamine 0.3kg；Tranexamic acid 1.5kg, allantoin
0.15kg, methyl esters 0.15kg, Papain ferment 4kg, warming while stirring is to 90 DEG C, and insulated and stirred 20min, and stirring is equal
It is even, form composition B；Niacinamide 3kg, water 5.5kg are added in No. 3 reaction kettles, stirs evenly, forms C in combination object；At No. 4
Tussol 2kg, macromolecular salicylic acid 2kg, propylene glycol 3.5kg, water 5kg are added in reaction kettle, stirs evenly, forms D composition；
Alpha-arbutin 2kg, water 6.5kg are added in No. 5 reaction kettles, stirs evenly, forms E composition；Moral is added in No. 6 reaction kettles
Quick easypro 0.2kg, Chinese herbaceous peony extracting solution 1.5kg, shea oil 0.75kg, stir evenly, and form F composition；
S2, vacuum emulsification pot is preheated to 50 DEG C, is added in S1 and prepares resulting composition B, be pumped into S1 while stirring
Resulting A composition is prepared, mixture, and vacuum homogenization mixture 10min are formed；
S3, the temperature of vacuum emulsification pot is adjusted to 65 DEG C, and is successively added in S1 into mixture and prepares resulting C group
Object, D composition are closed, is uniformly mixed, blend is formed；
S4, the temperature of vacuum emulsification pot is down to 45 DEG C, and is successively added in S1 into blend and prepares resulting E combination
Object, F composition, are uniformly mixed, and are cooled to 33 DEG C, condense into paste to get having effects that the skin whitener of skin whitening, moisturizing.
Embodiment 3
It is a kind of to have effects that the skin whitener of skin whitening, moisturizing, including A composition, composition B, C in combination object, D composition, E group
Close object and F composition；
A composition includes following components:
Cetostearyl alcohol 4kg；Emulsifier 8.5kg；Saualane 4kg；Isopropyl myristate 7kg；Isononyl isononanoate
4.5kg；Dimethyl silicone polymer 1kg；Vitamin E 0.8kg；Propyl ester 0.1kg；
Composition B includes following components:
Water 30kg；Triethanolamine 0.5kg；Tranexamic acid 2kg；Allantoin 0.1kg；Methyl esters 0.1kg；Papain ferment
4.5kg；
C in combination object includes following components:
Niacinamide 2kg；Water 6kg；
D composition includes following components:
Tussol 2.5kg；Macromolecular salicylic acid 1kg；Propylene glycol 4kg；Water 7kg；
E composition includes following components:
Alpha-arbutin 1kg；Water 8kg；
F composition includes following components:
De Minshu 0.5kg；Chinese herbaceous peony extracting solution 1kg；Shea oil 1kg.
In the present embodiment, emulsifier is octadecanoid acid.
Have effects that the skin whitener of skin whitening, moisturizing the preparation method is as follows:
S1, before manufacture, production equipment and apparatus are cleaned up and are sterilized, whale then is added in No. 1 reaction kettle
Wax stearyl alcohol 4kg, emulsifier 8.5kg, saualane 4kg, isopropyl myristate 7kg, isononyl isononanoate 4.5kg, poly- diformazan
Radical siloxane 1kg, vitamin E 0.8kg, propyl ester 0.1kg, warming while stirring is to 80 DEG C, and insulated and stirred 30min, and stirring is equal
It is even, form A composition；Water 30kg is added in No. 2 reaction kettles；Triethanolamine 0.5kg；Tranexamic acid 2kg, allantoin 0.1kg, first
Ester 0.1kg, Papain ferment 4.5kg, warming while stirring is to 90 DEG C, and insulated and stirred 20min, stirs evenly, and forms B group
Close object；Niacinamide 2kg, water 6kg are added in No. 3 reaction kettles, stirs evenly, forms C in combination object；It is added in No. 4 reaction kettles
Tussol 2.5kg, macromolecular salicylic acid 1kg, propylene glycol 4kg, water 7kg, stir evenly, and form D composition；In No. 5 reaction kettles
Middle addition alpha-arbutin 1kg, water 8kg, stir evenly, and form E composition；De Minshu 0.5kg, Chinese herbaceous peony are added in No. 6 reaction kettles
Medicament extracting solution 1kg, shea oil 1kg, stir evenly, and form F composition；
S2, vacuum emulsification pot is preheated to 50 DEG C, is added in S1 and prepares resulting composition B, be pumped into S1 while stirring
Resulting A composition is prepared, mixture, and vacuum homogenization mixture 10min are formed；
S3, the temperature of vacuum emulsification pot is adjusted to 65 DEG C, and is successively added in S1 into mixture and prepares resulting C group
Object, D composition are closed, is uniformly mixed, blend is formed；
S4, the temperature of vacuum emulsification pot is down to 45 DEG C, and is successively added in S1 into blend and prepares resulting E combination
Object, F composition, are uniformly mixed, and are cooled to 33 DEG C, condense into paste to get having effects that the skin whitener of skin whitening, moisturizing.
Embodiment 4
It is a kind of to have effects that the skin whitener of skin whitening, moisturizing, including A composition, composition B, C in combination object, D composition, E group
Close object and F composition；
A composition includes following components:
Cetostearyl alcohol 3kg；Emulsifier 10kg；Saualane 5kg；Isopropyl myristate 5kg；Isononyl isononanoate 6kg；
Dimethyl silicone polymer 1.5kg；Vitamin E 0.3kg；Propyl ester 0.2kg；
Composition B includes following components:
Water 32.5kg；Triethanolamine 0.1kg；Tranexamic acid 2.5kg；Allantoin 0.2kg；Methyl esters 0.2kg；Papain ferment
5kg；
C in combination object includes following components:
Niacinamide 2.5kg；Water 5kg；
D composition includes following components:
Tussol 3kg；Macromolecular salicylic acid 1.5kg；Propylene glycol 3kg；Water 6kg；
E composition includes following components:
Alpha-arbutin 1.5kg；Water 5kg；
F composition includes following components:
De Minshu 0.35kg；Chinese herbaceous peony extracting solution 1.25kg；Shea oil 0.5kg.
In the present embodiment, emulsifier is octadecanoid acid.
Have effects that the skin whitener of skin whitening, moisturizing the preparation method is as follows:
S1, before manufacture, production equipment and apparatus are cleaned up and are sterilized, whale then is added in No. 1 reaction kettle
Wax stearyl alcohol 3kg, emulsifier 10kg, saualane 5kg, isopropyl myristate 5kg, isononyl isononanoate 6kg, poly dimethyl silicon
Oxygen alkane 1.5kg, vitamin E 0.3kg, propyl ester 0.2kg, warming while stirring is to 90 DEG C, and insulated and stirred 20min, stirs evenly,
Form A composition；Water 32.5kg is added in No. 2 reaction kettles；Triethanolamine 0.1kg；Tranexamic acid 2.5kg, allantoin 0.2kg,
Methyl esters 0.2kg, Papain ferment 5kg, warming while stirring is to 80 DEG C, and insulated and stirred 30min, stirs evenly, and forms B group
Close object；Niacinamide 2.5kg, water 5kg are added in No. 3 reaction kettles, stirs evenly, forms C in combination object；Add in No. 4 reaction kettles
Enter tussol 3kg, macromolecular salicylic acid 1.5kg, propylene glycol 3kg, water 6kg, stir evenly, forms D composition；It is reacted at No. 5
Alpha-arbutin 1.5kg, water 5kg are added in kettle, stirs evenly, forms E composition；De Minshu is added in No. 6 reaction kettles
0.35kg, Chinese herbaceous peony extracting solution 1.25kg, shea oil 0.5kg, stir evenly, and form F composition；
S2, vacuum emulsification pot is preheated to 55 DEG C, is added in S1 and prepares resulting composition B, be pumped into S1 while stirring
Resulting A composition is prepared, mixture, and vacuum homogenization mixture 8min are formed；
S3, the temperature of vacuum emulsification pot is adjusted to 70 DEG C, and is successively added in S1 into mixture and prepares resulting C group
Object, D composition are closed, is uniformly mixed, blend is formed；
S4, the temperature of vacuum emulsification pot is down to 50 DEG C, and is successively added in S1 into blend and prepares resulting E combination
Object, F composition, are uniformly mixed, and are cooled to 35 DEG C, condense into paste to get having effects that the skin whitener of skin whitening, moisturizing.
Embodiment 5
The difference from embodiment 1 is that: emulsifier uses tristerin/PEG-100 stearate.
Embodiment 6
The difference from embodiment 1 is that: emulsifier is using polyoxyethylene -2 (21) stearic alcohol ether.
Embodiment 7
The difference from embodiment 1 is that: emulsifier is stearic using 3kg octadecanoid acid, 3kg tristerin/PEG-100
Acid esters is mixed with the stearic alcohol ether of 4kg polyoxyethylene -2 (21).
Embodiment 8
The difference from embodiment 1 is that: emulsifier is hard using 4kg octadecanoid acid, 2.5kg tristerin/PEG-100
Resin acid ester is mixed with the stearic alcohol ether of 3.5kg polyoxyethylene -2 (21).
Embodiment 9
The difference from embodiment 1 is that: emulsifier is hard using 3.5kg octadecanoid acid, 2kg tristerin/PEG-100
Resin acid ester is mixed with the stearic alcohol ether of 4.5kg polyoxyethylene -2 (21).
Embodiment 10
The difference from embodiment 1 is that: emulsifier uses 3.5kg octadecanoid acid, 2.5kg tristerin/PEG-100
Stearate is mixed with the stearic alcohol ether of 4kg polyoxyethylene -2 (21).
Embodiment 11
Difference with embodiment 10 is:
Composition B further includes following components:
Glycine betaine 2kg；
F composition further includes following components:
Preservative 0.3kg；Essence 0.03kg.
Embodiment 12
Difference with embodiment 10 is:
Composition B further includes following components:
Glycine betaine 2.25kg；
F composition further includes following components:
Preservative 0.25kg；Essence 0.02kg.
Embodiment 13
Difference with embodiment 10 is:
Composition B further includes following components:
Glycine betaine 2.5kg；
F composition further includes following components:
Preservative 0.2kg；Essence 0.01kg.
Comparative example 1
Difference with embodiment 10 is: lacking component tranexamic acid in composition B.
Comparative example 2
Difference with embodiment 10 is: lacking component allantoin in composition B.
Comparative example 3
Difference with embodiment 10 is: lacking component methyl esters in composition B.
Comparative example 4
Difference with embodiment 10 is: lacking component Papain ferment in composition B.
Comparative example 5
Difference with embodiment 10 is: lacking component De Minshu in F composition.
Comparative example 6
Difference with embodiment 10 is: lacking component Chinese herbaceous peony extracting solution in F composition.
Comparative example 7
Difference with embodiment 10 is: lacking component shea oil in F composition.
Experiment 1
It randomly selects 200 age brackets and is 25-45 years old female volunteers, and 200 volunteers are randomly divided into 20 groups,
Every group of volunteer is 10 people, and daily prepared by corresponding take in 4mL or more the same embodiment or comparative example respectively by each group volunteer
Resulting skin whitener is applied to cheek, adheres to using 60 days, and do following detection to each group volunteer, and record average value:
Detection 1
It is used using dermal melanin and ferroheme tester detection volunteer black in the cheek skin before and after skin whitener
Pigment content, wherein measured value is bigger, and melanin contained by skin is more.
Detection 2
Probe detection volunteer to be tested using skin Lab color difference meter and uses the L value before and after skin whitener, wherein L value is bigger,
Skin brightness is higher, and skin color is more biased to white.
Detection 3
Skin keratin before and after skin whitener is used using moisture of skin analyzer Corneometer CM825 detection volunteer
Layer moisture content, wherein measured value is higher, and keratoderma moisture content is higher.
The data detected above are shown in Table 1.
Table 1
It can be obtained according to the data comparison of embodiment 1-13 in table 1 and comparative example 1-7, the composition B in embodiment 1-13 is equal
Using tranexamic acid, allantoin, methyl esters and Papain ferment coordinated, F composition is all made of De Minshu, Chinese herbaceous peony extracting solution
And shea oil coordinated, and lacked component tranexamic acid in comparative example 1, component allantois has been lacked in comparative example 2
Element has lacked component methyl esters in comparative example 3, component Papain ferment has been lacked in comparative example 4, has lacked group in comparative example 5
Divide De Minshu, lacked component Chinese herbaceous peony extracting solution in comparative example 6, component shea oil has been lacked in comparative example 7, and uses
The decline degree of melanin after the skin whitener of embodiment 1-13 is above comparative example 1-7, and uses the beauty of embodiment 1-13
The raising degree of L value and moisture content after bloom is above comparative example 1-7, illustrate by using tranexamic acid, allantoin,
Methyl esters and Papain ferment compounding are multiple using De Minshu, Chinese herbaceous peony extracting solution and shea oil to form composition B
It is equipped with to form F composition, and by composition B and the synergistic effect of F composition to form skin whitener, is conducive to inhibit melanin
Generation, meanwhile, be conducive to accelerate melanin removing speed, also help and keep the skin wet in time for skin, so that skin is not
Be easy to appear dry phenomenon, and then be conducive to solve the problems, such as melanin from root so that skin do not allow more to be also easy to produce it is black
Pigment is conducive to the whitening effect and moistening effect that improve skin whitener；Meanwhile it illustrating only when tranexamic acid, allantoin, first
Ester and Papain ferment coordinated are to form composition B and while by De Minshu, Chinese herbaceous peony extracting solution and African junket
The oily coordinated of rouge tree could be cooperateed with preferably mutually with forming F composition to improve the whitening effect of skin whitener and moisturizing
Effect has lacked any component and has been easy to have an impact the whitening effect and moistening effect of skin whitener.
It can be obtained according to the data comparison of embodiment 1-6 in table 1, the amounts of components of the skin whitener in embodiment 1-3 is different, group
Divide and other preparation conditions are consistent；Embodiment 1 is different from the preparation temperature condition of embodiment 4, and component and dosage are uniform
It causes；Using octadecanoid acid as emulsifier in embodiment 1, embodiment 5 is made using tristerin/PEG-100 stearate
For emulsifier, for embodiment 6 using polyoxyethylene -2 (21) stearic alcohol ether as emulsifier, amounts of components and other conditions are uniform
It causes, and the equal difference of rising degree of the melanin of embodiment 1-6 decline degree and L value and moisture content is little, explanation passes through
Control dosage of each component in the framework of the present definition and through control preparation condition in the framework of the present definition,
The substantially similar skin whitener of whitening effect and moistening effect can be prepared.
It can be obtained according to the data comparison of embodiment 1, embodiment 5-6 and embodiment 7-10 in table 1, it is consistent in other conditions
In the case where, emulsifier is individually used as using octadecanoid acid in embodiment 1, individually use in embodiment 5 tristerin/
For PEG-100 stearate as emulsifier, embodiment 6 is individually real as emulsifier using polyoxyethylene -2 (21) stearic alcohol ether
Apply a 7-10 be all made of the stearic alcohol ether of octadecanoid acid, tristerin/PEG-100 stearate and polyoxyethylene -2 (21) with
Certain proportion is mixed to form emulsifier, and octadecanoid acid, tristerin/PEG-100 stearate and polyoxy in embodiment 7
The mixed proportion of ethylene -2 (21) tristearin alcohol ether is 3:3:4, and octadecanoid acid, tristerin/PEG-100 are hard in embodiment 8
The mixed proportion of resin acid ester and polyoxyethylene -2 (21) stearic alcohol ether is 4:2.5:3.5, octadecanoid acid, stearic acid in embodiment 9
The mixed proportion of glyceride/PEG-100 stearate and polyoxyethylene -2 (21) stearic alcohol ether is 3.5:2:4.5, embodiment 10
Middle octadecanoid acid, tristerin/PEG-100 stearate and the mixed proportion of the stearic alcohol ether of polyoxyethylene -2 (21) are
3.5:2.5:4, embodiment 1 is substantially close with the data of embodiment 5-6, the decline degree and L value of melanin in embodiment 7-9
It is higher than embodiment 1 and embodiment 5-6 to a certain extent with the rising degree of moisture content, and the melanin of embodiment 10
Decline degree and L value and moisture content rising degree to a certain extent higher than embodiment 7-9, illustrate to pass through and adopt
Emulsification is mixed to form with the stearic alcohol ether of octadecanoid acid, tristerin/PEG-100 stearate and polyoxyethylene -2 (21)
Agent is conducive to each component in skin whitener and is preferably uniformly dispersed mutually, and each component be conducive in skin whitener preferably emulsifies,
To be conducive to improve the stability of skin whitener product quality, so that the whitening effect and moistening effect of skin whitener are more preferable；It is logical
Cross the mixed proportion of control octadecanoid acid, tristerin/PEG-100 stearate and polyoxyethylene -2 (21) stearic alcohol ether
It is 3.5:2.5:4 to be mixed to form emulsifier, each component be conducive in skin whitener preferably emulsifies, so that skin whitener produces
The stability of quality is higher, so that the whitening effect and moistening effect of skin whitener further increase.
It can be obtained according to embodiment 10 in table 1 and the data comparison of embodiment 11-13, than embodiment 10 in embodiment 11-13
Increase component glycine betaine, preservative and essence newly, and the melanin of embodiment 11-13 decline degree and L value and moisture contain
The raising degree of amount illustrates to a certain extent higher than embodiment 10 by the way that glycine betaine is added as anti-caking agent, favorably
In the moistening effect of enhancing skin whitener, meanwhile, so that each component of skin whitener is not allowed more during preservation and use
Easily there is the case where agglomeration precipitating, to be conducive to improve the stability of skin whitener product quality, and then is conducive to skin whitener more
Its whitening effect and moistening effect are played well.
The embodiment of present embodiment is presently preferred embodiments of the present invention, not limits protection of the invention according to this
Range, therefore: the equivalence changes that all structures under this invention, shape, principle are done, should all be covered by protection scope of the present invention it
It is interior.
Claims (9)
1. a kind of have effects that the skin whitener of skin whitening, moisturizing, it is characterized in that: including A composition, composition B, C in combination object, D combination
Object, E composition and F composition；
The A composition includes the component of following mass fraction:
3-4 parts of cetostearyl alcohol；
7-10 parts of emulsifier；
4-6 parts of saualane；
5-7 parts of isopropyl myristate；
3-6 parts of isononyl isononanoate；
1-2 parts of dimethyl silicone polymer；
0.3-0.8 parts of vitamin E；
0.01-0.2 parts of propyl ester；
The composition B includes the component of following mass fraction:
30-35 parts of water；
0.1-0.5 parts of triethanolamine；
1.5-2.5 parts of tranexamic acid；
0.1-0.2 parts of allantoin；
0.1-0.2 parts of methyl esters；
4-5 parts of Papain ferment；
The C in combination object includes the component of following mass fraction:
2-3 parts of niacinamide；
5-6 parts of water；
The D composition includes the component of following mass fraction:
2-3 parts of tussol；
1-2 parts of macromolecular salicylic acid；
3-4 parts of propylene glycol；
5-7 parts of water；
The E composition includes the component of following mass fraction:
1-2 parts of alpha-arbutin；
5-8 parts of water；
The F composition includes the component of following mass fraction:
0.2-0.5 parts of De Minshu；
1-1.5 parts of Chinese herbaceous peony extracting solution；
0.5-1 parts of shea oil.
2. according to claim 1 have effects that the skin whitener of skin whitening, moisturizing, it is characterized in that: the emulsifier is by octadecane
Acid, tristerin/PEG-100 stearate, polyoxyethylene -2(21) stearic alcohol ether mix by the ratio of 3.5:2.5:4 and
At.
3. according to claim 1 to 2 have effects that the skin whitener of skin whitening, moisturizing, it is characterized in that: the composition B
Further include the component of following mass fraction:
2-2.5 parts of anti-caking agent.
4. according to claim 3 have effects that the skin whitener of skin whitening, moisturizing, it is characterized in that: the anti-caking agent is beet
Alkali.
5. according to claim 1 to 2 have effects that the skin whitener of skin whitening, moisturizing, it is characterized in that: the F composition
Further include the component of following mass fraction:
0.2-0.3 parts of preservative.
6. according to claim 1 to 2 have effects that the skin whitener of skin whitening, moisturizing, it is characterized in that: the F composition
Further include the component of following mass fraction:
0.01-0.03 parts of essence.
7. a kind of preparation method with the skin whitener of skin whitening, moisturizing as described in claim 1-6 is any, it is characterized in that:
The following steps are included:
S1, each component of A composition, composition B, C in combination object, D composition, E composition and F composition respectively pressed respectively
Mass parts ratio is mixed evenly, and obtains A composition, composition B, C in combination object, D composition, E composition and F combination
Object；
S2, in 50 DEG C -55 DEG C of at a temperature of mixing A compositions and composition B, form mixture, and homogenization mixture
8-10min；
S3,65 DEG C -70 DEG C at a temperature of C in combination object and D composition are added into mixture, be uniformly mixed, formed
Blend；
S4,45 DEG C -50 DEG C at a temperature of E composition and F composition are added into blend, stir evenly, then reduce temperature
Degree condenses into paste to 33 DEG C -35 DEG C to get having effects that the skin whitener of skin whitening, moisturizing.
8. the preparation method with the skin whitener of skin whitening, moisturizing according to claim 7, it is characterized in that: the step
In S1, the mixing temperature control of each component of A composition and composition B is 80 DEG C -90 DEG C, mixing time 20min-
30min。
9. the preparation method with the skin whitener of skin whitening, moisturizing according to claim 7, it is characterized in that: the step
In S2, homogenization operation carries out under vacuum conditions.
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN116019964A (en) * | 2022-12-23 | 2023-04-28 | 江苏嘉奥医疗科技有限公司 | Processing technology of medical dressing |
| CN116019964B (en) * | 2022-12-23 | 2024-03-15 | 江苏嘉奥医疗科技有限公司 | Processing technology of medical dressing |
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| CN110339118B (en) | 2022-08-16 |
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