CN110330377A - Multi-Functional Fertilizers and its steam granulation fertilizer manufacture - Google Patents
Multi-Functional Fertilizers and its steam granulation fertilizer manufacture Download PDFInfo
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- CN110330377A CN110330377A CN201910649994.2A CN201910649994A CN110330377A CN 110330377 A CN110330377 A CN 110330377A CN 201910649994 A CN201910649994 A CN 201910649994A CN 110330377 A CN110330377 A CN 110330377A
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- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05B—PHOSPHATIC FERTILISERS
- C05B1/00—Superphosphates, i.e. fertilisers produced by reacting rock or bone phosphates with sulfuric or phosphoric acid in such amounts and concentrations as to yield solid products directly
- C05B1/02—Superphosphates
-
- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05F—ORGANIC FERTILISERS NOT COVERED BY SUBCLASSES C05B, C05C, e.g. FERTILISERS FROM WASTE OR REFUSE
- C05F5/00—Fertilisers from distillery wastes, molasses, vinasses, sugar plant or similar wastes or residues, e.g. from waste originating from industrial processing of raw material of agricultural origin or derived products thereof
- C05F5/002—Solid waste from mechanical processing of material, e.g. seed coats, olive pits, almond shells, fruit residue, rice hulls
-
- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
- C05G3/00—Mixtures of one or more fertilisers with additives not having a specially fertilising activity
-
- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
- C05G3/00—Mixtures of one or more fertilisers with additives not having a specially fertilising activity
- C05G3/90—Mixtures of one or more fertilisers with additives not having a specially fertilising activity for affecting the nitrification of ammonium compounds or urea in the soil
-
- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
- C05G5/00—Fertilisers characterised by their form
- C05G5/30—Layered or coated, e.g. dust-preventing coatings
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- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Life Sciences & Earth Sciences (AREA)
- Pest Control & Pesticides (AREA)
- Engineering & Computer Science (AREA)
- Mechanical Engineering (AREA)
- Botany (AREA)
- Environmental & Geological Engineering (AREA)
- Soil Sciences (AREA)
- Fertilizers (AREA)
Abstract
Multi-Functional Fertilizers and its steam granulation fertilizer manufacture, multi-Functional Fertilizers include following components: charcoal base organic fertilizer, calcium superphosphate, potassium sulfate, urea, ammonium hydrogen carbonate, middle microelement, coated slow release formulation, and the charcoal base organic fertilizer mainly includes charcoal, humic acid, wood vinegar.Nutrition general equilibrium of the present invention, it is capable of providing nutrient needed for fruit growing, it can also realize the slow release of fertilizer nutrient, fruit tree is improved to the utilization rate of fertilizer, reduce Fertilizer application amount, in addition the application slow-release fertilizer can save soil moisture, improve soil texture, increase the yield of fruit and quality.
Description
Technical field
The present invention relates to modern agriculture field, especially multi-Functional Fertilizers and its steam granulation fertilizer manufactures.
Background technique
China's application is wide general, and kind is numerous, and commonplace has watermelon, apple, peach, orange etc., application
The use of fertilizer plays a key effect to its yield and quality in the process, but there are more defects for presently commercially available fertilizer, such as
Nutrient is single, based on chemical fertilizer, utilization rate is low, destroys soil texture etc..Demand of the fruit tree compared to rice, wheat etc., to fertilizer
Amount is bigger, and duplicate fertilising can bring heavy labour and economic cost.Developing has multi-functional application sustained release
Fertilizer becomes the demand of current agricultural production, and the offer nutrition that application slow-release fertilizer can be comprehensive, safe, long-acting is suitble to existing
For application industry.
Summary of the invention
The purpose of the present invention is to provide multi-Functional Fertilizers and its steam granulation fertilizer manufactures, to solve above-mentioned background technique
The problem of middle proposition.
The technical solution adopted by the present invention is that: multi-Functional Fertilizers, according to parts by weight, including following components: charcoal base is organic
10-20 parts fertile, 20-30 parts of calcium superphosphate, 25-40 parts of potassium sulfate, 10-20 parts of urea, 2-5 parts of ammonium hydrogen carbonate, middle microelement
2-5 parts, 5-10 parts of coated slow release formulation.
Multi-Functional Fertilizers and its steam granulation fertilizer manufacture, comprising the following steps:
(1) by weight it is that 5-10:1 is mixed by corn stover and orange peel, is crushed to obtain mixed powder after mixing and be minced, will mixed
Conjunction crushed material, which is added in 15-20 times of weight water, boil extraction 2-3 times, and filtrate and filter residue is obtained by filtration；Filter residue carries out heap
Fertilizer fermentation, compost fermentation time are 5-10 days, are dried, are obtained in 40-50 DEG C with baking oven after fermentation liquid is mixed with filtrate
Moisture content be 15-20% concentrate to get arrive machine active material；
(2) charcoal base organic fertilizer obtained in step (1), calcium superphosphate, potassium sulfate, urea, ammonium hydrogen carbonate are pressed into formula metering, mixed
It closes and uniformly obtains mixed material；
(3) mixed material of step (2) is granulated, dried, cooled down, sieved, obtain crude product particle；
(4) microelement, 20-50 a part deionized water in 2-5 parts are heated to 50-60 DEG C, be slowly added into 50-100 parts it is organic
In amine, 2-5 parts of furtherance films are added, stirring is uniformly mixed solution, and 10-20 parts of regulators are added and adjust pH value of solution
Value obtains coated slow release formulation to 6-8；
(5) it is uniformly sprayed on the crude product particle surface of step (3) after measuring the coated slow release formulation that step (4) obtains, then
It is dried under conditions of 60-90 DEG C, obtains application slow-release fertilizer finished product.
Preferably, organic amine is N- methylethanolamine, monoethanolamine, diethanol amine, triethanolamine in the step (4)
One of or it is a variety of.
Preferably, furtherance film is hydroxymethyl cellulose, carboxymethyl cellulose, hydroxy ethyl fiber in the step (4)
One of element, hydroxypropyl cellulose are a variety of.
Preferably, regulator is formic acid, acetic acid, phosphoric acid, hydrochloric acid, one in 20% aqueous sulfuric acid in the step (4)
Kind is a variety of.
Preferably, the middle microelement is magnesium sulfate, any multiple combinations in zinc sulfate, manganese sulfate, borax.
Preferably, the charcoal base organic fertilizer mainly includes charcoal, humic acid, wood vinegar.
Preferably, charcoal weight percent is not less than 50%, humic acid weight percent in the charcoal base organic fertilizer
It is not less than 12% not less than 5%, wood vinegar weight percent.
Nutrition general equilibrium of the present invention, is capable of providing nutrient needed for fruit growing, additionally it is possible to realize fertilizer nutrient
Slow release improves fruit tree to the utilization rate of fertilizer, reduces Fertilizer application amount, in addition the application slow-release fertilizer can be protected
It deposits soil moisture, improves soil texture, increase the yield of fruit and quality.
Specific embodiment
It is clearly and completely described below in conjunction with technical solution of the present invention, it is clear that described embodiment is only
It is a part of the embodiment of the present invention, instead of all the embodiments.Based on the embodiments of the present invention, ordinary skill people
Member's every other embodiment obtained without making creative work, shall fall within the protection scope of the present invention.
Embodiment 1
Multi-Functional Fertilizers, according to parts by weight, including following components: 20 parts of charcoal base organic fertilizer, 20 parts of calcium superphosphate, potassium sulfate 35
Part, 15 parts of urea, 2 parts of ammonium hydrogen carbonate, 0.5 part of magnesium sulfate, 0.5 part of zinc sulfate, 0.5 part of manganese sulfate, 0.5 part of borax, coating are slow
Release 6 parts of agent.
Multi-Functional Fertilizers and its steam granulation fertilizer manufacture, preparation method are as follows:
(1) by weight it is that 8:1 is mixed by corn stover and orange peel, is crushed to obtain mixed powder after mixing and be minced, will mixed
Crushed material, which is added in 16 times of weight waters, boil extraction 3 times, and filtrate and filter residue is obtained by filtration；Filter residue carries out compost fermentation,
The compost fermentation time is 10 days, is dried with baking oven in 50 DEG C after fermentation liquid is mixed with filtrate, and obtaining moisture content is 20%
Concentrate, as charcoal base organic fertilizer；
(2) 20 parts of charcoal base organic fertilizer, 20 parts of calcium superphosphate, 35 parts of potassium sulfate, 15 parts of urea, ammonium hydrogen carbonate 2 are weighed by weight
Part is uniformly mixed and obtains mixed material；
(3) mixed material of step (2) is granulated, dried, cooled down, sieved, obtain crude product particle；
(4) 0.5 part of magnesium sulfate, 0.5 part of zinc sulfate, 0.5 part of manganese sulfate, 0.5 part of borax, triethanolamine 60 are weighed by weight
Part, 20 parts of deionized water, 5 parts of hydroxyethyl cellulose, 15 parts of 20% aqueous sulfuric acid.Deionized water is heated to 50 DEG C, is slowly added
Enter into triethanolamine, add hydroxyethyl cellulose, stirring is uniformly mixed solution.20% aqueous sulfuric acid is added
Solution ph is adjusted to 6-8 to get coated slow release formulation；
(5) 6 parts of coated slow release formulation are weighed by weight, are uniformly sprayed onto obtaining on crude product particle surface for step 3), then at
It is dried under conditions of 60-90 DEG C, obtains application slow-release fertilizer finished product.
Embodiment 2
Multi-Functional Fertilizers, according to parts by weight, including following components: 16 parts of charcoal base organic fertilizer, 25 parts of calcium superphosphate, potassium sulfate 30
Part, 14 parts of urea, 4 parts of ammonium hydrogen carbonate, 8 parts of coated slow release formulation.
Multi-Functional Fertilizers and its steam granulation fertilizer manufacture, preparation method are as follows:
(1) by weight it is that 8:1 is mixed by corn stover and orange peel, is crushed to obtain mixed powder after mixing and be minced, will mixed
Crushed material, which is added in 16 times of weight waters, boil extraction 3 times, and filtrate and filter residue is obtained by filtration；Filter residue carries out compost fermentation,
The compost fermentation time is 10 days, is dried with baking oven in 50 DEG C after fermentation liquid is mixed with filtrate, and obtaining moisture content is 20%
Concentrate, as charcoal base organic fertilizer；
(2) 16 parts of charcoal base organic fertilizer, 25 parts of calcium superphosphate, 30 parts of potassium sulfate, 14 parts of urea, ammonium hydrogen carbonate 4 are weighed by weight
Part, 0.8 part of magnesium sulfate, 0.8 part of zinc sulfate, 0.7 part of manganese sulfate, 0.7 part of borax are uniformly mixed and obtain mixed material；
(3) mixed material of step (2) is granulated, dried, cooled down, sieved, obtain crude product particle；
(4) 0.8 part of magnesium sulfate, 0.8 part of zinc sulfate, 0.7 part of manganese sulfate, 0.7 part of borax, triethanolamine 60 are weighed by weight
Part, 20 parts of deionized water, 5 parts of hydroxyethyl cellulose, 15 parts of 20% aqueous sulfuric acid.Deionized water is heated to 50 DEG C, is slowly added
Enter into triethanolamine, add hydroxyethyl cellulose, stirring is uniformly mixed solution.20% aqueous sulfuric acid is added
Solution ph is adjusted to 6-8 to get coated slow release formulation；
(5) 8 parts of coated slow release formulation are weighed by weight, are uniformly sprayed on the crude product particle surface that step 3) obtains, then at
It is dried under conditions of 60-90 DEG C, obtains application slow-release fertilizer finished product.
Embodiment 3
Multi-Functional Fertilizers, according to parts by weight, including following components: 12 parts of charcoal base organic fertilizer, 28 parts of calcium superphosphate, potassium sulfate 28
Part, 13 parts of urea, 5 parts of ammonium hydrogen carbonate, 10 parts of coated slow release formulation.
Multi-Functional Fertilizers and its steam granulation fertilizer manufacture, preparation method are as follows:
(1) by weight it is that 8:1 is mixed by corn stover and orange peel, is crushed to obtain mixed powder after mixing and be minced, will mixed
Crushed material, which is added in 16 times of weight waters, boil extraction 3 times, and filtrate and filter residue is obtained by filtration；Filter residue carries out compost fermentation,
The compost fermentation time is 10 days, is dried with baking oven in 50 DEG C after fermentation liquid is mixed with filtrate, and obtaining moisture content is 20%
Concentrate, as charcoal base organic fertilizer；
(2) 12 parts of charcoal base organic fertilizer, 28 parts of calcium superphosphate, 28 parts of potassium sulfate, 13 parts of urea, ammonium hydrogen carbonate 5 are weighed by weight
Part, 1 part of magnesium sulfate, 1 part of zinc sulfate, 1 part of manganese sulfate, 1 part of borax are uniformly mixed and obtain mixed material；
(3) mixed material of step (2) is granulated, dried, cooled down, sieved, obtain crude product particle；
(4) 1 part of magnesium sulfate, 1 part of zinc sulfate, 1 part of manganese sulfate, 1 part of borax, 60 parts of triethanolamine, deionization are weighed by weight
20 parts of water, 5 parts of hydroxyethyl cellulose, 15 parts of 20% aqueous sulfuric acid.Deionized water is heated to 50 DEG C, is slowly added into three second
In hydramine, hydroxyethyl cellulose is added, stirring is uniformly mixed solution.20% aqueous sulfuric acid is added and adjusts solution
PH value is to 6-8 to get coated slow release formulation；
(5) 10 parts of coated slow release formulation are weighed by weight, are uniformly sprayed on the crude product particle surface that step 3) obtains, then at
It is dried under conditions of 60-90 DEG C, obtains application slow-release fertilizer finished product.
Charcoal base (superactivity) organic fertilizer includes charcoal, humic acid, wood vinegar, rice-straw ash, wormcast, bentonite
It is not less than 50% Deng, the charcoal, humic acid is not less than 12% not less than 5%, wood vinegar, other arbitrarily compare according to plant characteristic
Example configuration (not influencing main effect).
Comparative example 1
The common potassium sulphate fertilizer of one planting fruit-trees, raw material is by weight are as follows: 17 parts of ammonium sulfate, 17 parts of urea, monoammonium phosphate 32
Part, 28 parts of potassium sulfate, 6 parts of filler.
The common potassium sulphate fertilizer of one planting fruit-trees, preparation method are as follows: weighing 17 parts of ammonium sulfate, urea 17 by weight
Part, 32 parts of monoammonium phosphate, 28 parts of potassium sulfate, 6 parts of filler, through sour method drum granulating after mixing, then through drying, cooling, screening,
45%(N:P2O5:K2O=15:15:15 is obtained after packaging) potassium sulphate fertilizer.
Comparative example 2
The common potassium sulphate fertilizer of one planting fruit-trees, raw material is by weight are as follows: 20 parts of ammonium sulfate, 27 parts of urea, monoammonium phosphate 21
Part, 28 parts of potassium sulfate, 4 parts of filler.
The common potassium sulphate fertilizer of one planting fruit-trees, preparation method are as follows: weighing 20 parts of ammonium sulfate, urea 27 by weight
Part, 21 parts of monoammonium phosphate, 28 parts of potassium sulfate, 4 parts of filler, through sour method drum granulating after mixing, then through drying, cooling, screening,
45%(N:P2O5:K2O=20:10:15 is obtained after packaging) potassium sulphate fertilizer.
It is used respectively using the application slow-release fertilizer of embodiment 1-3 with the fruit tree potassium sulphate fertilizer in comparative example 1-2
The plantation of Mr. Yu city peach, compares, it is as follows to compare rate of fertilizer and peach yield, test result in a growth cycle
Table:
It can be seen that application slow-release fertilizer of the present invention compared with common fruit tree potassium sulphate fertilizer by upper table, dose
It reduces, yield-increasing efficiency increases.
It is obvious to a person skilled in the art that invention is not limited to the details of the above exemplary embodiments, Er Qie
In the case where without departing substantially from spirit or essential attributes of the invention, the present invention can be realized in other specific forms.Therefore, no matter
From the point of view of which point, the present embodiments are to be considered as illustrative and not restrictive, and the scope of the present invention is by appended power
Benefit requires rather than above description limits, it is intended that all by what is fallen within the meaning and scope of the equivalent elements of the claims
Variation is included within the present invention.
Claims (8)
1. multi-Functional Fertilizers, it is characterised in that according to parts by weight, including following components: 10-20 parts of charcoal base organic fertilizer, peroxophosphoric acid
20-30 parts of calcium, 25-40 parts of potassium sulfate, 10-20 parts of urea, 2-5 parts of ammonium hydrogen carbonate, microelement 2-5 parts middle, coated slow release formulation
5-10 parts.
2. multi-Functional Fertilizers according to claim 1, it is characterised in that the charcoal base organic fertilizer mainly includes charcoal, corruption
Phytic acid, wood vinegar.
3. multi-Functional Fertilizers according to claim 2, it is characterised in that in the charcoal base organic fertilizer, charcoal weight percent
Than being not less than 50%, humic acid weight percent is not less than 12% not less than 5%, wood vinegar weight percent.
4. multi-Functional Fertilizers according to claim 1, it is characterised in that the middle microelement be magnesium sulfate, zinc sulfate,
Any multiple combinations in manganese sulfate, borax.
5. multi-Functional Fertilizers according to claim 1 and its steam granulation fertilizer manufacture, it is characterised in that including following step
It is rapid:
(1) by weight it is that 5-10:1 is mixed by corn stover and orange peel, is crushed to obtain mixed powder after mixing and be minced, will mixed
Conjunction crushed material, which is added in 15-20 times of weight water, boil extraction 2-3 times, and filtrate and filter residue is obtained by filtration；Filter residue carries out heap
Fertilizer fermentation, compost fermentation time are 5-10 days, are dried, are obtained in 40-50 DEG C with baking oven after fermentation liquid is mixed with filtrate
Moisture content be 15-20% concentrate to get arrive machine active material；
(2) charcoal base organic fertilizer obtained in step (1), calcium superphosphate, potassium sulfate, urea, ammonium hydrogen carbonate are pressed into formula metering, mixed
It closes and uniformly obtains mixed material；
(3) mixed material of step (2) is granulated, dried, cooled down, sieved, obtain crude product particle；
(4) microelement, 20-50 a part deionized water in 2-5 parts are heated to 50-60 DEG C, be slowly added into 50-100 parts it is organic
In amine, 2-5 parts of furtherance films are added, stirring is uniformly mixed solution, and 10-20 parts of regulators are added and adjust pH value of solution
Value obtains coated slow release formulation to 6-8；
(5) it is uniformly sprayed on the crude product particle surface of step (3) after measuring the coated slow release formulation that step (4) obtains, then
It is dried under conditions of 60-90 DEG C, obtains application slow-release fertilizer finished product.
6. multi-Functional Fertilizers according to claim 5 and its steam granulation fertilizer manufacture, it is characterised in that the step (4)
Middle organic amine is one of N- methylethanolamine, monoethanolamine, diethanol amine, triethanolamine or a variety of.
7. multi-Functional Fertilizers according to claim 5 and its steam granulation fertilizer manufacture, it is characterised in that the step (4)
Middle furtherance film is one of hydroxymethyl cellulose, carboxymethyl cellulose, hydroxyethyl cellulose, hydroxypropyl cellulose or more
Kind.
8. multi-Functional Fertilizers according to claim 5 and its steam granulation fertilizer manufacture, it is characterised in that the step (4)
Middle regulator is one of formic acid, acetic acid, phosphoric acid, hydrochloric acid, 20% aqueous sulfuric acid or a variety of.
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112250510A (en) * | 2020-10-16 | 2021-01-22 | 东华大学 | Large-particle slow-release organic-inorganic compound fertilizer, preparation method and application |
| CN114273416A (en) * | 2021-12-30 | 2022-04-05 | 华中科技大学 | Preparation method, product and repair method of carbon-based bifunctional soil repair agent |
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|---|---|---|---|---|
| CN103880503A (en) * | 2014-03-04 | 2014-06-25 | 张超 | Disease prevention high-yield EM (Effective Microorganism) inoculant fermentation compound fertilizer for watermelon |
| CN104003804A (en) * | 2014-06-09 | 2014-08-27 | 山东红日阿康化工股份有限公司 | Moisture-retaining and nitrogen-fixing compound microbial fertilizer and preparation method thereof |
| CN104292058A (en) * | 2014-11-11 | 2015-01-21 | 合肥不老传奇保健科技有限公司 | Coated fertilizer for strawberry tree after bearing and preparation method thereof |
| CN109534919A (en) * | 2019-01-30 | 2019-03-29 | 韩亚博 | A kind of microorganism slow-release compound fertilizer and preparation method thereof |
-
2019
- 2019-07-18 CN CN201910649994.2A patent/CN110330377A/en active Pending
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103880503A (en) * | 2014-03-04 | 2014-06-25 | 张超 | Disease prevention high-yield EM (Effective Microorganism) inoculant fermentation compound fertilizer for watermelon |
| CN104003804A (en) * | 2014-06-09 | 2014-08-27 | 山东红日阿康化工股份有限公司 | Moisture-retaining and nitrogen-fixing compound microbial fertilizer and preparation method thereof |
| CN104292058A (en) * | 2014-11-11 | 2015-01-21 | 合肥不老传奇保健科技有限公司 | Coated fertilizer for strawberry tree after bearing and preparation method thereof |
| CN109534919A (en) * | 2019-01-30 | 2019-03-29 | 韩亚博 | A kind of microorganism slow-release compound fertilizer and preparation method thereof |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112250510A (en) * | 2020-10-16 | 2021-01-22 | 东华大学 | Large-particle slow-release organic-inorganic compound fertilizer, preparation method and application |
| CN114273416A (en) * | 2021-12-30 | 2022-04-05 | 华中科技大学 | Preparation method, product and repair method of carbon-based bifunctional soil repair agent |
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