CN110255903A - Transmutation crystallizes grape glaze, grape glaze ceramic and their preparation method - Google Patents
Transmutation crystallizes grape glaze, grape glaze ceramic and their preparation method Download PDFInfo
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- CN110255903A CN110255903A CN201910538553.5A CN201910538553A CN110255903A CN 110255903 A CN110255903 A CN 110255903A CN 201910538553 A CN201910538553 A CN 201910538553A CN 110255903 A CN110255903 A CN 110255903A
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- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C8/00—Enamels; Glazes; Fusion seal compositions being frit compositions having non-frit additions
- C03C8/02—Frit compositions, i.e. in a powdered or comminuted form
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- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C8/00—Enamels; Glazes; Fusion seal compositions being frit compositions having non-frit additions
- C03C8/14—Glass frit mixtures having non-frit additions, e.g. opacifiers, colorants, mill-additions
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B41/00—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
- C04B41/45—Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements
- C04B41/50—Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements with inorganic materials
- C04B41/5022—Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements with inorganic materials with vitreous materials
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B41/00—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
- C04B41/80—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone of only ceramics
- C04B41/81—Coating or impregnation
- C04B41/85—Coating or impregnation with inorganic materials
- C04B41/86—Glazes; Cold glazes
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Abstract
The invention discloses a kind of transmutation crystallization grape glaze, grape glaze ceramic and their preparation method, transmutation crystallization grape glaze includes the raw material of following parts by weight: 9~12 parts of fluorite, 14~17 parts of glass, quartzy 22~25 parts, 6~7.5 parts of feldspar, 1.5~2.5 parts of talcum, 23~25 parts of zinc oxide, 2~6 parts of barium monoxide, 8~11 parts of kaolin, 4.5~6.5 parts of bone meal, 2~4 parts of copper oxide, 3~7 parts of high boron frit.Transmutation crystallization grape glaze of the invention is made up of selected raw material, and rational proportion, fluorite, glass, quartz, feldspar, talcum, zinc oxide, barium monoxide, kaolin, bone meal, copper oxide, the high boron frit of appropriate proportion are selected, so that matrix surface obtained is formed with transmutation crystallization grape glaze or grape glaze ceramic, there is purple grape crystallization effect, i.e., unique transmutation crystallization, it is glittering and translucent, it is exquisite beautiful, do not have graceful bearing, artistic effect is strong；In addition, more special artistic effect ceramics can be obtained in glaze superposition.
Description
Technical field
The present invention relates to ceramic fields, and in particular to transmutation crystallize grape glaze, grape glaze ceramic and they
Preparation method.
Background technique
Ceramic material is with natural or synthetic compound by one kind inorganic non-metallic material made of forming and high temperature sintering
Material.It has many advantages, such as high-melting-point, high rigidity, high-wearing feature, resistance to oxidation.It can be used as structural material, cutter material, due to ceramics
Also there are certain special performances, but also as functional material.
Ceramic is one of most common utensil in people's daily life, and ceramic development history is the one of Chinese civilization history
A important component part, wherein the invention and development of ceramics have more unique meaning, with the development of modern science technology,
Occur many new ceramic kinds again in the last hundred years, they do not use or be rarely employed the tradition pottery such as clay, feldspar, quartz
Porcelain raw material, but other special materials are used, or even be expanded to non-silicate, the range of non-oxidized substance, and there is many
New technique makes ceramics be provided with various specific functions.
Coloring, glazing are a kind of effective means for increasing ceramic texture and aesthetic feeling on the surface of ceramic, and
And the artistic effect that each glaze colours or pattern rise is different, have currently on the market various glaze colours, pattern or
Its combination of person.Glaze various types in the market, but seldom low in glossiness that artistic effect is strong, waterproof is antifouling, antifriction
It is property, weak.
Summary of the invention
Based on the above situation, the purpose of the present invention is to provide transmutation crystallization grape glaze, grape glaze ceramic and they
Preparation method, can effectively solve problem above.
In order to solve the above technical problems, present invention provide the technical scheme that
A kind of transmutation crystallization grape glaze, the raw material including following parts by weight: 9~12 parts of fluorite, 14~17 parts of glass, quartz
22~25 parts, 6~7.5 parts of feldspar, 1.5~2.5 parts of talcum, 23~25 parts of zinc oxide, 2~6 parts of barium monoxide, kaolin 8~11
Part, 4.5~6.5 parts of bone meal, 2~4 parts of copper oxide, 3~7 parts of high boron frit.
Preferably, the transmutation crystallization grape glaze includes the raw material of following parts by weight: 10 parts of fluorite, 15 parts of glass, quartz
24 parts, 6 parts of feldspar, 2 parts of talcum, 24 parts of zinc oxide, 2 parts of barium monoxide, 10 parts of kaolin, 5 parts of bone meal, 3 parts of copper oxide, high boron it is molten
4 parts of block.
Preferably, the glass is alumina silicate glass.
Preferably, the feldspar is albite.
Preferably, the bone meal is any one or more in bovine bone powder, lamb bone meal and Os Sus domestica powder.
Preferably, the boron content of the high boron frit is greater than 10%, and lead content is less than 0.01%.
The present invention also provides a kind of preparation methods of transmutation crystallization grape glaze, including the following steps:
A, following raw material: fluorite, glass, quartz, feldspar, talcum, zinc oxide, barium monoxide, kaolinite is weighed by weight
Soil, bone meal, copper oxide, high boron frit；
B, mixture will be obtained after weighed each raw material mixes, 60~90min of ball milling, wherein when ball milling, mixture, ball
With the weight ratio of water are as follows: 1:2.5:(0.5~0.65)；
C, 200 meshes are crossed, 20~40min of froth in vacuum is then carried out and obtains glaze slip, continue 20~30min of stirring, and adjust
Saving glaze slip solid content is 55~65%；
D, glaze slip is imposed on into matrix surface, then is warming up to 1290~1310 DEG C, carry out glaze firing 110~150min hours, then
220 DEG C of heat preservation 2h are cooled to, described matrix surface forms the transmutation crystallization grape glaze.
The present invention also provides a kind of grape glaze ceramics, including green body and the glaze layer for being covered in the billet surface, institute
Stating glaze layer is that transmutation above-mentioned crystallizes grape glaze.
The present invention also provides a kind of preparation methods of grape glaze ceramic, including the following steps:
(1) following raw material: fluorite, glass, quartz, feldspar, talcum, zinc oxide, barium monoxide, kaolinite is weighed by weight
Soil, bone meal, copper oxide, high boron frit；
(2) mixture will be obtained after weighed each raw material mixes, 60~90min of ball milling, wherein when ball milling, mixture, ball
With the weight ratio of water are as follows: 1:2.5:(0.5~0.65)；
(3) 200 meshes are crossed, 20~40min of froth in vacuum is then carried out and obtains glaze slip, continue 20~30min of stirring, and adjust
Saving glaze slip solid content is 55~65%；
(4) glaze slip is imposed on into billet surface, then is warming up to 1290~1310 DEG C, carry out glaze firing 110~150min hours, then
220 DEG C of heat preservation 2h are cooled to get grape glaze ceramic.
Compared with prior art, the present invention have the following advantages that and the utility model has the advantages that
Transmutation crystallization grape glaze of the invention is made up of selected raw material, and rational proportion, has selected the firefly of appropriate proportion
Stone, glass, quartz, feldspar, talcum, zinc oxide, barium monoxide, kaolin, bone meal, copper oxide, high boron frit, matrix table obtained
Face is formed with transmutation crystallization grape glaze or grape glaze ceramic, has purple grape crystallization effect, i.e., unique transmutation crystallizes,
It is glittering and translucent, it is exquisite beautiful, do not have graceful bearing, artistic effect is strong；More special artistic effect ceramic systems can be obtained in glaze superposition
Product.
Preparation method simple process of the invention, it is easy to operate.
Specific embodiment
It is right combined with specific embodiments below in order to make those skilled in the art more fully understand technical solution of the present invention
The preferred embodiments of the invention are described, but should not be understood as the limitation to this patent.
Test method described in following embodiments or test method are unless otherwise specified conventional method；The reagent
And material is obtained from routine business approach, or prepare in conventional manner unless otherwise specified.
Alumina silicate glass of the present invention is with SiO2And Al2O3For main component, softening transform temperature is high, can be from routine
Commercial sources obtain.
Green body of the present invention can be made according to conventional method in that art, repeat no more its production method, and shape can be with
It is arbitrary shape；It can be used to carry out glazing using glaze slip of the invention, subsequently into lower one of work after sizing, air-drying
Sequence.
Embodiment 1:
A kind of transmutation crystallization grape glaze, the raw material including following parts by weight: 9~12 parts of fluorite, 14~17 parts of glass, quartz
22~25 parts, 6~7.5 parts of feldspar, 1.5~2.5 parts of talcum, 23~25 parts of zinc oxide, 2~6 parts of barium monoxide, kaolin 8~11
Part, 4.5~6.5 parts of bone meal, 2~4 parts of copper oxide, 3~7 parts of high boron frit.
Embodiment 2:
A kind of transmutation crystallization grape glaze, the raw material including following parts by weight: 9 parts of fluorite, 14 parts of glass, 22 parts of quartz, length
6 parts of stone, 1.5 parts of talcum, 23 parts of zinc oxide, 2 parts of parts of barium monoxide, 8 parts of kaolin, 4.5 parts of bone meal, 2 parts of copper oxide, high boron frit
3 parts.
In the present embodiment, the glass is alumina silicate glass.
In the present embodiment, the feldspar is albite.
In the present embodiment, the bone meal is bovine bone powder.
In the present embodiment, the boron content of the high boron frit is 12%, lead content 0%.
In the present embodiment, the preparation method of the transmutation crystallization grape glaze, including the following steps:
A, following raw material: fluorite, glass, quartz, feldspar, talcum, zinc oxide, barium monoxide, kaolinite is weighed by weight
Soil, bone meal, copper oxide, high boron frit；
B, mixture will be obtained after weighed each raw material mixes, ball milling 60min, wherein when ball milling, mixture, ball and water
Weight ratio are as follows: 1:2.5:0.5；
C, 200 meshes are crossed, froth in vacuum 20min is then carried out and obtains glaze slip, continue to stir 20min, and it is solid to adjust glaze slip
Content is 55%；
D, glaze slip is imposed on into matrix surface, then is warming up to 1290 DEG C, carry out glaze firing 110min hours, then be cooled to 220 DEG C
2h is kept the temperature, described matrix surface forms the transmutation crystallization grape glaze.
A kind of grape glaze ceramic, including green body and the glaze layer for being covered in the billet surface, the glaze layer is aforementioned
Transmutation crystallize grape glaze.
In the present embodiment, the preparation method of the grape glaze ceramic, including the following steps:
(1) following raw material: fluorite, glass, quartz, feldspar, talcum, zinc oxide, barium monoxide, kaolinite is weighed by weight
Soil, bone meal, copper oxide, high boron frit；
(2) mixture will be obtained after weighed each raw material mixes, ball milling 60min, wherein when ball milling, mixture, ball and water
Weight ratio are as follows: 1:2.5:0.5；
(3) 200 meshes are crossed, froth in vacuum 20min is then carried out and obtains glaze slip, continue to stir 20min, and it is solid to adjust glaze slip
Content is 55%；
(4) glaze slip is imposed on into billet surface, then is warming up to 1290 DEG C, carry out glaze firing 110min hours, then be cooled to 220 DEG C
2h is kept the temperature to get grape glaze ceramic.
Embodiment 3:
A kind of transmutation crystallization grape glaze, the raw material including following parts by weight: 12 parts of fluorite, 17 parts of glass, 25 parts of quartz, length
7.5 parts of stone, 2.5 parts of talcum, 75 parts of zinc oxide, 6 parts of barium monoxide, 11 parts of kaolin, 6.5 parts of bone meal, 4 parts of copper oxide, high boron are molten
7 parts of block.
In the present embodiment, the glass is alumina silicate glass.
In the present embodiment, the feldspar is albite.
In the present embodiment, the bone meal is lamb bone meal and Os Sus domestica powder.
In the present embodiment, the boron content of the high boron frit is 11%, lead content 0.001%.
In the present embodiment, the preparation method of the transmutation crystallization grape glaze, including the following steps:
A, following raw material: fluorite, glass, quartz, feldspar, talcum, zinc oxide, barium monoxide, kaolinite is weighed by weight
Soil, bone meal, copper oxide, high boron frit；
B, mixture will be obtained after weighed each raw material mixes, ball milling 90min, wherein when ball milling, mixture, ball and water
Weight ratio are as follows: 1:2.5:0.65；
C, 200 meshes are crossed, froth in vacuum 40min is then carried out and obtains glaze slip, continue to stir 30min, and it is solid to adjust glaze slip
Content is 65%；
D, glaze slip is imposed on into matrix surface, then is warming up to 1310 DEG C, carry out glaze firing 150min hours, then be cooled to 220 DEG C
2h is kept the temperature, described matrix surface forms the transmutation crystallization grape glaze.
A kind of grape glaze ceramic, including green body and the glaze layer for being covered in the billet surface, the glaze layer is aforementioned
Transmutation crystallize grape glaze.
In the present embodiment, the preparation method of the grape glaze ceramic, including the following steps:
(1) following raw material: fluorite, glass, quartz, feldspar, talcum, zinc oxide, barium monoxide, kaolinite is weighed by weight
Soil, bone meal, copper oxide, high boron frit；
(2) mixture will be obtained after weighed each raw material mixes, ball milling 90min, wherein when ball milling, mixture, ball and water
Weight ratio are as follows: 1:2.5:0.65；
(3) 200 meshes are crossed, froth in vacuum 40min is then carried out and obtains glaze slip, continue to stir 30min, and it is solid to adjust glaze slip
Content is 65%；
(4) glaze slip is imposed on into billet surface, then is warming up to 1310 DEG C, carry out glaze firing 150min hours, then be cooled to 220 DEG C
2h is kept the temperature to get grape glaze ceramic.
Embodiment 4:
A kind of transmutation crystallization grape glaze, the raw material including following parts by weight: 10 parts of fluorite, 15 parts of glass, 24 parts of quartz, length
6 parts of stone, 2 parts of talcum, 24 parts of zinc oxide, 2 parts of barium monoxide, 10 parts of kaolin, 5 parts of bone meal, 3 parts of copper oxide, 4 parts of high boron frit.
In the present embodiment, the glass is alumina silicate glass.
In the present embodiment, the feldspar is albite.
In the present embodiment, the bone meal is Os Sus domestica powder.
In the present embodiment, the boron content of the high boron frit is 12%, lead content 0%.
In the present embodiment, the preparation method of the transmutation crystallization grape glaze, including the following steps:
A, following raw material: fluorite, glass, quartz, feldspar, talcum, zinc oxide, barium monoxide, kaolinite is weighed by weight
Soil, bone meal, copper oxide, high boron frit；
B, mixture will be obtained after weighed each raw material mixes, ball milling 80min, wherein when ball milling, mixture, ball and water
Weight ratio are as follows: 1:2.5:0.55；
C, 200 meshes are crossed, froth in vacuum 35min is then carried out and obtains glaze slip, continue to stir 25min, and it is solid to adjust glaze slip
Content is 60%；
D, glaze slip is imposed on into matrix surface, then is warming up to 1305 DEG C, carry out glaze firing 130min hours, then be cooled to 220 DEG C
2h is kept the temperature, described matrix surface forms the transmutation crystallization grape glaze.
A kind of grape glaze ceramic, including green body and the glaze layer for being covered in the billet surface, the glaze layer is aforementioned
Transmutation crystallize grape glaze.
In the present embodiment, the preparation method of the grape glaze ceramic, including the following steps:
(1) following raw material: fluorite, glass, quartz, feldspar, talcum, zinc oxide, barium monoxide, kaolinite is weighed by weight
Soil, bone meal, copper oxide, high boron frit；
(2) mixture will be obtained after weighed each raw material mixes, ball milling 80min, wherein when ball milling, mixture, ball and water
Weight ratio are as follows: 1:2.5:0.55；
(3) 200 meshes are crossed, froth in vacuum 35min is then carried out and obtains glaze slip, continue to stir 25min, and it is solid to adjust glaze slip
Content is 60%；
(4) glaze slip is imposed on into billet surface, then is warming up to 1305 DEG C, carry out glaze firing 130min hours, then be cooled to 220 DEG C
2h is kept the temperature to get grape glaze ceramic.
Comparative example 1:
Difference with embodiment 4 is that, without fluorite, other are same as Example 4.
Comparative example 2:
Difference with embodiment 4 is that, without alumina silicate glass, other are same as Example 4.
Comparative example 3:
Difference with embodiment 4 is that, without barium monoxide, other are same as Example 4.
Comparative example 4:
Difference with embodiment 4 is that, without copper oxide, other are same as Example 4.
Comparative example 5:
Difference with embodiment 4 is that, without high boron frit, other are same as Example 4.
The grape glaze ceramic that the embodiment of the present invention 2 to embodiment 4, comparative example 1 to comparative example 5 obtain is carried out below
Performance test, test result are as shown in table 1:
In table, the test result of mobility, crystal property and appearance is the consistent mirror of expert in 5 ceramic fields
Determine result.
Table 1
As can be seen from the above table, transmutation of the invention crystallization grape glaze is made up of selected raw material, and rational proportion, selection
The fluorite of appropriate proportion, glass, quartz, feldspar, talcum, zinc oxide, barium monoxide, kaolin, bone meal, copper oxide, high boron are molten
Block, matrix surface obtained are formed with transmutation crystallization grape glaze or grape glaze ceramic, have purple grape crystallization effect, i.e.,
Unique transmutation crystallization, it is glittering and translucent, it is exquisite beautiful, do not have graceful bearing, artistic effect is strong；In addition, glaze superposition is available more
Mostly special artistic effect ceramic.
From upper table analysis it is found that transmutation crystallization grape glaze of the invention lacks fluorite, alumina silicate glass, barium monoxide, oxygen
Change any one in copper and high boron frit, it is unreasonable to will lead to crystallization, cannot obtain purple grape crystallization effect, accumulate
Glaze phenomenon, unsightly, rough surface etc..
The above is only the preferred embodiment of the present invention, it is noted that above-mentioned preferred embodiment is not construed as pair
Limitation of the invention, protection scope of the present invention should be defined by the scope defined by the claims..For the art
For those of ordinary skill, without departing from the spirit and scope of the present invention, several improvements and modifications can also be made, these change
It also should be regarded as protection scope of the present invention into retouching.
Claims (9)
1. a kind of transmutation crystallizes grape glaze, which is characterized in that the raw material including following parts by weight: 9~12 parts of fluorite, glass 14~
17 parts, 22~25 parts of quartz, 6~7.5 parts of feldspar, 1.5~2.5 parts of talcum, 23~25 parts of zinc oxide, 2~6 parts of barium monoxide, height
8~11 parts of ridge soil, 4.5~6.5 parts of bone meal, 2~4 parts of copper oxide, 3~7 parts of high boron frit.
2. transmutation according to claim 1 crystallizes grape glaze, which is characterized in that the transmutation crystallization grape glaze includes following
The raw material of parts by weight: 10 parts of fluorite, 15 parts of glass, quartz 24 parts, 6 parts of feldspar, 2 parts of talcum, 24 parts of zinc oxide, 2 parts of barium monoxide,
10 parts of kaolin, 5 parts of bone meal, 3 parts of copper oxide, 4 parts of high boron frit.
3. transmutation according to claim 1 crystallizes grape glaze, which is characterized in that the glass is alumina silicate glass.
4. transmutation according to claim 1 crystallizes grape glaze, which is characterized in that the feldspar is albite.
5. transmutation according to claim 1 crystallizes grape glaze, which is characterized in that the bone meal be bovine bone powder, lamb bone meal and
Any one or more in Os Sus domestica powder.
6. transmutation according to claim 1 crystallizes grape glaze, which is characterized in that the boron content of the high boron frit is greater than
10%, lead content is less than 0.01%.
7. a kind of preparation method for crystallizing grape glaze such as transmutation as claimed in any one of claims 1 to 6, which is characterized in that including
The following steps:
A, following raw material: fluorite, glass, quartz, feldspar, talcum, zinc oxide, barium monoxide, kaolin, bone is weighed by weight
Powder, copper oxide, high boron frit；
B, mixture will be obtained after weighed each raw material mixes, 60~90min of ball milling, wherein when ball milling, mixture, ball and water
Weight ratio are as follows: 1:2.5:(0.5~0.65)；
C, 200 meshes are crossed, 20~40min of froth in vacuum is then carried out and obtains glaze slip, continue 20~30min of stirring, and adjust glaze
Starching solid content is 55~65%；
D, glaze slip is imposed on into matrix surface, then is warming up to 1290~1310 DEG C, carry out glaze firing 110~150min hours, then cool down
To 220 DEG C of heat preservation 2h, described matrix surface forms the transmutation crystallization grape glaze.
8. a kind of grape glaze ceramic, which is characterized in that including green body and the glaze layer for being covered in the billet surface, the glaze
Layer is that transmutation as claimed in any one of claims 1 to 6 crystallizes grape glaze.
9. a kind of preparation method of grape glaze ceramic as claimed in claim 8, characterized in that it comprises the following steps:
(1) weigh following raw material by weight: fluorite, glass, quartz, feldspar, talcum, zinc oxide, barium monoxide, kaolin,
Bone meal, copper oxide, high boron frit；
(2) mixture will be obtained after weighed each raw material mixes, 60~90min of ball milling, wherein when ball milling, mixture, ball and
The weight ratio of water are as follows: 1:2.5:(0.5~0.65)；
(3) 200 meshes are crossed, 20~40min of froth in vacuum is then carried out and obtains glaze slip, continue 20~30min of stirring, and adjust
Glaze slip solid content is 55~65%；
Glaze slip is imposed on into billet surface, then is warming up to 1290~1310 DEG C, carries out glaze firing 110~150min hours, then be cooled to
220 DEG C of heat preservation 2h are to get grape glaze ceramic.
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Cited By (2)
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|---|---|---|---|---|
| CN110776256A (en) * | 2019-11-27 | 2020-02-11 | 蒙娜丽莎集团股份有限公司 | White radial crystal flower dry grain glaze, light-transmitting ceramic tile and preparation method thereof |
| CN113788618A (en) * | 2021-10-26 | 2021-12-14 | 福建省德化县恒翔工艺有限公司 | Crystalline glaze, crystalline glaze ceramic product and preparation method thereof |
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| CN113788618B (en) * | 2021-10-26 | 2023-08-08 | 福建省德化县恒翔工艺有限公司 | Crystallized glaze, crystallized glaze ceramic product and preparation method thereof |
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