CN110241503A - A kind of antistatic corduroy fabric and preparation method thereof - Google Patents
A kind of antistatic corduroy fabric and preparation method thereof Download PDFInfo
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- CN110241503A CN110241503A CN201910443455.3A CN201910443455A CN110241503A CN 110241503 A CN110241503 A CN 110241503A CN 201910443455 A CN201910443455 A CN 201910443455A CN 110241503 A CN110241503 A CN 110241503A
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- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
- D01F1/00—General methods for the manufacture of artificial filaments or the like
- D01F1/02—Addition of substances to the spinning solution or to the melt
- D01F1/09—Addition of substances to the spinning solution or to the melt for making electroconductive or anti-static filaments
-
- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
- D01F6/00—Monocomponent artificial filaments or the like of synthetic polymers; Manufacture thereof
- D01F6/88—Monocomponent artificial filaments or the like of synthetic polymers; Manufacture thereof from mixtures of polycondensation products as major constituent with other polymers or low-molecular-weight compounds
- D01F6/92—Monocomponent artificial filaments or the like of synthetic polymers; Manufacture thereof from mixtures of polycondensation products as major constituent with other polymers or low-molecular-weight compounds of polyesters
-
- D—TEXTILES; PAPER
- D02—YARNS; MECHANICAL FINISHING OF YARNS OR ROPES; WARPING OR BEAMING
- D02G—CRIMPING OR CURLING FIBRES, FILAMENTS, THREADS, OR YARNS; YARNS OR THREADS
- D02G3/00—Yarns or threads, e.g. fancy yarns; Processes or apparatus for the production thereof, not otherwise provided for
- D02G3/02—Yarns or threads characterised by the material or by the materials from which they are made
- D02G3/04—Blended or other yarns or threads containing components made from different materials
-
- D—TEXTILES; PAPER
- D02—YARNS; MECHANICAL FINISHING OF YARNS OR ROPES; WARPING OR BEAMING
- D02G—CRIMPING OR CURLING FIBRES, FILAMENTS, THREADS, OR YARNS; YARNS OR THREADS
- D02G3/00—Yarns or threads, e.g. fancy yarns; Processes or apparatus for the production thereof, not otherwise provided for
- D02G3/44—Yarns or threads characterised by the purpose for which they are designed
- D02G3/441—Yarns or threads with antistatic, conductive or radiation-shielding properties
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- D—TEXTILES; PAPER
- D03—WEAVING
- D03D—WOVEN FABRICS; METHODS OF WEAVING; LOOMS
- D03D15/00—Woven fabrics characterised by the material, structure or properties of the fibres, filaments, yarns, threads or other warp or weft elements used
- D03D15/40—Woven fabrics characterised by the material, structure or properties of the fibres, filaments, yarns, threads or other warp or weft elements used characterised by the structure of the yarns or threads
- D03D15/47—Woven fabrics characterised by the material, structure or properties of the fibres, filaments, yarns, threads or other warp or weft elements used characterised by the structure of the yarns or threads multicomponent, e.g. blended yarns or threads
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- D—TEXTILES; PAPER
- D03—WEAVING
- D03D—WOVEN FABRICS; METHODS OF WEAVING; LOOMS
- D03D15/00—Woven fabrics characterised by the material, structure or properties of the fibres, filaments, yarns, threads or other warp or weft elements used
- D03D15/50—Woven fabrics characterised by the material, structure or properties of the fibres, filaments, yarns, threads or other warp or weft elements used characterised by the properties of the yarns or threads
- D03D15/533—Woven fabrics characterised by the material, structure or properties of the fibres, filaments, yarns, threads or other warp or weft elements used characterised by the properties of the yarns or threads antistatic; electrically conductive
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- D—TEXTILES; PAPER
- D03—WEAVING
- D03D—WOVEN FABRICS; METHODS OF WEAVING; LOOMS
- D03D27/00—Woven pile fabrics
- D03D27/02—Woven pile fabrics wherein the pile is formed by warp or weft
- D03D27/04—Weft pile fabrics
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06C—FINISHING, DRESSING, TENTERING OR STRETCHING TEXTILE FABRICS
- D06C11/00—Teasing, napping or otherwise roughening or raising pile of textile fabrics
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06C—FINISHING, DRESSING, TENTERING OR STRETCHING TEXTILE FABRICS
- D06C7/00—Heating or cooling textile fabrics
- D06C7/02—Setting
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M10/00—Physical treatment of fibres, threads, yarns, fabrics, or fibrous goods made from such materials, e.g. ultrasonic, corona discharge, irradiation, electric currents, or magnetic fields; Physical treatment combined with treatment with chemical compounds or elements
- D06M10/02—Physical treatment of fibres, threads, yarns, fabrics, or fibrous goods made from such materials, e.g. ultrasonic, corona discharge, irradiation, electric currents, or magnetic fields; Physical treatment combined with treatment with chemical compounds or elements ultrasonic or sonic; Corona discharge
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/10—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing oxygen
- D06M13/184—Carboxylic acids; Anhydrides, halides or salts thereof
- D06M13/192—Polycarboxylic acids; Anhydrides, halides or salts thereof
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/50—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with organometallic compounds; with organic compounds containing boron, silicon, selenium or tellurium atoms
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- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
- D06M15/19—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with synthetic macromolecular compounds
- D06M15/21—Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds
- D06M15/263—Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds of unsaturated carboxylic acids; Salts or esters thereof
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- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M2101/00—Chemical constitution of the fibres, threads, yarns, fabrics or fibrous goods made from such materials, to be treated
- D06M2101/02—Natural fibres, other than mineral fibres
- D06M2101/04—Vegetal fibres
- D06M2101/06—Vegetal fibres cellulosic
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- D06M2101/00—Chemical constitution of the fibres, threads, yarns, fabrics or fibrous goods made from such materials, to be treated
- D06M2101/16—Synthetic fibres, other than mineral fibres
- D06M2101/30—Synthetic polymers consisting of macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
- D06M2101/32—Polyesters
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- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
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- D06M2200/00—Functionality of the treatment composition and/or properties imparted to the textile material
- D06M2200/20—Treatment influencing the crease behaviour, the wrinkle resistance, the crease recovery or the ironing ease
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- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M2200/00—Functionality of the treatment composition and/or properties imparted to the textile material
- D06M2200/50—Modified hand or grip properties; Softening compositions
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- D10—INDEXING SCHEME ASSOCIATED WITH SUBLASSES OF SECTION D, RELATING TO TEXTILES
- D10B—INDEXING SCHEME ASSOCIATED WITH SUBLASSES OF SECTION D, RELATING TO TEXTILES
- D10B2101/00—Inorganic fibres
- D10B2101/10—Inorganic fibres based on non-oxides other than metals
- D10B2101/12—Carbon; Pitch
- D10B2101/122—Nanocarbons
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- D—TEXTILES; PAPER
- D10—INDEXING SCHEME ASSOCIATED WITH SUBLASSES OF SECTION D, RELATING TO TEXTILES
- D10B—INDEXING SCHEME ASSOCIATED WITH SUBLASSES OF SECTION D, RELATING TO TEXTILES
- D10B2201/00—Cellulose-based fibres, e.g. vegetable fibres
- D10B2201/01—Natural vegetable fibres
- D10B2201/02—Cotton
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- D10B—INDEXING SCHEME ASSOCIATED WITH SUBLASSES OF SECTION D, RELATING TO TEXTILES
- D10B2201/00—Cellulose-based fibres, e.g. vegetable fibres
- D10B2201/20—Cellulose-derived artificial fibres
- D10B2201/22—Cellulose-derived artificial fibres made from cellulose solutions
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- D10B—INDEXING SCHEME ASSOCIATED WITH SUBLASSES OF SECTION D, RELATING TO TEXTILES
- D10B2331/00—Fibres made from polymers obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds, e.g. polycondensation products
- D10B2331/04—Fibres made from polymers obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds, e.g. polycondensation products polyesters, e.g. polyethylene terephthalate [PET]
Abstract
The invention discloses a kind of antistatic corduroy fabrics, include antistatic ground-tint tissue, antistatic pick float tissue, the antistatic ground-tint tissue includes antistatic warp thread, antistatic ground weft, antistatic warp thread and antistatic ground weft interweave with forming antistatic ground-tint tissue, and the antistatic pick float tissue is interwoven by antistatic warp thread and antistatic pile filling；Antistatic warp thread includes: 100~180 parts by weight of graphite alkene electrically conductive composite fibres, 35~50 parts by weight cottons, 12~18 parts by weight antistatic agents；Antistatic ground weft is polyester-cotton blend composite filament, and antistatic pile filling is copper ammonia fiber yarn, and graphene conductive composite fibre includes 0.5~1.6 part of graphene, 80~130 parts of terylene matrix fibers.Antistatic corduroy fabric of the invention has comfortable soft, the advantage that antistatic property is lasting, efficient.
Description
Technical field
The present invention relates to corduroy fabric technical field, in particular to a kind of antistatic corduroy fabric and its preparation side
Method.
Background technique
Fabric is the material for making clothes, can not only embody the style and characteristic of clothes, but also direct relation
To clothing color, the expression effect of moulding.With being gradually increased for living standard, people propose more and more functions to fabric
The requirement of the aspect of property and style.
Corduroy is that one kind cuts latitude fleece fabric, is similar to the wick-like suede item obviously swelled because fabric surface is presented, therefore
Referred to as corduroy.Its raw material also has the fiber blends such as cotton and terylene, acrylic fibers, spandex or intertexture, corduroy generally based on cotton
It is made of suede tissue and ground tissue two parts, the filling-backed weave that corduroy tissue is interweaved using two groups of weft yarns and one group of warp thread,
Ground group is woven with plain weave, twill etc..One group of weft yarn (claiming ground weft) is woven into consolidation villus with warp thread in two groups of weft yarns of corduroy
Ground cloth, another group of weft yarn (claiming pile filling) interweaves with warp thread constitutes regular pick float, and pick float forms villus after cutting off.
Existing notification number is the Chinese invention patent of CN105755648B, disclose a kind of three-dimensional square corduroy fabric and
Its method for weaving, the corduroy fabric include one group of warp thread, three groups of weft yarns, and three groups of weft yarns are respectively ground weft, the first pile filling and the
Two pile fillings, wherein ground weft and warp thread use 150D/48F DIY terylene net-thread, and the first pile filling is washed using 160D/72F CD/T sun
Composite filament, the second Velveteen use 160D/72F T/N polyamide composite filaments.Ground weft and warp thread interweave with forming fabric ground-tint tissue, fabric
Two side faces unit and a top surface unit with corresponding three-dimensional square pattern, one side unit are that the first pile filling floats on cloth cover, the
Two pile fillings sink to interweave with ground-tint；Another side unit is that the second pile filling floats on cloth cover, and the first pile filling sinks to interweave with ground-tint；Top
Face unit is that the first pile filling and the second pile filling float on cloth cover and constitute mixing pick float, is then carried out again to the semi-finished product fabric knitted
Dyeing processing, final obtained two side faces unit is not homochromy and top surface unit is the wick for showing the double-colored pattern of three-dimensional square of colour mixture
Suede.
Although traditional vertical bar corduroy to be modified to in prior art by three groups of weft yarn manufactures have solid
Criss-cross decorative pattern has polychrome sense, but in actual use, since face liber mostly uses chemical fibre raw material, is easy to produce
Electrostatic, especially the first pile filling and the second pile filling cut pile formed villus after, villus generate electrostatic be more easier adsorb dust and
Breed acarid and bacterium, it is therefore desirable to be further improved in terms of antistatic property.
Summary of the invention
The purpose of the present invention is to provide a kind of antistatic corduroy fabric and preparation method thereof, manufactured corduroy fabrics
With comfortable softness, antistatic property is lasting, efficient advantage.
To achieve the above object, the present invention provides the following technical scheme that a kind of antistatic corduroy fabric, including resist quiet
Electric ground-tint tissue, antistatic pick float tissue, the antistatic ground-tint tissue include antistatic warp thread, antistatic ground weft, antistatic
Warp thread and antistatic ground weft interweave with forming antistatic ground-tint tissue, the antistatic pick float tissue by antistatic warp thread with it is antistatic
Pile filling is interwoven；
Antistatic warp thread includes: 100~180 parts by weight of graphite alkene electrically conductive composite fibres, 35~50 parts by weight cottons, 12~18 weight
Part antistatic agent；
Antistatic ground weft is polyester-cotton blend composite filament, and antistatic pile filling is copper ammonia fiber yarn.
By using above-mentioned technical proposal, graphene conductive composite fibre is to form graphene in conjunction with special fiber
A kind of tencel can significantly improve fiber and fabric antistatic property using the antistatic property that graphene is excellent.Relatively
In traditional inorganic, organic antistatic agents, graphene is green safe, more suitable for human skin, has the function of pro-skin foster skin；
On the other hand, graphene conductive is high, in conjunction with general fibre, the electric conductivity of the persistent high efficiency of fiber can be improved, to increase
Add the antistatic property of fabric.
Cotton fiber softness skin-friendly is good, moisture absorbing and sweat releasing and abundant raw materials are cheap, can be further improved the dress of fabric
Comfort level, while the processing cost of fabric can also be reduced.
The fibre section of copper ammonia fiber is rounded, no skin-core structure, and fiber can bear high elongation, monofilament obtained compared with
Carefully, the feel and pliability of fabric can be improved；On the other hand, the sucting wet air permeability of copper ammonia fiber is good, drapability is high, and has
Preferable antistatic property can be further improved the antistatic property of fabric.The addition of antistatic agent, can be further improved
The antistatic property of fabric.
The present invention is further arranged to, and the graphene conductive composite fibre includes 0.5~1.6 part of graphene, 80~130
Part matrix fiber.
By using above-mentioned technical proposal, graphene and matrix fiber are organically combined, so that fiber has the spy of graphene
Property, to assign the electric conductivity of fabric persistent high efficiency, and then reduce the phenomenon that face liber gathers electrostatic charge.
The present invention is further arranged to, and described matrix fiber is terylene.
By using above-mentioned technical proposal, terylene has preferable elasticity, and intensity is high, and chemically-resistant degradation, resistance to acid and alkali,
And wearability is more excellent, so as to effectively improve the intensity and wear resistance of fabric.
The present invention is further arranged to, and the preparation method of the graphene conductive composite fibre includes the following steps:
The preparation method of the graphene conductive composite fibre, includes the following steps:
S1, pretreatment: graphene, matrix fiber are dried in vacuum drying oven, and drying temperature is 75~95 DEG C, drying time
For 6~8h；
It is S2, dry-mixed: graphene, matrix fiber are put into high-speed mixer, 250~320rpm of revolving speed is adjusted, mixes 1~3min,
850~950rpm of revolving speed is adjusted again, continuess to mix 1~2min, obtains conducting base fiber premix；
S3, granulation is blended: conducting base fiber premix, antistatic agent investment twin-screw blender is subjected to blending granulation,
Melt blending temperature is 255~260 DEG C, and revolving speed is 110~180rpm, and the melt blending time is 30~45min, melt blended material
Cooling is squeezed out, obtains conducting fibre master batch through pelletizing；
S4, melt spinning: using melt spinning machine to conducting fibre master batch melt spinning, spinning temperature is 260~265 DEG C, volume
It is set as 1500~2400m/min around speed, obtains nascent conductive fiber；
S5, drafting forming: carrying out drawing-off to nascent conductive fiber, and drawing temperature is 100~120 DEG C, and drafting multiple is 4~6 times,
Finally obtain graphene conductive composite fibre.
It is by using above-mentioned technical proposal, the graphene after vacuum drying, matrix fiber progress is dry-mixed, graphite can be made
Alkene is uniformly mixed with matrix fiber, then will obtain conducting base fibre blend, antistatic agent and twin-screw blender is added together
Melt blending is carried out, so that graphene, antistatic agent and matrix fiber be made to carry out depth integration, graphene and antistatic agent can
It is evenly dispersed to fiber surface and inside, to improve the binding strength of graphene, antistatic agent and fiber；Again by stone
Black alkene fiber master batch carries out melt spinning, obtains the higher nascent conductive fiber of dispersion degree, then make nascent lead by drafting forming
The degree of orientation and crystallinity of electric fibrous inside improve, to further increase the intensity and elongation of fiber.
The present invention is further arranged to, and the antistatic agent is organosilicon quaternary ammonium salt antistatic agent.
By using above-mentioned technical proposal, organosilicon quaternary ammonium salt is the good antistatic agent of a kind of comprehensive performance, and arrangement is knitted
Such antistatic agent does not need high temperature baking when object, just can produce lasting antistatic effect after general drying, knitting after arrangement
Object not only has excellent antistatic property, but also is also equipped with good moisture absorption absorption of perspiration, flexibility, resilience, static electricity resistance,
And pollution resistance.
The present invention is further arranged to, the preparation method of the antistatic corduroy fabric, comprising the following steps:
S1, scribbled: it carries out graphene conductive composite fibre, cotton blended to obtain conductive hybrid yarn；
S2, fabric weaving: it is knitted using dobbies line, warp thread, ground weft and pile filling is weaved, to form corduroy fabric；
S3, cut pile: corduroy fabric is subjected to tentering along broadwise, then fabric is inserted into the diameter of fabric by cut pile device, guide pin
Into suede lane, under pushing needle bar propulsion, the pick float yarn on fabric is cut into villus by cut pile blade, and cut pile speed is set as 5m/min
~7m/min, hobboing cutter revolving speed are set as 750rpm~950rpm；
S4, brushing: the fabric after cut pile passes through atmospheric plasma pretreatment unit with the speed of 18m/min~35m/min, into
The processing of row plasma discharge, plasma discharge power are set as 100w~65w, and the discharge treatment time is 20s~45s, through putting
After electric treatment, fabric carries out jet humidification, brushing again；
S5, cut velvet: corduroy fabric is uniformly sprayed in fabric tapetum and stands conducive to what villus was stood upright after carrying out abundant brushing
Suede composite assistant；
S6, sizing arrange: the corduroy fabric after cut velvet being carried out high-temperature shaping by forming machine, setting temperature is set as 125
DEG C~140 DEG C, setting time is 30s~40s.
It is blended to obtain conductive hybrid yarn by using above-mentioned technical proposal, so that yarn is had the compound spy of multiple fiber
Property and function, especially mention assign fabric high-efficient and lasting antistatic property；Plasma discharge treatment can be to polyester fiber table
Face is modified, and is made fiber surface that division, etching occur, and form pit and crackle, the surface area of fiber is increased, to mention
High terylene and other interfibrous cohesive forces, also effectively increase wetability, dye-uptake and the dyefastness of terylene, brushing can
It stands upright so that the villus of corduroy fabric is unfolded；Cut velvet, sizing can use the conditions such as cut velvet composite assistant, high temperature to corduroy
Material treatment, to further increase the standing upright property and wrinkle resistance of fabric and villus.
The present invention is further arranged to, and cut velvet composite assistant comprises the following components in parts by weight in the S6 step:
40~60 parts of stiffening agents, 30~40 parts of crease-shedding finishing agents, 10~2 parts of organosilicon quaternary ammonium salt antistatic agents, 30~45 parts
Deionized water.
By using above-mentioned technical proposal, stiffening agent can be attached to fuzzy surface and form specific film, make after film forming
It obtains standing upright property of villus to improve, crease-shedding finishing agent can be further improved the wrinkle resistance of fabric, and machine silicon quaternary ammonium salt antistatic agent is attached
And infiltrate into fibrous inside, so as to further increase the antistatic property of fabric.
The present invention is further arranged to, and the stiffening agent is fluorinated acrylate polymer.
By using above-mentioned technical proposal, fluorinated acrylate polymer introduces perfluoroalkyl on side chain, in film forming
In the process, the rich product of perfluoroalkyl meeting arrives the interface of polymer and air, and stretches into air, since perfluorinated side chains tend to court
Outside, " shielding protection " is formed to main chain and interior molecules, so as to which carbon carbon backbone chain is closely encased, so that fluorine-containing
Esters polymer durability and chemical-resistant stability are good；On the other hand, fluorinated acrylate polymer have good film forming,
Flexibility and adhesive property can significantly improve the stiffness of fiber, waterproofness and antifouling after villus and fiber surface film forming
Performance, while also improving the stereoscopic and sense of fullness of corduroy villus.
The present invention is further arranged to, and the crease-shedding finishing agent is butane tetracarboxylic acid.
By using above-mentioned technical proposal, butane tetracarboxylic acid is a kind of formaldehyde-free anti-crease finish, highly-safe, water-soluble
It is good, it is easily configured compounding agent solution, and be significantly improved effect to the wrinkle resistance of fabric, washability.
In conclusion the invention has the following advantages:
1. the graphene conductive composite fibre in the present invention, by by graphene, antistatic agent, terylene matrix fiber in twin-screw
It is blended and is granulated in blender, form conducting fibre master batch, then conducting fibre master batch is formed into graphene conductive by melt spinning
Composite fibre obtains graphene in conjunction with high degree of dispersion in molecular level with fiber, to obtain the almost permanent antistatic spy of property
Property；
2. it is good using copper ammonia fiber sucting wet air permeability height, drapability using copper ammonia fiber as antistatic weft yarn in the present invention, and have
The characteristics of standby preferable antistatic property, achieve the effect that further increase fabric snugness of fit and antistatic property；
3. the fabric in the present invention is by the way that organosilicon quaternary ammonium salt antistatic agent to be added in conducting base fiber premix, into
Row, which is blended, to be granulated so that antistatic agent is evenly dispersed to fiber surface and inside, thus reach improve fabric persistent high efficiency resist it is quiet
Electrical effect；
4. arranging using cut velvet composite assistant to villus during brushing in the present invention, the stiffness of villus is improved,
Reduce villus lodging phenomenon, but also corduroy fabric appearance more horn of plenty.
Specific embodiment
Invention is further described in detail with reference to embodiments.
Embodiment
Embodiment 1:
A kind of antistatic corduroy fabric, including antistatic ground-tint tissue, antistatic pick float tissue, the antistatic ground-tint tissue
Including antistatic warp thread, antistatic ground weft, antistatic warp thread and antistatic ground weft interweave with forming antistatic ground-tint tissue, described anti-
Electrostatic pick float tissue is interwoven by antistatic warp thread and antistatic pile filling；Wherein, antistatic warp thread includes: 100 parts by weight stones
Black alkene electrically conductive composite fibre, 35 parts by weight cottons, 12 parts by weight antistatic agents；Antistatic ground weft is polyester-cotton blend composite filament, antistatic suede
Latitude is copper ammonia fiber yarn；
The preparation step of graphene conductive composite fibre is as follows:
S1, pretreatment: 0.5 part of graphene, 80 parts of matrix fibers are put into vacuum drying oven drying, drying temperature is 75 DEG C, dry
Time is 6h；
It is S2, dry-mixed: graphene, matrix fiber being put into high-speed mixer, revolving speed 250rpm is adjusted, mixes 1min, then adjust and turn
Fast 850rpm, continuess to mix 1min, obtains conducting base fiber premix；
S3, granulation is blended: conducting base fiber premix, antistatic agent investment twin-screw blender is subjected to blending granulation,
Melt blending temperature is 255 DEG C, revolving speed 110rpm, and the melt blending time is 30min, and melt blended material squeezes out cooling, through cutting
Grain obtains conducting fibre master batch；
S4, melt spinning: using melt spinning machine to conducting fibre master batch melt spinning, spinning temperature is 260 DEG C, winding speed
It is set as 1500m/min, obtains nascent conductive fiber；
S5, drafting forming: carrying out drawing-off to nascent conductive fiber, and drawing temperature is 100 DEG C, and drafting multiple is 4 times, is finally obtained
Graphene conductive composite fibre；
The preparation method of antistatic corduroy fabric, comprising the following steps:
S1, scribbled: it carries out graphene conductive composite fibre, cotton blended to obtain conductive hybrid yarn；
S2, fabric weaving: it is knitted using dobbies line, warp thread, ground weft and pile filling is weaved, to form corduroy fabric；
S3, cut pile: corduroy fabric is subjected to tentering along broadwise, then fabric is inserted into the diameter of fabric by cut pile device, guide pin
Into suede lane, under pushing needle bar propulsion, the pick float yarn on fabric is cut into villus by cut pile blade, and cut pile speed is set as 5m/
Min, hobboing cutter revolving speed are set as 750rpm；
S4, brushing: the fabric after cut pile, by atmospheric plasma pretreatment unit, carries out plasma with the speed of 18m/min
Body discharge treatment, plasma discharge power are set as 100w, and the discharge treatment time is 20s, and after discharge treatment, fabric carries out again
Jet humidification, brushing；
S5, cut velvet: corduroy fabric is uniformly sprayed in fabric tapetum and stands conducive to what villus was stood upright after carrying out abundant brushing
Suede composite assistant, cut velvet composite assistant include 40 parts by weight fluorinated acrylate polymer stiffening agents, 30 parts by weight butane tetracarboxylics
Sour crease-shedding finishing agent, 10 parts by weight organosilicon quaternary ammonium salt antistatic agents, 30 parts by weight deionized water；
S6, sizing arrange: the corduroy fabric after cut velvet being carried out high-temperature shaping by forming machine, setting temperature is set as 125
DEG C, setting time 30s.
Embodiment 2:
A kind of antistatic corduroy fabric, antistatic warp thread include: 120 parts by weight of graphite alkene electrically conductive composite fibres, 38 parts by weight
Cotton, 13 parts by weight antistatic agents；Antistatic ground weft is polyester-cotton blend composite filament, and antistatic pile filling is copper ammonia fiber yarn；
The preparation step of graphene conductive composite fibre is as follows:
S1, pretreatment: 0.7 part of graphene, 90 parts of matrix fibers are put into vacuum drying oven drying, drying temperature is 80 DEG C, dry
Time is 7h；
It is S2, dry-mixed: graphene, matrix fiber being put into high-speed mixer, revolving speed 270rpm is adjusted, mixes 2min, then adjust and turn
Fast 880rpm, continuess to mix 2min, obtains conducting base fiber premix；
S3, granulation is blended: conducting base fiber premix, antistatic agent investment twin-screw blender is subjected to blending granulation,
Melt blending temperature is 257 DEG C, revolving speed 120rpm, and the melt blending time is 33min, and melt blended material squeezes out cooling, through cutting
Grain obtains conducting fibre master batch；
S4, melt spinning: using melt spinning machine to conducting fibre master batch melt spinning, spinning temperature is 262 DEG C, winding speed
It is set as 1800m/min, obtains nascent conductive fiber；
S5, drafting forming: carrying out drawing-off to nascent conductive fiber, and drawing temperature is 105 DEG C, and drafting multiple is 5 times, is finally obtained
Graphene conductive composite fibre；
The preparation method of antistatic corduroy fabric, comprising the following steps:
S1, scribbled: it carries out graphene conductive composite fibre, cotton blended to obtain conductive hybrid yarn；
S2, fabric weaving: it is knitted using dobbies line, warp thread, ground weft and pile filling is weaved, to form corduroy fabric；
S3, cut pile: corduroy fabric is subjected to tentering along broadwise, then fabric is inserted into the diameter of fabric by cut pile device, guide pin
Into suede lane, under pushing needle bar propulsion, the pick float yarn on fabric is cut into villus by cut pile blade, and cut pile speed is set as 6m/
Min, hobboing cutter revolving speed are set as 780rpm；
S4, brushing: the fabric after cut pile, by atmospheric plasma pretreatment unit, carries out plasma with the speed of 22m/min
Body discharge treatment, plasma discharge power are set as 90w, and the discharge treatment time is 25s, and after discharge treatment, fabric carries out again
Jet humidification, brushing；
S5, cut velvet: corduroy fabric is uniformly sprayed in fabric tapetum and stands conducive to what villus was stood upright after carrying out abundant brushing
Suede composite assistant, cut velvet composite assistant include 45 parts by weight fluorinated acrylate polymer stiffening agents, 32 parts by weight butane tetracarboxylics
Sour crease-shedding finishing agent, 12 parts by weight organosilicon quaternary ammonium salt antistatic agents, 34 parts by weight deionized water；
S6, sizing arrange: the corduroy fabric after cut velvet being carried out high-temperature shaping by forming machine, setting temperature is set as 127
DEG C, setting time 33s.
Embodiment 3:
A kind of antistatic corduroy fabric, antistatic warp thread include: 140 parts by weight of graphite alkene electrically conductive composite fibres, 41 parts by weight
Cotton, 14 parts by weight antistatic agents；Antistatic ground weft is polyester-cotton blend composite filament, and antistatic pile filling is copper ammonia fiber yarn；
The preparation step of graphene conductive composite fibre is as follows:
S1, pretreatment: 1.0 parts of graphenes, 100 parts of matrix fibers are put into vacuum drying oven drying, drying temperature is 85 DEG C, dry
Time is 8h；
It is S2, dry-mixed: graphene, matrix fiber being put into high-speed mixer, revolving speed 290rpm is adjusted, mixes 3min, then adjust and turn
Fast 900rpm, continuess to mix 2min, obtains conducting base fiber premix；
S3, granulation is blended: conducting base fiber premix, antistatic agent investment twin-screw blender is subjected to blending granulation,
Melt blending temperature is 258 DEG C, revolving speed 150rpm, and the melt blending time is 38min, and melt blended material squeezes out cooling, through cutting
Grain obtains conducting fibre master batch；
S4, melt spinning: using melt spinning machine to conducting fibre master batch melt spinning, spinning temperature is 263 DEG C, winding speed
It is set as 1900m/min, obtains nascent conductive fiber；
S5, drafting forming: carrying out drawing-off to nascent conductive fiber, and drawing temperature is 110 DEG C, and drafting multiple is 6 times, is finally obtained
Graphene conductive composite fibre；
The preparation method of antistatic corduroy fabric, comprising the following steps:
S1, scribbled: it carries out graphene conductive composite fibre, cotton blended to obtain conductive hybrid yarn；
S2, fabric weaving: it is knitted using dobbies line, warp thread, ground weft and pile filling is weaved, to form corduroy fabric；
S3, cut pile: corduroy fabric is subjected to tentering along broadwise, then fabric is inserted into the diameter of fabric by cut pile device, guide pin
Into suede lane, under pushing needle bar propulsion, the pick float yarn on fabric is cut into villus by cut pile blade, and cut pile speed is set as 7m/
Min, hobboing cutter revolving speed are set as 850rpm；
S4, brushing: the fabric after cut pile, by atmospheric plasma pretreatment unit, carries out plasma with the speed of 26m/min
Body discharge treatment, plasma discharge power are set as 80w, and the discharge treatment time is 35s, and after discharge treatment, fabric carries out again
Jet humidification, brushing；
S5, cut velvet: corduroy fabric is uniformly sprayed in fabric tapetum and stands conducive to what villus was stood upright after carrying out abundant brushing
Suede composite assistant, cut velvet composite assistant include 50 parts by weight fluorinated acrylate polymer stiffening agents, 38 parts by weight butane tetracarboxylics
Sour crease-shedding finishing agent, 16 parts by weight organosilicon quaternary ammonium salt antistatic agents, 38 parts by weight deionized water；
S6, sizing arrange: the corduroy fabric after cut velvet being carried out high-temperature shaping by forming machine, setting temperature is set as 135
DEG C, setting time 36s.
Embodiment 4:
A kind of antistatic corduroy fabric, antistatic warp thread include: 160 parts by weight of graphite alkene electrically conductive composite fibres, 45 parts by weight
Cotton, 16 parts by weight antistatic agents；Antistatic ground weft is polyester-cotton blend composite filament, and antistatic pile filling is copper ammonia fiber yarn；
The preparation step of graphene conductive composite fibre is as follows:
S1, pretreatment: 1.3 parts of graphenes, 115 parts of matrix fibers are put into vacuum drying oven drying, drying temperature is 90 DEG C, dry
Time is 8h；
It is S2, dry-mixed: graphene, matrix fiber being put into high-speed mixer, revolving speed 310rpm is adjusted, mixes 3min, then adjust and turn
Fast 930rpm, continuess to mix 2min, obtains conducting base fiber premix；
S3, granulation is blended: conducting base fiber premix, antistatic agent investment twin-screw blender is subjected to blending granulation,
Melt blending temperature is 260 DEG C, revolving speed 160rpm, and the melt blending time is 42min, and melt blended material squeezes out cooling, through cutting
Grain obtains conducting fibre master batch；
S4, melt spinning: using melt spinning machine to conducting fibre master batch melt spinning, spinning temperature is 265 DEG C, winding speed
It is set as 2000m/min, obtains nascent conductive fiber；
S5, drafting forming: carrying out drawing-off to nascent conductive fiber, and drawing temperature is 115 DEG C, and drafting multiple is 6 times, is finally obtained
Graphene conductive composite fibre；
The preparation method of antistatic corduroy fabric, comprising the following steps:
S1, scribbled: it carries out graphene conductive composite fibre, cotton blended to obtain conductive hybrid yarn；
S2, fabric weaving: it is knitted using dobbies line, warp thread, ground weft and pile filling is weaved, to form corduroy fabric；
S3, cut pile: corduroy fabric is subjected to tentering along broadwise, then fabric is inserted into the diameter of fabric by cut pile device, guide pin
Into suede lane, under pushing needle bar propulsion, the pick float yarn on fabric is cut into villus by cut pile blade, and cut pile speed is set as 7m/
Min, hobboing cutter revolving speed are set as 900rpm；
S4, brushing: the fabric after cut pile, by atmospheric plasma pretreatment unit, carries out plasma with the speed of 30m/min
Body discharge treatment, plasma discharge power are set as 75w, and the discharge treatment time is 40s, and after discharge treatment, fabric carries out again
Jet humidification, brushing；
S5, cut velvet: corduroy fabric is uniformly sprayed in fabric tapetum and stands conducive to what villus was stood upright after carrying out abundant brushing
Suede composite assistant, cut velvet composite assistant include 55 parts by weight fluorinated acrylate polymer stiffening agents, 38 parts by weight butane tetracarboxylics
Sour crease-shedding finishing agent, 18 parts by weight organosilicon quaternary ammonium salt antistatic agents, 42 parts by weight deionized water；
S6, sizing arrange: the corduroy fabric after cut velvet being carried out high-temperature shaping by forming machine, setting temperature is set as 135
DEG C, setting time 37s.
Embodiment 5:
A kind of antistatic corduroy fabric, antistatic warp thread include: 180 parts by weight of graphite alkene electrically conductive composite fibres, 50 parts by weight
Cotton, 18 parts by weight antistatic agents；Antistatic ground weft is polyester-cotton blend composite filament, and antistatic pile filling is copper ammonia fiber yarn；
The preparation step of graphene conductive composite fibre is as follows:
S1, pretreatment: 1.6 parts of graphenes, 130 parts of matrix fibers are put into vacuum drying oven drying, drying temperature is 95 DEG C, dry
Time is 8h；
It is S2, dry-mixed: graphene, matrix fiber being put into high-speed mixer, revolving speed 320rpm is adjusted, mixes 3min, then adjust and turn
Fast 950rpm, continuess to mix 2min, obtains conducting base fiber premix；
S3, granulation is blended: conducting base fiber premix, antistatic agent investment twin-screw blender is subjected to blending granulation,
Melt blending temperature is 260 DEG C, revolving speed 180rpm, and the melt blending time is 45min, and melt blended material squeezes out cooling, through cutting
Grain obtains conducting fibre master batch；
S4, melt spinning: using melt spinning machine to conducting fibre master batch melt spinning, spinning temperature is 265 DEG C, winding speed
It is set as 2400m/min, obtains nascent conductive fiber；
S5, drafting forming: carrying out drawing-off to nascent conductive fiber, and drawing temperature is 120 DEG C, and drafting multiple is 6 times, is finally obtained
Graphene conductive composite fibre；
The preparation method of antistatic corduroy fabric, comprising the following steps:
S1, scribbled: it carries out graphene conductive composite fibre, cotton blended to obtain conductive hybrid yarn；
S2, fabric weaving: it is knitted using dobbies line, warp thread, ground weft and pile filling is weaved, to form corduroy fabric；
S3, cut pile: corduroy fabric is subjected to tentering along broadwise, then fabric is inserted into the diameter of fabric by cut pile device, guide pin
Into suede lane, under pushing needle bar propulsion, the pick float yarn on fabric is cut into villus by cut pile blade, and cut pile speed is set as 7m/
Min, hobboing cutter revolving speed are set as 950rpm；
S4, brushing: the fabric after cut pile, by atmospheric plasma pretreatment unit, carries out plasma with the speed of 35m/min
Body discharge treatment, plasma discharge power are set as 65w, and the discharge treatment time is 45s, and after discharge treatment, fabric carries out again
Jet humidification, brushing；
S5, cut velvet: corduroy fabric is uniformly sprayed in fabric tapetum and stands conducive to what villus was stood upright after carrying out abundant brushing
Suede composite assistant, cut velvet composite assistant include 60 parts by weight fluorinated acrylate polymer stiffening agents, 40 parts by weight butane tetracarboxylics
Sour crease-shedding finishing agent, 20 parts by weight organosilicon quaternary ammonium salt antistatic agents, 45 parts by weight deionized water；
S6, sizing arrange: the corduroy fabric after cut velvet being carried out high-temperature shaping by forming machine, setting temperature is set as 140
DEG C, setting time 40s.
Performance detection respectively prepares the consistent sample fabric of 5 block specifications according to the method for Examples 1 to 5, and according to following
Item Indexs measure sample fabric, the test result of sample fabric as made from the same embodiment are averaged, test result such as table 1
It is shown:
Antistatic property: according to GB/T24249-2009 standard, the surface resistivity of fabric is tested；
The indices test result of sample fabric made from 1 the above various embodiments of table
| Test item | Feel and pliability | Grammes per square metre g/m2 | Surface resistivity/Ω |
| Embodiment 1 | Comfortable feel is soft | 138 | 8.6×108 |
| Embodiment 2 | Comfortable feel is soft | 140 | 9.1×108 |
| Embodiment 3 | Comfortable feel is soft | 139 | 8.8×108 |
| Embodiment 4 | Comfortable feel is soft | 137 | 9.1×108 |
| Embodiment 5 | Comfortable feel is soft | 135 | 9.9×108 |
As can be seen from Table 1, the comfortable feel and pliability of 1~5 sample fabric of the embodiment of the present invention are preferable, and embodiment 1
The grammes per square metre of~5 sample fabrics is relatively low, and illustrates that fabric of the invention is slim and graceful, is more suitable dress；In terms of antistatic property,
The surface resistivity of Examples 1 to 5 fabric reaches 8.5 × 108More than, illustrate in fabric of the invention using graphene conductive
Composite fibre and cuprammonium antistatic fibre, and granulation is directly blended with graphene conductive composite fibre by antistatic agent, make to resist
Electrostatic agent is evenly dispersed to fibrous inside and surface, to achieve the effect that significantly improve fabric antistatic property.
This specific embodiment is only explanation of the invention, is not limitation of the present invention, those skilled in the art
Member can according to need the modification that not creative contribution is made to the present embodiment after reading this specification, but as long as at this
All by the protection of Patent Law in the scope of the claims of invention.
Claims (9)
1. a kind of antistatic corduroy fabric, it is characterised in that: described including antistatic ground-tint tissue, antistatic pick float tissue
Antistatic ground-tint tissue includes antistatic warp thread, antistatic ground weft, antistatic warp thread interweave with antistatic ground weft to be formed it is antistatic
Ground-tint tissue, the antistatic pick float tissue are interwoven by antistatic warp thread and antistatic pile filling；
Antistatic warp thread includes: 100~180 parts by weight of graphite alkene electrically conductive composite fibres, 35~50 parts by weight cottons, 12~18 weight
Part antistatic agent；
Antistatic ground weft is polyester-cotton blend composite filament, and antistatic pile filling is copper ammonia fiber yarn.
2. a kind of antistatic corduroy fabric according to claim 1, it is characterised in that: the compound fibre of graphene conductive
Dimension includes 0.5~1.6 part of graphene, 80~130 parts of matrix fibers.
3. a kind of antistatic corduroy fabric according to claim 2, it is characterised in that: described matrix fiber is terylene.
4. a kind of antistatic corduroy fabric according to claim 1, it is characterised in that: the compound fibre of graphene conductive
The preparation method of dimension, includes the following steps:
S1, pretreatment: graphene, matrix fiber are dried in vacuum drying oven, and drying temperature is 75~95 DEG C, drying time
For 6~8h；
It is S2, dry-mixed: graphene, matrix fiber are put into high-speed mixer, 250~320rpm of revolving speed is adjusted, mixes 1~3min,
850~950rpm of revolving speed is adjusted again, continuess to mix 1~2min, obtains conducting base fiber premix；
S3, granulation is blended: conducting base fiber premix, antistatic agent investment twin-screw blender is subjected to blending granulation,
Melt blending temperature is 255~260 DEG C, and revolving speed is 110~180rpm, and the melt blending time is 30~45min, melt blended material
Cooling is squeezed out, obtains conducting fibre master batch through pelletizing；
S4, melt spinning: using melt spinning machine to conducting fibre master batch melt spinning, spinning temperature is 260~265 DEG C, volume
It is set as 1500~2400m/min around speed, obtains nascent conductive fiber；
S5, drafting forming: carrying out drawing-off to nascent conductive fiber, and drawing temperature is 100~120 DEG C, and drafting multiple is 4~6 times,
Finally obtain graphene conductive composite fibre.
5. a kind of antistatic corduroy fabric according to claim 1, it is characterised in that: the antistatic agent is organosilicon
Quaternary ammonium salt antistatic agent.
6. the preparation method of described in any item antistatic corduroy fabrics according to claim 1~5, which is characterized in that including
Following steps:
S1, scribbled: it carries out graphene conductive composite fibre, cotton blended to obtain conductive hybrid yarn；
S2, fabric weaving: it is knitted using dobbies line, warp thread, ground weft and pile filling is weaved, to form corduroy fabric；
S3, cut pile: corduroy fabric is subjected to tentering along broadwise, then fabric is inserted into the diameter of fabric by cut pile device, guide pin
Into suede lane, under pushing needle bar propulsion, the pick float yarn on fabric is cut into villus by cut pile blade, and cut pile speed is set as 5m/min
~7m/min, hobboing cutter revolving speed are set as 750rpm~950rpm；
S4, brushing: the fabric after cut pile passes through atmospheric plasma pretreatment unit with the speed of 18m/min~35m/min, into
The processing of row plasma discharge, plasma discharge power are set as 100w~65w, and the discharge treatment time is 20s~45s, through putting
After electric treatment, fabric carries out jet humidification, brushing again；
S5, cut velvet: corduroy fabric is uniformly sprayed in fabric tapetum and stands conducive to what villus was stood upright after carrying out abundant brushing
Suede composite assistant；
S6, sizing arrange: the corduroy fabric after cut velvet being carried out high-temperature shaping by forming machine, setting temperature is set as 125
DEG C~140 DEG C, setting time is 30s~40s.
7. a kind of preparation method of antistatic corduroy fabric according to claim 6, it is characterised in that: the cut velvet is multiple
Auxiliary agent is closed to comprise the following components in parts by weight:
40~60 parts of stiffening agents, 30~40 parts of crease-shedding finishing agents, 10~20 parts of organosilicon quaternary ammonium salt antistatic agents, 30~45 parts
Deionized water.
8. a kind of preparation method of antistatic corduroy fabric according to claim 7, it is characterised in that: the stiffening agent
For fluorinated acrylate polymer.
9. a kind of preparation method of antistatic corduroy fabric according to claim 7, it is characterised in that: described crease-resistant whole
Reason agent is butane tetracarboxylic acid.
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| CN113789598A (en) * | 2021-08-13 | 2021-12-14 | 广东职业技术学院 | Antistatic easy-to-clean clothing material and preparation method thereof |
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Application publication date: 20190917 |