CN110075013A - A kind of makeup removing, face cleaning and the facial cleanser of antibacterial three-in-one and preparation method thereof - Google Patents
A kind of makeup removing, face cleaning and the facial cleanser of antibacterial three-in-one and preparation method thereof Download PDFInfo
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- CN110075013A CN110075013A CN201910450395.8A CN201910450395A CN110075013A CN 110075013 A CN110075013 A CN 110075013A CN 201910450395 A CN201910450395 A CN 201910450395A CN 110075013 A CN110075013 A CN 110075013A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
- A61K8/44—Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/46—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing sulfur
- A61K8/466—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing sulfur containing sulfonic acid derivatives; Salts
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/63—Steroids; Derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61P—SPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
- A61P17/00—Drugs for dermatological disorders
- A61P17/10—Anti-acne agents
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q1/00—Make-up preparations; Body powders; Preparations for removing make-up
- A61Q1/14—Preparations for removing make-up
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q17/00—Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
- A61Q17/005—Antimicrobial preparations
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/10—Washing or bathing preparations
Abstract
The present invention provides a kind of makeup removing, face cleaning and the facial cleanser of antibacterial three-in-one and preparation method thereof.The facial cleanser includes: sapindoside liquid, amino acid-based surfactant, cocoyl isethionate, crude vegetal, emulsifier and water.The facial cleanser the preparation method is as follows: first by crude vegetal, amino acid-based surfactant, cocoyl isethionate and emulsifier mix；Water and optionally moisturizer are added, is mixed；It is eventually adding sapindoside liquid, optionally antioxidant and optionally preservative, mixes, obtains the facial cleanser.The present invention for the first time combines said components, and each component cooperates, synergistic, and obtained facial cleanser has effects that significantly makeup removing, face cleaning, while can also effectively promote bacteria resistance function.In addition, facial cleanser provided by the invention it is safe and non-toxic, it is low stimulation, it is degradable, environmentally friendly.
Description
Technical field
The present invention relates to daily personal care fields, and in particular to a kind of makeup removing, face cleaning and antibacterial three-in-one facial cleanser and
Preparation method.
Background technique
In recent years, as rhythm of life is constantly accelerated, people increasingly focus on self-image management, and cosmetics are played the part of wherein
The role drilled becomes more and more important.However, the minerals in cosmetics, the dirts such as grease are easy residual, and a series of skin is caused to be asked
Topic, such as long acne, long spot, serious person even will appear the exanthemv of large area.Makeup removal products currently on the market predominantly unload
Adornment oil, makeup remover etc., are two kinds of products of different functionalities with spatter property facial cleanser, consumer need first using makeup remover or
Makeup remover is removed ornaments and formal dress, and is then reused facial cleanser and is carried out face's cleaning, this adds increased consumer's answering in use
Polygamy.
Acne is commonly called as whelk, acne etc., is a kind of chronic inflammatory skin, in puberty and adult-onset rate
Up to 85%.The reason of acne occurs is more complicated, not only related with human body oneself factor, also related to external condition.It is modern
Medicine is it is believed that the external cause for causing acne to generate is broadly divided at following 4 points: first, the mistake of hair follicle and sebaceous gland duct epithelium
Spend angling；Second, the field planting of microorganism；Third, sebaceous glands excessive secretion；Fourth, inflammatory reaction.The wherein field planting of microorganism,
It is primarily referred to as the intrusion of propionibacterium acnes, sebum is resolved into free fatty acid, hair follicle and its surrounding is further promoted to generate
Inflammatory reaction, so as to cause the generation of acne.The appearance that acne has seriously affected people is beautiful, causes barrier of choosing a job, choose spouse and communicate
Hinder, be easy to cause melancholia, personality becomes unsociable and eccentric, feels oneself inferior, and influences mental health.And the antibacterial cleaning products in existing market,
It is usually used and adds drug or antibiotic into facial cleanser to kill propionibacterium acnes, alleviate and treat whelk, so
And be used for a long time, skin can be made to generate drug resistance, damage skin interior tissue, lead to bigger skin hidden danger.
CN108272724A disclose it is a kind of with makeup removing function without alveolitoid facial cleanser formula and preparation method thereof, for oil
The emulsifying formula of water mixing, including surfactant, water, grease and additive, the additive include to be concentrated by evaporation work
Skill prepares and accounts for the mixed extract of entire facial cleanser formula 10-15%；The mixed extract includes Abelmoschus Esculentus Linn extract, sea
At least two in Germinatus Phragmitis extract, cowberry leaf extract and aloe extract.Surfactant is stirred evenly first, then
The water of half and half surfactant are poured into stirring in emulsion tank and form substrate；Again grease is poured into stir in emulsion tank and be caused
It enables grease to dissolve, while the essence in additive and citric acid is added；Substrate is added in ready mixed extract again
The other half water is added thereto while being stirred by middle vacuum stirring.The invention has makeup removing function, by mixing a variety of plants
Object essence can keep the skin wet and improve oxidation resistance.But the invention procedure of processing is more, complex process, and does not have suppression
The effect of bacterium propionibacterium acnes.
Therefore, a kind of makeup removing is developed, the facial cleanser of face cleaning and antibacterial three-in-one already becomes the urgent of makeups market and is essential
It asks.
Summary of the invention
For overcome the deficiencies in the prior art, the object of the present invention is to provide a kind of makeup removing, face cleaning and antibacterial three-in-ones
Facial cleanser and preparation method thereof.The present invention passes through the cooperation of sapindoside liquid and other components, and the facial cleanser made is not
Only have effects that good makeup removing and face cleaning, and bacteriostasis property with higher.Meanwhile facial cleanser safety of the present invention
It is nontoxic, low to stimulate, is degradable, environmentally friendly.
To achieve this purpose, the present invention adopts the following technical scheme:
In a first aspect, the present invention provides the facial cleanser of a kind of makeup removing, face cleaning and antibacterial three-in-one, the facial cleanser includes
Sapindoside liquid, amino acid-based surfactant, cocoyl isethionate, crude vegetal, emulsifier and water.
Soapberry, also known as fruit of washing one's hands, You Luoshu, root, skin, leaf, pericarp, seed etc. all have very strong medical value,
It is rare natural resources.Saponin(e, protein, fat, a variety of amino acid, organic acid and phenol rich in its pericarp
The substances such as acid, wherein the saponin(e is mainly pentacyclic triterpene oleanane type.The saponin(e is mainly by sapogenin and different length
The sugar chain of degree is constituted, and wherein sugar chain is mainly made of carboxyl and glucosyl group, has preferable hydrophily, and sapogenin then has one
Fixed lipophilicity, therefore sapindoside is a kind of natural nonionic surface active agent, has very strong reduction surface
The effect of power can be used for skin cleaning (take a shower, wash one's face, washing one's hands, having one's hair wash), remove skin surface dirt, free from extraneous odour, antibacterial beauty
Hold, brighten, nti-freckle, anti-acne, prevention and treatment skin disease, 100% degradation is mild non-stimulated, environmentally friendly.
Amino acid-based surfactant is a kind of mild, degradable anionic surfactant, weakly acidic, pH value
It is close with human skin, along with amino acid is the base substance for constituting protein, so being added in facial cleanser of the invention
It can achieve the effect of mild face cleaning, sensitive skin can also be safe to use.
Cocoyl isethionate have good biological degradability, cloud point is low, resistance to hard water is strong, foaming characteristic
The features such as concertedness good, small to skin irritation and with other surfactants is good.
Crude vegetal is made by the seed, pulp or plumule etc. of plant through squeezing method or solvent extraction method, in the present invention
Crude vegetal is added, can effectively clean color make-up and oil-soluble dirt using the similar principle to mix, while with co-emulsifier,
Play the role of significantly remove ornaments and formal dress, it is clean, mild pro-skin can make skin clearly penetrating.
Emulsifier can stablize soap base system, reduce the irritation of product, and can occur after restoring room temperature to avoid system
Coarse phenomenon.
The present invention is for the first time by sapindoside liquid, amino acid-based surfactant, cocoyl isethionate, natural
These substances of vegetable oil, emulsifier and water are combined together, and are interacted between component, synergistic, realize makeup removing and clean
While the effect of face, moreover it is possible to effectively promotion fungistatic effect.Meanwhile sapindoside liquid of the present invention, amino acid system table
Face activating agent, cocoyl isethionate and crude vegetal are all safe and non-toxic, and all have good biological degradability,
So that the mild pro-skin of the facial cleanser being prepared, it is low stimulation, it is environmentally friendly.
As the preferred technical solution of the present invention, the facial cleanser includes the component of following parts by weight: sapindoside
15-20 parts of liquid, 14-18 parts of amino acid-based surfactant, 3-4 parts of cocoyl isethionate, crude vegetal 10-17
Part, 7-10 parts of emulsifier and 18-20 parts of water.
Each component is synergistic by cooperating under above-mentioned special ratios, obtained facial cleanser have significant makeup removing,
While face cleaning effect, inhibits the effect of propionibacterium acnes growth to be obviously improved, act on the minimum of propionibacterium acnes
Mlc (MIC) can be down to 0.046-0.050mg/mL (in terms of saponin content).
15-20 parts of sapindoside liquid in the present invention, such as can be 15 parts, 16 parts, 17 parts, 18 parts, 19 parts or 20 parts
Deng.
14-18 parts of amino acid-based surfactant, such as can be 14 parts, 15 parts, 16 parts, 17 parts or 18 parts etc..
3-4 parts of cocoyl isethionate, such as can be 3 parts, 3.2 parts, 3.5 parts, 3.7 parts, 3.8 parts, 3.9 parts
Or 4 parts etc..
10-17 parts of crude vegetal, such as can be 10 parts, 11 parts, 12 parts, 13 parts, 14 parts, 15 parts, 16 parts or 17 parts
Deng.
7-10 parts of emulsifier, such as can be 7 parts, 8 parts, 9 parts or 10 parts etc..
18-20 parts of water, such as can be 18 parts, 18.3 parts, 18.5 parts, 18.7 parts, 18.8 parts, 19 parts, 19.1 parts, 19.3
Part, 19.4 parts, 19.8 parts or 20 parts etc..
Preferably, the solid content of the sapindoside liquid is 25-40%, for example, can be 25%, 28%,
30%, 31%, 33%, 35%, 36%, 38% or 40% etc..
Preferably, the amino acid-based surfactant is selected from sodium lauroyl sarcosine, sodium cocoyl glycinate or laurel
In acyl sodium glutamate any one or at least two combination；The combination is typical but non-limiting example has: lauroyl flesh
Propylhomoserin sodium and sodium cocoyl glycinate, sodium lauroyl sarcosine and sodium lauroyl glutamate, sodium cocoyl glycinate and lauroyl
Sodium glutamate etc..
Preferably, the cocoyl isethionate is sodium cocoyl isethionate.
Preferably, the crude vegetal selected from olive oil, tea-seed oil, soybean oil, sunflower oil, wheat-germ oil or in
Any one or at least two combination, preferably olive oil, tea-seed oil or soybean oil；The combination typical case but non-limiting reality
Example has: olive oil and tea-seed oil, olive oil and soybean oil, tea-seed oil and soybean oil, sunflower oil and wheat-germ oil, olive oil and
Wheat-germ oil etc..
Preferably, the emulsifier is in glycol distearate, polyxyethylated sodium sulphate or alkyl glycosides
Any one or at least two combination；The combination is typical but non-limiting example has: glycol distearate and poly-
Ethylene oxide sodium alkyl sulfate, polyxyethylated sodium sulphate and alkyl glycosides, alkyl glycosides and glycol distearate etc..
Preferably, the facial cleanser further includes moisturizer.
Preferably, the parts by weight of the moisturizer be 9-12 parts, such as can be 9 parts, 9.3 parts, 9.5 parts, 9.8 parts,
10 parts, 10.3 parts, 10.5 parts, 10.7 parts, 11 parts, 11.4 parts, 11.8 parts or 12 parts etc..
Preferably, the moisturizer is glycerol and/or propylene glycol.
Preferably, the facial cleanser further includes antioxidant.
Preferably, the parts by weight of the antioxidant be 1-2 parts, such as can be 1 part, 1.1 parts, 1.2 parts, 1.4 parts,
1.5 parts, 1.6 parts, 1.7 parts, 1.8 parts, 1.9 parts or 2 parts etc..
Preferably, the antioxidant is Q10 coenzyme.
Preferably, the facial cleanser further includes preservative.
Preferably, the weight fraction of the preservative is 0.01-0.05 parts, such as can be 0.01 part, 0.02 part, 0.03
Part, 0.04 part or 0.05 part etc..
Preferably, the preservative is food-grade potassium sorbate.
Preferably, the facial cleanser includes the component of following parts by weight: 15-20 parts of sapindoside liquid, amino acid system
It is 14-18 parts of surfactant, 3-4 parts of sodium cocoyl isethionate, 10-17 parts of crude vegetal, 7-10 parts of emulsifier, sweet
6-8 parts oily, 3-4 parts of propylene glycol, -2 parts of Q10 DPN diphosphopyridine nucleotide, 0.01-0.05 parts of preservative and 18-20 parts of distilled water.
Glycerol 6-8 parts in the present invention, such as it can be 6 parts, 6.5 parts, 7 parts, 7.2 parts, 7.5 parts, 7.8 parts or 8 parts etc..
3-4 parts of propylene glycol, such as can be 3 parts, 3.2 parts, 3.5 parts, 3.7 parts, 3.8 parts, 3.9 parts or 4 parts etc..
- 2 parts of Q10 DPN diphosphopyridine nucleotide, for example, can be 1 part, 1.1 parts, 1.2 parts, 1.4 parts, 1.5 parts, 1.6 parts, 1.7 parts, 1.8 parts,
1.9 parts or 2 parts etc..
Second aspect, the present invention also provides a kind of makeup removing as described in relation to the first aspect, face cleaning and antibacterial three-in-ones
The preparation method of facial cleanser, the preparation method comprises the following steps:
(1) crude vegetal, amino acid-based surfactant, cocoyl isethionate and emulsifier are mixed,
Obtain the first mixed liquor；
(2) by water and optionally, moisturizer is added in the first mixed liquor that step (1) obtains, and mixing obtains the second mixing
Liquid；
(3) sapindoside liquid, optionally antioxidant and optionally are added in the second mixed liquor obtained to step (2)
Preservative is mixed, and the facial cleanser is obtained.
Preferably, mixing described in the preparation method step (1) and step (2) is carried out at 55-75 DEG C, such as can
To be 55 DEG C, 58 DEG C, 60 DEG C, 63 DEG C, 65 DEG C, 68 DEG C, 70 DEG C, 73 DEG C or 75 DEG C etc..
Preferably, step (3) further include: before the mixing, the second mixed liquor that step (2) obtains is cooled to
15-45 DEG C, such as can be 15 DEG C, 18 DEG C, 19 DEG C, 20 DEG C, 23 DEG C, 25 DEG C, 26 DEG C, 29 DEG C, 30 DEG C, 33 DEG C, 35 DEG C, 38
DEG C, 40 DEG C, 41 DEG C, 43 DEG C or 45 DEG C etc..
Preferably, the preparation method comprises the following steps:
(1) oil is added in crude vegetal, amino acid-based surfactant, sodium cocoyl isethionate and emulsifier
In phase pot, it is heated to 70 DEG C while stirring, obtains the first mixed liquor；
(2) it by glycerol, propylene glycol and distilled water addition step (1) obtained first mixed liquor, is stirred, obtains the
Two mixed liquors；
(3) after the second mixed liquor that step (2) obtains being cooled to 45 DEG C, sapindoside liquid, Q10 coenzyme is added and prevents
Rotten agent is mixed, and the facial cleanser is obtained.
Preparation method provided by the present invention can guarantee that all materials uniformly mix in the facial cleanser, to be formed steady
Determine continuous uniform mixture, comes into full contact with, interact between each component, it is synergistic, so that the facial cleanser is being reinforced
While makeup removing and face cleaning effect, the effect for inhibiting propionibacterium acnes growth can be further promoted.
Compared with prior art, the beneficial effects of the present invention are:
1, the present invention is for the first time by sapindoside liquid, amino acid-based surfactant, cocoyl isethionate, day
Right vegetable oil, emulsifier and water these substances are combined, and are cooperated between each component, synergistic, what is made washes
While face milk has effects that significantly makeup removing, face cleaning, moreover it is possible to which effectively promotion bacteria resistance function acts on propionibacterium acnes
MIC can be down to 0.046-0.050mg/mL (in terms of saponin content).
2, facial cleanser provided by the invention is nontoxic, pollution-free, degradable, environmentally friendly.
3, preparation method of the present invention can guarantee that all materials uniformly mix in the facial cleanser, to be formed
Steady and continuous uniform mixture comes into full contact between each component, realizes makeup removing, face cleaning and antibacterial three-in-one, function is more
It is perfect, it is provided convenience for consumer.
Specific embodiment
The technical scheme of the invention is further explained by means of specific implementation.Those skilled in the art should be bright
, the described embodiments are merely helpful in understanding the present invention, should not be regarded as a specific limitation of the invention.
Embodiment 1
Present embodiments provide a kind of makeup removing, face cleaning and the facial cleanser of antibacterial three-in-one and preparation method thereof
Wherein, facial cleanser includes the component of following parts by weight: 15 parts of sapindoside liquid, sodium lauroyl sarcosine 14
Part, 3 parts of sodium cocoyl isethionate, 16 parts of olive oil, 7 parts of glycol distearate, 6 parts of glycerol, 3 parts of propylene glycol,
2 parts of Q10 coenzyme, 0.01 part of food-grade potassium sorbate, 18 parts of distilled water.
The present embodiment facial cleanser the preparation method is as follows:
(1) olive oil, sodium lauroyl sarcosine salt, sodium cocoyl isethionate and glycol distearate are added
Enter into oily phase pot, be heated to 70 DEG C while stirring, obtains the first mixed liquor；
(2) glycerol, propylene glycol and distilled water are slowly added in the first mixed liquor that step (1) obtains under stiring, are stirred
It mixes uniformly, obtains the second mixed liquor；
(3) after the second mixed liquor that step (2) obtains being cooled to 40 DEG C, sapindoside liquid, Q10 coenzyme and food is added
Grade potassium sorbate, after evenly dispersed, cooling takes the dish out of the pot, and obtains the facial cleanser.
Embodiment 2
Present embodiments provide a kind of makeup removing, face cleaning and the facial cleanser of antibacterial three-in-one and preparation method thereof
Wherein, facial cleanser includes the component of following parts by weight: 20 parts of sapindoside liquid, sodium cocoyl glycinate 18
Part, 4 parts of sodium cocoyl isethionate, 17 parts of tea-seed oil, 10 parts of polyxyethylated sodium sulphate, 8 parts of glycerol, propylene glycol 4
Part, 2 parts of Q10 coenzyme, 0.02 part of food-grade potassium sorbate, 20 parts of distilled water.
The present embodiment facial cleanser the preparation method is as follows:
(1) tea-seed oil, sodium cocoyl glycinate, sodium cocoyl isethionate and polyxyethylated sodium sulphate are added
Enter into oily phase pot, be heated to 65 DEG C while stirring, obtains the first mixed liquor；
(2) glycerol, propylene glycol and distilled water are slowly added in the first mixed liquor that step (1) obtains under stiring, are stirred
It mixes uniformly, obtains the second mixed liquor；
(3) after the second mixed liquor that step (2) obtains being cooled to 35 DEG C, sapindoside liquid, Q10 coenzyme and food is added
Grade potassium sorbate, after evenly dispersed, cooling takes the dish out of the pot, and obtains the facial cleanser.
Embodiment 3
Present embodiments provide a kind of makeup removing, face cleaning and the facial cleanser of antibacterial three-in-one and preparation method thereof
Wherein, facial cleanser includes the component of following parts by weight: 15 parts of sapindoside liquid, sodium lauroyl glutamate 18
Part, 3.5 parts of sodium cocoyl isethionate, 16 parts of soybean oil, 10 parts of alkyl glycosides, 8 parts of glycerol, 4 parts of propylene glycol, Q10 are auxiliary
1.5 parts of enzyme, 0.03 part of food-grade potassium sorbate, 20 parts of distilled water.
The present embodiment facial cleanser the preparation method is as follows:
(1) soybean oil, sodium lauroyl glutamate, sodium cocoyl isethionate and alkyl glycosides are added to oily phase pot
It is interior, it is heated to 60 DEG C while stirring, obtains the first mixed liquor；
(2) glycerol, propylene glycol and distilled water are slowly added in the first mixed liquor that step (1) obtains under stiring, are stirred
It mixes uniformly, obtains the second mixed liquor；
(3) after the second mixed liquor that step (2) obtains being cooled to 30 DEG C, sapindoside liquid, Q10 coenzyme and food is added
Grade potassium sorbate, after evenly dispersed, cooling takes the dish out of the pot, and obtains the facial cleanser.
Embodiment 4
Present embodiments provide a kind of makeup removing, face cleaning and the facial cleanser of antibacterial three-in-one and preparation method thereof
Wherein, facial cleanser includes the component of following parts by weight: 16 parts of sapindoside liquid, sodium lauroyl sarcosine 14
Part, 3 parts of sodium cocoyl isethionate, 15 parts of sunflower oil, 8 parts of glycol distearate, 6 parts of glycerol, 3 parts of propylene glycol,
Q10 DPN diphosphopyridine nucleotide part, 0.04 part of food-grade potassium sorbate, 18 parts of distilled water.
The present embodiment facial cleanser the preparation method is as follows:
(1) sunflower oil, sodium lauroyl sarcosine, sodium cocoyl isethionate and glycol distearate are added
Into oily phase pot, it is heated to 70 DEG C while stirring, obtains the first mixed liquor；
(2) glycerol, propylene glycol and distilled water are slowly added in the first mixed liquor that step (1) obtains under stiring, are stirred
It mixes uniformly, obtains the second mixed liquor；
(3) after the second mixed liquor that step (2) obtains being cooled to 40 DEG C, sapindoside liquid, Q10 coenzyme and food is added
Grade potassium sorbate, after evenly dispersed, cooling takes the dish out of the pot, and obtains the facial cleanser.
Embodiment 5
Present embodiments provide a kind of makeup removing, face cleaning and the facial cleanser of antibacterial three-in-one and preparation method thereof
Wherein, facial cleanser includes the component of following parts by weight: 18 parts of sapindoside liquid, sodium lauroyl sarcosine 17
Part, 3 parts of sodium cocoyl isethionate, 15 parts of wheat-germ oil, 8 parts of glycol distearate, 4 parts of glycerol, propylene glycol 4
Part, Q10 DPN diphosphopyridine nucleotide part, 0.05 part of food-grade potassium sorbate, 18 parts of distilled water.
The present embodiment facial cleanser the preparation method is as follows:
(1) by wheat-germ oil, sodium lauroyl sarcosine, sodium cocoyl isethionate and glycol distearate
It is added in oily phase pot, is heated to 55 DEG C while stirring, obtain the first mixed liquor；
(2) glycerol, propylene glycol and distilled water are slowly added in the first mixed liquor that step (1) obtains under stiring, are stirred
It mixes uniformly, obtains the second mixed liquor；
(3) after the second mixed liquor that step (2) obtains being cooled to 30 DEG C, sapindoside liquid, Q10 coenzyme and food is added
Grade potassium sorbate, after evenly dispersed, cooling takes the dish out of the pot, and obtains the facial cleanser.
Embodiment 6
Present embodiments provide a kind of makeup removing, face cleaning and the facial cleanser of antibacterial three-in-one and preparation method thereof
Wherein, facial cleanser includes the component of following parts by weight: 15 parts of sapindoside liquid, sodium lauroyl sarcosine 14
Part, 3 parts of sodium cocoyl isethionate, 10 parts of sunflower oil, 8 parts of glycol distearate, 18 parts of distilled water.
The present embodiment facial cleanser the preparation method is as follows:
(1) sunflower oil, sodium lauroyl sarcosine, sodium cocoyl isethionate and glycol distearate are added
Into oily phase pot, it is heated to 70 DEG C while stirring, obtains the first mixed liquor；
(2) distilled water is slowly added in the first mixed liquor that step (1) obtains under stiring, is stirred evenly, obtain
Two mixed liquors；
(3) after the second mixed liquor that step (2) obtains being cooled to 40 DEG C, sapindoside liquid is added, to evenly dispersed
Afterwards, cooling takes the dish out of the pot, and obtains the facial cleanser.
Embodiment 7
A kind of makeup removing, face cleaning and the facial cleanser of antibacterial three-in-one and preparation method thereof are present embodiments provided, with implementation
The difference of example 4 is only that the weight fraction of sapindoside liquid is 6 parts.
Embodiment 8
A kind of makeup removing, face cleaning and the facial cleanser of antibacterial three-in-one and preparation method thereof are present embodiments provided, with implementation
The difference of example 4 is only that the weight fraction of sapindoside liquid is 8 parts.
Embodiment 9
A kind of makeup removing, face cleaning and the facial cleanser of antibacterial three-in-one and preparation method thereof are present embodiments provided, with implementation
The difference of example 4 is only that the weight fraction of sapindoside liquid is 10 parts.
Embodiment 10
A kind of makeup removing, face cleaning and the facial cleanser of antibacterial three-in-one and preparation method thereof are present embodiments provided, with implementation
The difference of example 4 is only that the weight fraction of sapindoside liquid is 12 parts.
Embodiment 11
A kind of makeup removing, face cleaning and the facial cleanser of antibacterial three-in-one and preparation method thereof are present embodiments provided, with implementation
The difference of example 4 is only that the weight fraction of sapindoside liquid is 22 parts.
Embodiment 12
A kind of makeup removing, face cleaning and the facial cleanser of antibacterial three-in-one and preparation method thereof are present embodiments provided, with implementation
The difference of example 4 is only that the weight fraction of sapindoside liquid is 24 parts.
Embodiment 13
A kind of makeup removing, face cleaning and the facial cleanser of antibacterial three-in-one and preparation method thereof are present embodiments provided, with implementation
The difference of example 4 is only that the weight fraction of sapindoside liquid is 26 parts.
Embodiment 14
A kind of makeup removing, face cleaning and the facial cleanser of antibacterial three-in-one and preparation method thereof are present embodiments provided, with implementation
The difference of example 4 is only that the weight fraction of sapindoside liquid is 30 parts.
Comparative example 1
A kind of makeup removing, face cleaning and the facial cleanser of antibacterial three-in-one and preparation method thereof are present embodiments provided, with implementation
The difference of example 4 is only that, is not added with sapindoside liquid.
As follows, 1-14 of the embodiment of the present invention and comparative example 1 facial cleanser provided are tested for the property:
1. safety experiment
With reference to the safety evaluation of cosmetics program in GB 7919-1987 " safety evaluation of cosmetics program and method ",
Carry out acute dermal toxicity test and skin irritation test.
Acute dermal toxicity test: the rabbit (2kg) of two kinds of genders is randomly divided into 4 groups, every group 10, is smeared respectively
The facial cleanser of 500mg/kg, 1000mg/kg, 1500mg/kg and 2000mg/kg saponin content in four groups of family's rabbit backs, and with oil
Paper and two layers of gauze cover, then are fixed with nonirritant adhesive plaster, with anti-dropout, and apply and smear for 24 hours.After the test, it uses
Warm water removes residual facial cleanser, observes one week, record observation result.
Skin irritation test: preparing 4 rabbit (2kg), family's rabbit back backbone diamond wool cut, epidermis can not be injured,
The each about 3cm × 6cm of left and right sides unhairing range.It takes 0.1mL facial cleanser drop on four layers of gauze of 2.5cm × 2.5cm size, applies
It is attached on the skin of side, is covered with one layer of oilpaper, then fixed with non-stimulated adhesive tape.Other side skin is as control.Application is for 24 hours
Afterwards, residual facial cleanser is removed with warm water, whether there is or not allergic phenomenas for observation.
2, the measurement of saponin content
Content of oleanolic acid and absorbance standard curve make: dissolving oleanolic acid with methanol, be configured to the molten of 1mg/mL
Liquid, takes 18 20mL colorimetric cylinders, number 1-6, be arranged each three groups of number it is parallel, 1-6 test tube takes 0 respectively, 200,400,
600,800 and 1000 μ L oleanolic acid standard solution, water-bath volatilize.0.4mL 5wt% vanillic aldehyde-ice is added to each colorimetric cylinder
Acetum and 1.4mL perchloric acid solution are color developing agent, are shaken up, the cooling 3min in 70 DEG C of heating water bath 20min, ice-water bath,
Adding 10mL glacial acetic acid is solvent, is shaken up, and with spectrophotometer in 400-600nm scanning optical spectrum, and surveys absorbance in 550nm
OD value.Standard curve is made, the accounting equation of content of oleanolic acid y (μ g), y (μ g)=0.0006 × OD+0.0838, R are obtained2
=0.9996.
The measurement of sapindoside content: sapindoside extracting solution is diluted 50 times, takes 100 μ L dilutions in 20mL ratio
In colour tube, the dilution is then measured into absorbance according to the method described above, calculated content of oleanolic acid y (μ g), sample repeats to survey
Determine three times.Measurement result arithmetic mean of instantaneous value will be calculated three times, and substitute into the content that following equation calculation goes out sapindoside.
The accounting equation of sapindoside content and content of oleanolic acid: the content of saponin(e=y (μ g) × 2.3.
Using the above method, the solid content for measuring sapindoside liquid is 29.09%.
3, sapindoside MIC is measured
15 sterilizing test tubes are formed a line, 1-15 is numbered respectively, double nutrition is respectively added into each test tube
Nutrient agar 1.0mL, is added 1.0mL sapindoside liquid in the first pipe, and 1.0mL to the 2nd is drawn after mixing and is managed, is mixed
It is even take again 1.0mL to the 3rd manage, and so on to the 14th pipe, discard 1.0mL, sapindoside liquid is not added in the 15th pipe.To culture medium
After solidification, it is 10 that bacterial concentration, which is added, in every pipe6The 20.0 μ L of bacterium solution of CFU mixes, is placed in 37 DEG C of anaerobic culture box stationary cultures
24h。
With physiological saline as blank control, positive control of the ampicillin solution as bacterium, Natamycin conduct
Positive control.
Result judgement: sterile MIC of the long highest dilution as sapindoside that be born of media surface.
Adopting and obtaining the MIC value of sapindoside liquid with the aforedescribed process is 0.25mg/mL (in terms of saponin content).
4, facial cleanser MIC is measured
15 sterilizing test tubes are formed a line, 1-15 is numbered respectively, double nutrition is respectively added into each test tube
Nutrient agar 1.0mL, is added 1.0mL facial cleanser in the first pipe, and 1.0mL to the 2nd is drawn after mixing and is managed, mixing takes again
1.0mL to the 3rd manage, and so on to the 14th pipe, discard 1.0mL, facial cleanser is not added in the 15th pipe.After culture medium solidification, every pipe
It is 10 that bacterial concentration, which is added,6The 20.0 μ L of bacterium solution of CFU mixes, is placed in 37 DEG C of anaerobic culture box stationary cultures for 24 hours.
With physiological saline as blank control, positive control of the ampicillin solution as bacterium, Natamycin conduct
Positive control.
Result judgement: sterile MIC of the long highest dilution as facial cleanser that be born of media surface.
5, makeup removing and face cleaning effect assessment
Makeup removing effect evaluation: with 20 people (by 10 with the specialty background boy student and 10 schoolgirls of related training) group
At the group of judge, respectively with facial cleanser makeup removing effect degree, with good (indicating that makeup removing ability is strong, unload completely), general (expression
With makeup removing ability, but unload to be not thorough), poor (indicate makeup removing ability poor) be Comment gathers, consider the evaluation knot of all testers
Fruit, the comprehensive evaluation result obtained.
Face cleaning effect assessment: with 20 people (by 10 with the specialty background boy student and 10 schoolgirls of related training) group
At the group of judge, respectively with facial cleanser face cleaning effect degree, with good (indicating that face cleaning ability is strong, wash completely), general (expression
With face cleaning ability, but wash to be not thorough), poor (indicate face cleaning ability poor) be Comment gathers, consider the evaluation knot of all testers
Fruit, the comprehensive evaluation result obtained.The result of above-mentioned performance test is as shown in table 1 below:
Safety, makeup removing, face cleaning and the fungistatic effect evaluation of 1 embodiment 1-14 of table and 1 facial cleanser of comparative example
It can be seen that from embodiment 1-6 and all had according to the facial cleanser that formula of the present invention and preparation method obtain
The effect of excellent inhibition propionibacterium acnes, the minimum reachable 0.046mg/mL of MIC (in terms of saponin content).From table 1 also
As can be seen that the MIC of embodiment 1-14 is significantly lower than the MIC of sapindoside liquid one-component, this is also indicated that in facial cleanser
Sapindoside and other components between interacted, coordinated, improve inhibit propionibacterium acnes growth
The effect of.
The makeup removing of embodiment 1-5 and face cleaning effect are excellent in, this shows that sapindoside exists with other components and cooperates with
Effect, can not only promote bacteriostasis property, moreover it is possible to reinforce the effect of its makeup removing and face cleaning.The face cleaning effect assessment of embodiment 6 be it is poor,
This is because being free of moisturizer in the formula system of embodiment 6, the facial skin after leading to cleaning is tight, dry and astringent, face cleaning experience
Difference, but its cleaning effect is unaffected.
Embodiment 7-10 only reduces the ratio of sapindoside liquid compared with Example 4, from table 1 it follows that implementing
For the MIC of example 7-10 obviously higher than the MIC of embodiment 4, this also illustrates that there are phase interactions between sapindoside and other components
With coordinated improves the inhibitory effect to propionibacterium acnes.In addition, the makeup removing of embodiment 7-10 and face cleaning effect are commented
Valence be it is general or even poor, this is because reducing the content of sapindoside liquid in formula, lead to sapindoside liquid and other
The synergistic effect of component weakens, and weakens the effect of its makeup removing and face cleaning, however the effect of its makeup removing and face cleaning is still better than comparison
Example 1.
Embodiment 11-13 improves only the ratio of sapindoside liquid compared with Example 4, from table 1 it follows that real
The MIC for applying a 11-13 remains at 0.046mg/mL, this shows to further increase containing for sapindoside liquid in formula system
Amount, fungistatic effect will not be promoted again.
Compared with Example 4, difference is only that is not added with sapindoside liquid to comparative example 1.The MIC of comparative example 1 is
0.50mg/mL, higher than any one MIC of embodiment 1-14, this shows to add sapindoside liquid in formula system can be obvious
MIC is reduced, the inhibiting effect to propionibacterium acnes is promoted.In addition, the makeup removing of comparative example 1 and face cleaning effect are evaluated as difference,
This also illustrates that the addition of sapindoside liquid can not only promote the bacteriostasis property of facial cleanser, moreover it is possible to reinforce the effect of makeup removing and face cleaning
Fruit.
The Applicant declares that the foregoing is merely a specific embodiment of the invention, but protection scope of the present invention not office
It is limited to this, it should be clear to those skilled in the art, any to belong to those skilled in the art and take off in the present invention
In the technical scope of dew, any changes or substitutions that can be easily thought of, and all of which fall within the scope of protection and disclosure of the present invention.
Claims (10)
1. the facial cleanser of a kind of makeup removing, face cleaning and antibacterial three-in-one, which is characterized in that the facial cleanser includes sapindoside
Liquid, amino acid-based surfactant, cocoyl isethionate, crude vegetal, emulsifier and water.
2. facial cleanser according to claim 1, which is characterized in that the facial cleanser includes the component of following parts by weight:
It is 15-20 parts of sapindoside liquid, 14-18 parts of amino acid-based surfactant, 3-4 parts of cocoyl isethionate, natural
10-17 parts of vegetable oil, 7-10 parts of emulsifier and 18-20 parts of water.
3. facial cleanser according to claim 1 or 2, which is characterized in that the solid content of the sapindoside liquid is
25-40%；
Preferably, the amino acid-based surfactant is selected from sodium lauroyl sarcosine, sodium cocoyl glycinate or lauroyl paddy
One of propylhomoserin sodium or at least two combination；
Preferably, the cocoyl isethionate is sodium cocoyl isethionate；
Preferably, the crude vegetal is any in sunflower oil, wheat-germ oil, soybean oil, tea-seed oil or olive oil
It is a kind of or at least two combination, further preferably olive oil, soybean oil or tea-seed oil；
Preferably, the emulsifier appointing in glycol distearate, polyxyethylated sodium sulphate or alkyl glycosides
It anticipates a kind of or at least two combinations.
4. facial cleanser according to claim 1-3, which is characterized in that the facial cleanser further includes moisturizer；
Preferably, the parts by weight of the moisturizer are 9-12 parts；
Preferably, the moisturizer is glycerol and/or propylene glycol.
5. facial cleanser according to claim 1-4, which is characterized in that the facial cleanser further includes antioxidant；
Preferably, the parts by weight of the antioxidant are 1-2 parts；
Preferably, the antioxidant is Q10 coenzyme.
6. facial cleanser according to claim 1-5, which is characterized in that the facial cleanser further includes preservative；
Preferably, the weight fraction of the preservative is 0.01-0.05 parts；
Preferably, the preservative is food-grade potassium sorbate.
7. facial cleanser according to claim 1-6, which is characterized in that the facial cleanser includes following parts by weight
Component: 15-20 parts of sapindoside liquid, 14-18 parts of amino acid-based surfactant, sodium cocoyl isethionate 3-4
Part, 10-17 parts of crude vegetal, 7-10 parts of emulsifier, 6-8 parts of glycerol, 3-4 parts of propylene glycol, -2 parts of Q10 DPN diphosphopyridine nucleotide, preservative
0.01-0.05 parts and distilled water 18-20 parts.
8. a kind of makeup removing according to claim 1-7, face cleaning and antibacterial three-in-one facial cleanser preparation side
Method, which is characterized in that the preparation method comprises the following steps:
(1) crude vegetal, amino acid-based surfactant, cocoyl isethionate and emulsifier are mixed, is obtained
First mixed liquor；
(2) by water and optionally, moisturizer is added in the first mixed liquor that step (1) obtains, and mixing obtains the second mixed liquor；
(3) sapindoside liquid, optionally antioxidant and optionally anti-corrosion are added in the second mixed liquor obtained to step (2)
Agent is mixed, and the facial cleanser is obtained.
9. preparation method according to claim 8, which is characterized in that described in step (1) and step (2) mixing be
It is carried out at 55-75 DEG C；
Preferably, step (3) further include: before the mixing, the second mixed liquor that step (2) obtains is cooled to 15-45
℃。
10. preparation method according to claim 8 or claim 9, which is characterized in that the preparation method comprises the following steps:
(1) oily phase pot is added in crude vegetal, amino acid-based surfactant, sodium cocoyl isethionate and emulsifier
In, it is heated to 70 DEG C while stirring, obtains the first mixed liquor；
(2) it in the first mixed liquor for obtaining glycerol, propylene glycol and distilled water addition step (1), is stirred, it is mixed to obtain second
Close liquid；
(3) after the second mixed liquor that step (2) obtains being cooled to 45 DEG C, sapindoside liquid, Q10 coenzyme and preservative is added
It is mixed, obtains the facial cleanser.
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