CN109971532A - 高润滑、高脱模性钛合金锻造专用水性热锻加工油 - Google Patents
高润滑、高脱模性钛合金锻造专用水性热锻加工油 Download PDFInfo
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- 238000005242 forging Methods 0.000 title claims abstract description 25
- 229910001069 Ti alloy Inorganic materials 0.000 title claims abstract description 22
- 238000005461 lubrication Methods 0.000 title claims abstract description 12
- KKEYFWRCBNTPAC-UHFFFAOYSA-N Terephthalic acid Chemical compound OC(=O)C1=CC=C(C(O)=O)C=C1 KKEYFWRCBNTPAC-UHFFFAOYSA-N 0.000 claims abstract description 28
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 claims abstract description 24
- LYCAIKOWRPUZTN-UHFFFAOYSA-N ethylene glycol Natural products OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 claims abstract description 16
- 229920001577 copolymer Polymers 0.000 claims abstract description 15
- 239000000839 emulsion Substances 0.000 claims abstract description 15
- 229910052582 BN Inorganic materials 0.000 claims abstract description 8
- PZNSFCLAULLKQX-UHFFFAOYSA-N Boron nitride Chemical compound N#B PZNSFCLAULLKQX-UHFFFAOYSA-N 0.000 claims abstract description 8
- 229940077388 benzenesulfonate Drugs 0.000 claims abstract description 8
- ZPWVASYFFYYZEW-UHFFFAOYSA-L dipotassium hydrogen phosphate Chemical compound [K+].[K+].OP([O-])([O-])=O ZPWVASYFFYYZEW-UHFFFAOYSA-L 0.000 claims abstract description 8
- 229910000396 dipotassium phosphate Inorganic materials 0.000 claims abstract description 8
- 235000019797 dipotassium phosphate Nutrition 0.000 claims abstract description 8
- 229910052708 sodium Inorganic materials 0.000 claims abstract description 8
- 239000011734 sodium Substances 0.000 claims abstract description 8
- -1 sodium alkyl benzene Chemical class 0.000 claims abstract description 8
- BXQNSPXDWSNUKE-UHFFFAOYSA-N 1,3-benzothiazole 1-oxide Chemical compound C1=CC=C2S(=O)C=NC2=C1 BXQNSPXDWSNUKE-UHFFFAOYSA-N 0.000 claims abstract description 7
- 239000004205 dimethyl polysiloxane Substances 0.000 claims abstract description 7
- 235000013870 dimethyl polysiloxane Nutrition 0.000 claims abstract description 7
- YDEXUEFDPVHGHE-GGMCWBHBSA-L disodium;(2r)-3-(2-hydroxy-3-methoxyphenyl)-2-[2-methoxy-4-(3-sulfonatopropyl)phenoxy]propane-1-sulfonate Chemical compound [Na+].[Na+].COC1=CC=CC(C[C@H](CS([O-])(=O)=O)OC=2C(=CC(CCCS([O-])(=O)=O)=CC=2)OC)=C1O YDEXUEFDPVHGHE-GGMCWBHBSA-L 0.000 claims abstract description 7
- 239000012530 fluid Substances 0.000 claims abstract description 7
- 229920000435 poly(dimethylsiloxane) Polymers 0.000 claims abstract description 7
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 7
- 239000004615 ingredient Substances 0.000 claims description 3
- 239000003921 oil Substances 0.000 description 9
- 239000000126 substance Substances 0.000 description 6
- RTAQQCXQSZGOHL-UHFFFAOYSA-N Titanium Chemical compound [Ti] RTAQQCXQSZGOHL-UHFFFAOYSA-N 0.000 description 5
- 239000010936 titanium Substances 0.000 description 5
- 229910052719 titanium Inorganic materials 0.000 description 5
- 238000005260 corrosion Methods 0.000 description 3
- 230000000694 effects Effects 0.000 description 3
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 description 2
- VQTUBCCKSQIDNK-UHFFFAOYSA-N Isobutene Chemical compound CC(C)=C VQTUBCCKSQIDNK-UHFFFAOYSA-N 0.000 description 2
- 239000000956 alloy Substances 0.000 description 2
- 230000007797 corrosion Effects 0.000 description 2
- 238000005516 engineering process Methods 0.000 description 2
- 229910052739 hydrogen Inorganic materials 0.000 description 2
- 229910052760 oxygen Inorganic materials 0.000 description 2
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 description 1
- OAICVXFJPJFONN-UHFFFAOYSA-N Phosphorus Chemical compound [P] OAICVXFJPJFONN-UHFFFAOYSA-N 0.000 description 1
- 206010043458 Thirst Diseases 0.000 description 1
- ATJFFYVFTNAWJD-UHFFFAOYSA-N Tin Chemical compound [Sn] ATJFFYVFTNAWJD-UHFFFAOYSA-N 0.000 description 1
- 231100000921 acute inhalation toxicity Toxicity 0.000 description 1
- 231100000460 acute oral toxicity Toxicity 0.000 description 1
- 229910045601 alloy Inorganic materials 0.000 description 1
- 229910021529 ammonia Inorganic materials 0.000 description 1
- 150000004945 aromatic hydrocarbons Chemical class 0.000 description 1
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 1
- 229910002092 carbon dioxide Inorganic materials 0.000 description 1
- 229910002091 carbon monoxide Inorganic materials 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
- 238000013329 compounding Methods 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 230000006870 function Effects 0.000 description 1
- 239000007789 gas Substances 0.000 description 1
- 229910001385 heavy metal Inorganic materials 0.000 description 1
- 239000001257 hydrogen Substances 0.000 description 1
- 239000000314 lubricant Substances 0.000 description 1
- 238000003754 machining Methods 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 229910052751 metal Inorganic materials 0.000 description 1
- 239000002184 metal Substances 0.000 description 1
- 238000000034 method Methods 0.000 description 1
- 230000008450 motivation Effects 0.000 description 1
- 229910052757 nitrogen Inorganic materials 0.000 description 1
- 239000001301 oxygen Substances 0.000 description 1
- 229910052698 phosphorus Inorganic materials 0.000 description 1
- 239000011574 phosphorus Substances 0.000 description 1
- 231100000614 poison Toxicity 0.000 description 1
- 230000007096 poisonous effect Effects 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
- 238000011160 research Methods 0.000 description 1
- 210000001533 respiratory mucosa Anatomy 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 230000000638 stimulation Effects 0.000 description 1
- 230000035922 thirst Effects 0.000 description 1
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- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M169/00—Lubricating compositions characterised by containing as components a mixture of at least two types of ingredient selected from base-materials, thickeners or additives, covered by the preceding groups, each of these compounds being essential
- C10M169/04—Mixtures of base-materials and additives
- C10M169/048—Mixtures of base-materials and additives the additives being a mixture of compounds of unknown or incompletely defined constitution, non-macromolecular and macromolecular compounds
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- C10M2201/00—Inorganic compounds or elements as ingredients in lubricant compositions
- C10M2201/06—Metal compounds
- C10M2201/061—Carbides; Hydrides; Nitrides
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- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
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- C10M2201/00—Inorganic compounds or elements as ingredients in lubricant compositions
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- C10M2201/00—Inorganic compounds or elements as ingredients in lubricant compositions
- C10M2201/085—Phosphorus oxides, acids or salts
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- C10M2205/00—Organic macromolecular hydrocarbon compounds or fractions, whether or not modified by oxidation as ingredients in lubricant compositions
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- C10M2205/026—Butene
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- C10M2207/00—Organic non-macromolecular hydrocarbon compounds containing hydrogen, carbon and oxygen as ingredients in lubricant compositions
- C10M2207/10—Carboxylix acids; Neutral salts thereof
- C10M2207/14—Carboxylix acids; Neutral salts thereof having carboxyl groups bound to carbon atoms of six-membered aromatic rings
- C10M2207/142—Carboxylix acids; Neutral salts thereof having carboxyl groups bound to carbon atoms of six-membered aromatic rings polycarboxylic
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Abstract
本发明公开了一种高润滑、高脱模性钛合金锻造专用水性热锻加工油，由氮化硼、异丁烯—马来酸酐共聚物、有机硅乙二醇共聚体蜡乳液、木质素磺酸钠、对苯二甲酸、氢氧化钠、磷酸氢钾、烷基苯磺酸钠、聚二甲基硅氧烷乳液、苯并噻唑啉酮、纯水组成。本发明具有高润滑、高脱模性。
Description
技术领域
本发明涉及一种钛合金锻造用水性热锻加工油。
背景技术
钛是20世纪50年代发展起来的一种重要的结构金属，钛合金因具有强度高、 耐蚀性好、 耐热性高等特点而被广泛用于各个领域。世界上许多国家都认识到钛合金材料的重要性，相继对其进行研究开发，并得到了实际应用。20世纪50～60年代，主要是发展航空发动机用的高温钛合金和机体用的结构钛合金，70年代开发出一批耐蚀钛合金，80年代以来，耐蚀钛合金和高强钛合金得到进一步发展。钛合金主要用于制作飞机发动机压气机部件，其次为火箭、导弹和高速飞机的结构件。
钛的化学活性大，与大气中O、N、H、CO、CO2、水蒸气、氨气等产生强烈的化学反应。含碳量大于0.2%时，会在钛合金中形成硬质TiC；温度较高时，与N作用也会形成TiN硬质表层；在600℃以上时，钛吸收氧形成硬度很高的硬化层；氢含量上升，也会形成脆化层。吸收气体而产生的硬脆表层深度可达0.1～0.15 mm，硬化程度为20%～30%。钛的化学亲和性也大，易与摩擦表面产生粘附现象。这对钛合金加工过程、特别是锻造工艺提出了更高的要求。
由于钛的化学活泼性和化学亲和性大，目前市售的采用高分子化合物制备的水性锻造加工油，其润滑性能、脱模性能难于满足钛合金锻造加工工艺使用要求，客户渴望生产厂家能开发出一种适用于钛合金锻造的专用水性锻造加工油。
发明内容
本发明的目的在于提供一种润滑性能和脱模性能优异的高润滑、高脱模性钛合金锻造专用水性热锻加工油。
本发明的技术解决方案是：
一种高润滑、高脱模性钛合金锻造专用水性热锻加工油，其特征是：由下列重量百分比的组分混合制成：
氮化硼 1-5%
异丁烯—马来酸酐共聚物 5-15%
有机硅乙二醇共聚体蜡乳液 2-8%
木质素磺酸钠 1-3%
对苯二甲酸 5-10%
氢氧化钠 3-8%
磷酸氢钾 0.5-2%
烷基苯磺酸钠 0.5-2%
聚二甲基硅氧烷乳液 0.5-1%
苯并噻唑啉酮 0.5-1%
纯水 余量。
所述的高润滑、高脱模性钛合金锻造专用水性热锻加工油，由下列重量百分比的组分混合制成：
氮化硼 3%
异丁烯—马来酸酐共聚物 10%
有机硅乙二醇共聚体蜡乳液 5%
木质素磺酸钠 2%
对苯二甲酸 8%
氢氧化钠 5%
磷酸氢钾 1%
烷基苯磺酸钠 1%
聚二甲基硅氧烷乳液 0.5%
苯并噻唑啉酮 0.5%
纯水 余量。
本发明具有高润滑、高脱模性：
1. 项目选用异丁烯───马来酸酐共聚物、有机硅乙二醇共聚体蜡乳液等配伍，产品具有优异的润滑性能（150℃时摩擦系数≤0.10）。
2. 项目选用氢氧化钠、磷酸氢钾、烷基苯磺酸钠复配及固体润滑剂氮化硼等配伍，产品具有优异的脱模性能（150 ℃时脱模力负荷≤25/kg）。
3. 使用不使用重金属、芳香烃等有毒有害物质（选用性能优良、对人和环境友好的可替代物质），产品急性经口毒性LD50≥5000mg/kg，急性吸入毒性LC50≥5000mg/m3，无呼吸道粘膜刺激，安全卫生质量高。
下面结合实施例对本发明作进一步说明。
具体实施方式
实施例1：
一种高润滑、高脱模性钛合金锻造专用水性热锻加工油，由下列重量百分比的组分混合制成：
氮化硼 5%
异丁烯—马来酸酐共聚物 8%
有机硅乙二醇共聚体蜡乳液 6%
木质素磺酸钠 1%
对苯二甲酸 9%
氢氧化钠 6%
磷酸氢钾 1%
烷基苯磺酸钠 1%
聚二甲基硅氧烷乳液 0.5%
苯并噻唑啉酮 1%
纯水 余量。
实施例2：
一种高润滑、高脱模性钛合金锻造专用水性热锻加工油，由下列重量百分比的组分混合制成：
氮化硼 3%
异丁烯—马来酸酐共聚物 10%
有机硅乙二醇共聚体蜡乳液 5%
木质素磺酸钠 2%
对苯二甲酸 8%
氢氧化钠 5%
磷酸氢钾 1%
烷基苯磺酸钠 1%
聚二甲基硅氧烷乳液 0.5%
苯并噻唑啉酮 0.5%
纯水 余量。
Claims (2)
1.一种高润滑、高脱模性钛合金锻造专用水性热锻加工油，其特征是：由下列重量百分比的组分混合制成：
氮化硼 1-5%
异丁烯—马来酸酐共聚物 5-15%
有机硅乙二醇共聚体蜡乳液 2-8%
木质素磺酸钠 1-3%
对苯二甲酸 5-10%
氢氧化钠 3-8%
磷酸氢钾 0.5-2%
烷基苯磺酸钠 0.5-2%
聚二甲基硅氧烷乳液 0.5-1%
苯并噻唑啉酮 0.5-1%
纯水 余量。
2. 根据权利要求1所述的高润滑、高脱模性钛合金锻造专用水性热锻加工油，其特征是：由下列重量百分比的组分混合制成：
氮化硼 3%
异丁烯—马来酸酐共聚物 10%
有机硅乙二醇共聚体蜡乳液 5%
木质素磺酸钠 2%
对苯二甲酸 8%
氢氧化钠 5%
磷酸氢钾 1%
烷基苯磺酸钠 1%
聚二甲基硅氧烷乳液 0.5%
苯并噻唑啉酮 0.5%
纯水 余量。
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