CN109954011A - A kind of bacteriostatic agent and its preparation process - Google Patents

A kind of bacteriostatic agent and its preparation process Download PDF

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Publication number
CN109954011A
CN109954011A CN201910321599.1A CN201910321599A CN109954011A CN 109954011 A CN109954011 A CN 109954011A CN 201910321599 A CN201910321599 A CN 201910321599A CN 109954011 A CN109954011 A CN 109954011A
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bacteriostatic agent
stirred tank
oil
calcium sulphate
yellow lead
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赵英存
滕德林
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Huizhou Renren Biotechnology Co Ltd
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Huizhou Renren Biotechnology Co Ltd
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Priority to CN201910321599.1A priority Critical patent/CN109954011A/en
Publication of CN109954011A publication Critical patent/CN109954011A/en
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    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K33/00—Medicinal preparations containing inorganic active ingredients
    • A61K33/06—Aluminium, calcium or magnesium; Compounds thereof, e.g. clay
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K33/00—Medicinal preparations containing inorganic active ingredients
    • A61K33/24—Heavy metals; Compounds thereof
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18—Magnoliophyta (angiosperms)
    • A61K36/185—Magnoliopsida (dicotyledons)
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18—Magnoliophyta (angiosperms)
    • A61K36/185—Magnoliopsida (dicotyledons)
    • A61K36/23—Apiaceae or Umbelliferae (Carrot family), e.g. dill, chervil, coriander or cumin
    • A61K36/234—Cnidium (snowparsley)
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18—Magnoliophyta (angiosperms)
    • A61K36/185—Magnoliopsida (dicotyledons)
    • A61K36/61—Myrtaceae (Myrtle family), e.g. teatree or eucalyptus
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61P—SPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
    • A61P17/00—Drugs for dermatological disorders
    • A61P17/02—Drugs for dermatological disorders for treating wounds, ulcers, burns, scars, keloids, or the like
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61P—SPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
    • A61P31/00—Antiinfectives, i.e. antibiotics, antiseptics, chemotherapeutics
    • A61P31/04—Antibacterial agents

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  • Health & Medical Sciences (AREA)
  • Natural Medicines & Medicinal Plants (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Chemical & Material Sciences (AREA)
  • Medicinal Chemistry (AREA)
  • Pharmacology & Pharmacy (AREA)
  • Animal Behavior & Ethology (AREA)
  • General Health & Medical Sciences (AREA)
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  • Veterinary Medicine (AREA)
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  • Alternative & Traditional Medicine (AREA)
  • Biotechnology (AREA)
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  • Microbiology (AREA)
  • Medical Informatics (AREA)
  • Botany (AREA)
  • Organic Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Nuclear Medicine, Radiotherapy & Molecular Imaging (AREA)
  • General Chemical & Material Sciences (AREA)
  • Dermatology (AREA)
  • Communicable Diseases (AREA)
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Abstract

The present invention discloses a kind of bacteriostatic agent, comprises the following components in parts by weight: 10~35 parts of yellow lead powder, 20~40 parts of calcium sulphate dihydrate, 25~45 parts of dead plaster, 165~360 parts of vegetable oil.Yellow lead powder is added in vegetable oil, calcium sulphate dihydrate, dead plaster simultaneously goes out finely dispersed oily bacteriostatic agent by certain technique adjustment, yellow lead meal component plays a part of to destroy and eliminate pathogenic microorganism, calcium sulphate dihydrate, dead plaster can carry out covering protection at skin trauma to caused by boiling hot burning or sore, reduce the chance contacted with air environment, myogenic is played simultaneously, the effect of hemostasis, sesame oil, tea oil, the vegetable oil such as selinum oil vitamin E rich in and linolenic acid, there are good nourishes effect and moisturizing effect to skin, with calcium sulphate dihydrate, dead plaster is collectively formed one layer of protection and sticks oil reservoir, to being protected at skin trauma, bacteriostatic agent pharmacological property simultaneously in the present invention is mild, it is non-stimulated, it can guarantee the comfort of patient.

Description

A kind of bacteriostatic agent and its preparation process
Technical field
The invention belongs to bacteriostatic agent technical fields, and in particular to a kind of bacteriostatic agent and its preparation process.
Background technique
With the raising of people's health care consciousness and to safe and healthy attention, the disinfection of wound is treated in daily life Antibacterial processing is extremely paid attention to, and wound caused by scalding or burning is damaged due to receptor so that patient's sense organ when preliminary injured Feel extremely uncomfortable, and in wound healing process, patient is low to the perceptual sensitivity of wound, can not know whether wound has cause of disease Microbial growth easily causes infection to injure.The effective bacteriostatic agent of most strengths is usually chemical bacteriostatic agent at present, this kind of antibacterial Pathogenic microorganism can quickly and effectively be eliminated and be inhibited to agent, but big to the Skin and mucosa irritation of wound, largely make The sense of discomfort of adult body when at the sufferer for scalding or burning, may destroy wound, contain Chinese patent drug ingredient as a result, Bacteriostatic agent occur gradually over market, this is because its reaction is more mild and irritation is small, it may have certain fungistatic effect.
Calcined gypsum in the field of Chinese medicines frequently as liniment, to skin hot burn and sore wound have good therapeutic effect and Skin sparing effect, plays myogenic, hemostasis, and sesame oil etc. contains the vegetable oil pair of linoleic acid and vitamin E abundant Skin plays the role of antipruritic anti-inflammatory and moist, and vegetable oil, the pharmacological property of calcined gypsum are mild, and the two is applied in bacteriostatic agent, It has a good application prospect.
Summary of the invention
In order to solve the above technical problems, the present invention provides a kind of bacteriostatic agent and its preparation process.
The technical scheme adopted by the invention to achieve the purpose is as follows:
A kind of bacteriostatic agent, comprises the following components in parts by weight:
It further illustrates, the vegetable oil is selected from one or more of sesame oil, tea oil, selinum oil Mixture.
It further illustrates, the particle size distribution of the dead plaster is in 80~120 mesh.
It further illustrates, the constituent content of the vegetable oil is yellow lead powder, calcium sulphate dihydrate, dead plaster group Three times for dividing the sum of content.
It further illustrates, the preparation process of the bacteriostatic agent includes following implementation steps:
A. 20%~30% vegetable oil is added in a stirring kettle, and yellow lead powder is added in backward stirred tank, with 400~ After the mixing speed stirring 15min of 600rpm, continue to put into 20%~30% vegetable oil to stirred tank, with 400~600rpm Mixing speed stir 10min；
B. after the completion of step a, calcium sulphate dihydrate, dead plaster are put into, successively to stirred tank with 400~600rpm's After mixing speed stirs 20min, surplus vegetable oil is put into stirred tank, 40min is stirred with the mixing speed of 800~1000rpm Afterwards, 40 mesh screens are crossed after the completion of stirring, gained filtrate takes supernatant liquid, as bacteriostatic agent after standing 1~2h；
It further illustrates, yellow lead powder is first put into flour mill and is ground before putting into stirred tank in the step a 10min, crosses 50 meshes after the completion of grinding, stirred tank is added in the filter powder of gained yellow lead powder.
Further illustrate, in the step b calcium sulphate dihydrate before putting into stirred tank, be first put into flour mill into Row grinding 10min, crosses 50 meshes after the completion of grinding, stirred tank is added in the filter powder of gained calcium sulphate dihydrate.
Compared with prior art, the beneficial effects of the present invention are:
Yellow lead powder, calcium sulphate dihydrate, dead plaster are added in vegetable oil and go out to disperse by certain technique adjustment Uniform oily bacteriostatic agent, yellow lead meal component play sterilization, and calcium sulphate dihydrate, dead plaster can be to boiling hot burning or sores Covering protection is carried out at skin trauma caused by poison, the chance contacted with air environment is reduced, to reduce the micro- life of site of injury cause of disease The growth of object, while playing myogenic, hemostasis, the vegetable oil such as sesame oil, tea oil, selinum oil vitamin rich in E and linolenic acid have good nourishes effect and moisturizing to act on skin, with calcium sulphate dihydrate, the common shape of dead plaster Stick oil reservoir at one layer of protection, to protecting at skin trauma, while the bacteriostatic agent pharmacological property in the present invention is mild, non-stimulated, It can guarantee the sense organ comfort at patient trauma.
Specific embodiment
In order to further understand the content, features and effects of the present invention, hereby enumerating following embodiment explanation.
Embodiment 1
A kind of bacteriostatic agent, comprises the following components in parts by weight:
Yellow lead powder 20g,
Calcium sulphate dihydrate 35g,
Dead plaster 35g,
Sesame oil 270g.
Preparation process:
Material preparation: yellow lead powder, which is put into flour mill, carries out grinding 10min, and 50 meshes are crossed after the completion of grinding, are saved backup； Yellow lead powder, which is put into flour mill, carries out grinding 10min, and 50 meshes are crossed after the completion of grinding, 20g yellow lead powder is taken to save backup.
Material mixing: the sesame oil of 60g is added in a stirring kettle, and yellow lead powder is added in backward stirred tank, with 600rpm Mixing speed stirring 15min after, continue the sesame oil for putting into 60g to stirred tank, stirred with the mixing speed of 600rpm 10min；35g calcium sulphate dihydrate, 35g dead plaster are successively put into stirred tank, are stirred with the mixing speed of 600rpm After 20min, surplus sesame oil is put into stirred tank, after stirring 40min with the mixing speed of 800rpm, 40 mesh are crossed after the completion of stirring Sieve, gained filtrate take supernatant liquid, as bacteriostatic agent after standing 1.5h.
Embodiment 2
A kind of bacteriostatic agent, comprises the following components in parts by weight:
Yellow lead powder 25g,
Calcium sulphate dihydrate 37g,
Dead plaster 32g,
Sesame oil 282g.
Preparation process:
Material preparation: yellow lead powder, which is put into flour mill, carries out grinding 10min, and 50 meshes are crossed after the completion of grinding, are saved backup； Yellow lead powder, which is put into flour mill, carries out grinding 10min, and 50 meshes are crossed after the completion of grinding, 25g yellow lead powder is taken to save backup.
Material mixing: the sesame oil of 80g is added in a stirring kettle, and yellow lead powder is added in backward stirred tank, with 600rpm Mixing speed stirring 15min after, continue the sesame oil for putting into 60g to stirred tank, stirred with the mixing speed of 600rpm 10min；37g calcium sulphate dihydrate, 32g dead plaster are successively put into stirred tank, are stirred with the mixing speed of 600rpm After 20min, surplus sesame oil is put into stirred tank, after stirring 40min with the mixing speed of 800rpm, 40 mesh are crossed after the completion of stirring Sieve, gained filtrate take supernatant liquid, as bacteriostatic agent after standing 1.5h.
Embodiment 3
A kind of bacteriostatic agent, comprises the following components in parts by weight:
Yellow lead powder 30g,
Calcium sulphate dihydrate 37g,
Dead plaster 33g,
Sesame oil 153g,
Tea oil 147g.
Preparation process:
Material preparation: yellow lead powder, which is put into flour mill, carries out grinding 10min, and 50 meshes are crossed after the completion of grinding, take 30g yellow lead Powder saves backup；Calcium sulphate dihydrate, which is put into flour mill, carries out grinding 10min, and 50 meshes are crossed after the completion of grinding, take bis- water of 37g Calcium sulfate is closed to save backup.
Material mixing: the tea oil of 80g is added in a stirring kettle, and yellow lead powder is added in backward stirred tank, with 600rpm Mixing speed stirring 15min after, continue the tea oil for putting into 67g to stirred tank, stirred with the mixing speed of 600rpm 10min；37g calcium sulphate dihydrate, 33g dead plaster are successively put into stirred tank, are stirred with the mixing speed of 600rpm After 20min, 153g sesame oil is put into stirred tank, after stirring 40min with the mixing speed of 800rpm, 40 mesh are crossed after the completion of stirring Sieve, gained filtrate take supernatant liquid, as bacteriostatic agent after standing 1.5h.
Embodiment 4
A kind of bacteriostatic agent, comprises the following components in parts by weight:
Yellow lead powder 26g,
Calcium sulphate dihydrate 38g,
Dead plaster 34g,
Sesame oil 143g,
Selinum oil 151g.
Preparation process:
Material preparation: yellow lead powder, which is put into flour mill, carries out grinding 10min, and 50 meshes are crossed after the completion of grinding, take 26g yellow lead Powder saves backup；Calcium sulphate dihydrate, which is put into flour mill, carries out grinding 10min, and 50 meshes are crossed after the completion of grinding, take bis- water of 38g Calcium sulfate is closed to save backup.
Material mixing: the sesame oil of 73g being added in a stirring kettle, and 26g yellow lead powder is added in backward stirred tank, with After the mixing speed stirring 15min of 600rpm, continues the sesame oil for putting into 70g to stirred tank, stirred with the mixing speed of 600rpm Mix 10min；38g calcium sulphate dihydrate, 34g dead plaster are successively put into stirred tank, are stirred with the mixing speed of 600rpm After 20min, 151g selinum oil is put into stirred tank, after stirring 40min with the mixing speed of 800rpm, 40 are crossed after the completion of stirring Mesh screen, gained filtrate take supernatant liquid, as bacteriostatic agent after standing 1.5h.
Embodiment 5
A kind of bacteriostatic agent, comprises the following components in parts by weight:
Yellow lead powder 30g,
Calcium sulphate dihydrate 42g,
Dead plaster 40g,
Sesame oil 160g,
Tea oil 98g,
Selinum oil 78g.
Preparation process:
Material preparation: yellow lead powder, which is put into flour mill, carries out grinding 10min, and 50 meshes are crossed after the completion of grinding, take 30g yellow lead Powder saves backup；Calcium sulphate dihydrate, which is put into flour mill, carries out grinding 10min, and 50 meshes are crossed after the completion of grinding, take bis- water of 42g Calcium sulfate is closed to save backup.
Material mixing: the sesame oil of 80g is added in a stirring kettle, and yellow lead powder is added in backward stirred tank, with 600rpm Mixing speed stirring 15min after, continue the sesame oil for putting into 80g to stirred tank, stirred with the mixing speed of 600rpm 10min；42g calcium sulphate dihydrate, 40g dead plaster are successively put into stirred tank, are stirred with the mixing speed of 600rpm After 20min, 98g tea oil, 78g selinum oil are put into stirred tank, after stirring 40min with the mixing speed of 800rpm, stirring 40 mesh screens are crossed after the completion, and gained filtrate takes supernatant liquid, as bacteriostatic agent after standing 1.5h.
Embodiment 1 is tested for the property to 5 gained bacteriostatic agent of embodiment and safety test, sensory test result are shown in Table One.
Table one
Project Characterization result
Color Orange blush
Form Oily liquids
Smell Special fragranced
Impurity It is visible by naked eyes exogenous impurity
Its physical and chemical index the results are shown in Table two.
Table two
Project As a result
pH 7.0~8.2
Relative density (20 DEG C/20 DEG C) 9.8~1.0
Mercury (in terms of Hg), mg/kg <1
Arsenic (in terms of As), mg/kg <10
Lead (in terms of Pb), mg/kg <40
Cadmium (in terms of Cd), mg/kg <5
Its microbial safety testing result is shown in Table three.
Table three
Inspection project Unit Inspection result Standard limited value As a result
Total plate count CFU/g <10 ≤1000 It is qualified
Mould and yeast CFU/g 70 ≤100 It is qualified
Heat-resisting coliform CFU/g It is not detected It must not detect It is qualified
Pseudomonas aeruginosa /g It is not detected It must not detect It is qualified
Staphylococcus aureus /g It is not detected It must not detect It is qualified
The above is only the preferred embodiments of the present invention, and is not intended to limit the present invention in any form, Any simple modification made to the above embodiment according to the technical essence of the invention, equivalent variations and modification, belong to The range of technical solution of the present invention.

Claims (7)

1. a kind of bacteriostatic agent, which is characterized in that comprise the following components in parts by weight:
2. a kind of bacteriostatic agent according to claim 1, it is characterised in that: the vegetable oil is selected from sesame oil, tea oil, snake One or more mixtures of machine tool oil.
3. a kind of bacteriostatic agent according to claim 1, it is characterised in that: the particle size distribution of the dead plaster exists 80~120 mesh.
4. a kind of bacteriostatic agent according to claim 1, it is characterised in that: the constituent content of the vegetable oil be yellow lead powder, Three times of the sum of calcium sulphate dihydrate, dead plaster constituent content.
5. a kind of bacteriostatic agent according to claim 1, which is characterized in that the preparation process of the bacteriostatic agent includes following reality Apply step:
A. 20%~30% vegetable oil is added in a stirring kettle, and yellow lead powder is added in backward stirred tank, with 400~600rpm Mixing speed stirring 15min after, continue to stirred tank put into 20%~30% vegetable oil, with the stirring of 400~600rpm Speed stirs 10min；
B. after the completion of step a, calcium sulphate dihydrate, dead plaster are successively put into stirred tank, with the stirring of 400~600rpm After speed stirs 20min, surplus vegetable oil is put into stirred tank, after stirring 40min with the mixing speed of 800~1000rpm, is stirred 40 mesh screens are crossed after the completion of mixing, gained filtrate takes supernatant liquid, as bacteriostatic agent after standing 1~2h.
6. a kind of bacteriostatic agent according to claim 5, it is characterised in that: yellow lead powder is in investment stirred tank in the step a Before, it is first put into flour mill and carries out grinding 10min, 50 meshes are crossed after the completion of grinding, stirred tank is added in the filter powder of gained yellow lead powder.
7. a kind of bacteriostatic agent according to claim 5, it is characterised in that: calcium sulphate dihydrate is put into the step b It before stirred tank, is first put into flour mill and carries out grinding 10min, 50 meshes, the filter of gained calcium sulphate dihydrate are crossed after the completion of grinding Stirred tank is added in powder.
CN201910321599.1A 2019-04-22 2019-04-22 A kind of bacteriostatic agent and its preparation process Pending CN109954011A (en)

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Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101919885A (en) * 2009-06-16 2010-12-22 刘建伟 Ointment for treating burns and scalds and preparation method thereof
CN109200137A (en) * 2018-10-17 2019-01-15 赣州哈克生物科技有限公司 A kind of tea oil bacteriostatic agent and preparation method thereof

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101919885A (en) * 2009-06-16 2010-12-22 刘建伟 Ointment for treating burns and scalds and preparation method thereof
CN109200137A (en) * 2018-10-17 2019-01-15 赣州哈克生物科技有限公司 A kind of tea oil bacteriostatic agent and preparation method thereof

Non-Patent Citations (3)

* Cited by examiner, † Cited by third party
Title
（美）施瓦茨编: "《美国儿科专家临床会诊 2版》", 31 October 2007, 天津科技翻译出版公司 *
ATHENA: "黄丹粉的功效与作用 吃黄丹粉的药用价值", 《果蔬百科全说 中药知识 HTTPS://ZIP.XIZIWANG.NET/ZHONGYAO/52955/》 *
侯连兵 等: "《现代个体化药物新剂型 西药卷》", 30 September 2009, 人民军医出版社 *

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Application publication date: 20190702