CN109929044A - A kind of instant Cassia bean gum preparation method and applications - Google Patents
A kind of instant Cassia bean gum preparation method and applications Download PDFInfo
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- CN109929044A CN109929044A CN201711349493.XA CN201711349493A CN109929044A CN 109929044 A CN109929044 A CN 109929044A CN 201711349493 A CN201711349493 A CN 201711349493A CN 109929044 A CN109929044 A CN 109929044A
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Abstract
The present invention provides a kind of instant Cassia bean gum preparation method, method includes the following steps: pre-treatment: cassia seed is peeled through peeling machine, obtains endosperm;Gained endosperm is crushed, and comminuted powder is obtained;Gained comminuted powder is separated, and is obtained thick glue and is mixed with alcohol water blend, swelling, heat preservation, cooling, de- starch processing is carried out using rubber mill, the thick glue glue of de- starch is obtained, acid or alkali is added, bleaching agent processing is added, white glue is obtained and is handled by purification system, high colourless glue thoroughly is obtained and is concentrated using film concentration systems, concentrate, using ultrasonic depolymerization, obtains depolymerization glue and carry out alcohol analysis or saltout, glue after being dehydrated, it is dried, obtains instant Cassia bean gum.
Description
Technical field
The invention belongs to application in TCM fields, are specifically related to a kind of instant Cassia bean gum preparation method and applications.
Background technique
Cassia seed is the dry mature seed of legume cassia or little cassia tora, bitter, sweet, salty, cold nature, enter liver, kidney,
Large intestine channel;Containing multivitamin and amino acid abundant, fat, carbohydrate etc., there is relax bowel and defecation, lipid-loweringing improving eyesight,
The effects for the treatment of constipation and hyperlipidemia, hypertension, it is widely used in the related fieldss such as drug, health care product at present.
Cassia bean gum is the hydrophilic gel with certain medical care effect extracted from the sub- endosperm of legume cassia
Body, main component are to polymerize the galactomannans formed by galactolipin and mannose.Its structure with other kinds of subclass glue phases
Like such as locust bean gum structure, long-chain molecule structure, and average every 5- are formed in β-Isosorbide-5-Nitrae glycosidic bond form for unit by mannose
6 mannose molecules link a galactose molecule, and average molecular weight is between ten thousand dalton of 10-30.Cassia bean gum and OK a karaoke club
Glue and xanthan gum all have good synergistic effect, and the product for helping to improve Related product are used together with both colloids
Matter, while reducing dosage and reduce cost.Common Cassia bean gum exists in application process because agglomerating caused by quickly absorbing water at present
It is the problems such as indissoluble solution, poor transparency, excessively high solution temperature, serious to limit the application of Cassia bean gum.
Summary of the invention
Exist in application process to solve common Cassia bean gum because of the indissoluble solution, transparency of agglomerating caused by quickly absorbing water
Difference, the problems such as solution temperature is excessively high, the present invention provides a kind of preparation method of new Cassia bean gum, specific as follows.
The present invention provides a kind of instant Cassia bean gum preparation method, method includes the following steps:
(1) pre-treatment: cassia seed is peeled through peeling machine, obtains endosperm;Gained endosperm is crushed, and comminuted powder is obtained;Gained
Comminuted powder is separated, and thick glue is obtained;
(2) it takes off starch: thick glue obtained by step (1) being mixed with alcohol water blend, swelling keeps the temperature, is cooling, grinds using glue
Machine carries out de- starch processing, obtains the thick glue glue of de- starch;
(3) it bleaches: the thick glue glue of starch will be taken off obtained by step (2), acid or alkali is added, bleaching agent processing is being added, is obtaining white
Coloring agent liquid;
(4) purifying concentration: white glue obtained by step (3) is handled by purification system, obtains high colourless glue thoroughly;Institute
It obtains high colourless glue to be concentrated by film concentration systems, obtains concentrate;
(5) concentrate obtained by step (4) depolymerization: is obtained into depolymerization glue using ultrasonic depolymerization;
(6) be dehydrated again: depolymerization glue obtained by step (5) carries out alcohol analysis or saltouts, and glue after being dehydrated is dried,
Obtain instant Cassia bean gum.
Cassia seed described in step (1) is de- through peeling machine in preferred instant Cassia bean gum preparation method of the present invention
The peeling rate of skin is 80-100%;It is endosperm through low speed grinder progress air-flow crushing, hammer leaf linear speed that the endosperm, which crush,
Degree control is in 60-120 meter per second;The comminuted powder carries out being separated into cyclonic separation: comminuted powder is transported to whirlwind point by air-flow
Machine is selected to carry out crude separation, charging rate is controlled at 20-300 kgs/hour, and blast velocity control is separated at 0.1-100 ms/min
Except most of pigment, fiber, starch and albumen, thick glue is obtained.
Thick glue and alcohol water blend described in step (2) in preferred instant Cassia bean gum preparation method of the present invention
Mixing is to mix in mass ratio for the ratio of 1:20-1:200, and alcohol content is 10-50% in the alcohol water blend;Swelling
Form stable glue within 15-30 minutes;Heat preservation 10-60 minutes, holding temperature are 95-105 DEG C;After being cooled to 20-50 DEG C, then pass through
It crosses rubber mill and carries out de- starch processing, obtain the thick glue glue of de- starch.
Sour sulfuric acid, hydrochloric acid, grass described in step (3) in preferred instant Cassia bean gum preparation method of the present invention
One of acid, acetic acid, malic acid, citric acid are a variety of, and the pH of glue is 5-7 after acid adding;The alkali is sodium hydroxide, hydrogen-oxygen
Change potassium, one of sodium carbonate or a variety of, adding the pH of glue after alkali is 7.5-13;The bleaching agent is hydrogen peroxide, hypochlorous acid
One of sodium, sodium sulfite are a variety of, and dosage is the 0.01%-15% of reaction solution.
The purifying of step (4) the purification system processing in preferred instant Cassia bean gum preparation method of the present invention
Membrane aperture is 0.5-50 microns in system membrane assembly, and operating pressure is controlled in 0.5-20MPa;The system of the film concentration systems
Membrane aperture 5000-80000Dalton in membrane assembly, operating pressure control are 1- in 0.1-10MPa, the solid content of concentrate
60%.
Ultrasonic depolymerization described in step (5) is concentrate in preferred instant Cassia bean gum preparation method of the present invention
It is transported to the infrared reaction kettle of ultrasound, opens ultrasonic generator, supersonic frequency is controlled in 50-120KHZ, ultrasonic depolymerization reaction 5-50
Minute.
Ultrasonic depolymerization described in step (5) is concentrate in preferred instant Cassia bean gum preparation method of the present invention
It sets in ultrasonic device, opens infrared heating, at 40-100 DEG C, supersonic frequency is controlled between 10-60KHz for temperature control, and ultrasound is anti-
It answers 20-120 minutes, cools to 20-35 DEG C.
Alcohol analysis described in step (6) is addition depolymerization glue in preferred instant Cassia bean gum preparation method of the present invention
The alcohol or isopropanol of liquid quality 5-200% carries out alcohol analysis, removes liquid by high speed centrifugation system and obtains semi-dried product, centrifuge
2500-8000 revs/min of revolving speed;Instant Cassia bean gum, vacuum drying temperature 25- are dried to obtain by vacuum drying system again
80 DEG C, drying chamber pressure is controlled in 0-85KPa.
It is saltoutd described in step (6) in preferred instant Cassia bean gum preparation method of the present invention as to concentration glue
Middle addition sodium tetraborate is saltoutd, sodium tetraborate dosage be glue quality 0.001-2%, then by press filteration system carry out into
The dehydration of one step and desalination, the control of press filteration system pressure obtain film, film forms slurries by beater, then leads in 3-35MPa
It crosses spray drying and obtains instant Cassia bean gum, at 220-550 DEG C, leaving air temp control exists for the inlet air temperature control of spray drying
80-180 DEG C, high pressure pump pressure 3-20MPa, atomization revolving speed control is at 6000-28000 revs/min.
A kind of cassia gum compound is also claimed in the present invention, and the compound is by instant Cassia bean gum of the present invention
The instant Cassia bean gum and carragheen or xanthan gum of preparation method preparation form.The instant Cassia bean gum and carragheen or xanthan
Glue weight ratio is 1:1-1:8.
The present invention is also claimed the preparation method of cassia gum compound, this method be instant Cassia bean gum and carragheen or
Xanthan gum in three-dimensional mixer mixed processing 10-60 minutes to get cassia gum compound.
The utility model has the advantages that
1, this technique solves common Cassia bean gum in application process because of difficult problems of dissolution of agglomerating caused by quickly absorbing water;
2, common Cassia bean gum greatly limits their application territory because of poor transparency, and the instant Cassia of the present invention
Sub- glue transparency is high, the very good solution problem;
3, common Cassia bean gum solution temperature is excessively high, at 90-105 DEG C, limits its application in cryogenic product, this hair
Bright high-purity instant Cassia bean gum solution temperature can further expansion its application field at 35-75 DEG C.
Specific embodiment
The instant Cassia bean gum preparation method of embodiment 1, method includes the following steps:
(1) pre-treatment: cassia seed is peeled through peeling machine, peeling rate 98%;Obtain endosperm;Endosperm through low speed grinder into
Row air-flow crushing, hammer leaf wire velocity control obtain comminuted powder in 100 meter per seconds;Comminuted powder is into be separated into cyclonic separation: crushing
Powder is transported to whirlwind sorting machine by air-flow and carries out crude separation, and charging rate is controlled at 90 kgs/hour, and blast velocity control is 55
M/min, separation removes most of pigment, fiber, starch and albumen, obtains thick glue;
(2) take off starch: it is mixed for the ratio of 1:20 in mass ratio that thick glue and alcohol water blend obtained by step (1), which are mixed,
It closes, alcohol content is 50% in the alcohol water blend;It is swollen 15 minutes and forms stable glue;Heat preservation 30 minutes, heat preservation temperature
Degree is 100 DEG C;After being cooled to 45 DEG C, de- starch processing is carried out using rubber mill, obtains the thick glue of de- starch.Swelling keeps the temperature, is cold
But, de- starch processing is carried out using rubber mill, obtains the thick glue of de- starch;
(3) it bleaches: the thick glue of starch will be taken off obtained by step (2), sulfuric acid is added, glue pH is 6.5, then plus glue weight
3% hydrogen peroxide bleaching processing, obtains white glue;
(4) purifying concentration: white glue obtained by step (3) is handled by purification system, the purifying of purification system processing
Membrane aperture is 20 microns in system membrane assembly, and operating pressure is controlled in 8MPa;The system membrane assembly of the film concentration systems
Middle membrane aperture 20000Dalton, operating pressure control are 40% in 0.8MPa, the solid content of concentrate
(5) depolymerization: by concentrate obtained by step (4), using ultrasonic depolymerization, ultrasonic depolymerization is transported to ultrasonic red for concentrate
Outer reaction kettle opens ultrasonic generator, and supersonic frequency is controlled in 85KHZ, and ultrasonic depolymerization reaction 30 minutes obtains depolymerization glue;
(6) be dehydrated again: depolymerization glue obtained by step (5) carries out alcohol analysis, and the alcohol analysis is addition depolymerization glue quality
70% alcohol or isopropanol carries out alcohol analysis, removes liquid by high speed centrifugation system and obtains semi-dried product, centrifuge speed 5000
Rev/min;Instant Cassia bean gum is dried to obtain by vacuum drying system again, vacuum drying temperature is 55 DEG C, drying chamber pressure
Control obtains instant Cassia bean gum in 50KPa.
The preparation of cassia gum compound
Instant Cassia bean gum and carragheen prepared by Example 1 is 1:1 proportion according to weight ratio, is set in three-dimensional mixer
Mixed processing 50 minutes to get cassia gum compound (carragheen).
Instant Cassia bean gum and xanthan gum prepared by Example 1 is 1:1 proportion according to weight ratio, is set in three-dimensional mixer
Mixed processing 30 minutes to get cassia gum compound (xanthan gum).
The instant Cassia bean gum preparation method of embodiment 2, method includes the following steps:
(1) pre-treatment: cassia seed is peeled through peeling machine, peeling rate 90%;Obtain endosperm;Endosperm through low speed grinder into
Row air-flow crushing, hammer leaf wire velocity control obtain comminuted powder in 110 meter per seconds;Comminuted powder is into be separated into cyclonic separation: crushing
Powder is transported to whirlwind sorting machine by air-flow and carries out crude separation, and charging rate is controlled at 150 kgs/hour, and blast velocity control exists
80 ms/min, separation removes most of pigment, fiber, starch and albumen, obtains thick glue;
(2) take off starch: it is mixed for the ratio of 1:100 in mass ratio that thick glue and alcohol water blend obtained by step (1), which are mixed,
It closes, alcohol content is 30% in the alcohol water blend;It is swollen 30 minutes and forms stable glue;Heat preservation 50 minutes, heat preservation temperature
Degree is 102 DEG C;After being cooled to 40 DEG C, de- starch processing is carried out using rubber mill, obtains the thick glue of de- starch.Swelling keeps the temperature, is cold
But, de- starch processing is carried out using rubber mill, obtains the thick glue glue of de- starch;
(3) it bleaches: the thick glue glue of starch will be taken off obtained by step (2), oxalic acid is added, glue pH is 6, then plus the thick glue of de- starch
The 8% of glue weight crosses white dose of sodium hypochlorite processing, obtains white glue;
(4) purifying concentration: white glue obtained by step (3) is handled by purification system, the purifying of purification system processing
Membrane aperture is 45 microns in system membrane assembly, and operating pressure is controlled in 15MPa;The system membrane assembly of the film concentration systems
Middle membrane aperture 50000Dalton, operating pressure control are 20% in 5MPa, the solid content of concentrate
(5) depolymerization: concentrate obtained by step (4) is set in the infrared reaction kettle of ultrasound, opens infrared heating, and temperature control exists
70 DEG C, supersonic frequency controls between 20KHz, and ultrasonic reaction 60 minutes, then cool to 30 DEG C;
(6) be dehydrated again: depolymerization glue obtained by step (5) carries out alcohol analysis, and the alcohol analysis is addition depolymerization glue quality
70% isopropanol carries out alcohol analysis, removes liquid by high speed centrifugation system and obtains semi-dried product, and 6000 revs/min of centrifuge speed
Clock;Instant Cassia bean gum is dried to obtain by vacuum drying system again, vacuum drying temperature is 80 DEG C, and drying chamber pressure control exists
30KPa obtains instant Cassia bean gum.
The preparation of cassia gum compound
Instant Cassia bean gum and carragheen prepared by Example 1 is 1:5 proportion according to weight ratio, is set in three-dimensional mixer
Mixed processing 50 minutes to get cassia gum compound (carragheen).
Instant Cassia bean gum and xanthan gum prepared by Example 1 is 1:5 proportion according to weight ratio, is set in three-dimensional mixer
Mixed processing 30 minutes to get cassia gum compound (xanthan gum).
The instant Cassia bean gum preparation method of embodiment 3, method includes the following steps:
(1) pre-treatment: cassia seed is peeled through peeling machine, peeling rate 88%;Obtain endosperm;Endosperm through low speed grinder into
Row air-flow crushing, hammer leaf wire velocity control obtain comminuted powder in 80 meter per seconds;Comminuted powder is into carrying out being separated into cyclonic separation: comminuted powder
End is transported to whirlwind sorting machine by air-flow and carries out crude separation, and charging rate is controlled at 200 kgs/hour, and blast velocity control is 70
M/min, separation removes most of pigment, fiber, starch and albumen, obtains thick glue;
(2) take off starch: it is mixed for the ratio of 1:60 in mass ratio that thick glue and alcohol water blend obtained by step (1), which are mixed,
It closes, alcohol content is 20% in the alcohol water blend;It is swollen 20 minutes and forms stable glue;Heat preservation 60 minutes, heat preservation temperature
Degree is 95 DEG C;After being cooled to 30 DEG C, de- starch processing being carried out using rubber mill, obtains the thick glue of de- starch, swelling keeps the temperature, is cooling,
De- starch processing is carried out using rubber mill, obtains the thick glue glue of de- starch;
(3) it bleaches: the thick glue glue of starch will be taken off obtained by step (2), sodium hydroxide is added, glue pH is 9, then plus de- starch
The 12% sodium sulfite bleaching agent processing of thick glue glue weight, obtains white glue;
(4) purifying concentration: white glue obtained by step (3) is handled by purification system, the purifying of purification system processing
Membrane aperture is 15 microns in system membrane assembly, and operating pressure is controlled in 3MPa;The system membrane assembly of the film concentration systems
Middle membrane aperture 7000Dalton, operating pressure control are 50% in 6MPa, the solid content of concentrate
(5) depolymerization: concentrate obtained by step (4) is set in the infrared reaction kettle of ultrasound, opens infrared heating, and temperature control exists
50 DEG C, supersonic frequency controls between 50KHz, and ultrasonic reaction 30 minutes, then cool to 30 DEG C;
(6) be dehydrated again: depolymerization glue obtained by step (5) carries out alcohol analysis, and the alcohol analysis is addition depolymerization glue quality
90% isopropanol carries out alcohol analysis, removes liquid by high speed centrifugation system and obtains semi-dried product, and 4000 revs/min of centrifuge speed
Clock;Instant Cassia bean gum is dried to obtain by vacuum drying system again, vacuum drying temperature is 70 DEG C, and drying chamber pressure control exists
50KPa obtains instant Cassia bean gum.
The preparation of cassia gum compound
Instant Cassia bean gum and carragheen prepared by Example 1 is 1:8 proportion according to weight ratio, is set in three-dimensional mixer
Mixed processing 50 minutes to get cassia gum compound (carragheen).
Instant Cassia bean gum and xanthan gum prepared by Example 1 is 1:8 proportion according to weight ratio, is set in three-dimensional mixer
Mixed processing 30 minutes to get cassia gum compound (xanthan gum).
Test example: performance comparison is carried out with the instant Cassia bean gum of embodiment 1-3 preparation and common Cassia bean gum
Instant Cassia bean gum quality versus table made from common Cassia bean gum and embodiment
As can be seen from the above table, reached 98% using instant Cassia bean gum light transmittance prepared by preparation method of the invention
It is significantly larger than the 55% of common Cassia bean gum above, solubility is lower than 75 DEG C, lower than 99 DEG C of common Cassia bean gum, in terms of character
It is tasteless for white, therefore, apparent advantage is all had relative to common cassia seed using Cassia bean gum prepared by the method for the present invention.
The method of the present invention prepares winged Cassia bean gum simultaneously and the compound product of other glue preparation is intended to significantly in terms of intensity and viscosity
Better than common Cassia bean gum preparation compound.
Claims (9)
1. a kind of instant Cassia bean gum preparation method, which is characterized in that method includes the following steps:
(1) pre-treatment: cassia seed is peeled through peeling machine, obtains endosperm;Gained endosperm is crushed, and comminuted powder is obtained;Gained crushes
Powder is separated, and thick glue is obtained;
(2) take off starch: thick glue obtained by step (1) mix with alcohol water blend, swelling is kept the temperature, cooling, using rubber mill into
The de- starch processing of row, obtains the thick glue glue of de- starch;
(3) it bleaches: the thick glue glue of starch will be taken off obtained by step (2), acid or alkali is added, add bleaching agent processing, obtain white size
Liquid;
(4) purifying concentration: white glue obtained by step (3) is handled by purification system, obtains high colourless glue thoroughly;Gained is high
Saturating colourless glue is concentrated by film concentration systems, obtains concentrate;
(5) concentrate obtained by step (4) depolymerization: is obtained into depolymerization glue using ultrasonic depolymerization;
(6) be dehydrated again: depolymerization glue obtained by step (5) carries out alcohol analysis or saltouts, and glue after being dehydrated is dried, and obtains fast
Molten Cassia bean gum.
2. instant Cassia bean gum preparation method according to claim 1, which is characterized in that
The peeling rate that cassia seed described in this method step (1) is peeled through peeling machine is 80-100%;The endosperm is crushed
Air-flow crushing is carried out through low speed grinder for endosperm, hammer leaf wire velocity control is in 60-120 meter per second;The comminuted powder is separated
For cyclonic separation: comminuted powder is transported to whirlwind sorting machine by air-flow and carries out crude separation, and charging rate control is in 20-300 public affairs
Jin/hour, for blast velocity control at 0.1-100 ms/min, separation removes most of pigment, fiber, starch and albumen, obtains thick glue;
Thick glue described in this method step (2) and alcohol water blend mixing are to mix in mass ratio for the ratio of 1:20-1:200,
Alcohol content is 10-50% in the alcohol water blend;Form stable glue within swelling 15-30 minutes;Heat preservation 10-60 minutes,
Holding temperature is 95-105 DEG C;After being cooled to 20-50 DEG C, de- starch processing is carried out using rubber mill, obtains the thick glue glue of de- starch
Liquid;
One of sour sulfuric acid, hydrochloric acid, oxalic acid, acetic acid, malic acid, citric acid described in this method step (3) or a variety of, acid adding
The pH of glue is 5-7 afterwards;The alkali is one of sodium hydroxide, potassium hydroxide, sodium carbonate or a variety of, adds the pH of glue after alkali
For 7.5-13;The bleaching agent is one of hydrogen peroxide, sodium hypochlorite, sodium sulfite or a variety of, and dosage is that de- starch is thick
The 0.01%-15% of glue glue weight;
Membrane aperture is 0.5-50 microns in the purification system membrane assembly of this method step (4) purification system processing, operation
Pressure is controlled in 0.5-20MPa;Membrane aperture 5000-80000Dalton in the system membrane assembly of the film concentration systems, operation
Pressure control is 1-60% in 0.1-10MPa, the solid content of concentrate.
3. instant Cassia bean gum preparation method according to claim 1, which is characterized in that described in this method step (5)
Ultrasonic depolymerization is that concentrate is transported to the infrared reaction kettle of ultrasound, opens ultrasonic generator, and supersonic frequency is controlled in 50-120KHZ,
Ultrasonic depolymerization reaction 5-50 minutes.
4. instant Cassia bean gum preparation method according to claim 1, which is characterized in that described in this method step (5)
Ultrasonic depolymerization is that concentrate is set in the infrared reaction kettle of ultrasound, opens infrared heating, and temperature control is at 40-100 DEG C, supersonic frequency control
System is between 10-60KHz, and ultrasonic reaction 20-120 minutes, then cool to 20-35 DEG C.
5. instant Cassia bean gum preparation method according to claim 1, which is characterized in that described in this method step (6)
Alcohol analysis carries out alcohol analysis for the alcohol or isopropanol that depolymerization glue quality 5-200% is added, and removes liquid by high speed centrifugation system
Obtain semi-dried product, 2500-8000 revs/min of centrifuge speed;Instant Cassia bean gum is dried to obtain by vacuum drying system again,
Vacuum drying temperature is 25-80 DEG C, and drying chamber pressure is controlled in 0-85KPa.
6. instant Cassia bean gum preparation method according to claim 1, which is characterized in that described in this method step (6)
It saltouts as sodium tetraborate is added into depolymerization glue and saltouts, sodium tetraborate dosage is the 0.001-2% of depolymerization glue, then leads to
It crosses press filteration system to be further dehydrated and desalination, the control of press filteration system pressure obtains film, film is by beating in 3-35MPa
Pulp grinder forms slurries, then obtains instant Cassia bean gum by spray drying, and the inlet air temperature of spray drying is controlled in 220-550
DEG C, leaving air temp is controlled at 80-180 DEG C, high pressure pump pressure 3-20MPa, and atomization revolving speed control is at 6000-28000 revs/min.
7. a kind of cassia gum compound, which is characterized in that the compound is prepared by any one of claim 1-6 the method
Instant Cassia bean gum and carragheen or xanthan gum form.
8. cassia gum compound according to claim 7, which is characterized in that the instant Cassia bean gum and carragheen or Huang
Virgin rubber weight ratio is 1:1-1:8.
9. the preparation method of cassia gum compound according to claim 7 or 8, which is characterized in that this method is instant determines
Pine torch glue and carragheen or xanthan gum in three-dimensional mixer mixed processing 10-60 minutes to get cassia gum compound.
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CN101528058A (en) * | 2006-10-27 | 2009-09-09 | 路博润高级材料公司 | Improved thickener composition for food products |
CN101607997A (en) * | 2009-07-22 | 2009-12-23 | 广州城市职业学院 | The extracting method of study of semen cassia polysaccharide compound |
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Application publication date: 20190625 |