CN109874960A - A kind of preparation process of Bee Pollen pollen crystalline substance - Google Patents
A kind of preparation process of Bee Pollen pollen crystalline substance Download PDFInfo
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Abstract
The invention discloses a kind of preparation processes of Bee Pollen pollen crystalline substance, including one: weighing camellia pollen, fructus lycii pollen, motherwort pollen, Flos Rosae Rugosas pollen, milk powder, pumpkin powder, cocoa power, hydrophilic colloid, liquid component and additive；Two: removal camellia pollen, fructus lycii pollen, motherwort pollen, the impurity in Flos Rosae Rugosas pollen, and sterilize, dry, it carries out broken wall treatment and simultaneously collects；Three: the broken pollen being collected into being extracted with ethanol solution, with macroporous resin column to enrichment, and with ethanol elution, collection obtains mixture A；Step 4: milk powder, pumpkin powder, cocoa power supersonic jet mill are crushed, and mixing obtains mixture B；Step 5: mixing A is mixed with mixture B, hydrophilic colloid, liquid component and additive is added, loose crisp graininess finished product is made to get Bee Pollen pollen crystalline substance；The pollen crystalline substance nutritive value prepared through the invention is high, and nutritional ingredient is easily absorbed by the body, easy to carry, drink.
Description
Technical field
The present invention relates to food processing technology fields, are specifically related to a kind of preparation process of Bee Pollen pollen crystalline substance
Background technique
According to Historical Data Data About, Bee Pollen refers to the pollen load taken back when honeybee producting honey, in honeycomb after storage and fermentation
The pollen of formation.Bee Pollen is the male sex-cell in flowering plant stamen, it not only carries the hereditary information of life, and
And include complete nutrients matter necessary to breeding new life, basic, the source of thermal energy that is that plant is produced a male heir to continue the family line；Honeybee exists
When gathering honey, corbiculate leg can collect pollen, form pollen load, and after entering honeycomb, pollen load can be stored.Its main dietotherapy
Ingredient is: protein, amino acid, vitamin, Bee Pollen element, microelement, organized enzyme, flavone compound, lipid, nucleic acid,
Brassin, phytic acid etc..Wherein amino acid content and ratio be closest to FAO (Food and Agriculture Organization of the United Nation) recommendation amino acid pattern, this
It is extremely rare in wholefood.Concentrate composed by the substance that Bee Pollen is nutritious and drug effect is worth, it contains albumen
Matter, carbohydrate, minerals, vitamin and other active materials.Bee Pollen is both fabulous natural nutrient food, while
It is a kind of ideal invigorant, and there is certain medical function.
However, fresh Bee Pollen is not easy to maintain after collecting, within hot humid environment middle or short term will moldy metamorphism, room temperature
Wherein content of microorganisms also will increase long-term preservation；In addition, content of cellulose is high in pollen wall, not readily dissolve, influences in water
The mouthfeel and absorption of human body of pollen.
Summary of the invention
For the above technical problems, that the present invention provides manufacture crafts is simple, nutritive value is high, easy absorption is convenient for
The preparation process of the Bee Pollen pollen crystalline substance of carrying.
The technical solution of the present invention is as follows: a kind of preparation process of Bee Pollen pollen crystalline substance, comprising the following steps:
Step 1: it weighs respectively by weight: 28-45 parts of camellia pollen, 5-15 parts of fructus lycii pollen, motherwort pollen 8-14
Part, 2-3 parts of Flos Rosae Rugosas pollen, 10-18 parts of milk powder, 8-15 parts of pumpkin powder, 5-12 parts of cocoa power, 14-25 parts of hydrophilic colloid, liquid at
Divide 40-60 points, 0.1-0.2 parts of additive；
Wherein, hydrophilic colloid be selected from locust bean gum, carrageenan, gum arabic, guar gum, pectin and agar or this
The combination of a little components；The mixture that liquid component is made of by a certain percentage water, milk, syrup；The syrup is selected from high fruit
Any one in sugared corn syrup, sugar beet molasses, isomerized corn syrups or 50 type syrup or two or more any combination；
Step 2: removing above-mentioned camellia pollen, fructus lycii pollen, motherwort pollen, the impurity in Flos Rosae Rugosas pollen respectively, and with micro-
Wave device is sterilized, is dried, dry to be lower than 3% to moisture content, and the pollen after drying is then put into supercritical carbon dioxide
In extraction equipment, broken wall treatment is carried out；Wherein, controlling carbon dioxide temperature in extraction equipment is 25-36 DEG C, pressure 40-
75MPa, processing time are 15-30min, then empty the carbon dioxide in extraction equipment, collect broken pollen；
Step 3: the broken pollen that step 2 is collected into being extracted with ethanol solution respectively, obtains ethanol extract,
Then ethanol extract is enriched with non-polar macroporous resin column, and is eluted with ethyl alcohol, collect alcohol elution,
Concentration, dry, mixing, obtain mixed extract A, spare；
Step 4: milk powder, pumpkin powder, the cocoa power in step 1 through supersonic jet mill are respectively crushed into particle
Superfine powder less than 10 microns is uniformly mixed through the continuous mixing device of vertical multiscrew, obtains mixture B, spare；
Step 5: mixed extract A is mixed with mixture B, and above-mentioned hydrophilic colloid, liquid component, additional is added
Agent simultaneously stirs evenly, and the particle that partial size is 20-25 mesh is made with granulator, finally freezes under-10-- 50 DEG C of temperature
It is 120-150 minutes dry, it is brilliant to get Bee Pollen pollen that loose crisp graininess finished product is made.
Further, in step 1, adding agent is CBD, and CBD has the function of improving sleep quality, loosens body and mind.
Further, in step 2, supercritical carbon dioxide extraction apparatus addition has 0.03-0.06 parts of wall breaking enzymes, broken wall
Enzyme is any one in glycosidase, protease and peptase or any two or three of mixture；Glycosidase, protease and peptase
It can act on the corresponding macromolecular substances at pollen wall surface and germinal aperature, promote the release of germinal aperature opening and content,
With high efficiency.
Further, in step 3, when being extracted with ethanol solution to broken pollen, broken pollen is taken to be added 9-20 times
The volume fraction of amount is to impregnate 3-8 days under the conditions of 18-42 DEG C in the ethanol water of 45-60%, filters and extracts up to ethyl alcohol
Object；
Further, in step 3, tool that non-polar macroporous resin column is enriched with the effective component in broken pollen
Gymnastics conduct: after ethanol extract is splined on non-polar macroporous resin column, removal of impurities is first eluted with water, then be with volume fraction
The ethanol water of 30%-85% elutes non-polar macroporous resin column, and concentration, dry, mixing obtain mixed extract A.
Further, in step 5, in pelletization, into granulator be added 0.15-0.2 parts of binders, binder by
Dehydrated alcohol and pure water are mixed according to the ratio of 1:3.
Further, in step 4, the vertical continuous mixing device of multiscrew includes support frame, blending bunker, blender, blanking
Storehouse；Blending bunker setting runs through the upper surface of support frame in support frame lower end, blending bunker, and blending bunker lower end is provided with collection port, mixes
Glassware is movably arranged on inside blending bunker, and there are three blanking storehouses, and three blanking storehouses are uniformly arranged on the upper surface of support frame, and three
The blanking port in a blanking storehouse and blending bunker penetrate through, and are provided with screw feeder inside three blanking storehouses, and three blanking storehouses are fallen
Be provided with charging in material mouth and adjust plate, three blanking storehouses are respectively used to place milk powder, pumpkin powder and cocoa power, blender and
Screw feeder is powered by external power supply.
Further, before step 2, the ozone that concentration is 45ug/ml is injected in pure water, according to mass ratio 1:3 points
Camellia pollen, fructus lycii pollen, motherwort pollen are not added in pure water, stir evenly to obtain pollen liquid；Then filter pair is used
Pollen liquid is filtered, and obtains filtering pollen liquid；Finally filtering pollen liquid is separated using spiral discharge sedimentation centrifuge, is arranged
Sewage after separating out, obtains pure pollen.
Compared with prior art, beneficial effects of the present invention: the present invention will be prepared into flower through processing after fresh pollen broken wall
Powder crystal, then other auxiliary materials are equipped with, not only nutritive value is high, and nutritional ingredient is easy to be absorbed by the body, is also convenient for carrying, drink；It is broken
The addition of wall enzyme, the fermentation enzymatic hydrolysis broken wall method rate of breaking pollen wall substantially increased, it is intact that nutriment loses small and vital preservation；
Any food additives are not added in pollen crystalline substance preparation process, improve foodsafety；Use non-polar macroporous resin column pair
Effective component in broken pollen is enriched with, and is eluted using ethanol solution to non-polar macroporous resin column, is collected broken
Effective component in wall pollen, the loss of nutritional ingredient in limited reduction pollen, improves the nutritive value of pollen crystalline substance.
Detailed description of the invention
Fig. 1 is the structural schematic diagram of the continuous mixing device of vertical multiscrew of the invention；
Fig. 2 is the top view of the continuous mixing device of vertical multiscrew of the invention；
Wherein, 1- support frame, 2- blending bunker, 20- collection port, 3- blender, 4- blanking storehouse, 40- screw feeder, 41-
Charging adjusts plate.
The major function for constituting the various raw materials of the present invention is as follows:
Camellia pollen: the effect of camellia pollen the glamour and drug effect intrinsic from camellia pollen, camellia pollen can remain good new
Old metabolism keeps skin gloss.It is water-soluble that the effect of camellia pollen, which promotes the vitamin b it is ensured that human body abundance, vitamin b,
Vitamin adjusts metabolism, maintains the health of skin and muscle, promotes the function of immune system and nervous system, promotes thin
Intracellular growth and division.The effect of camellia pollen, which can also be that you are younger, more beautiful, makes you confident；Camellia pollen is rich in protein,
Amino acid, fatty acid, vitamin, a variety of effective active compositions such as organized enzyme, wherein protein, the content of amino acid are eggs,
5-7 times of milk is referred to as complete protein in nutrition；Unsaturated fatty acid in fatty acid is more than other dynamic plants
The content of object is high, there are also it is several be essential fatty acid that human body cannot synthesize；Vitamin content is most, tea with b family vitamin
Pollen can make adipose conversion into energy and be used；Tea flower pollen is king of pollen；Camellia pollen to beauty, cut down fat,
Functions of removing chloasma, acne have special effect, and can delay senescence, and Chinese red, smell faint scent is slightly sweet palatable, amino acid, vitamin and micro
Constituent content is high, and wherein amino acid content is first of pollen, and trace element manganese, cobalt, inscription and Nicotinic Acid Content are than common pollen
It is high.It therefore is health care and the preferred pollen of medical treatment.Pollen is to heart disease, diabetes, hepatitis, constipation, dysentery, enteritis, difficult urination, water
Swollen, neurasthenia and prostatitis etc. have good therapeutic effect；Tumour, artery sclerosis, old silly can also be prevented and treated
Slow-witted, children mental retardation, endocrine disorder etc.；To prevention and treatment artery sclerosis, enhancing myocardial contraction, accelerate heart rate, the myocardium function of improvement
Energy etc. is effectively.
Fructus lycii pollen: the ingredient of fructus lycii pollen is very complicated, mainly contains: protein 20%-25%, total amino acid content 20%
More than, free amino acid 1%-2%, carbohydrate 40%-50%, lipid 5%-10%；It is vitamin also rich in, micro-
A variety of nutriments such as secondary element, enzyme, nucleic acid, hormone, the nutritional ingredient isolated now through scientific research is just up to more than 200 kinds, also
It is not recognized by people there are many effective component.Fructus lycii carrotene rich in, vitamin B1, vitamin B2, Ni Ke
A variety of beautifying face and moisturizing skins such as acid, vitamin C, vitamin E, a variety of amino acid, linoleic acid, glycine betaine, iron, potassium, zinc, calcium, phosphorus, selenium at
Point；Abundant carrotene, vitamin B1, vitamin B2, vitamin C, calcium, iron for containing etc. are the required nutrition of healthy eye；
Containing a variety of unsaturated fatty acids of glycine betaine, glycine betaine can inhibit fat in intrahepatic deposition, prevent cirrhosis, to protection normal hepatocytes
Cell has effect；Fructus lycii also has certain effect to reducing blood lipid, blood glucose；Fructus lycii has enhancing body's immunity, enhances body
Resistance promotes the new life of cell, reduces blood middle cholesterol content, and anti arteriosclerosis improves skin elasticity, anti-internal organs and skin
The effects of aging, delaying skin wrinkle.Fructus lycii is a kind of worth big numerous health foods eaten, and energy enriching yin improving eyesight kidney tonifying is healthy and strong,
Informal dress fructus lycii can cure smelting rheumatalgia with strengthening muscles and bones；Blood circulation can be improved again, improve body adaptation power.And fructus lycii is most people
The curative effect taken delight in talking about, in the function of its beauty treatment, informal dress has the effect of skin whitening, improving eyesight and quiet nerves, or even is considered to make us long-lived
It makes light of one's life by commiting suicide.Fructus lycii bitter is cold in nature, there is the effect of cool blood, if fruit has cough with lung heat's even blood-stained sputum, fructus lycii cooking, which takes, can play smelting
Treatment effect.
Motherwort pollen: motherwort pollen is to enshrine and worship acquire various flowers and plants, look over so as to check, the essence on the flowers stamen such as medicinal material,
Also known as all sorts of flowers essence, it is valuable crude drug.The pollen of different plants, color also have difference.Taste slightly sweet tea, a small number of bitternesses.Melissa
Powder is the substance with high activity high-quality, and non-broken pollen ingredient is not easy to be destroyed, and is easily absorbed by the human body, quality is better than broken wall
Pollen.It is full of nutrition, charming inexpensive beauty and health care good merchantable brand.Bee Pollen contains various nutriments required for living organism
And abundant bioactive substance, there is stronger anti-aging, builds up health, eliminate fatigue, improve immunity of organisms effect.Foreign countries are permitted
The person of doing more physical exercises often eats pollen, and pollen is formally set to the health food of China sportsman by the State Physical Culture and Sports Commission.
Specific embodiment
A kind of embodiment 1: preparation process of Bee Pollen pollen crystalline substance, comprising the following steps:
Step 1: it weighs respectively by weight: 28 parts of camellia pollen, 5 parts of fructus lycii pollen, 8 parts of motherwort pollen, rose
2 parts of powder, 10 parts of milk powder, 8 parts of pumpkin powder, 5 parts of cocoa power, 14 parts of hydrophilic colloid, 40 parts of liquid component, 0.1 part of additive；Its
In, adding agent is CBD, and CBD has the function of improving sleep quality, loosens body and mind；
Wherein, hydrophilic colloid be selected from locust bean gum, carrageenan, gum arabic, guar gum, pectin and agar or this
The combination of a little components；The mixture that liquid component is made of by a certain percentage water, milk, syrup；It is beautiful that syrup is selected from high fructose
Rice syrup；
Step 2: removing above-mentioned camellia pollen, fructus lycii pollen, motherwort pollen, the impurity in Flos Rosae Rugosas pollen respectively, and with micro-
Wave device is sterilized, is dried, and drying to moisture content is 2%, and the pollen after drying is then put into supercritical carbon dioxide extraction
It takes in device, carries out broken wall treatment；Wherein, controlling carbon dioxide temperature in extraction equipment is 25 DEG C, pressure 40MPa, processing
Time is 15min, then empties the carbon dioxide in extraction equipment, collects broken pollen；
Step 3: the broken pollen that step 2 is collected into is extracted with ethanol solution respectively, and broken pollen is taken to be added 9
It in the ethanol water that the volume fraction of amount is 45% again, impregnates 3 days, is filtered up to ethanol extract under the conditions of 18 DEG C；It will
After ethanol extract is splined on non-polar macroporous resin column, removal of impurities, then the ethanol water for being 30% with volume fraction is first eluted with water
Solution elutes non-polar macroporous resin column, collects alcohol elution, and concentration, dry, mixing obtain mixed extract A, spare；
Step 4: milk powder, pumpkin powder, the cocoa power in step 1 through supersonic jet mill are respectively crushed into particle
For 9 microns of superfine powder, it is uniformly mixed through the continuous mixing device of vertical multiscrew, obtains mixture B, it is spare；
Step 5: mixed extract A is mixed with mixture B, hydrophilic colloid, liquid component and additive in addition
And stir evenly, the particle that partial size is 20 mesh is made with granulator, 120 points are finally freeze-dried under -50 DEG C of temperature
It is brilliant to get Bee Pollen pollen that loose crisp graininess finished product is made in clock.
A kind of embodiment 2: preparation process of Bee Pollen pollen crystalline substance, comprising the following steps:
Step 1: it weighs respectively by weight: 36 parts of camellia pollen, 9 parts of fructus lycii pollen, 10 parts of motherwort pollen, rose
2 parts of pollen, 15 parts of milk powder, 13 parts of pumpkin powder, 9 parts of cocoa power, 18 parts of hydrophilic colloid, 45 parts of liquid component, 0.15 part of additive；
Wherein, adding agent is CBD, and CBD has the function of improving sleep quality, loosens body and mind；
Hydrophilic colloid is selected from locust bean gum, carrageenan, gum arabic, guar gum, pectin and agar or these groups
The combination divided；The mixture that liquid component is made of by a certain percentage water, milk, syrup；Syrup is selected from sugar beet molasses；
Step 2: removing above-mentioned camellia pollen, fructus lycii pollen, motherwort pollen, the impurity in Flos Rosae Rugosas pollen respectively, and with micro-
Wave device is sterilized, is dried, dry to moisture content position 1%, and the pollen after drying is then put into supercritical carbon dioxide extraction
It takes in device, carries out broken wall treatment；Wherein, controlling carbon dioxide temperature in extraction equipment is 30 DEG C, pressure 58MPa, processing
Time is 22min, then empties the carbon dioxide in extraction equipment, collects broken pollen, supercritical carbon dioxide extraction apparatus
Addition has 0.05 part of wall breaking enzyme, and wall breaking enzyme is glycosidase；Glycosidase can act on corresponding at pollen wall surface and germinal aperature
Macromolecular substances promote the release of germinal aperature opening and content, have high efficiency；
Step 3: the broken pollen that step 2 is collected into is extracted with ethanol solution respectively, broken pollen is taken to be added
It in the ethanol water that the volume fraction of 15 times of amounts is 52%, impregnates 6 days, is filtered up to ethanol extract under the conditions of 31 DEG C；
After ethanol extract is splined on non-polar macroporous resin column, removal of impurities, then the ethyl alcohol for being 56% with volume fraction is first eluted with water
Aqueous solution elutes non-polar macroporous resin column, collects alcohol elution, and concentration, dry, mixing obtain mixed extract A, standby
With；
Step 4: milk powder, pumpkin powder, the cocoa power in step 1 through supersonic jet mill are respectively crushed into particle
For 7 microns of superfine powder, it is uniformly mixed through the continuous mixing device of vertical multiscrew, obtains mixture B, it is spare；
Step 5: mixed extract A is mixed with mixture B, and above-mentioned hydrophilic colloid, liquid component and additional is added
Agent simultaneously stirs evenly, and the particle that partial size is 23 mesh is made with granulator, is finally freeze-dried 136 under -35 DEG C of temperature
Minute, it is brilliant to get Bee Pollen pollen that loose crisp graininess finished product is made.
A kind of embodiment 3: preparation process of Bee Pollen pollen crystalline substance, comprising the following steps:
Step 1: it weighs respectively by weight: 45 parts of camellia pollen, 15 parts of fructus lycii pollen, 14 parts of motherwort pollen, rose
3 parts of pollen, 18 parts of milk powder, 15 parts of pumpkin powder, 12 parts of cocoa power, 19 parts of hydrophilic colloid, liquid component 60 divide, 0.2 part of additive；
Wherein, adding agent is CBD, and CBD has the function of improving sleep quality, loosens body and mind；
Hydrophilic colloid is selected from locust bean gum, carrageenan, gum arabic, guar gum, pectin and agar or these groups
The combination divided；The mixture that liquid component is made of by a certain percentage water, milk, syrup；Syrup is selected from isomerized corn sugar
Slurry；
Step 2: removing above-mentioned camellia pollen, fructus lycii pollen, motherwort pollen, the impurity in Flos Rosae Rugosas pollen respectively, and with micro-
Wave device is sterilized, is dried, and drying to moisture content is 2%, and the pollen after drying is then put into supercritical carbon dioxide extraction
It takes in device, carries out broken wall treatment；Wherein, controlling carbon dioxide temperature in extraction equipment is 36 DEG C, pressure 75MPa, processing
Time is 30min, then empties the carbon dioxide in extraction equipment, collects broken pollen, supercritical carbon dioxide extraction apparatus
Addition has 0.06 part of wall breaking enzyme, and wall breaking enzyme is the mixture of glycosidase and protease；Glycosidase and protease can act on flower
Corresponding macromolecular substances at powder wall surface and germinal aperature promote the release of germinal aperature opening and content, have high efficiency；
Step 3: the broken pollen that step 2 is collected into is extracted with ethanol solution respectively, broken pollen is taken to be added
It in the ethanol water that the volume fraction of 20 times of amounts is 60%, impregnates 8 days, is filtered up to ethanol extract under the conditions of 42 DEG C；
After ethanol extract is splined on non-polar macroporous resin column, removal of impurities, then the ethyl alcohol for being 85% with volume fraction is first eluted with water
Aqueous solution elutes non-polar macroporous resin column, collects alcohol elution, and concentration, dry, mixing obtain mixed extract A, standby
With；
Step 4: milk powder, pumpkin powder, the cocoa power in step 1 through supersonic jet mill are respectively crushed into particle
For 8 microns of superfine powder, it is uniformly mixed through the continuous mixing device of vertical multiscrew, obtains mixture B, it is spare；
Step 5: mixed extract A is mixed with mixture B, and above-mentioned hydrophilic colloid, liquid component and additional is added
Agent simultaneously stirs evenly, and partial size is made as the particle of 25 mesh with granulator, in pelletization, 0.2 part of bonding is added into granulator
Agent, binder are mixed by dehydrated alcohol and pure water according to the ratio of 1:3；Finally freezed under -25 DEG C of temperature
It is 150 minutes dry, it is brilliant to get Bee Pollen pollen that loose crisp graininess finished product 3% is made.
A kind of embodiment 4: preparation process of Bee Pollen pollen crystalline substance, comprising the following steps:
Step 1: it weighs respectively by weight: 28 parts of camellia pollen, 5 parts of fructus lycii pollen, 8 parts of motherwort pollen, rose
2 parts of powder, 10 parts of milk powder, 8 parts of pumpkin powder, 5 parts of cocoa power, 19 parts of hydrophilic colloid, 50 parts of liquid component, 0.2 part of additive；Its
In, adding agent is CBD, and CBD has the function of improving sleep quality, loosens body and mind；
Wherein, hydrophilic colloid be selected from locust bean gum, carrageenan, gum arabic, guar gum, pectin and agar or this
The combination of a little components；The mixture that liquid component is made of by a certain percentage water, milk, syrup；Syrup is selected from high 50 type sugar
Slurry；
Step 2: removing above-mentioned camellia pollen, fructus lycii pollen, motherwort pollen, the impurity in Flos Rosae Rugosas pollen respectively, and with micro-
Wave device is sterilized, is dried, and drying to moisture content is 2%, and the pollen after drying is then put into supercritical carbon dioxide extraction
It takes in device, carries out broken wall treatment；Wherein, controlling carbon dioxide temperature in extraction equipment is 25 DEG C, pressure 40MPa, processing
Time is 15min, then empties the carbon dioxide in extraction equipment, collects broken pollen, supercritical carbon dioxide extraction apparatus
Addition has 0.03 part of wall breaking enzyme, and wall breaking enzyme is the mixture of glycosidase, protease and peptase；Glycosidase, protease and peptase energy
The corresponding macromolecular substances at pollen wall surface and germinal aperature are enough acted on, the release of germinal aperature opening and content, tool are promoted
There is high efficiency；
Step 3: the broken pollen that step 2 is collected into is extracted with ethanol solution respectively, and broken pollen is taken to be added 9
It in the ethanol water that the volume fraction of amount is 45% again, impregnates 3 days, is filtered up to ethanol extract under the conditions of 18 DEG C；It will
After ethanol extract is splined on non-polar macroporous resin column, removal of impurities, then the ethanol water for being 30% with volume fraction is first eluted with water
Solution elutes non-polar macroporous resin column, collects alcohol elution, and concentration, dry, mixing obtain mixed extract A, spare；
Step 4: the milk powder in step 1, pumpkin powder, cocoa powder are respectively crushed into through supersonic jet mill
The superfine powder that grain is 6 microns is uniformly mixed through the continuous mixing device of vertical multiscrew, obtains mixture B, spare；
Step 5: mixed extract A is mixed with mixture B, and above-mentioned hydrophilic colloid, liquid component and additional is added
Agent simultaneously stirs evenly, and partial size is made as the particle of 20 mesh with granulator, in pelletization, 0.15 part of bonding is added into granulator
Agent, binder are mixed by dehydrated alcohol and pure water according to the ratio of 1:3；Finally freezed under -15 DEG C of temperature
It is 120 minutes dry, it is brilliant to get Bee Pollen pollen that loose crisp graininess finished product is made.
A kind of embodiment 5: preparation process of Bee Pollen pollen crystalline substance, comprising the following steps:
Step 1: it weighs respectively by weight: 45 parts of camellia pollen, 15 parts of fructus lycii pollen, 14 parts of motherwort pollen, rose
3 parts of pollen, 18 parts of milk powder, 15 parts of pumpkin powder, 12 parts of cocoa power, 22 parts of hydrophilic colloid, 55 parts of liquid component, 0.2 part of additive；
Wherein, adding agent is CBD, and CBD has the function of improving sleep quality, loosens body and mind；The ozone that concentration is 45ug/ml is injected pure
In water purification, camellia pollen, fructus lycii pollen, motherwort pollen are added in pure water respectively according to mass ratio 1:3, stir evenly colored
Powder liquid；Then pollen liquid is filtered using filter, obtains filtering pollen liquid；Finally use spiral discharge sedimentation centrifuge pair
Filtering pollen liquid is separated, and the sewage after discharge separation obtains pure pollen；Wherein, adding agent is CBD, and CBD, which has to improve, to sleep
Quality, the effect for loosening body and mind；
Wherein, hydrophilic colloid be selected from locust bean gum, carrageenan, gum arabic, guar gum, pectin and agar or this
The combination of a little components；The mixture that liquid component is made of by a certain percentage water, milk, syrup；It is beautiful that syrup is selected from high fructose
Rice syrup, sugar beet molasses, isomerized corn syrups and 50 type syrup composition；
Step 2: remove respectively above-mentioned camellia pollen, fructus lycii pollen, in motherwort pollen, the impurity of Flos Rosae Rugosas pollen, and with micro-
Wave device is sterilized, is dried, dry to moisture content to 2%, and the pollen after drying is then put into supercritical carbon dioxide extraction
It takes in device, carries out broken wall treatment；Wherein, controlling carbon dioxide temperature in extraction equipment is 36 DEG C, pressure 75MPa, processing
Time is 30min, then empties the carbon dioxide in extraction equipment, collects broken pollen, supercritical carbon dioxide extraction apparatus
Addition has 0.06 part of wall breaking enzyme, and wall breaking enzyme is the mixture of glycosidase, protease and peptase；Glycosidase, protease and peptase energy
The corresponding macromolecular substances at pollen wall surface and germinal aperature are enough acted on, the release of germinal aperature opening and content, tool are promoted
There is high efficiency；
Step 3: the broken pollen that step 2 is collected into is extracted with ethanol solution respectively, broken pollen is taken to be added
It in the ethanol water that the volume fraction of 20 times of amounts is 60%, impregnates 8 days, is filtered up to ethanol extract under the conditions of 42 DEG C；
After ethanol extract is splined on non-polar macroporous resin column, removal of impurities, then the ethyl alcohol for being 85% with volume fraction is first eluted with water
Aqueous solution elutes non-polar macroporous resin column, collects alcohol elution, and concentration, dry, mixing obtain mixed extract A, standby
With；
Step 4: milk powder, pumpkin powder, the cocoa power in step 1 through supersonic jet mill are respectively crushed into particle
For 5 microns of superfine powder, it is uniformly mixed through the continuous mixing device of vertical multiscrew, obtains mixture B, it is spare；
Step 5: mixed extract A is mixed with mixture B, and above-mentioned hydrophilic colloid, liquid component and additional is added
Agent simultaneously stirs evenly, and partial size is made as the particle of 25 mesh with granulator, in pelletization, 0.2 part of bonding is added into granulator
Agent, binder are mixed by dehydrated alcohol and pure water according to the ratio of 1:3；It is finally freezed under 40 DEG C of temperature dry
Dry 150 minutes, it is brilliant to get Bee Pollen pollen that loose crisp graininess finished product is made.
A kind of embodiment 6: preparation process of Bee Pollen pollen crystalline substance, comprising the following steps: step 1: distinguish by weight
Weigh: 45 parts of camellia pollen, 15 parts of fructus lycii pollen, 14 parts of motherwort pollen, 3 parts of Flos Rosae Rugosas pollen, 18 parts of milk powder, 15 parts of pumpkin powder,
12 parts of cocoa power, 18 parts of hydrophilic colloid, 55 parts of liquid component, 0.1 part of additive；Wherein, adding agent is CBD, and CBD, which has to improve, to sleep
Dormancy quality, the effect for loosening body and mind；The ozone that concentration is 45ug/ml is injected in pure water, according to mass ratio 1:3 respectively by tea
Pollen, fructus lycii pollen, motherwort pollen are added in pure water, stir evenly to obtain pollen liquid；Then using filter to pollen liquid
It is filtered, obtains filtering pollen liquid；Finally filtering pollen liquid is separated using spiral discharge sedimentation centrifuge, discharge separation
Sewage afterwards obtains pure pollen；
Wherein, hydrophilic colloid be selected from locust bean gum, carrageenan, gum arabic, guar gum, pectin and agar or this
The combination of a little components；The mixture that liquid component is made of by a certain percentage water, milk, syrup；It is beautiful that syrup is selected from high fructose
Rice syrup, sugar beet molasses, isomerized corn syrups and 50 type syrup composition；
Step 2: above-mentioned camellia pollen, fructus lycii pollen, the impurity in motherwort pollen are removed respectively, and is carried out with microwave device
Then pollen after drying is put into supercritical carbon dioxide extraction apparatus by sterilizing, drying, drying to moisture content to 2%,
Carry out broken wall treatment；Wherein, control extraction equipment in carbon dioxide temperature be 36 DEG C, pressure 75MPa, processing the time be
Then 30min empties the carbon dioxide in extraction equipment, collect broken pollen, and supercritical carbon dioxide extraction apparatus addition has
0.06 part of wall breaking enzyme, wall breaking enzyme are the mixture of glycosidase, protease and peptase；Glycosidase, protease and peptase can act on
Corresponding macromolecular substances at pollen wall surface and germinal aperature promote the release of germinal aperature opening and content, have efficient
Property；
Step 3: the broken pollen that step 2 is collected into is extracted with ethanol solution respectively, broken pollen is taken to be added
It in the ethanol water that the volume fraction of 20 times of amounts is 60%, impregnates 8 days, is filtered up to ethanol extract under the conditions of 42 DEG C；
After ethanol extract is splined on non-polar macroporous resin column, removal of impurities, then the ethyl alcohol for being 85% with volume fraction is first eluted with water
Aqueous solution elutes non-polar macroporous resin column, collects alcohol elution, and concentration, dry, mixing obtain mixed extract A, standby
With；
Step 4: milk powder, pumpkin powder, the cocoa power in step 1 through supersonic jet mill are respectively crushed into particle
For 6 microns of superfine powder, it is uniformly mixed through the continuous mixing device of vertical multiscrew, obtains mixture B, it is spare；Vertical multiscrew connects
Continuous mixing device includes support frame 1, blending bunker 2, blender 3, blanking storehouse 4；Blending bunker 2 is arranged in 1 lower end of support frame, blending bunker
2 run through the upper surface of support frame 1, and 2 lower end of blending bunker is provided with collection port 20, and blender 3 is movably arranged on inside blending bunker 2,
There are three blanking storehouses 4, and three blanking storehouses 4 are uniformly arranged on the upper surface of support frame 1, and the blanking port in three blanking storehouses 4 and mixed
Feed bin 2 penetrates through, and is provided with screw feeder 40 inside three blanking storehouses 4, be provided on the blanking port in three blanking storehouses 4 into
Material adjusts plate 41, and three blanking storehouses 4 are respectively used to place milk powder, pumpkin powder and cocoa power, blender 3 and screw feeder 40
It is powered by external power supply；
Step 5: mixed extract A is mixed with mixture B, and above-mentioned hydrophilic colloid, liquid component and additional is added
Agent simultaneously stirs evenly, and partial size is made as the particle of 25 mesh with granulator, in pelletization, 0.2 part of bonding is added into granulator
Agent, binder are mixed by dehydrated alcohol and pure water according to the ratio of 1:3；It is finally freezed under 40 DEG C of temperature dry
Dry 150 minutes, it is brilliant to get Bee Pollen pollen that loose crisp graininess finished product is made.
Finally, it should be noted that the above embodiments are merely illustrative of the technical solutions of the present invention, rather than its limitations；Although
Present invention has been described in detail with reference to the aforementioned embodiments, those skilled in the art should understand that: it still may be used
To modify to technical solution documented by previous embodiment or equivalent replacement of some of the technical features；And
These are modified or replaceed, the spirit and model of technical solution of the embodiment of the present invention that it does not separate the essence of the corresponding technical solution
It encloses.
Claims (8)
1. a kind of preparation process of Bee Pollen pollen crystalline substance, which comprises the following steps:
Step 1: weigh respectively by weight: 28-45 parts of camellia pollen, 5-15 parts of fructus lycii pollen, 8-14 parts of motherwort pollen,
2-3 parts of Flos Rosae Rugosas pollen, 10-18 parts of milk powder, 8-15 parts of pumpkin powder, 5-12 parts of cocoa power, 14-25 parts of hydrophilic colloid, liquid component
40-60 points, 0.1-0.2 parts of additive；
Wherein, the hydrophilic colloid be selected from locust bean gum, carrageenan, gum arabic, guar gum, pectin and agar or this
The combination of a little components；The mixture that the liquid component is made of by a certain percentage water, milk, syrup；The syrup is selected from
In high-fructose corn syrup, sugar beet molasses, isomerized corn syrups or 50 type syrup any one or it is two or more any
Combination；
Step 2: above-mentioned camellia pollen, fructus lycii pollen, motherwort pollen, the impurity in Flos Rosae Rugosas pollen are removed respectively, and uses microwave device
It sterilized, dried, it is dry to be lower than 3% to moisture content, the pollen after drying is then put into supercritical carbon dioxide extracting
In device, broken wall treatment is carried out；Wherein, controlling carbon dioxide temperature in extraction equipment is 25-36 DEG C, pressure 40-75MPa,
The processing time is 15-30min, then empties the carbon dioxide in extraction equipment, collects broken pollen；
Step 3: the broken pollen that step 2 is collected into is extracted with ethanol solution respectively, obtains ethanol extract, then
The ethanol extract is enriched with non-polar macroporous resin column, and is eluted with ethyl alcohol, alcohol elution is collected,
Concentration, dry, mixing, obtain mixed extract A, spare；
Step 4: milk powder, pumpkin powder, the cocoa power in step 1 are respectively crushed into particle through supersonic jet mill and are less than
10 microns of superfine powder is uniformly mixed through the continuous mixing device of vertical multiscrew, obtains mixture B, spare；
Step 5: mixed extract A is mixed with mixture B, above-mentioned hydrophilic colloid, liquid component, additive is added simultaneously
Stir evenly, the particle that partial size is 20-25 mesh be made with granulator, finally-10-- 50 DEG C at a temperature of be freeze-dried 120-
150 minutes, loose crisp graininess finished product is made, the as described Bee Pollen pollen is brilliant.
2. a kind of preparation process of Bee Pollen pollen crystalline substance according to claim 1, which is characterized in that in the step 1,
Additive is CBD.
3. a kind of preparation process of Bee Pollen pollen crystalline substance according to claim 1, which is characterized in that in the step 2,
Supercritical carbon dioxide extraction apparatus addition has 0.03-0.06 parts of wall breaking enzymes, and the wall breaking enzyme is glycosidase, protease and peptase
In any one or any two or three of mixture.
4. a kind of preparation process of Bee Pollen pollen crystalline substance according to claim 1, which is characterized in that in the step 3,
When being extracted with ethanol solution to broken pollen, take broken pollen that the second that the 9-20 times of volume fraction measured is 45-60% is added
It in alcohol solution, impregnates 3-8 days, is filtered up to ethanol extract under the conditions of 18-42 DEG C.
5. a kind of preparation process of Bee Pollen pollen crystalline substance according to claim 1, which is characterized in that in the step 3,
The concrete operations that non-polar macroporous resin column is enriched with the effective component in broken pollen are as follows: be splined on ethanol extract
After non-polar macroporous resin column, removal of impurities is first eluted with water, then the ethanol water for being 30%-85% with volume fraction elutes non-pole
Property macroporous resin column, concentration, dry, mixing obtain mixed extract A.
6. a kind of preparation process of Bee Pollen pollen crystalline substance according to claim 1, which is characterized in that in the step 5,
In pelletization, 0.15-0.2 parts of binders are added into granulator, the binder is by dehydrated alcohol and pure water according to 1:3
Ratio mix.
7. a kind of preparation process of Bee Pollen pollen crystalline substance according to claim 1, which is characterized in that in the step 5,
In pelletization, 0.25-0.40 parts of binders are added into granulator, the binder is by dehydrated alcohol and pure water according to 3:
1 ratio mixes.
8. a kind of preparation process of Bee Pollen pollen crystalline substance according to claim 1, which is characterized in that described in step 4
The vertical continuous mixing device of multiscrew includes support frame (1), blending bunker (2), blender (3), blanking storehouse (4)；The blending bunker
(2) setting runs through the upper surface of support frame (1) in support frame (1) lower end, blending bunker (2), and blending bunker (2) lower end is provided with collection
Mouth (20), the blender (3) are movably arranged on blending bunker (2) inside, and there are three the blanking storehouses (4), three blanking storehouses (4)
It is uniformly arranged on the upper surface of support frame (1), and the blanking port of three blanking storehouses (4) and blending bunker (2) penetrate through, three blanking storehouses
(4) internal to be provided with screw feeder (40), it is provided with charging on the blanking port of three blanking storehouses (4) and adjusts plate
(41), three blanking storehouses (4) are respectively used to place milk powder, pumpkin powder and cocoa power, and blender (3) and screw feeder (40) are equal
It is powered by external power supply.
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN112322465A (en) * | 2020-10-22 | 2021-02-05 | 何申明 | A quantitative charging equipment for maize production lysine |
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