CN109735404A - A kind of solid detergent composition and preparation method thereof containing purple common perilla seed - Google Patents
A kind of solid detergent composition and preparation method thereof containing purple common perilla seed Download PDFInfo
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- CN109735404A CN109735404A CN201910026312.2A CN201910026312A CN109735404A CN 109735404 A CN109735404 A CN 109735404A CN 201910026312 A CN201910026312 A CN 201910026312A CN 109735404 A CN109735404 A CN 109735404A
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- perilla seed
- common perilla
- detergent composition
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Abstract
The present invention relates to daily chemicals fields, disclose a kind of solid detergent composition containing purple common perilla seed, including following mass percent component: filler 10-60%；Anionic surfactant 5-20%；Nonionic surfactant 1-5%；Adhesive 1-20%；Conditioner 1-5%；Surplus is deionized water.The invention also discloses preparation methods.Present invention application purple common perilla seed alleviates the unhealthy situation of skin, it goes to reduce cleaning compositions after washing to skin bring stimulation by the reasonably combined reduction of different surfaces activating agent and conditioner, to play the role of delaying inflammation, improve skin appearance.
Description
Technical field
The present invention relates to daily chemicals fields, and in particular to a kind of solid detergent composition and its preparation containing purple common perilla seed
Method.
Background technique
The purpose of Cleaning preparations is the dirt removed in target.It can make skin refreshing on skin, help to protect skin
Skin normal physiological condition.When cleaning hair, sebum on the dirt and scalp being adhered to above hair can be cleaned and cuticula is broken
Piece and its oxygenolysis object keep hair clean and tidy and scalp health.These residual metabolins can breed bacterium, and various physics occur
Chemistry and biological respinse form some possible harmful substances.In order to guarantee health, there are many washing systems of type on the market
Product are broadly divided into: surfactant is matrix clean skin product, solvent borne clean skin product and other products.Most commercial
Cleaning preparations be flowing product volume big squash type tube body packaging, and different type is prepared according to different seasons
Cleaning preparations, cause outgoing to carry puzzlement inconvenient to use.Certainly also there are the solid Cleaning preparations being convenient for carrying, it is such as fragrant
Soap, but perfumed soap is the product reused, and pollution soap body is easy after being used for multiple times, breeds bacterium.Such issues that in order to solve,
Also occurs the clean skin product being convenient for carrying in the market.
Similar, number of patent application is that CN201510916838.X and CN201611260357.9 discloses a kind of novel cleaning
Face composition and its finished product preparation method, the combination mainly use starch, volcanic ash, diatomite, amino acid surfactant
It is added in molding machine and is shaped to pelletiod, by semi-finished product after molding in 50-60 DEG C of baking 4-5h.
Although such product use easy to carry, these can not provide abundant exquisiteness using the product of much starch
Foam if wanting to generate foam abundant, and has used a large amount of surfactant, has kept skin tight, and effect is single, and hardness
It is not strong, crushing is be easy to cause in transport.
Present most of cleaning products have used a large amount of surfactant plus external condition to reach abundant foam
Influence, to generate biggish irritation to skin.Although most of product be by be added a large amount of moisturizer it is anti-or
Scorching agent goes to achieve the purpose that make skin not tight not red and swollen, but the dosage of surfactant of its chemical industry synthesis is still in compared with Gao Shui
Standard, therefore be unfavorable for reducing the irritation of detergent itself.
Summary of the invention
It is an object of the invention to pass through the collocation and raw material key parameter limitation offer one to composition system structure
The preparation method of kind purple common perilla seed, and contain purple common perilla seed, it is convenient for carrying, with different function, it is easy to rinse
With foaming abundancy it is fine and smooth and be not easy the solid detergent composition crushed in transport, to reduce cleaning compositions after washing
Improve skin appearance to play the role of delaying inflammation to skin bring stimulation.
Technical scheme is as follows:
A kind of solid detergent composition containing purple common perilla seed, including following mass percent component:
Filler 10-60%；
Anionic surfactant 5-20%；
Nonionic surfactant 1-5%；
Adhesive 1-20%；
Conditioner 1-5%；-
Surplus is deionized water.Solid detergent composition of the present invention containing purple common perilla seed can also add mass percent
The preservative of 0.01-1%, preservative include K-2000, Kathon CG, benzoic acid, benzyl alcohol, parabens, imidazolidinyl ureas,
At least one of polyalcohols.It is preferred that one or both of Phenoxyethanol and Sensiva SC50 combine.
Further, anionic surfactant includes high carboxylic acid's salt, sulfonate, sulfuric acid, phosphate ester salt, fat
At least one of acyl-peptide condensation product.
Further, nonionic surfactant includes alkyl phenol polyoxyethylene ether, high-carbon fatty alcohol polyoxyethylene ether, rouge
Fat acid polyoxyethylene ester, fatty acid methyl ester ethoxylate, the ethylene oxide adduct of polypropylene glycol, polyoxyethylated ion
At least one of type surfactant, sorbitan ester, sucrose ester, alkylolamides type, alkyl heteroside.From to compounding
From the point of view of system makees mild cosurfactant and raising foam performance, optimizing alkyl heteroside of the present invention.
Further, adhesive includes organic synthetic polymer acrylic polymer and its derivative and organic
Semi-synthetic water-soluble polymer.
Further, filler includes modified starch.The preferred hydroxypropyl cellulose of filler, microcrystalline cellulose and modification
The combination of one or more of cornstarch.
Further, conditioner include glycerol, propylene glycol, 1,3-BDO, amides moisturizer, lactic acid and sodium lactate,
Pyrrolidone sodium carboxylate, polyethylene glycol, poly ethyldiol modified glyceride type, olive oil derivative, in ionic moisturizer
It is at least one.Preferably at least containing 1,3-BDO, poly ethyldiol modified glyceride type, olive oil derivative and polyethylene glycol
One or more combination.
Further, it is R-O(CH that anionic surfactant, which includes general formula,2-CH2O) n-CH2High carboxylic acid's salt of COOX
With at least one of N- fatty acyl group glutamate, fatty acyl group glycinate.The wherein alkane of the preferred 12-18 of the R of high carboxylic acid's salt
Base, X preferred as alkali potassium, the alkyl carboxylic acid potassium of 12-18 have a good foam, excellent cleaning capacity, but mildness compared with
Difference can improve its usage experience sense, generate rich by being compounded with mild surfactant fatty acyl-peptide condensation product
Rich fine and smooth foam.
Further, organic synthesis water-soluble polymer acrylic polymer and its derivative include acroleic acid polymerization
Object, 600 series polypropylenes acid resin of Carbopol, acrylic acid/sodium acrylate polymer, acrylate/C10-30 alkyl
Acid esters cross-linked polymer, acrylates/C10-30 alkyl acrylate copolymer emulsifier, lead to acrylic acid/acrylonitrile copolymer
Formula is HO (CH2CH2O)nThe polyethylene glycol of H, organic semi-synthetic water-soluble polymer include alkyl or hydroxy alkyl cellulose, carboxylic first
Base cellulose, hydroxyethyl cellulose, hydroxypropyl cellulose, hydrophobically modified hydroxyethyl cellulose, microcrystalline cellulose, carboxymethyl cellulose
Plain sodium salt compound.Preferably at least containing polyethylene glycol and acrylate/C10-30 alkyl acrylate cross-linked polymer and carboxylic
The one or two kinds of combination of the above of methylcellulose sodium salt compound.Further, polyethylene glycol HO (CH2CH2O)nH is preferably
Relative molecular weight Mw200-2000, further polyethylene glycol relative molecular weight is more preferably Mw200-700。
Purple common perilla seed of the invention the preparation method is as follows:
A. selected, removal impurity, cleaning, drying are carried out to purple perilla seed；
B. dry purple perilla seed crush and roll pretreatment；
C. pretreated purple perilla seed powder is extracted using supercritical CO 2 extraction technology, set extracting pressure as
10MPa-40MPa, extraction temperature are 20-70 DEG C, and extraction time 2-4h, fill factor is set as 0.4-0.9, obtains coarse extraction
Object；
D. obtained crude extract is filtered, obtains purple common perilla seed.It is 50- that purple perilla seed recovery rate, which is made, with this technique
60%, it is applied in the present invention, and there is antiallergic and antipruritic, anti-microbial effect reduces irritating effect.
The present invention can also contain pigment, essence, menthol, bamboo charcoal powder, hydrocarbon ils, silicon other than above-mentioned essential component
Oil and the one or more for waiting other effect substances and its derivative.
A kind of preparation method of the solid detergent composition containing purple common perilla seed of the present invention, includes the following steps:
A. deionized water, anionic ion surfactant, nonionic surfactant are weighed respectively in suitable container, are added
Heat is warming up to 50-60 DEG C；
B. filler is added, is sufficiently mixed uniformly；
C. adhesive and conditioner and and purple common perilla seed are added under stirring conditions；
D. other this field conven-tional adjuvants are added, mixture is made；
E. mixture is put into after being formed in molding machine, finished product is made in baking mixture.It is of the invention containing purple common perilla seed
Solid detergent composition finished product is graininess, circular graininess, naturally it is also possible to be other shapes as needed.
In conjunction with above-mentioned technical proposal, the invention has the benefit that
1. containing considerably less water, it is convenient for carrying, and be disposable, safety and sanitation.
2. containing natural origin, the mild raw starch of food sources and cellulose and its derivates, there are also natural
Moisturizer can provide the function of the clean clothes of mild deep layer.And different effects can be made according to color, and different color is brought
Pleasant visual effect.
3. containing soap base surfactant, good foam is provided, excellent cleaning capacity can easily remove skin dirt
Dirt, color make-up, blackhead and dead skin can improve its usage experience sense, to skin by compounding with mild amino acid surfactant
Skin is mild.By the collocation with nonionic surfactant alkyl glucoside, enhance the consistency and elasticity of foam.
4. improving the hardness of composition containing efficient adhesive fiber element and its derivative.
5. the present invention provides a kind of method of purple common perilla seed, and alleviates not being good for for skin using purple common perilla seed
Health situation goes to reduce cleaning compositions after washing to skin tape by the reasonably combined reduction of different surfaces activating agent and conditioner
The stimulation come improves skin appearance to play the role of delaying inflammation.
Specific embodiment
Solid detergent composition below in conjunction with specific embodiment to the present invention containing purple common perilla seed is made further detailed
Thin description.
It is prepared into product of the present invention, the following table 1 is 3 preferred embodiments of the present invention and 2 comparative examples.
The preparation method of the solid cleaning composition of embodiment, includes the following steps:
A. deionized water, anionic ion surfactant, nonionic surfactant are weighed respectively in suitable container, are added
Heat is warming up to 50-60 DEG C；
B. filler is added, is sufficiently mixed uniformly；
C. adhesive and conditioner and purple common perilla seed are added under stirring conditions；
D. other this field conven-tional adjuvants are added, mixture is made；
E. mixture is put into after being formed in molding machine, finished product is made in baking mixture.It is of the invention containing purple common perilla seed
Solid detergent composition finished product is graininess, circular graininess, naturally it is also possible to be other shapes as needed.
Wherein, the purple common perilla seed of embodiment the preparation method is as follows:
A. selected, removal impurity, cleaning, drying are carried out to purple perilla seed；
B. dry purple perilla seed crush and roll pretreatment；
C. pretreated purple perilla seed powder is extracted using supercritical CO 2 extraction technology, set extracting pressure as
10MPa-40MPa, extraction temperature are 20-70 DEG C, and extraction time 2-4h, fill factor is set as 0.4-0.9, obtains coarse extraction
Object；
D. obtained crude extract is filtered, obtains purple common perilla seed.
The solid detergent composition finished product containing purple common perilla seed obtained in this way be graininess, circular graininess,
It can certainly be other shapes as needed, can be used as the clean skins groups such as whole body cleaning compositions, face cleaning composition, ball of washing one's hands
Object is closed, can also be used as hair cleaning compositions, laundry detergent composition and the cleaning combination of animal hair etc..Especially
Ground, solid composite of the invention is preferably as skin cleansing compositions, such as face cleaning composition, hand wash composition and hair
Cleaning compositions etc..
In addition, when in use as composition, it need to be taken out from storage tank only, pulverized with hand in the palm of the hand, dilute with water
After releasing and sufficiently blistering, sufficiently rub with target is used, it is clean being rinsed with water.
Table 1: embodiment and comparative example component:
It manufactures table 1 illustrated embodiment 1-3 and comparative example 1-2 and evaluates their bubbling character, foam using obtained composition
Quality, foam volume rinse sense and hardness and antiphlogistic effects.The results are shown in Table 1.
1. evaluation: 10 special evaluation group members are ground sample with hand with the consistent sample of ready granular size
It is broken in the palm of the hand, two palm rubs mutuallies 15 are enclosed to blister, according to following 4 grades (3 points 2 points 1 point 0 point) evaluation criterion
To evaluate foaming properties.Total by what is scored, according to 3 grades, (C: A: evaluation total score 20-30, B: evaluation total score 10-19 are commented
Determine total score 0-9) scoring evaluation criteria determine their bubbling character, foam quality, foams using embodiment 1 as standard
Product rinses sense and hardness.
2. antiphlogistic effects are evaluated: the antiphlogistic effects in order to assess the present composition, by embodiment 1-3 and comparative example 1-2
Product obtained is tested on 15 volunteer's arms, is used continuously 1 month, daily using once, uses this product phase
Between, test skin area does not use other skin care item, and finally observation uses as a result, as shown in table 2.
Table 2: test result:
1-3 of the embodiment of the present invention contains soap base surfactant, provides good foam, excellent cleaning capacity, by with temperature
The amino acid surfactant of sum compounds, and can improve its usage experience sense, with nonionic surfactant alkyl glucoside
Collocation, enhances the consistency and elasticity of foam, is provided by the collocation with cellulose and its derivates and polyvinylpyrrolidone
Good hardness, and contain purple common perilla seed effectively reduces surfactant and extraneous stimulates to skin bring
Effect, to play the role of delaying inflammation, improves skin appearance.Filler is more compared to embodiment 1-3 in comparative example 2 and is free of
There is soap base surfactant, has used conventional surfactants AES, foam is relatively fewer, and it is not fine and smooth enough, and do not add purple perilla seed
Extract, it is larger to the stimulation of skin；Polyvinylpyrrolidone is not contained in comparative example 1, although obtained product has abundant
Foam, but hardness is compared with the difference of embodiment 1-3 and comparative example 2, and does not add purple common perilla seed, irritation is relatively large.
Although description of this invention combination embodiments above carries out, those skilled in the art
Member can carry out many replacements based on the above contents, modifications and variations, be obvious.Therefore, all such substitutions,
Improvements and changes are included in the spirit and scope of appended claims.
Claims (10)
1. a kind of solid detergent composition containing purple common perilla seed, which is characterized in that including following mass percent component:
Purple common perilla seed 5-10%；
Filler 10-60%；
Anionic surfactant 5-20%；
Nonionic surfactant 1-5%；
Adhesive 1-20%；
Conditioner 1-5%；
Surplus is deionized water.
2. the solid detergent composition according to claim 1 containing purple common perilla seed, which is characterized in that the described yin from
Sub- surfactant includes high carboxylic acid's salt, sulfonate, sulfuric acid, phosphate ester salt, at least one in fatty acyl-peptide condensation product
Kind.
3. the solid detergent composition according to claim 1 containing purple common perilla seed, which is characterized in that it is described it is non-from
Sub- surfactant includes alkyl phenol polyoxyethylene ether, high-carbon fatty alcohol polyoxyethylene ether, polyoxyethylene carboxylate, fatty acid
Methyl ester ethoxylates, the ethylene oxide adduct of polypropylene glycol, polyoxyethylated ionic surfactant, Sorbitan
At least one of alcohol ester, sucrose ester, alkylolamides type, alkyl heteroside.
4. the solid detergent composition according to claim 1 containing purple common perilla seed, which is characterized in that the bonding
Agent includes organic synthetic polymer acrylic polymer and its derivative and organic semi-synthetic water-soluble polymer.
5. the solid detergent composition according to claim 1 containing purple common perilla seed, which is characterized in that the filling
Agent includes modified starch.
6. the solid detergent composition according to claim 1 containing purple common perilla seed, which is characterized in that the conditioning
Agent includes glycerol, propylene glycol, 1,3-BDO, amides moisturizer, lactic acid and sodium lactate, pyrrolidone sodium carboxylate, poly- second two
At least one of alcohol, poly ethyldiol modified glyceride type, olive oil derivative, ionic moisturizer.
7. the solid detergent composition according to claim 2 containing purple common perilla seed, which is characterized in that the described yin from
Sub- surfactant includes that general formula is R-O(CH2-CH2O) n-CH2The high carboxylic acid's salt and N- fatty acyl group glutamate, rouge of COOX
At least one of acylglycine salt.
8. the solid detergent composition according to claim 4 containing purple common perilla seed, which is characterized in that described is organic
Synthetic polymer acrylic polymer and its derivative include acrylate copolymer, 600 series poly- third of Carbopol
Olefin(e) acid resin, acrylic acid/sodium acrylate polymer, acrylate/C10-30 alkyl acrylate cross-linked polymer, acrylic acid
Salt/C10-30 alkyl acrylate copolymer emulsifier, acrylic acid/acrylonitrile copolymer, general formula are HO (CH2CH2O)nH's is poly-
Ethylene glycol, organic semi-synthetic water-soluble polymer include alkyl or hydroxy alkyl cellulose, carboxymethyl cellulose, ethoxy
Cellulose, hydroxypropyl cellulose, hydrophobically modified hydroxyethyl cellulose, microcrystalline cellulose, sanlose compound.
9. the solid detergent composition according to any one of claims 1 to 8 containing purple common perilla seed, which is characterized in that
The purple common perilla seed the preparation method is as follows:
A. selected, removal impurity, cleaning, drying are carried out to purple perilla seed；
B. dry purple perilla seed crush and roll pretreatment；
C. pretreated purple perilla seed powder is extracted using supercritical CO 2 extraction technology, set extracting pressure as
10MPa-40MPa, extraction temperature are 20-70 DEG C, and extraction time 2-4h, fill factor is set as 0.4-0.9, obtains coarse extraction
Object；
D. obtained crude extract is filtered, obtains purple common perilla seed.
10. a kind of preparation method of the solid detergent composition containing purple common perilla seed described in claim 1-8 any one,
It is characterized by comprising the following steps:
A. deionized water, anionic ion surfactant, nonionic surfactant are weighed respectively in suitable container, are added
Heat is warming up to 50-60 DEG C；
B. filler is added, is sufficiently mixed uniformly；
C. adhesive and conditioner and purple common perilla seed are added under stirring conditions；
D. other this field conven-tional adjuvants are added, mixture is made；
E. mixture is put into after being formed in molding machine, finished product is made in baking mixture.
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Citations (7)
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|---|---|---|---|---|
| CN85109737A (en) * | 1984-12-24 | 1986-09-17 | B·F·谷德里奇公司 | The perfumed soap that contains polymeric viscosifier |
| CN1145400A (en) * | 1995-09-11 | 1997-03-19 | 贵州省生物资源超临界流体萃取研究开发中心 | Method of extracting perilla plant oil by using super-critical CO2 |
| CN102242017A (en) * | 2010-05-15 | 2011-11-16 | 杜文玲 | Synthetic detergent soap slab |
| CN103110559A (en) * | 2012-11-15 | 2013-05-22 | 沈阳洪达信息科技有限公司 | Pawpaw hand cream |
| CN104611124A (en) * | 2015-01-05 | 2015-05-13 | 大连卓尔高科技有限公司 | Method for extracting oil from perilla seeds by squeezing and supercritical CO2 extraction technology |
| CN105456066A (en) * | 2015-12-11 | 2016-04-06 | 彭再辉 | Novel face-cleansing composition and preparation method of finished product of face-cleansing composition |
| CN106833873A (en) * | 2017-02-28 | 2017-06-13 | 上海时迅农业科技发展有限公司 | A kind of supercritical CO2The method of low-temperature extraction vegetable oil |
-
2019
- 2019-01-11 CN CN201910026312.2A patent/CN109735404B/en active Active
Patent Citations (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN85109737A (en) * | 1984-12-24 | 1986-09-17 | B·F·谷德里奇公司 | The perfumed soap that contains polymeric viscosifier |
| CN1145400A (en) * | 1995-09-11 | 1997-03-19 | 贵州省生物资源超临界流体萃取研究开发中心 | Method of extracting perilla plant oil by using super-critical CO2 |
| CN102242017A (en) * | 2010-05-15 | 2011-11-16 | 杜文玲 | Synthetic detergent soap slab |
| CN103110559A (en) * | 2012-11-15 | 2013-05-22 | 沈阳洪达信息科技有限公司 | Pawpaw hand cream |
| CN104611124A (en) * | 2015-01-05 | 2015-05-13 | 大连卓尔高科技有限公司 | Method for extracting oil from perilla seeds by squeezing and supercritical CO2 extraction technology |
| CN105456066A (en) * | 2015-12-11 | 2016-04-06 | 彭再辉 | Novel face-cleansing composition and preparation method of finished product of face-cleansing composition |
| CN106833873A (en) * | 2017-02-28 | 2017-06-13 | 上海时迅农业科技发展有限公司 | A kind of supercritical CO2The method of low-temperature extraction vegetable oil |
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