CN109731912A - A kind of titanium/aluminium/magnesium composite plate tooth form faying face rolling preparation method - Google Patents

A kind of titanium/aluminium/magnesium composite plate tooth form faying face rolling preparation method Download PDF

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Publication number
CN109731912A
CN109731912A CN201910158985.3A CN201910158985A CN109731912A CN 109731912 A CN109731912 A CN 109731912A CN 201910158985 A CN201910158985 A CN 201910158985A CN 109731912 A CN109731912 A CN 109731912A
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titanium
composite
rolling
aluminium
magnesium
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CN109731912B (en
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马品奎
李志刚
查敏
王慧远
宋家旺
赵泼
任明文
韩洪江
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Jilin University
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Jilin University
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Abstract

The invention discloses a kind of titanium/aluminium/magnesium composite plate tooth form faying faces to roll preparation method, this method is using aluminium alloy sheet as intermediate layer, titanium alloy and aluminum alloy plate materials Rolling compund and are made into composite surface toothed surface at high temperature first, magnesium alloy plate is rolled at high temperature makes face toothed surface to be composite, then it will be pressed after the engagement of the toothed surface of titanium/aluminum composite board and magnesium alloy plate, Rolling compund at high temperature again obtains titanium/aluminium/magnesium composite plate finished product.The present invention can carry out titanium/aluminium/magnesium composite rolling after titanium/aluminium toothed surface composite rolling, the rolling of magnesium alloy toothed surface and toothed surface engagement at different temperatures, be conducive to the realization of Rolling compund;Rolling bites after the engagement of tooth form composite surface convenient for synchronizing for multilayer sheet alloy, effectively increases composite contact area, prevents composite surface high-temperature oxydation, improve the stress state of compound board interface, has many advantages, such as that composite plate interface quality is good, intensity is high.

Description

A kind of titanium/aluminium/magnesium composite plate tooth form faying face rolling preparation method
Technical field
The present invention relates to a kind of titanium/aluminium/magnesium composite plate tooth form faying faces to roll preparation method, belongs to composite metal plate system Standby field.
Background technique
Magnesium and magnesium alloy are structural metallic materials most light in current engineer application, due to high specific strength, Gao Bigang Degree, thermal conductivity is excellent, high damping vibration attenuation and the advantages that electromagnetic shielding and excellent reproducibility, it has also become after steel, The third-largest metal engineering material after aluminum alloy materials is the environment-friendly and energy-efficient structural material for 21 century having development potentiality, Wide application prospect is showed in auto industry field, aerospace field.However, due to the temperature-room type plasticity of magnesium alloy and resistance to Corrosive nature is poor, greatlys restrict its development.In addition to magnesium alloy, there are also aluminium alloys and titanium alloy for common light-alloy, wherein Aluminium and its alloy have many advantages, such as stronger inoxidizability, impact resistance and corrosion resistance, and titanium alloy has intensity height, corrosion resistance The features such as good, heat resistance height.Therefore, magnesium alloy and aluminium alloy and titanium alloy is compound, titanium alloy can be given full play to and aluminium closes The advantages that golden high-intensitive and corrosion-resistant advantage, quality of magnesium alloy is light, damping property and electromagnetic shielding performance are good, magnesium is overcome well It the shortcomings that alloy material poor corrosion resistance, maximizes favourable factors and minimizes unfavourable ones, obtains excellent structure and functional characteristic, widen the application neck of magnesium alloy Domain.
Mainly there are explosion composite method and roll-bonding method suitable for titanium/aluminium/magnesium composite metal plate preparation method.Explosion is multiple Close using explosive as the energy, explosive high speed ignition under percussion by different metal large-area welding together with.It is quick-fried The compound composite plate that can produce various metals is fried, but vibration, noise and the smoke contamination generated that explode can cause shadow to environment It rings, and production efficiency is lower.Rolling compund is to be rolled metal to be composite using the roll-force of milling train under certain temperature The features such as system, and then formation metallurgical bonding, have stable product quality good, high production efficiency, simple process, it is easy to accomplish work Industryization batch production.
However, three kinds of titanium, aluminium, magnesium alloy compound tenses, since the performance of most titanium alloys is substantially better than magnesium alloy and aluminium conjunction Gold, especially yield strength are very high, and resistance of deformation is very big, the deformation very little of titanium alloy when leading to three's Rolling compund, thus shadow The composite effect between titanium/aluminium, titanium/magnesium is rung, keeps boundary strength lower.
Summary of the invention
The object of the present invention is to provide a kind of titanium/aluminium/magnesium composite plate tooth form faying faces to roll preparation method, by aluminium alloy As intermediate layer, make full use of between titanium/aluminium, aluminum/magnesium alloy have good compound ability, preparation have superperformance and Titanium/aluminium/magnesium composite plate of combination interface intensity.
Technical solution of the present invention is as follows:
A kind of titanium/aluminium/magnesium composite plate tooth form faying face rolling preparation method, using aluminium alloy sheet as middle layer, by titanium Alloy and magnesium alloy plate rolling are composite plate, the specific steps are as follows:
1) composite surface is cleared up, and the face to be composite of titanium alloy, aluminium alloy and magnesium alloy is coarse to coarse with wire brush polishing Degree uniformly, with being dried up after alcohol washes buffed surface;
2) the compound tooth-shaped rolling of titanium/aluminium, the face paste combined pressure to be composite of titanium alloy and aluminum alloy plate materials is tight, one after heating A roller is Rolling compund on the milling train of serrated roller, and titanium/aluminium face to be composite is toothed surface after rolling;The heating of plate when tooth form rolls Temperature is 450~550 DEG C, and roll preheating temperature is 150 DEG C, and overall reduction is 5~10%;
3) magnesium alloy tooth form rolls, and rolls, rolls on the milling train that a roller is serrated roller after magnesium alloy plate is heated Face to be composite is toothed surface afterwards;Tooth form is identical as tooth form in step 2), and rolling temperature is 300~400 DEG C, and roll preheating temperature is 150 DEG C, drafts is 5~10%;
4) toothed surface pressing, the toothed surface of titanium/aluminum composite board and the toothed surface alcohol washes of magnesium alloy simultaneously dry up, tooth form It is pressed after engagement;
5) liner plate Rolling compund is rolled after titanium/aluminium after pressing/magnesium composite plate base heating using the method that liner plate rolls It makes compound;Rolling temperature is 300~400 DEG C when Rolling compund, and roll preheating temperature is 150 DEG C, and overall reduction is 35~50%;
6) it is straightened trimming, to there is curved rolling composite plate shaping to be straightened, excision composite plate deforms irregular front and back end Head obtains qualified titanium/aluminium/magnesium composite plate;
The toothed surface pressing of titanium/aluminum composite board and magnesium alloy in step 4) is to carry out at normal temperature, can be on a hydraulic press To implement, can also implement on milling train, it is ensured that toothed surface generates part and is plastically deformed, and presses two toothed surfaces to be composite sufficiently, High-temperature oxydation when preventing from heating;
Alignment described in step 6) carries out immediately after Rolling compund, and alignment can carry out on a hydraulic press, can also be more Roller mill rolling alignment;
The above method be suitable for thicker titanium alloy plate and aluminium alloy, magnesium alloy plate it is compound, if titanium alloy plate Thickness be less than 5mm, then milling train double roller is serrated roller, titanium/aluminium after Rolling compund when the compound tooth-shaped rolling of titanium/aluminium in step 2) The two sides of composite plate is toothed surface, Rolling compund after then engaging with the tooth form of magnesium alloy plate face to be composite.
Method is also applied for the rolling of other composite metal plates.
Beneficial effects of the present invention:
1. titanium/aluminium/magnesium composite plate milling method of the present invention is using aluminium alloy as middle layer, first by titanium/aluminium compared with Then Rolling compund under high-temperature again rolls magnesium and titanium/aluminium under relatively lower temp, realize that titanium/aluminium/magnesium is compound, rolling It is compound to be easily achieved;
2. rolling plate composite surface for tooth form composite surface, tooth form composite surface engages and is heated and rolled after pressing and is multiple It closes, not only increases composite contact area, and composite surface in heating process can be effectively prevent to generate oxidation, therefore, composite plate Interface quality is good, intensity is high.
3. titanium/aluminium/magnesium composite plate has high-strength light, corrosion resistance is good, and heat resistance is high, damping property and electromagnetic shielding performance Many advantages, such as good.
Detailed description of the invention
Fig. 1 is titanium/aluminium of the invention/magnesium slab composite plate rolling mill practice figure;
Fig. 2 is titanium/aluminium of the invention/magnesium sheet composite plate rolling mill practice figure;
Specific embodiment
Present invention will be further explained below with reference to the attached drawings and examples, and the present invention includes but are not limited to following implementations Example.
+ 3003 aluminium alloy+TC4 titanium alloy composite panel of embodiment 1:AZ31 magnesium alloy rolls (slab).
Thick 3003 aluminium alloys of 3mm thickness AZ31 magnesium alloy, 2mm and each one piece of 1mm thickness TC4 titanium alloy are taken, length and width dimensions are 90mm×45mm;
The composite surface of three kinds of alloys is coarse uniform to roughness with wire brush polishing, with alcohol washes buffed surface after-blow It is dry;
The composite surface of TC4 titanium alloy and 3003 aluminum alloy plate materials is bonded and is compressed, is heated to 450 DEG C, after heat preservation 8 minutes One roller is Rolling compund on the milling train of serrated roller, and roll preheating temperature is 150 DEG C, overall reduction 8%, after rolling TC4 and 3003 composite surface is toothed surface;
AZ31 magnesium alloy plate is heated to 300 DEG C, heat preservation rolls on the milling train that a roller is serrated roller after ten minutes, Roll preheating temperature is 150 DEG C, drafts 5%.Composite surface is toothed surface after rolling;
Tooth form after the toothed surface alcohol washes of the toothed surface and AZ31 of TC4 and 3003 composite plates and drying is engaged, It is pressed on 200 t hydraulic press;
Titanium/aluminium/magnesium composite plate base after pressing is heated to 300 DEG C, Rolling compund, roll preheating are warm after twenty minutes for heat preservation Degree is 150 DEG C, overall reduction 50%;
Composite plate after rolling is straightened on 200 t hydraulic press, obtains qualified AZ31/3003/TC4 composite plate.
+ 6062 aluminium alloy+TC4 titanium alloy composite panel of embodiment 2:AZ91 magnesium alloy rolls (slab).
Thick 6062 aluminium alloys of 3mm thickness AZ91 magnesium alloy, 2mm and each one piece of 1mm thickness TC4 titanium alloy are taken, length and width dimensions are 90mm×45mm;
The composite surface of three kinds of alloys is coarse uniform to roughness with wire brush polishing, with alcohol washes buffed surface after-blow It is dry;
The composite surface of TC4 titanium alloy and 6062 aluminum alloy plate materials is bonded and is compressed, is heated to 550 DEG C, after heat preservation 8 minutes One roller is Rolling compund on the milling train of serrated roller, and roll preheating temperature is 150 DEG C, overall reduction 8%, after rolling TC4 and 6062 composite surface is toothed surface;
AZ91 magnesium alloy plate is heated to 350 DEG C, heat preservation rolls on the milling train that a roller is serrated roller after ten minutes, Roll preheating temperature is 150 DEG C, drafts 5%.Composite surface is toothed surface after rolling;
Tooth form after the toothed surface alcohol washes of the toothed surface and AZ91 of TC4 and 6062 composite plates and drying is engaged, It is pressed on 200 t hydraulic press;
Titanium/aluminium/magnesium composite plate base after pressing is heated to 350 DEG C, Rolling compund, roll preheating are warm after twenty minutes for heat preservation Degree is 150 DEG C, overall reduction 50%;
Composite plate after rolling is straightened on 200 t hydraulic press, obtains qualified AZ91/6062/TC4 composite plate.
+ 6062 aluminium alloy+TC4 titanium alloy composite panel of embodiment 3:AZ31 magnesium alloy rolls (thin plate).
Take thick 6062 aluminium alloys of 3mm thickness AZ31 magnesium alloy, 1mm and each one piece of TC4 titanium alloy, length and width dimensions be 90mm × 45mm;
The composite surface of three kinds of alloys is coarse uniform to roughness with wire brush polishing, with alcohol washes buffed surface after-blow It is dry;
The composite surface of TC4 titanium alloy and 6062 aluminum alloy plate materials is bonded and is compressed, is heated to 550 DEG C, after heat preservation 8 minutes Two rollers are Rolling compund on the milling train of serrated roller, and roll preheating temperature is 150 DEG C, overall reduction 10%, TC4 after rolling Two-sided with 6062 composite plates is toothed surface;
AZ31 magnesium alloy plate is heated to 300 DEG C, heat preservation rolls on the milling train that a roller is serrated roller after ten minutes, Roll preheating temperature is 150 DEG C, drafts 5%.Composite surface is toothed surface after rolling;
Tooth form after the toothed surface alcohol washes of the toothed surface and AZ31 of TC4 and 6062 composite plates and drying is nibbled It closes, is pressed on 200 t hydraulic press;
Titanium/aluminium/magnesium composite plate base after pressing is heated to 350 DEG C, Rolling compund, roll preheating are warm after twenty minutes for heat preservation Degree is 150 DEG C, overall reduction 50%;
Composite plate after rolling is straightened on 200 t hydraulic press, obtains qualified AZ31/6062/TC4 composite plate.
Magnesium/aluminium/titanium composite panel prepared by embodiment 1,2 and 3 is observed, each layer alloy deformation is more uniform, interface cohesion Well;Using drawing-cut experiment to carry out interface bond strength test to magnesium/aluminium prepared by embodiment 3/titanium composite panel, titanium/aluminium, Magnesium/aluminium interface bond strength is above 140MPa.

Claims (5)

1. a kind of titanium/aluminium/magnesium composite plate tooth form faying face rolling preparation method closes titanium using aluminium alloy sheet as middle layer Gold and magnesium alloy plate rolling are composite plate, the specific steps are as follows:
1) composite surface is cleared up, and the face to be composite of titanium alloy, aluminium alloy and magnesium alloy is coarse equal to roughness with wire brush polishing It is even, with being dried up after alcohol washes buffed surface;
2) the compound tooth-shaped rolling of titanium/aluminium, the face paste combined pressure to be composite of titanium alloy and aluminum alloy plate materials is tight, in a roller after heating For Rolling compund on the milling train of serrated roller, titanium/aluminium face to be composite is toothed surface after rolling;The heating temperature of plate when tooth form rolls It is 450~550 DEG C, roll preheating temperature is 150 DEG C, and overall reduction is 5~10%;
3) magnesium alloy tooth form roll, after magnesium alloy plate is heated a roller be serrated roller milling train on roll, after rolling to Composite surface is toothed surface;Tooth form is identical as tooth form in step 2), and rolling temperature is 300~400 DEG C, and roll preheating temperature is 150 DEG C, drafts is 5~10%;
4) toothed surface pressing, the toothed surface of titanium/aluminum composite board and the toothed surface alcohol washes of magnesium alloy simultaneously dry up, tooth form engagement After press;
5) liner plate Rolling compund is rolled multiple after titanium/aluminium after pressing/magnesium composite plate base heating using the method for liner plate rolling It closes;Rolling temperature is 300~400 DEG C when Rolling compund, and roll preheating temperature is 150 DEG C, and overall reduction is 35~50%;
6) it is straightened trimming, to there is curved rolling composite plate shaping to be straightened, excision composite plate deforms irregular front and back end, obtains Obtain qualified titanium/aluminium/magnesium composite plate.
2. titanium according to claim 1/aluminium/magnesium composite plate tooth form faying face rolls preparation method, which is characterized in that step It is rapid 4) in titanium/aluminum composite board and magnesium alloy toothed surface pressing be to carry out at normal temperature, implement on a hydraulic press, or in milling train Upper implementation.
3. titanium according to claim 1/aluminium/magnesium composite plate tooth form faying face rolls preparation method, which is characterized in that step It is rapid 6) described in alignment carried out immediately after Rolling compund, alignment can carry out on a hydraulic press, or multi-roll mill roll Alignment.
4. titanium according to claim 1/aluminium/magnesium composite plate tooth form faying face rolls preparation method, which is characterized in that such as The thickness of fruit titanium alloy plate is less than 5mm, then milling train double roller is serrated roller when the compound tooth-shaped rolling of titanium/aluminium in step 2), rolls The two sides for making compound rear titanium/aluminum composite board is toothed surface, is rolled after then engaging with the tooth form of magnesium alloy plate face to be composite It is compound.
5. titanium according to claim 1/aluminium/magnesium composite plate tooth form faying face rolling preparation method is suitable for other metals The rolling of composite plate.
CN201910158985.3A 2019-03-04 2019-03-04 Rolling preparation method for tooth-shaped joint surface of titanium/aluminum/magnesium composite plate Expired - Fee Related CN109731912B (en)

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CN110303079A (en) * 2019-05-13 2019-10-08 太原理工大学 A kind of corrugated-crossed milling method of ply-metal
CN111230513A (en) * 2020-02-04 2020-06-05 太原理工大学 Preparation method of aluminum alloy-aluminum-steel transition joint with metallurgical bonding interface space
CN111570512A (en) * 2020-05-21 2020-08-25 吉林大学 High-toughness magnesium alloy plate and laminating and rolling preparation method thereof
CN111659747A (en) * 2020-05-26 2020-09-15 南京理工大学 Method for obtaining heterogeneous metal sheet by composite stamping
CN111922079A (en) * 2020-08-19 2020-11-13 太原理工大学 Steel/aluminum alloy layered composite plate wave-flat rolling composite method
CN112108518A (en) * 2020-08-03 2020-12-22 北京科技大学 Preparation method of metal layered composite material with strong metallurgical bonding interface
CN113002111A (en) * 2021-02-24 2021-06-22 山东济钢鲍德金属复合板科技有限公司 Preparation method of high-strength and high-flexibility metal composite plate
CN113020924A (en) * 2021-02-26 2021-06-25 醴陵千汇实业有限公司 Production method for improving durability of rolling type die
CN113210432A (en) * 2021-04-28 2021-08-06 太原理工大学 Lubricating process method for improving surface quality of corrugated roller rolled metal sheet
CN113210430A (en) * 2021-04-28 2021-08-06 太原理工大学 Method for improving shape and surface quality of corrugated roller rolled metal plate
CN113815295A (en) * 2021-09-24 2021-12-21 上海交通大学 Method and device for preparing composite metal sheet by utilizing surface microstructure to form gradient transition
CN115026139A (en) * 2022-08-10 2022-09-09 太原科技大学 Method for preparing nickel-magnesium composite board by rolling
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CN110303079A (en) * 2019-05-13 2019-10-08 太原理工大学 A kind of corrugated-crossed milling method of ply-metal
CN111230513A (en) * 2020-02-04 2020-06-05 太原理工大学 Preparation method of aluminum alloy-aluminum-steel transition joint with metallurgical bonding interface space
CN111230513B (en) * 2020-02-04 2021-04-06 太原理工大学 Preparation method of aluminum alloy-aluminum-steel transition joint with metallurgical bonding interface space
CN111570512A (en) * 2020-05-21 2020-08-25 吉林大学 High-toughness magnesium alloy plate and laminating and rolling preparation method thereof
CN111659747A (en) * 2020-05-26 2020-09-15 南京理工大学 Method for obtaining heterogeneous metal sheet by composite stamping
CN112108518A (en) * 2020-08-03 2020-12-22 北京科技大学 Preparation method of metal layered composite material with strong metallurgical bonding interface
CN112108518B (en) * 2020-08-03 2022-01-18 北京科技大学 Preparation method of metal layered composite material with strong metallurgical bonding interface
CN111922079B (en) * 2020-08-19 2021-08-10 太原理工大学 Steel/aluminum alloy layered composite plate wave-flat rolling composite method
CN111922079A (en) * 2020-08-19 2020-11-13 太原理工大学 Steel/aluminum alloy layered composite plate wave-flat rolling composite method
WO2022036823A1 (en) * 2020-08-19 2022-02-24 太原理工大学 Corrugated-flat rolling lamination method for steel/aluminum/aluminum alloy laminated plate
CN113002111A (en) * 2021-02-24 2021-06-22 山东济钢鲍德金属复合板科技有限公司 Preparation method of high-strength and high-flexibility metal composite plate
CN113020924A (en) * 2021-02-26 2021-06-25 醴陵千汇实业有限公司 Production method for improving durability of rolling type die
CN113210430A (en) * 2021-04-28 2021-08-06 太原理工大学 Method for improving shape and surface quality of corrugated roller rolled metal plate
CN113210432A (en) * 2021-04-28 2021-08-06 太原理工大学 Lubricating process method for improving surface quality of corrugated roller rolled metal sheet
CN113815295A (en) * 2021-09-24 2021-12-21 上海交通大学 Method and device for preparing composite metal sheet by utilizing surface microstructure to form gradient transition
CN115026139A (en) * 2022-08-10 2022-09-09 太原科技大学 Method for preparing nickel-magnesium composite board by rolling
CN115026129A (en) * 2022-08-10 2022-09-09 太原科技大学 Method for preparing magnesium/titanium layered waveform interface composite material based on rolling method

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