CN109721871A - A kind of High-strength compression resistant thermal insulation aluminium and preparation method thereof - Google Patents
A kind of High-strength compression resistant thermal insulation aluminium and preparation method thereof Download PDFInfo
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- CN109721871A CN109721871A CN201910058820.9A CN201910058820A CN109721871A CN 109721871 A CN109721871 A CN 109721871A CN 201910058820 A CN201910058820 A CN 201910058820A CN 109721871 A CN109721871 A CN 109721871A
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Abstract
The present invention provides a kind of High-strength compression resistant thermal insulation aluminium and preparation method thereof, is related to thermal insulation aluminium production technical field.The thermal insulation aluminium includes insulation board, adhesive and aluminum veneer, and the insulation board is made of raw material from the following weight: 50-60 parts of polystyrene resin, 20-30 parts of expanded perlite, 12-16 parts of polyphenylene sulfide, 8-10 parts of cyanate ester resin, 5-7 parts of polycarbonate, 10-14 parts of aluminum oxide, 8-10 parts of zirconium oxide, 5-7 parts of sodium metasilicate, 4-6 parts of chromium carbide, 4-6 parts of tungsten carbide, 0.4-0.6 parts of crosslinking agent, 2-4 parts of dispersing agent, 2-4 parts of toughener, 1-3 parts of nucleating agent.The present invention overcomes the deficiencies in the prior art, the intensity and compressive property of thermal insulation aluminium can be effectively improved, prevent thermal insulation aluminium from being occurred to be recessed or even crack by hitting, and then influence the heat insulation effect of thermal insulation aluminium, effectively enhance the thermal insulation property of insulation board by second time of foaming simultaneously, thermal insulation aluminium superior performance, using effect is good, is suitable for promoting.
Description
Technical field
The present invention relates to thermal insulation aluminium production technical fields, and in particular to a kind of High-strength compression resistant thermal insulation aluminium and its preparation
Method.
Background technique
Insulation board is said easy-to-understand exactly to the plank of building heat preservation.Insulation board is using polystyrene resin as raw material
In addition other auxiliary materials and manufactured rigid foam plate, have moisture-proof, waterproof performance, can reduce building envelope
Thickness, to increase indoor usable floor area.Aluminum veneer refers to after the processing such as chromaking, then uses fluorocarbon-sprayed technology, adds
The building decoration materials that work is formed.Thermal insulation aluminium is then through adhesive in conjunction with aluminum veneer, so that one kind be made by insulation board
Insulation board with decorative performance.
The formula composition and production technology of insulation board are unreasonable in thermal insulation aluminium at present, lead to the intensity of thermal insulation aluminium and resist
Press performance poor.Since thermal insulation aluminium is used for interior decoration and heat preservation, if thermal insulation aluminium is largely hit by the external world,
Then thermal insulation aluminium easily occurs to be recessed and even crack, and has seriously affected the heat insulation effect of thermal insulation aluminium in this way.Therefore, Yi Zhongqiang
The thermal insulation aluminium of effect High-strength compression resistant is the hot spot of researchers' research.
Summary of the invention
In view of the shortcomings of the prior art, the present invention provides a kind of High-strength compression resistant thermal insulation aluminium and preparation method thereof, the present invention
The deficiencies in the prior art are overcome, the intensity and compressive property of thermal insulation aluminium can be effectively improved, prevent thermal insulation aluminium from being hit
Recess occurs even to crack, and then influences the heat insulation effect of thermal insulation aluminium, while insulation board is effectively enhanced by second time of foaming
Thermal insulation property, thermal insulation aluminium superior performance, using effect is good, is suitable for promoting.
In order to achieve the above object, technical solution of the present invention is achieved by the following technical programs:
A kind of High-strength compression resistant thermal insulation aluminium, the thermal insulation aluminium include insulation board, adhesive and aluminum veneer, the heat preservation
Plate is made of raw material from the following weight: 50-60 parts of polystyrene resin, 20-30 parts of expanded perlite, polyphenylene sulfide 12-16
Part, 8-10 parts of cyanate ester resin, 5-7 parts of polycarbonate, 10-14 parts of aluminum oxide, 8-10 parts of zirconium oxide, sodium metasilicate 5-
7 parts, 4-6 parts of chromium carbide, 4-6 parts of tungsten carbide, 0.4-0.6 parts of crosslinking agent, 2-4 parts of dispersing agent, 2-4 parts of toughener, nucleating agent 1-3
Part.
Preferably, the insulation board is made of raw material from the following weight: 55 parts of polystyrene resin, expanded perlite 25
Part, 14 parts of polyphenylene sulfide, 9 parts of cyanate ester resin, 6 parts of polycarbonate, 12 parts of aluminum oxide, 9 parts of zirconium oxide, sodium metasilicate
6 parts, 5 parts of chromium carbide, 5 parts of tungsten carbide, 0.5 part of crosslinking agent, 3 parts of dispersing agent, 3 parts of toughener, 2 parts of nucleating agent.
Preferably, the adhesive is one of polymethyl acrylate, Lauxite and glycerol resin or a variety of.
Preferably, the crosslinking agent is that N hydroxymethyl acrylamide, methylene diacrylamide and 1,4-butanediol two are shunk
One of glycerin ether is a variety of.
Preferably, the dispersing agent be one of lauryl sodium sulfate, triethyl group hexyl phosphoric acid and stearmide or
It is a variety of.
Preferably, the toughener is one of blocked polyurethane, polyamide and polyvinyl butyral or a variety of.
Preferably, the nucleating agent is one of calcium carbonate, gold bubble mother and sodium benzoate or a variety of.
The preparation method of the thermal insulation aluminium the following steps are included:
(1) it is added in ball mill after mixing polystyrene resin, expanded perlite and crosslinking agent, after grinding 20-30min
It is mixed object to squeeze into autoclave, is warming up to 140-160 DEG C, adjustment revolving speed to 80-100r/min, heat preservation is kneaded 1-2h；
(2) above-mentioned step is added after mixing polyphenylene sulfide, cyanate ester resin, polycarbonate, dispersing agent and toughener
Suddenly in the autoclave in (1), adjustment revolving speed to 300-400r/min, heat preservation is kneaded the nucleating agent of addition 1/2 amount of formula after 2-4h,
It is passed through argon gas after insulated and stirred 5-10min, boosts to 3-5MPa, pressure maintaining restores after permeating 1-2h to normal pressure, then thermal insulation foaming 20-
30min；
(3) it is added in ball mill and is ground to after mixing aluminum oxide, zirconium oxide, sodium metasilicate, chromium carbide and tungsten carbide
Granularity is 0.03-0.07mm, after be mixed powder be added above-mentioned steps (2) in autoclave in, heat preservation be kneaded 2-4h after plus
Enter remaining nucleating agent, be passed through argon gas, boost to 6-8MPa, pressure maintaining restores after permeating 1-2h to normal pressure, then thermal insulation foaming 20-
30min obtains insulation board raw material for standby；
(4) heat preservation board raw material obtained is squeezed into mold, is pressed and molded by high-temperature steam, then cooled to room temperature
It is spare to obtain insulation board；
(5) aluminum veneer is put into mold, and adhesive is uniformly coated in the surface of aluminum veneer, then will be obtained
Insulation board is placed on aluminum veneer, obtains product by composite pressure machine compression moulding.
The present invention provides a kind of High-strength compression resistant thermal insulation aluminium and preparation method thereof, and advantage is compared with prior art:
(1) present invention is added with polyphenylene sulfide, cyanate ester resin and polycarbonate, can effectively improve thermal insulation aluminium
Intensity prevents thermal insulation aluminium from being occurred to be recessed or even crack by hitting, and then influences the heat insulation effect of thermal insulation aluminium, thermal insulation aluminium
Intensity is high, and heat insulation effect is good, by being passed through argon gas into autoclave and nucleating agent being cooperated to carry out first time foaming, can make to be made
Insulation board there is stomata abundant to store a large amount of air to enhance the thermal insulation property of insulation board, thermal insulation aluminium intensity
Height, good heat insulating, using effect are good；
(2) present invention is added with aluminum oxide, zirconium oxide, sodium metasilicate, chromium carbide and tungsten carbide, can effectively improve guarantor
The compressive property of warm aluminium sheet can be such that insulation board obtained and foaming for the first time generates not by foaming again to raw material
The stomata of same specification enhances the thermal insulation property of insulation board to store the air of different volumes, and thermal insulation aluminium compressive property is high,
Thermal insulation aluminium superior performance is suitable for promoting.
Specific embodiment
In order to make the object, technical scheme and advantages of the embodiment of the invention clearer, below with reference to the embodiment of the present invention pair
Technical solution in the embodiment of the present invention is clearly and completely described, it is clear that described embodiment is a part of the invention
Embodiment, instead of all the embodiments.Based on the embodiments of the present invention, those of ordinary skill in the art are not making wound
Every other embodiment obtained under the premise of the property made labour, shall fall within the protection scope of the present invention.
Embodiment 1:
A kind of High-strength compression resistant thermal insulation aluminium, the thermal insulation aluminium include insulation board, adhesive and aluminum veneer, the heat preservation
Plate is made of raw material from the following weight: 50 parts of polystyrene resin, 20 parts of expanded perlite, 12 parts of polyphenylene sulfide, cyanate
8 parts of resin, 5 parts of polycarbonate, 10 parts of aluminum oxide, 8 parts of zirconium oxide, 5 parts of sodium metasilicate, 4 parts of chromium carbide, tungsten carbide 4
Part, 0.4 part of crosslinking agent, 2 parts of dispersing agent, 2 parts of toughener, 1 part of nucleating agent.
Wherein, the adhesive is one of polymethyl acrylate, Lauxite and glycerol resin or a variety of；The friendship
Connection agent is one of N hydroxymethyl acrylamide, methylene diacrylamide and 1,4-butanediol diglycidyl ether or a variety of；
The dispersing agent is one of lauryl sodium sulfate, triethyl group hexyl phosphoric acid and stearmide or a variety of；The toughener
For one of blocked polyurethane, polyamide and polyvinyl butyral or a variety of；The nucleating agent be calcium carbonate, gold bubble it is female and
One of sodium benzoate is a variety of.
The preparation method of the thermal insulation aluminium the following steps are included:
(1) it is added in ball mill after mixing polystyrene resin, expanded perlite and crosslinking agent, after grinding 20-30min
It is mixed object to squeeze into autoclave, is warming up to 140-160 DEG C, adjustment revolving speed to 80-100r/min, heat preservation is kneaded 1-2h；
(2) above-mentioned step is added after mixing polyphenylene sulfide, cyanate ester resin, polycarbonate, dispersing agent and toughener
Suddenly in the autoclave in (1), adjustment revolving speed to 300-400r/min, heat preservation is kneaded the nucleating agent of addition 1/2 amount of formula after 2-4h,
It is passed through argon gas after insulated and stirred 5-10min, boosts to 3-5MPa, pressure maintaining restores after permeating 1-2h to normal pressure, then thermal insulation foaming 20-
30min；
(3) it is added in ball mill and is ground to after mixing aluminum oxide, zirconium oxide, sodium metasilicate, chromium carbide and tungsten carbide
Granularity is 0.03-0.07mm, after be mixed powder be added above-mentioned steps (2) in autoclave in, heat preservation be kneaded 2-4h after plus
Enter remaining nucleating agent, be passed through argon gas, boost to 6-8MPa, pressure maintaining restores after permeating 1-2h to normal pressure, then thermal insulation foaming 20-
30min obtains insulation board raw material for standby；
(4) heat preservation board raw material obtained is squeezed into mold, is pressed and molded by high-temperature steam, then cooled to room temperature
It is spare to obtain insulation board；
(5) aluminum veneer is put into mold, and adhesive is uniformly coated in the surface of aluminum veneer, then will be obtained
Insulation board is placed on aluminum veneer, obtains product by composite pressure machine compression moulding.
Embodiment 2:
A kind of High-strength compression resistant thermal insulation aluminium, the thermal insulation aluminium include insulation board, adhesive and aluminum veneer, the heat preservation
Plate is made of raw material from the following weight: 55 parts of polystyrene resin, 25 parts of expanded perlite, 14 parts of polyphenylene sulfide, cyanate
9 parts of resin, 6 parts of polycarbonate, 12 parts of aluminum oxide, 9 parts of zirconium oxide, 6 parts of sodium metasilicate, 5 parts of chromium carbide, tungsten carbide 5
Part, 0.5 part of crosslinking agent, 3 parts of dispersing agent, 3 parts of toughener, 2 parts of nucleating agent.
Wherein, the adhesive is one of polymethyl acrylate, Lauxite and glycerol resin or a variety of；The friendship
Connection agent is one of N hydroxymethyl acrylamide, methylene diacrylamide and 1,4-butanediol diglycidyl ether or a variety of；
The dispersing agent is one of lauryl sodium sulfate, triethyl group hexyl phosphoric acid and stearmide or a variety of；The toughener
For one of blocked polyurethane, polyamide and polyvinyl butyral or a variety of；The nucleating agent be calcium carbonate, gold bubble it is female and
One of sodium benzoate is a variety of.
The preparation method of the thermal insulation aluminium the following steps are included:
(1) it is added in ball mill after mixing polystyrene resin, expanded perlite and crosslinking agent, after grinding 20-30min
It is mixed object to squeeze into autoclave, is warming up to 140-160 DEG C, adjustment revolving speed to 80-100r/min, heat preservation is kneaded 1-2h；
(2) above-mentioned step is added after mixing polyphenylene sulfide, cyanate ester resin, polycarbonate, dispersing agent and toughener
Suddenly in the autoclave in (1), adjustment revolving speed to 300-400r/min, heat preservation is kneaded the nucleating agent of addition 1/2 amount of formula after 2-4h,
It is passed through argon gas after insulated and stirred 5-10min, boosts to 3-5MPa, pressure maintaining restores after permeating 1-2h to normal pressure, then thermal insulation foaming 20-
30min；
(3) it is added in ball mill and is ground to after mixing aluminum oxide, zirconium oxide, sodium metasilicate, chromium carbide and tungsten carbide
Granularity is 0.03-0.07mm, after be mixed powder be added above-mentioned steps (2) in autoclave in, heat preservation be kneaded 2-4h after plus
Enter remaining nucleating agent, be passed through argon gas, boost to 6-8MPa, pressure maintaining restores after permeating 1-2h to normal pressure, then thermal insulation foaming 20-
30min obtains insulation board raw material for standby；
(4) heat preservation board raw material obtained is squeezed into mold, is pressed and molded by high-temperature steam, then cooled to room temperature
It is spare to obtain insulation board；
(5) aluminum veneer is put into mold, and adhesive is uniformly coated in the surface of aluminum veneer, then will be obtained
Insulation board is placed on aluminum veneer, obtains product by composite pressure machine compression moulding.
Embodiment 3:
A kind of High-strength compression resistant thermal insulation aluminium, the thermal insulation aluminium include insulation board, adhesive and aluminum veneer, the heat preservation
Plate is made of raw material from the following weight: 60 parts of polystyrene resin, 30 parts of expanded perlite, 16 parts of polyphenylene sulfide, cyanate
10 parts of resin, 7 parts of polycarbonate, 14 parts of aluminum oxide, 10 parts of zirconium oxide, 7 parts of sodium metasilicate, 6 parts of chromium carbide, tungsten carbide
6 parts, 0.6 part of crosslinking agent, 4 parts of dispersing agent, 4 parts of toughener, 3 parts of nucleating agent.
Wherein, the adhesive is one of polymethyl acrylate, Lauxite and glycerol resin or a variety of；The friendship
Connection agent is one of N hydroxymethyl acrylamide, methylene diacrylamide and 1,4-butanediol diglycidyl ether or a variety of；
The dispersing agent is one of lauryl sodium sulfate, triethyl group hexyl phosphoric acid and stearmide or a variety of；The toughener
For one of blocked polyurethane, polyamide and polyvinyl butyral or a variety of；The nucleating agent be calcium carbonate, gold bubble it is female and
One of sodium benzoate is a variety of.
The preparation method of the thermal insulation aluminium the following steps are included:
(1) it is added in ball mill after mixing polystyrene resin, expanded perlite and crosslinking agent, after grinding 20-30min
It is mixed object to squeeze into autoclave, is warming up to 140-160 DEG C, adjustment revolving speed to 80-100r/min, heat preservation is kneaded 1-2h；
(2) above-mentioned step is added after mixing polyphenylene sulfide, cyanate ester resin, polycarbonate, dispersing agent and toughener
Suddenly in the autoclave in (1), adjustment revolving speed to 300-400r/min, heat preservation is kneaded the nucleating agent of addition 1/2 amount of formula after 2-4h,
It is passed through argon gas after insulated and stirred 5-10min, boosts to 3-5MPa, pressure maintaining restores after permeating 1-2h to normal pressure, then thermal insulation foaming 20-
30min；
(3) it is added in ball mill and is ground to after mixing aluminum oxide, zirconium oxide, sodium metasilicate, chromium carbide and tungsten carbide
Granularity is 0.03-0.07mm, after be mixed powder be added above-mentioned steps (2) in autoclave in, heat preservation be kneaded 2-4h after plus
Enter remaining nucleating agent, be passed through argon gas, boost to 6-8MPa, pressure maintaining restores after permeating 1-2h to normal pressure, then thermal insulation foaming 20-
30min obtains insulation board raw material for standby；
(4) heat preservation board raw material obtained is squeezed into mold, is pressed and molded by high-temperature steam, then cooled to room temperature
It is spare to obtain insulation board；
(5) aluminum veneer is put into mold, and adhesive is uniformly coated in the surface of aluminum veneer, then will be obtained
Insulation board is placed on aluminum veneer, obtains product by composite pressure machine compression moulding.
It should be noted that, in this document, relational terms such as first and second and the like are used merely to a reality
Body or operation are distinguished with another entity or operation, are deposited without necessarily requiring or implying between these entities or operation
In any actual relationship or order or sequence.Moreover, the terms "include", "comprise" or its any other variant are intended to
Non-exclusive inclusion, so that the process, method, article or equipment including a series of elements is not only wanted including those
Element, but also including other elements that are not explicitly listed, or further include for this process, method, article or equipment
Intrinsic element.In the absence of more restrictions, the element limited by sentence "including a ...", it is not excluded that
There is also other identical elements in process, method, article or equipment including the element.
The above embodiments are merely illustrative of the technical solutions of the present invention, rather than its limitations；Although with reference to the foregoing embodiments
Invention is explained in detail, those skilled in the art should understand that: it still can be to aforementioned each implementation
Technical solution documented by example is modified or equivalent replacement of some of the technical features；And these modification or
Replacement, the spirit and scope for technical solution of various embodiments of the present invention that it does not separate the essence of the corresponding technical solution.
Claims (8)
1. a kind of High-strength compression resistant thermal insulation aluminium, which is characterized in that the thermal insulation aluminium includes insulation board, adhesive and aluminium list
Plate, the insulation board are made of raw material from the following weight: 50-60 parts of polystyrene resin, gathers 20-30 parts of expanded perlite
12-16 parts of diphenyl sulfide, 8-10 parts of cyanate ester resin, 5-7 parts of polycarbonate, 10-14 parts of aluminum oxide, zirconium oxide 8-10
Part, 5-7 parts of sodium metasilicate, 4-6 parts of chromium carbide, 4-6 parts of tungsten carbide, 0.4-0.6 parts of crosslinking agent, 2-4 parts of dispersing agent, toughener 2-4
Part, 1-3 parts of nucleating agent.
2. a kind of High-strength compression resistant thermal insulation aluminium according to claim 1, which is characterized in that the insulation board is by following heavy
The raw material of amount part is made: 55 parts of polystyrene resin, 14 parts of polyphenylene sulfide, 9 parts of cyanate ester resin, gathers 25 parts of expanded perlite
6 parts of carbonic acid ester fiber, 12 parts of aluminum oxide, 9 parts of zirconium oxide, 6 parts of sodium metasilicate, 5 parts of chromium carbide, 5 parts of tungsten carbide, crosslinking agent
0.5 part, 3 parts of dispersing agent, 3 parts of toughener, 2 parts of nucleating agent.
3. a kind of High-strength compression resistant thermal insulation aluminium according to claim 1, which is characterized in that the adhesive is polypropylene
One of sour methyl esters, Lauxite and glycerol resin are a variety of.
4. a kind of High-strength compression resistant thermal insulation aluminium according to claim 1, which is characterized in that the crosslinking agent is N- hydroxyl first
One of base acrylamide, methylene diacrylamide and 1,4-butanediol diglycidyl ether are a variety of.
5. a kind of High-strength compression resistant thermal insulation aluminium according to claim 1, which is characterized in that the dispersing agent is dodecane
One of base sodium sulphate, triethyl group hexyl phosphoric acid and stearmide are a variety of.
6. a kind of High-strength compression resistant thermal insulation aluminium according to claim 1, which is characterized in that the toughener is that sealing end is poly-
One of urethane, polyamide and polyvinyl butyral are a variety of.
7. a kind of High-strength compression resistant thermal insulation aluminium according to claim 1, which is characterized in that the nucleating agent is carbonic acid
One of calcium, gold bubble mother and sodium benzoate are a variety of.
8. a kind of preparation method of High-strength compression resistant thermal insulation aluminium, which is characterized in that the preparation method of the thermal insulation aluminium includes
Following steps:
(1) it is added in ball mill after mixing polystyrene resin, expanded perlite and crosslinking agent, by it after grinding 20-30min
Mixture is squeezed into autoclave, is warming up to 140-160 DEG C, adjustment revolving speed to 80-100r/min, heat preservation is kneaded 1-2h；
(2) above-mentioned steps (1) is added after mixing polyphenylene sulfide, cyanate ester resin, polycarbonate, dispersing agent and toughener
In autoclave in, for adjustment revolving speed to 300-400r/min, heat preservation is kneaded the nucleating agent that 1/2 amount of formula is added after 2-4h, keeps the temperature
It is passed through argon gas after stirring 5-10min, boosts to 3-5MPa, pressure maintaining restores after permeating 1-2h to normal pressure, then thermal insulation foaming 20-
30min；
(3) it is added in ball mill after mixing aluminum oxide, zirconium oxide, sodium metasilicate, chromium carbide and tungsten carbide and is ground to granularity
For 0.03-0.07mm, after be mixed powder and be added in the autoclave in above-mentioned steps (2), heat preservation be kneaded after 2-4h be added it is surplus
Remaining nucleating agent, is passed through argon gas, boosts to 6-8MPa, and pressure maintaining restores after permeating 1-2h to normal pressure, then thermal insulation foaming 20-30min
Obtain insulation board raw material for standby；
(4) heat preservation board raw material obtained is squeezed into mold, is pressed and molded by high-temperature steam, then cooled to room temperature must protect
Warm plate is spare；
(5) aluminum veneer is put into mold, and adhesive is uniformly coated in the surface of aluminum veneer, then by heat preservation obtained
Plate is placed on aluminum veneer, obtains product by composite pressure machine compression moulding.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
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| CN201910058820.9A CN109721871A (en) | 2019-01-22 | 2019-01-22 | A kind of High-strength compression resistant thermal insulation aluminium and preparation method thereof |
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| Application Number | Priority Date | Filing Date | Title |
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| CN201910058820.9A CN109721871A (en) | 2019-01-22 | 2019-01-22 | A kind of High-strength compression resistant thermal insulation aluminium and preparation method thereof |
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Family
ID=66299231
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| CN110183788A (en) * | 2019-06-26 | 2019-08-30 | 保定威尔达节能科技有限公司 | A kind of fire prevention styrofoam and its production technology |
| CN110305439A (en) * | 2019-06-10 | 2019-10-08 | 安徽蓝润自动化仪表有限公司 | A kind of High-strength compression resistant plastics power control cabinet case material and preparation method thereof |
| CN110498979A (en) * | 2019-07-11 | 2019-11-26 | 安徽金九鼎复合材料有限公司 | A kind of architectural decoration wear-resistant pressure-resistant insulation board and preparation method thereof |
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