CN109706740A - Silk scarf superfine mulberry silk fiber chiffon fabric - Google Patents
Silk scarf superfine mulberry silk fiber chiffon fabric Download PDFInfo
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- CN109706740A CN109706740A CN201811555504.4A CN201811555504A CN109706740A CN 109706740 A CN109706740 A CN 109706740A CN 201811555504 A CN201811555504 A CN 201811555504A CN 109706740 A CN109706740 A CN 109706740A
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Abstract
The invention discloses a kind of silk scarf superfine mulberry silk fiber chiffon fabrics, preparation method, which is specifically included, impregnates the starching solution being made of water-soluble poly ester polyether slurry, turkey red oil, 1- orthododecyl nitrogen heterocyclo heptane-2-ketone, nanoparticle, adhesive SD28, curcumin and water for ultra-fine Raw Silk, carry out starching processing, then it dries, obtain starching ultrafine mulberry silk, by starching ultrafine mulberry silk by winder and silk twisting, preparation is through to silk fiber and broadwise silk fiber；It then will be through being woven as silk scarf superfine mulberry silk fiber chiffon fabric to silk fiber and broadwise silk fiber.Silk scarf prepared by the present invention has the characteristics that be not easy to break end when weaving with superfine mulberry silk fiber chiffon fabric.In addition, the strong operability of the processing method, is suitble to industrialized production, and production cost is low.
Description
Technical field
The invention belongs to field of fabric producing technology, and in particular to a kind of silk scarf superfine mulberry silk fiber chiffon face
Material.
Background technique
Silk has the characteristics that elongated, soft, moisture absorption, good luster, traditional silk (four moultinism silks or five dormancy age silkworms
Silk) wrinkle resistance is poor, it is unable to fabric ultrathin type silk and product；The method of existing modified silk fiber is the three moultinism product that are bred as
Kind silkworm, such as dawn, SG, 305, production fiber number are about the silk of 2.0 daniers；It is bred as three moultinism kind silkworm of mutagenesis, uses drug
By common four moultinisms silk mutagenesis at three molt silkworms, silk ultra-fine is produced；Or with " ultra-fine element " (the chloro- N- phenylimidazole of 2,4- bis-)
Four molt silkworms, three dormancyization is induced, silk ultra-fine is produced；Or be uniformly sprayed on mulberry leaf surface with anti-JH and add food to silkworm, make
Common four dormancies silkworm, three dormancyization produces silk ultra-fine.The most of scarf are the long scarve being trapped among in neck, the method for production
Have it is woven, by hand woollen yarn knitting etc., for material based on silk and wool, the sense of touch of silk scarf is smooth, have it is soft, frivolous,
Elasticity is good, washing shrinkage is low, the feature of the feel of smooth softness as silk and pendency sense.Prior art discloses silk chiffon fabrics
Manufacture craft, first add Z to twist 7-10 strands of cocoon fibers and 1-2 strands of elastomers, by 6-9 strands of cocoon fibers and 2-3 bursts elasticity
Fiber adds Z to twist, then warp and weft cross woven, and intersecting angle is 20-40 degree, prepares silk chiffon fabric.Due to ultra-fine mulberry
Silk fiber number is small, and fibre strength is lower, therefore, and silk twisting process in because the problem of strength, frequent fracture of wire, and
Due to often breaking end, being not used to produce through the factor to tension and reed friction during looming weaving.
Summary of the invention
Finished product scarf is dyed to obtain by scarf fabrics, and the performance of scarf fabrics determines the application effect of finished product scarf substantially,
Scarf fabrics are generally prepared by degumming after raw silk and silk twisting, weaving, and wherein degumming is removal silk silk gum, shows silk fiber
Excellent properties, the prior art is more mature, key be raw silk and silk twisting, weaving process because fine denier filament is had excellent performance,
But raw silk and silk twisting, the easy fracture of wire of weaving process, suitable longitude and latitude fiber can not be formed, so that fine denier filament can not be showed
Excellent properties.The present invention is handled using the very poor ultrafine mulberry silk raw silk of mechanical property itself by starching, it is effectively improved
Mechanical property avoids fracture of wire phenomenon, to obtain silk scarf ultrafine mulberry silk so that simultaneously silk twisting, weaving process are smooth
Fiber chiffon fabric can sufficiently show the excellent properties of fine denier filament.
The present invention adopts the following technical scheme:
A kind of silk scarf superfine mulberry silk fiber chiffon fabric, preparation method includes the following steps:
(1) ultra-fine Raw Silk is impregnated by water-soluble poly ester polyether slurry, turkey red oil, 1- dodecyl azacyclo-
The starching solution that hept- 2- ketone, nanoparticle, adhesive SD28, curcumin and water form carries out starching processing, then dries, obtain
To starching ultrafine mulberry silk；The nanoparticle is prepared by nano yttrium oxide, boric acid, urea；
(2) starching ultrafine mulberry silk is twisted by winder and silk, preparation is through to silk fiber and broadwise silk fiber；Then
It will be through being woven as silk scarf superfine mulberry silk fiber chiffon fabric to silk fiber and broadwise silk fiber.
A kind of preparation method of silk scarf superfine mulberry silk fiber chiffon fabric, comprising the following steps:
(1) ultra-fine Raw Silk is impregnated by water-soluble poly ester polyether slurry, turkey red oil, 1- dodecyl azacyclo-
The starching solution that hept- 2- ketone, nanoparticle, adhesive SD28, curcumin and water form carries out starching processing, then dries, obtain
To starching ultrafine mulberry silk；The nanoparticle is prepared by nano yttrium oxide, boric acid, urea；
(2) starching ultrafine mulberry silk is twisted by winder and silk, preparation is through to silk fiber and broadwise silk fiber；Then
It will be through being woven as silk scarf superfine mulberry silk fiber chiffon fabric to silk fiber and broadwise silk fiber.
Silk scarf of the invention has silk gum with superfine mulberry silk fiber chiffon fabric, therefore names as chiffon fabric,
To be distinguished with degumming fabric；Refining face can be obtained by degumming process with superfine mulberry silk fiber chiffon fabric in silk scarf
Material.
A kind of silk scarf preparation method of starching ultrafine mulberry silk, includes the following steps, ultra-fine Raw Silk is soaked
Bubble is by water-soluble poly ester polyether slurry, turkey red oil, 1- orthododecyl nitrogen heterocyclo heptane-2-ketone, nanoparticle, adhesive
The starching solution of SD28, curcumin and water composition, carry out starching processing, then dry, obtain the ultra-fine mulberry of silk scarf starching
Silk；The nanoparticle is prepared by nano yttrium oxide, boric acid, urea.
A kind of ultrafine mulberry silk scarf preparation method of raw silk starching solution, includes the following steps, by water-soluble polyester
Polyethers slurry, turkey red oil, 1- orthododecyl nitrogen heterocyclo heptane-2-ketone, nanoparticle, adhesive SD28, curcumin and water
Mixing composition ultrafine mulberry silk scarf raw silk starching solution；The nanoparticle is prepared by nano yttrium oxide, boric acid, urea
It arrives.
In the present invention, the specification of ultra-fine Raw Silk is 9/11D, by the ultra-fine silkworm list that fiber number is 1.0~1.2 daniers
Silk filature obtains, and is existing product, and raw silk is by filature by product made of the mutual obvolvent of several Bombyx-mori Baves, and fine denier is raw
Silk weaving at fabric have wrinkle resistance it is strong, rich in the characteristics such as gloss, dyeing effect be good, but the prior art has no with this fineness
Report of the mulberry silk as scarf fabrics, main cause is exactly that mechanical strength is too low, and the present invention is solved by starching processing
Existing technical problem.
Different from existing conventional organic slurry, the present invention is directed to special superfine mulberry silk fiber, has developed nanoparticle
Son, preparation method are to be dispersed in water urea, and boric acid and ethyl alcohol is then added, nano yttrium oxide is added after stirring, are stirred
Remove solvent after 2~2.5 hours, obtain solids, then by solids under nitrogen, 950~1000 DEG C calcine 5 hours, then
Nanoparticle is obtained by crushing.Preferably, nano yttrium oxide, boric acid, urea mass ratio be 50: 65: 100；Nanoparticle
It is not directly used in starching by any surface treatment, on the one hand since surface treatment does not have effect to silk gum, on the other hand
Avoid the coupling agent of surface treatment to the unfavorable of paste compound and to the unfavorable of subsequent desizing, general untreated nanometer
Particle application effect is poor, this is common sense, and the present invention is added using turkey red oil and 1- orthododecyl nitrogen heterocyclo heptane-2-ketone
In water-soluble poly ester polyether slurry, it is evident that the dispersibility that can improve nanoparticle, in conjunction with curcumin, several additives have
Effect improves nanoparticle in the attachment on superfine mulberry silk fiber surface.The stretching of fiber can be improved using nanoparticle by the present invention
Intensity, more important is avoid the residual to silk gum in desizing processes, improve desizing effect.
In the present invention, in starching solution, the mass fraction of water-soluble poly ester polyether slurry is 10%~20%, turkey red oil
Mass fraction be the mass fraction of 0.4%~0.6%, 1- orthododecyl nitrogen heterocyclo heptane-2-ketone be 0.2%~0.5%, adhesive
The mass fraction of SD28 is 3%~5%, and the mass fraction of nanoparticle is 3~3.3%, and the mass fraction of curcumin is 2~2.2%,
Remaining is water.It is such to match the effect of impregnation that superfine mulberry silk fiber can be improved, so that size composition is in fiber surface
It is uniformly dispersed, in terms of embodiment effect, the tensile strength of superfine mulberry silk fiber is improved, and desizing effect is good.
In the present invention, water-soluble poly ester polyether slurry, turkey red oil, 1- orthododecyl nitrogen heterocyclo heptane-2-ketone, bonding
Agent SD28, curcumin are all existing product, wherein water-soluble poly ester polyether slurry, turkey red oil, 1- dodecyl azepine
Cycloheptyl -2- ketone, curcumin are commercial products, for example water-soluble poly ester polyether slurry SH, adhesive SD28 are open product.This hair
It is bright to configure new size composition using these open substances, silk ultra-fine fiber is surface-treated, can be increased ultra-fine
The intensity of silk fiber, make its and silk twisting process and looming weaving during avoid being broken, water-soluble poly ester polyether slurry
Material is as basic processes composition, its dispersibility can be improved in turkey red oil, and the guess of 1- orthododecyl nitrogen heterocyclo heptane-2-ketone can
To increase organic matter in the even flat effect on superfine mulberry silk fiber surface, adhesive improves the bonding force of organic component, curcumin
Size composition especially nanoparticle should be can be further improved in the combination effect of fiber surface.
In the present invention, starching handle when, bath raio be 1:5~1:10, temperature be 30 DEG C~40 DEG C, the time be 25min~
30min；After the completion of starching, ultrafine mulberry silk is dry in hot-air drying device after centrifugal dehydration, obtains the ultra-fine mulberry of starching
Silk.
In the present invention, winder, simultaneously silk twisting and weaving can carry out network originally as the prior art on slack winder
Cylinder processing carries out simultaneously silk twisting processing on simultaneously silk twisting mill, is weaved on loom；The present invention is preferably through to silk fiber
For 4/9/11D mulberry silk 14T/2S2Z, broadwise silk fiber is 2/9/11D mulberry silk 18T/2S2Z.Mulberry silk of the present invention
Fiber chiffon fabric is plain weave, and through being 48/10cm to density, latitudinal density is 51/10cm.The product of this specification
In desizing, effect is fine, and obtained fabric warmth retention property is good, wrinkle resistance is excellent.
The present invention is surface-treated ultra-fine Raw Silk using size composition, improves raw silk breaking strength, thus
Efficiently solve the problems, such as that fine denier filament of the existing technology is that fine denier filament can industry life in the fracture of wire of simultaneously silk twisting weaving process
Production prepares silk scarf fabrics and provides possibility, and silk scarf obtained is with superfine mulberry silk fiber chiffon fabric by ultrafine mulberry silk
Fiber preparation can embody the excellent properties of silk fiber, such as warming, soft, crease-resistant, provide optimality for silk fabric
Energy；The present invention is also an advantage that it is unfavorable will not to generate to subsequent degumming process using starching condition, silk gum can be handled
Completely.
Compared with thick denier (filament number is 2.6~3.0 daniers) silk, fine-denier (1.0~1.2 danier of monofilament) silk
Refractive property it is more preferable, reflecting feel is strong, and pendency sense is strong, can improve the smooth and elastic of squeeze, and dyeing and printing products are bright in luster
Degree is preferable.But since ultrafine mulberry silk fiber number is small, fibre strength is lower.Therefore, because of strength in simultaneously silk twisting process
Problem, frequent fracture of wire, in addition due to often breaking end through the factor to tension and reed friction during looming weaving, it can not
For producing.Therefore, improve the sizing technique of fine-denier silk, improve ultrafine mulberry silk strength and cohesive force, be prepare it is ultra-fine true
The key technology of silk chiffon fabric.
The present invention improves strength of raw silk by starching processing, and the scarf fabrics of preparation have the function of wear-resisting, high-strength, increase
The service life of scarf fabrics can effectively remove silk gum by refining treatment, so that scarf fabrics have good warmth retention property
Energy；The mulberry silk that the present invention uses intensity originally relatively low is raw material, and in conjunction with preparation process, not only wool type is rich for manufactured scarf fabrics
Full, warming moisture-absorbing is good, luxurious, beautiful top grade ventilative to light, comfortable, and it is crease-resistant, intensity is good, harmless to human skin.
Compared with prior art, the sizing technique that the present invention limits improves the intensity of fiber, hence it is evident that reduces ultra-fine mulberry
Silk fiber the phenomenon that fracture of wire frequent occurrence, improves the cohesive force of superfine mulberry silk fiber in simultaneously silk twisting process, increases
Lubricity；It in concise scouring processes, can remove completely, not influence the service performance of mulberry silk fiber, especially starching and handle
Effect is also improved to the silk performance after degumming, estimation is swollen in soaking process silk gum, and inorganic agent is allowed to have a little infiltration
Effect thoroughly, has modifying function to fibroin, obtained silk scarf fabrics gas permeability and warmth retention property is preferable；And the present invention processes
The strong operability of method, is suitble to industrialized production, and processing cost is low.
Specific embodiment
The invention patent is further described below with reference to embodiment:
Polyester polyethers slurry SH, turkey red oil, 1- orthododecyl nitrogen heterocyclo heptane-2-ketone, curcumin are commercially available, open produce
Product, adhesive are commercial product, such as adhesive SD28, adhesive HD.
Synthesis example
10Kg urea is dispersed in 30 liters of water, 13Kg boric acid and 5L ethyl alcohol is then added, it is nano oxidized that 20Kg is added after stirring
Yttrium stirs 2.5 hours back spins and boils off except solvent, obtains solids, then by solids under nitrogen, 950 DEG C calcine 5 hours,
Nanoparticle is obtained using crushing, aerodynamic particle size is between 500~700 nanometers.
Embodiment one
On cone dyeing machine, by 9/11D superfine mulberry silk fiber cheese, (raw silk is 1.0~1.2 daniers by fiber number
Ultra-fine silkworm monofilament filature obtains, breaking strength 0.9CN/dtex) impregnate it is bis- macro by 50Kg polyester polyethers slurry SH(), 2 Kg it is native
Ear its red oil, 2Kg 1- orthododecyl nitrogen heterocyclo heptane-2-ketone (letter health), 15 Kg adhesive SD28,16Kg nanoparticles,
The starching solution of 10Kg curcumin and 405Kg water mixing composition, bath raio 1:8,30 DEG C of soaking temperature, soaking time 30min.Starching
After the completion, it is dehydrated on centrifugal dehydrator, then, is dried in hot wind drying plant, the silk fiber cheese dried,
For starching ultrafine mulberry silk (breaking strength 2.1CN/dtex).Directly adopt partial size boron nitride nanometer between 400~500 nanometers
The above-mentioned nanoparticle of particle replacement, obtained starching ultrafine mulberry silk breaking strength 1.7CN/dtex, elongation at break 16.03,
Guess may be easier in conjunction with fiber when silk gum swelling since nanoparticle prepared by the present invention is irregular.
The silk fiber cheese of above-mentioned drying is subjected to winder processing on slack winder, then in simultaneously silk twisting mill
It is upper to carry out and silk twisting processing, it prepares through to silk fiber and broadwise silk fiber；Wherein through being 4/9/11D to silk fiber
Mulberry silk 14T/2S2Z, broadwise silk fiber are 2/9/11D mulberry silk 18T/2S2Z.It will be through to silk fiber and latitude on loom
Silk scarf superfine mulberry silk fiber chiffon fabric is prepared to silk fiber weaving, obtained silk scarf ultrafine mulberry silk
Fiber chiffon fabric is plain weave, and through being 48/10cm to density, latitudinal density is 51/10cm；Starching ultrafine mulberry silk
In addition to other than monofilament surface improves filament strength, also increasing the cohesive force between monofilament, it is strong that the two combination effectively increases raw silk
Degree, solves the problems, such as existing ultra-fine raw silk and silk twisting process in because of the frequent fracture of wire of strength, during looming weaving by
The problem of factor of Yu Jingxiang tension and reed friction often breaks end, is not used to production, entire production process is smooth, without disconnected
It splits, fracture of wire situation occurs if directly being twisted with 9/11D superfine mulberry silk fiber cheese and silk, weaving process is even more to occur
Broken end problem.Raw silk elongation at break is 15.23%, 16.62% before and after starching, and it is soft that elongation at break can be used as measurement silk fiber
Soft indirect indexes, the raw silk deformability for illustrating that the present invention is handled is more preferable, than having better flexibility before handling；Using
Fabric air-permeability amount instrument tests the gas permeability of scarf fabrics, 3 average out to 249mm/S, using flat insulation instrument to enclosing
Towel fabric carries out heat preservation rate test, 3 average out to 22.2%, good warmth retention effect.
Silk scarf superfine mulberry silk fiber chiffon fabric degumming process according to the following steps can be obtained into silk scarf
Fabric, technical effect of the invention can be further illustrated by testing its performance:
Hang and practice in slot in silk, above-mentioned silk scarf is impregnated with superfine mulberry silk fiber chiffon fabric by 48Kg sodium carbonate and
The desizing solution of 2955Kg water composition, bath raio 1:30 are warming up to 80 DEG C, and handle 30min at this temperature, and processing is completed
Afterwards, drain；The enzymatic treatment liquid of 6 Kg alkali proteases, 5Kg sodium sulphate, 15Kg sodium carbonate and 2974Kg water composition, bath raio is added
For 1:30,60 DEG C are warming up to, and handles 90min at this temperature, after the completion of processing, drain；7Kg acetic acid and 2993Kg is added
Water, bath raio 1:30 are warming up to 90 DEG C, and handle 30min at this temperature.After the completion of processing, successively with 80 DEG C, 60 DEG C of water
It washes, then is washed 3 times with cold water, drying processing is finally carried out in single roller blanket equipment, silk scarf fabrics, unit area is made
Weight is 25.8 grams/m, thickness 0.98mm；Soft, wrinkling resistance is good, crease-resistant using turnaround time after folding as characterizing
The auxiliary characteristics of ability, the scarf fabrics prepared after starching improve 48% compared with scarf fabrics prepared by non-starching；Using fabric air-permeability
Amount instrument the gas permeability of scarf fabrics is tested, 3 average out to 352mm/S, using flat insulation instrument to scarf fabrics into
The test of row heat preservation rate, 3 average out to 22.8%, the scarf fabrics warmth retention property and gas permeability of non-starching preparation are poor, respectively
20.1%、319 mm/S。
Comparative example one
On cone dyeing machine, by 9/11D superfine mulberry silk fiber cheese, (raw silk is 1.0~1.2 daniers by fiber number
Ultra-fine silkworm monofilament filature obtains, breaking strength 0.9CN/dtex) impregnate it is bis- macro by 50Kg polyester polyethers slurry SH(), 2 Kg it is native
Ear its red oil, 2Kg 1- orthododecyl nitrogen heterocyclo heptane-2-ketone (letter health), 15 Kg adhesive SD28,10Kg curcumins and
The starching solution of 421Kg water mixing composition, bath raio 1:8,30 DEG C of soaking temperature, soaking time 30min.After the completion of starching, from
It is dehydrated on heart dewaterer, then, is dried in hot wind drying plant, the silk fiber cheese dried is that starching is ultra-fine
Mulberry silk (breaking strength 1.7CN/dtex, elongation at break 15.99%).By the silk fiber cheese of above-mentioned drying in pine
Winder processing is carried out on formula bobbin-winding machine, then and silk twisting mill on carry out and silk twisting processing, prepare through to silk fiber
With broadwise silk fiber；Wherein through being 4/9/11D mulberry silk 14T/2S2Z to silk fiber, broadwise silk fiber is 2/9/11D
Mulberry silk 18T/2S2Z.It will be through preparing mulberry silk fiber chiffon face to silk fiber and broadwise silk fiber weaving on loom
Material, obtained mulberry silk fiber chiffon fabric be plain weave, through to density be 48/10cm, latitudinal density be 51/
10cm；Entire production process is broken, than directly using 9/11D superfine mulberry silk fiber cheese and silk twisting generation fracture of wire feelings
Condition is few；It is tested using gas permeability of the fabric air-permeability amount instrument to scarf fabrics, 3 average out to 229mm/S, using flat guarantor
Wen Yi carries out heat preservation rate test, 3 average out to 21.1% to scarf fabrics；There is fracture of wire in production, does not carry out degumming process.
Comparative example two
On cone dyeing machine, by 9/11D superfine mulberry silk fiber cheese, (raw silk is 1.0~1.2 daniers by fiber number
Ultra-fine silkworm monofilament filature obtains, breaking strength 0.9CN/dtex) impregnate it is bis- macro by 50Kg polyester polyethers slurry SH(), 2 Kg it is native
Ear its red oil, 2Kg 1- orthododecyl nitrogen heterocyclo heptane-2-ketone (letter health), 15 Kg adhesive SD28,16Kg nanoparticles and
The starching solution of 415Kg water mixing composition, bath raio 1:8,30 DEG C of soaking temperature, soaking time 30min.After the completion of starching, from
It is dehydrated on heart dewaterer, then, is dried in hot wind drying plant, the silk fiber cheese dried is that starching is ultra-fine
Mulberry silk (breaking strength 1.5CN/dtex, elongation at break 16.23%).By the silk fiber cheese of above-mentioned drying in pine
Winder processing is carried out on formula bobbin-winding machine, then and silk twisting mill on carry out and silk twisting processing, prepare through to silk fiber
With broadwise silk fiber；Wherein through being 4/9/11D mulberry silk 14T/2S2Z to silk fiber, broadwise silk fiber is 2/9/11D
Mulberry silk 18T/2S2Z.It will be through preparing mulberry silk fiber chiffon face to silk fiber and broadwise silk fiber weaving on loom
Material, obtained mulberry silk fiber chiffon fabric be plain weave, through to density be 48/10cm, latitudinal density be 51/
10cm；Entire production process is broken, than directly using 9/11D superfine mulberry silk fiber cheese and silk twisting generation fracture of wire feelings
Condition is few；It is tested using gas permeability of the fabric air-permeability amount instrument to scarf fabrics, 3 average out to 232mm/S, using flat guarantor
Wen Yi carries out heat preservation rate test, 3 average out to 21.3% to scarf fabrics；There is fracture of wire in production, does not carry out degumming process.
Scarf is as one of winter warming ornament, and the performances such as warming, comfortable of fabric material are increasingly by people
Attention.The fine-denier of fiber is the pursuit of the mankind, and the textile fabric used earliest is natural fiber-cotton, fiber crops, hair, silk,
Middle mulberry silk surely belongs to best one of the fiber of wears performance, no matter dress comfort or appearance in terms of have
Unique advantage.Unfortunately, ultrafine mulberry silk poor mechanical property is not used to the preparation of scarf fabrics, is easy fracture of wire, the present invention
It sets about from the simultaneously fracture of wire of silk twisting and weaving process is solved, by the combination of size composition and technique, realizes that raw silk is disconnected
The raising of resistance to spalling in production process without fracture of wire phenomenon, while improving the wrinkling resistance of finished fabric, breathable heat insulating ability.
Claims (10)
1. a kind of silk scarf superfine mulberry silk fiber chiffon fabric, which is characterized in that the silk scarf is with ultra-fine silkworm
The preparation method of silk fiber chiffon fabric the following steps are included:
(1) ultra-fine Raw Silk is impregnated by water-soluble poly ester polyether slurry, turkey red oil, 1- dodecyl azacyclo-
The starching solution that hept- 2- ketone, nanoparticle, adhesive SD28, curcumin and water form carries out starching processing, then dries, obtain
To starching ultrafine mulberry silk；The nanoparticle is prepared by nano yttrium oxide, boric acid, urea；
(2) starching ultrafine mulberry silk is twisted by winder and silk, preparation is through to silk fiber and broadwise silk fiber；Then
It will be through being woven as mulberry silk fiber chiffon fabric to silk fiber and broadwise silk fiber.
2. silk scarf superfine mulberry silk fiber chiffon fabric according to claim 1, which is characterized in that nanoparticle
Preparation method is to be dispersed in water urea, and boric acid and ethyl alcohol is then added, and is added nano yttrium oxide after stirring, stirring 2~
Remove solvent after 2.5 hours, obtain solids, then by solids under nitrogen, 950~1000 DEG C calcine 5 hours, using
Crushing obtains nanoparticle.
3. silk scarf superfine mulberry silk fiber chiffon fabric according to claim 2, which is characterized in that nano oxidized
Yttrium, boric acid, urea mass ratio be 50: 65: 100.
4. silk scarf superfine mulberry silk fiber chiffon fabric according to claim 1, which is characterized in that starching solution
In, the mass fraction of water-soluble poly ester polyether slurry is 10%~20%, and the mass fraction of turkey red oil is 0.4%~0.6%, 1-
The mass fraction of orthododecyl nitrogen heterocyclo heptane-2-ketone is 0.2%~0.5%, and the mass fraction of adhesive SD28 is 3%~5%, is received
The mass fraction of rice corpuscles is 3~3.3%, and the mass fraction of curcumin is 2~2.2%, remaining is water.
5. silk scarf superfine mulberry silk fiber chiffon fabric according to claim 1, which is characterized in that starching processing
When, bath raio is 1:5~1:10, and temperature is 30 DEG C~40 DEG C, and the time is 25min~30min；After the completion of starching, ultrafine mulberry silk
It is dry in hot-air drying device after centrifugal dehydration, obtain starching ultrafine mulberry silk.
6. silk scarf superfine mulberry silk fiber chiffon fabric according to claim 1, which is characterized in that ultra-fine silkworm is raw
The specification of silk is 9/11D, is obtained by the ultra-fine silkworm monofilament filature that fiber number is 1.0~1.2 daniers；Through being 4/ to silk fiber
9/11D mulberry silk 14T/2S2Z, broadwise silk fiber are 2/9/11D mulberry silk 18T/2S2Z.
7. silk scarf superfine mulberry silk fiber chiffon fabric according to claim 1, which is characterized in that the silk encloses
Towel is plain weave with superfine mulberry silk fiber chiffon fabric, and through being 48/10cm to density, latitudinal density is 51/10cm.
8. a kind of preparation method of silk scarf superfine mulberry silk fiber chiffon fabric, which comprises the following steps:
(1) ultra-fine Raw Silk is impregnated by water-soluble poly ester polyether slurry, turkey red oil, 1- dodecyl azacyclo-
The starching solution that hept- 2- ketone, nanoparticle, adhesive SD28, curcumin and water form carries out starching processing, then dries, obtain
To starching ultrafine mulberry silk；The nanoparticle is prepared by nano yttrium oxide, boric acid, urea；
(2) starching ultrafine mulberry silk is twisted by winder and silk, preparation is through to silk fiber and broadwise silk fiber；Then
It will be through being woven as mulberry silk fiber chiffon fabric to silk fiber and broadwise silk fiber.
9. the preparation method of silk scarf superfine mulberry silk fiber chiffon fabric according to claim 8, which is characterized in that
The preparation method of nanoparticle is to be dispersed in water urea, and boric acid and ethyl alcohol is then added, is added after stirring nano oxidized
Yttrium, stirring remove solvent after 2~2.5 hours, obtain solids, then by solids under nitrogen, 950~1000 DEG C of calcinings 5
Hour, nanoparticle is obtained using crushing；In starching solution, the mass fraction of water-soluble poly ester polyether slurry is 10%~
20%, the mass fraction of turkey red oil is that the mass fraction of 0.4%~0.6%, 1- orthododecyl nitrogen heterocyclo heptane-2-ketone is
The mass fraction of 0.2%~0.5%, adhesive SD28 are 3%~5%, and the mass fraction of nanoparticle is 3~3.3%, curcumin
Mass fraction is 2~2.2%, remaining is water；When starching is handled, bath raio is 1:5~1:10, and temperature is 30 DEG C~40 DEG C, and the time is
25min~30min；After the completion of starching, ultrafine mulberry silk is dry in hot-air drying device after centrifugal dehydration, obtains
Starch ultrafine mulberry silk.
10. the preparation method of silk scarf superfine mulberry silk fiber chiffon fabric, feature exist according to claim 8
In the specification of ultra-fine Raw Silk is 9/11D, is obtained by the ultra-fine silkworm monofilament filature that fiber number is 1.0~1.2 daniers；Through
It is 4/9/11D mulberry silk 14T/2S2Z to silk fiber, broadwise silk fiber is 2/9/11D mulberry silk 18T/2S2Z；It is described true
Silk scarf with superfine mulberry silk fiber chiffon fabric is plain weave, through being 48/10cm to density, latitudinal density is 51/
10cm。
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201811555504.4A CN109706740B (en) | 2018-12-18 | 2018-12-18 | Superfine mulberry silk fiber chiffon fabric for silk scarf |
Applications Claiming Priority (1)
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| CN201811555504.4A CN109706740B (en) | 2018-12-18 | 2018-12-18 | Superfine mulberry silk fiber chiffon fabric for silk scarf |
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| CN109706740B CN109706740B (en) | 2021-06-04 |
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| CN105002762A (en) * | 2015-07-10 | 2015-10-28 | 湖州三佳纺织有限公司 | Silk digital ink-jet printing method |
| CN106245384A (en) * | 2016-09-21 | 2016-12-21 | 东莞市联洲知识产权运营管理有限公司 | A kind of concentrator based on nanometer gold and the application on silk fabric thereof |
| CN107503131A (en) * | 2017-08-14 | 2017-12-22 | 南通泰慕士服装有限公司 | A kind of high definition screen printing technique |
| CN108085837A (en) * | 2018-01-18 | 2018-05-29 | 达利丝绸（浙江）有限公司 | Natural elasticity color-woven fabric production technology comprising mulberry silk boiled-off silk tram |
| CN108677568A (en) * | 2017-09-13 | 2018-10-19 | 海宁市盛祥线业有限公司 | The printing technology of improved real silk fabric |
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Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105002762A (en) * | 2015-07-10 | 2015-10-28 | 湖州三佳纺织有限公司 | Silk digital ink-jet printing method |
| CN106245384A (en) * | 2016-09-21 | 2016-12-21 | 东莞市联洲知识产权运营管理有限公司 | A kind of concentrator based on nanometer gold and the application on silk fabric thereof |
| CN107503131A (en) * | 2017-08-14 | 2017-12-22 | 南通泰慕士服装有限公司 | A kind of high definition screen printing technique |
| CN108677568A (en) * | 2017-09-13 | 2018-10-19 | 海宁市盛祥线业有限公司 | The printing technology of improved real silk fabric |
| CN108085837A (en) * | 2018-01-18 | 2018-05-29 | 达利丝绸（浙江）有限公司 | Natural elasticity color-woven fabric production technology comprising mulberry silk boiled-off silk tram |
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| CN109706740B (en) | 2021-06-04 |
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Denomination of invention: Ultra fine mulberry silk fiber chiffon fabric for silk scarves Effective date of registration: 20230804 Granted publication date: 20210604 Pledgee: Shanghai Rural Commercial Bank Co.,Ltd. Huangpu sub branch Pledgor: SHANGHAI ZHAOWU BRAND MANAGEMENT CO.,LTD. Registration number: Y2023310000432 |