CN109662932A - A kind of moisture-keeping crease-shedding cosmetics - Google Patents
A kind of moisture-keeping crease-shedding cosmetics Download PDFInfo
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- CN109662932A CN109662932A CN201910162226.4A CN201910162226A CN109662932A CN 109662932 A CN109662932 A CN 109662932A CN 201910162226 A CN201910162226 A CN 201910162226A CN 109662932 A CN109662932 A CN 109662932A
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- moisture
- shedding
- extract
- diosmetin
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- 235000010447 xylitol Nutrition 0.000 description 1
Classifications
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9789—Magnoliopsida [dicotyledons]
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/49—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds
- A61K8/4973—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with oxygen as the only hetero atom
- A61K8/498—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with oxygen as the only hetero atom having 6-membered rings or their condensed derivatives, e.g. coumarin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/55—Phosphorus compounds
- A61K8/553—Phospholipids, e.g. lecithin
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
- A61K8/731—Cellulose; Quaternized cellulose derivatives
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
- A61K8/733—Alginic acid; Salts thereof
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
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- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
- A61K8/735—Mucopolysaccharides, e.g. hyaluronic acid; Derivatives thereof
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- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/08—Anti-ageing preparations
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Abstract
The invention discloses a kind of moisture-keeping crease-shedding cosmetics, by weight, including following components: 5~15 parts of passion fruit shell extract, 1~5 part of Moringa seed extract, 1~5 part of Maca extract, 20~100 parts of polysaccharide solution, 2~10 parts of prinsepia utilis royle oil, 1~5 part of walnut oil, 1~3 part of diosmetin, 1~6 part of emulsifier, 0.1~0.3 part of antibacterial agent.Cosmetics quality of the present invention is soft and smooth, mild pro-skin, good penetrability, easy absorption safety are non-stimulated, but also has the function of long-acting moisturizing, anti-aging, repair microgroove, increase skin elasticity.
Description
Technical field
The present invention relates to cosmetic fields, and in particular to a kind of moisture-keeping crease-shedding cosmetics.
Background technique
Remaining youthful forever is everyone dream and pursuit.With increasingly prominent, the anti-aging of population in the world Aging Problem
The topic being keen to as people.
Aging is the inevitable outcome that function of human body slows down, its performance the most intuitive of the aging of skin and appearance.Skin is old
Change phenomenon and be mainly manifested in following aspect: (1) connecting loose, hydratability decline between the skin epidermal cells of aging.Newborn
Moisture content of skin it is most, with function of human body gradually aging, the hydratability of skin also declines, in skin water content also gradually under
Drop, the elderly's moisture content of skin is only the 75% of normal young people, therefore often shows as having dry skin.(2) thickness of skin with
The increase at age and it is gradually thinning, to senescence phase epidermis stratum granulosum it is atrophic to disappear, epidermal cell short survival.For
This, moisture-keeping crease-shedding class cosmetics are firmly got middle-aged and the old's consumption and are liked, while also becoming the Main way of research and development cosmetics.
In patent CN105147591B, a kind of crease-resistant face cream and preparation method thereof is disclosed.The crease-resistant face cream includes
Butanediol, ethylhexyl palmitate, caprylic/capric triglyceride, glycerol, Natrulon H-10, isononanoic acid ethylhexyl, poly- methyl
Methyl acrylate, dimethyl silicone polymer, stereth -21, cetostearyl alcohol, stereth -2, acrylic acid (ester) class/
Acrylamide copolymer, glycine betaine, Butyrospermum parkii fruit rouge, Bacillus acidi lactici/pomegranate fruit tunning extract, arctic Ascophyllum nodosum essence
China, starfish essence, ginseng extract, Ganodenna Lucidum P.E, apple extract, tocopherol acetate etc..The crease-resistant face cream of the present invention seeps
Permeability is good, easily absorbs, effective replenishing water and preserving moisture, repairs wrinkle of skin, inhibits wrinkle regeneration, delay skin aging.
In patent CN104856892B, a kind of cosmetics rich in growth factor or skin care item preparation and its system are disclosed
Preparation Method, it is Porcine HGF that the present invention, which provides a kind of main component, and small molecule wins peptide, water, grease, surfactant, guarantor
Humectant, antioxidant, the cosmetics rich in growth factor of preservative composition or skin care item preparation and preparation method thereof.The group
It is collocated with each other the metabolism that can not only accelerate Skin Cell between the formula of conjunction object preparation, the superficial Cortical fiber for repairing fracture is thin
Born of the same parents have a quick repair function outstanding to skin wound, but also have whitening wrinkle-removing, calm antiallergic, skin softening, it is crease-resistant, brighten,
Clearly, the multiple efficacies such as anti-aging, anti-radiation, prevention and mitigation color spot.
In patent CN105125476B, a kind of anti-wrinkle essence and preparation method thereof is disclosed.The re-surface intensive wrinkle correct
Liquid includes cyclomethicone, butanediol, dimethyl silicone polymer, polyglutamic acid sodium, glycerol, propylene glycol, polyglycereol-
10, dipropylene glycol, erythrite, hydroxy-ethyl acrylate/sodium acryloyldimethyl taurate copolymers, biological carbohydrate gum -1, xylitol,
C20-22 alcohol phosphate/C20-22 alcohol, Bacillus acidi lactici/pomegranate fruit tunning extract, arctic Ascophyllum nodosum essence, starfish essence
China, hexapeptide -3, flores aurantii essence, rough gentian root extract, arbutin, milk protein, tranexamic acid etc., good penetrability easily absorb, have
Replenishing water and preserving moisture is imitated, wrinkle of skin is repaired, inhibits wrinkle regeneration, delay skin aging.
In invention CN103876947B, a kind of sea cucumber peptide stabilization formulations are disclosed, by sea cucumber peptide, low molecule hyalomitome
Acid, trehalose and water composition, wherein the mass concentration of each component are as follows: sea cucumber peptide 0.4~0.6%, ultra-low molecular hyaluronic acid 0.1
~0.5%, trehalose 1~5%, surplus is water；The molecular weight of the low molecular weight hyaluronic acid is 5000~10000 dalton.This
The sea cucumber peptide stabilization formulations of invention can keep the uniform state of sea cucumber peptide liquid, in stable condition, and nutritive value is abundant, health care
Effect is good, has crease-resistant, moisturizing, enhancing skin elasticity and other effects, can be used as food or cosmetics or health care product is applied.
Foregoing invention be primarily present synthesis composition it is more, poor to skin compatibility, water holding capacity is insufficient, irritation is larger
The defects of.
Summary of the invention
The problem of according to above-mentioned patented technology, the present invention provide a kind of moisture-keeping crease-shedding cosmetics, natural component
The advantages that ratio is high, preferable, nourishing moistening effect is preferable and nonirritant to skin compatibility.
The invention adopts the following technical scheme:
A kind of moisture-keeping crease-shedding cosmetics, by weight, including following components: 5~15 parts of passion fruit shell extract, moringa seeds mention
Take 1~5 part of object, 1~5 part of Maca extract, 20~100 parts of polysaccharide solution, 2~10 parts of prinsepia utilis royle oil, 1~5 part of walnut oil,
1~3 part of diosmetin, 1~6 part of emulsifier, 0.1~0.3 part of antibacterial agent.
Heretofore described passion fruit shell extract is prepared using following steps:
(1) it is cleaned after peeling passion fruit shell, the passion fruit shell cleaned is placed in crusher and carries out pulverization process；
(2) Extraction solvent ethyl alcohol is added in the passion fruit shell crushed, carries out immersion treatment, is then added on ultrasonator
Carry out ultrasonication processing；
(3) warm water immersion treatment is carried out to the passion fruit shell by ultrasonication processing, is then centrifuged, filtration treatment obtains
Supernatant carries out concentration filtrate to gained supernatant and handles to obtain passion fruit shell extract.
Moringa seed extract of the present invention uses volume fraction of ethanol 60~80%, 70~80 DEG C of extraction temperature, feed liquid
It is prepared than 1: 10~15 g/mL, 0.5~1.5h of extraction time.
Maca extract of the present invention is prepared using following steps:
(1) maca fresh root crush after low temperature drying, cross 40~60 meshes and obtain pueraria root powder；(2) with pueraria root powder in above-mentioned step 1)
For raw material, solid-to-liquid ratio 1:10~20 water
It extracts, is decocted at 70~90 DEG C and extract 60~80min；
(3) by above-mentioned steps 2) in filtrate filtered again through cryogenic freezing centrifuge, revolving speed is 1000~2000r/min, when centrifugation
Between 5~10min, collect supernatant to get Maca extract.
Diosmetin of the present invention is prepared using following steps:
(1) using aurantiamarin as raw material, pyridine is solvent, the mass ratio of aurantiamarin and solvent are as follows: auxiliary material iodine, carbon is added in 1:5~15
Sour sodium, 5~15% potassium hydroxide solutions, the mass ratio with auxiliary material are 1:0.01~0.05:0.02~0.05:0.1~0.2, instead
Answering temperature is 90~100 DEG C, 5~12h of reaction time；
(2) it is concentrated under reduced pressure with diosmetin reaction solution in above-mentioned step 1), purified water is added and is sufficiently stirred, filters, filter cake adds again
Purified water stirs into paste, precipitates, and filtering obtains wet diosmetin crude product；
(3) by above-mentioned steps 2) in solvent is added in dissolution kettle, be added with stirring diosmetin crude product, stirring and dissolving is added and lives
Property carbon decoloring, filtering obtains stand-by after filtrate；
(4) by above-mentioned steps 3) in the wet filtrate of diosmetin be adjusted to neutrality with glacial acetic acid after precipitate 5~10h, filters pressing, filter cake
With purifying water washing, it is filtered dry；
(5) by above-mentioned steps 4) in diosmetin wet cake be transferred in double conic rotary vacuum dryer it is dry at 70~80 DEG C of temperature
Up to diosmetin after dry.
Preferably, it is by hyaluronic acid, sodium alginate, potassium alginate, carboxymethyl that polysaccharide solution of the present invention, which is adopted,
One of cellulose, hemicellulose or mixture are dissolved in water acquisition, mass percent concentration 3%.
Preferably, emulsifier of the present invention is hydrogenated soy phosphatidyl choline.
Preferably, emulsifier of the present invention can be substituted with hemicellulose.
Preferably, its molecular weight of emulsifier hemicellulose of the present invention is not more than 10000.
Preferably, preservative of the present invention is Phenoxyethanol.
The beneficial effects of the present invention are:
(1) present invention uses passion fruit shell extract as excellent cosmetics moisturizing antioxidant, for moisturizing anti-wrinkle effect
Significantly.
(2) Moringa seed extract in the present invention, the moringa seeds polyphenol in extraction have been proved to the anti-oxidant function for having fabulous
Energy.
(3) Maca extract in the present invention, the alkaloid component containing maca in extraction.Alkaloid is that maca is mostly important
One of active constituent, wherein again energy can be enhanced, and can eliminate climacteric obstacle, slow down aging based on macamide.
(4) polysaccharide solution in the present invention, facilitates the effect of moisturizing, moisturizing and anti-aging.
(5) prinsepia utilis royle oil is remarkably improved the moisture of skin in the present invention, has good preserving moisture and protecting skin effect.
(6) squalene rich in, Flavonoid substances, polyphenolic substance, these substances tool in walnut oil in the present invention
Promote blood circulation, activate soma, anti-inflammation and sterilization, reduce blood lipid, cholesterol and other effects, human body can be improved comprehensively
Autoimmunity, the effect of playing anti-aging.
(7) diosmetin has anti-oxidant, antibacterial and other effects in the present invention, and applying to cosmetics has removing DPPH free radical
Effect.
(8) emulsifier used in the present invention can be substituted with hemicellulose, further reduce cosmetics long-time service pair
The irritation of skin.
Specific embodiment
With reference to embodiments, the technical solution in the present invention is clearly and completely described.Based in the present invention
Embodiment, every other embodiment obtained by those of ordinary skill in the art without making creative efforts, all
Belong to the scope of protection of the invention.
Embodiment 1
A kind of moisture-keeping crease-shedding cosmetics, by weight, including following components: 5 parts of passion fruit shell extract, Moringa seed extract
1 part, 1 part of Maca extract, 20 parts of polysaccharide (hyaluronic acid) aqueous solution, 2 parts of prinsepia utilis royle oil, 1 part of walnut oil, 1 part of diosmetin,
1 part of emulsifier (hydrogenated soy phosphatidyl choline), 0.1 part of antibacterial agent (Phenoxyethanol).
A kind of preparation method of moisture-keeping crease-shedding cosmetics the following steps are included:
(1) passion fruit shell extract, Moringa seed extract, Maca extract heating stirring is added to being completely dissolved in pure water, protects
Warm 30min；
(2) in above-mentioned steps 1) in be added polysaccharide solution stir evenly, obtain component A；
(3) prinsepia utilis royle oil, walnut oil, diosmetin and emulsifier are merged and is added and stirs to is completely dissolved, it is mutually mixed to form oil
Close object B；
(4) oil mixture B is added in component A, lasting to stir, temperature rises to 55 DEG C, maintains 10min, is added after cooling
Antibacterial agent obtains a kind of moisture-keeping crease-shedding cosmetics.
Embodiment 2
A kind of moisture-keeping crease-shedding cosmetics, by weight, including following components: 15 parts of passion fruit shell extract, moringa seeds extract
5 parts of object, 5 parts of Maca extract, 100 parts of polysaccharide (hyaluronic acid, sodium alginate, potassium alginate, mass ratio 1:1:1) aqueous solution,
10 parts of prinsepia utilis royle oil, 5 parts of walnut oil, 3 parts of diosmetin, 6 parts of emulsifier (hydrogenated soy phosphatidyl choline), antibacterial agent (Phenoxyethanol)
0.2 part.
A kind of preparation method of moisture-keeping crease-shedding cosmetics the following steps are included:
(1) heating is stirred to completely molten after passion fruit shell extract, Moringa seed extract, Maca extract are added in pure water
Solution keeps the temperature 30min；
(2) in above-mentioned steps 1) in be added polysaccharide solution stir evenly, obtain component A；
(3) prinsepia utilis royle oil, walnut oil, diosmetin and emulsifier are merged and is added and stirs to is completely dissolved, it is mutually mixed to form oil
Close object B；
(4) oil mixture B is added in component A, lasting to stir, temperature rises to 60 DEG C, maintains 5min, is added after cooling
Antibacterial agent obtains a kind of moisture-keeping crease-shedding cosmetics.
Embodiment 3
A kind of moisture-keeping crease-shedding cosmetics, by weight, including following components: 10 parts of passion fruit shell extract, moringa seeds extract
3 parts of object, 3 parts of Maca extract, 60 parts of polysaccharide (hemicellulose) aqueous solution, 6 parts of prinsepia utilis royle oil, 3 parts of walnut oil, diosmetin 2
Part, 4 parts of emulsifier (hydrogenated soy phosphatidyl choline), 0.2 part of antibacterial agent (Phenoxyethanol).
A kind of preparation method of moisture-keeping crease-shedding cosmetics the following steps are included:
(1) passion fruit shell extract, Moringa seed extract, Maca extract is added in pure water and is heated to 65 DEG C, stirring and dissolving is made
For A phase；
(2) polysaccharide solution is heated to 70 DEG C, stirred evenly, 20min is kept the temperature, as B phase；
(3) prinsepia utilis royle oil, walnut oil, diosmetin and emulsifier are merged and is added and stirs to is completely dissolved, it is mutually mixed to form oil
Close object C phase；
(4) B is added in A phase, keeps the temperature 70 DEG C after mixing evenly for use；
(5) oil mixture C is added in A phase, lasting to stir, temperature is down to 45 DEG C, insulated and stirred 2h, is added after cooling anti-
Microbial inoculum stirs evenly, and discharging obtains a kind of moisture-keeping crease-shedding cosmetics when room temperature.
Embodiment 4
A kind of moisture-keeping crease-shedding cosmetics, by weight, including following components: 12 parts of passion fruit shell extract, moringa seeds extract
2 parts of object, 3 parts of Maca extract, 40 parts of polysaccharide (carboxymethyl cellulose, hemicellulose, mass ratio 1:1) aqueous solution, prinsepia utilis royle oil 4
Part, 2 parts of walnut oil, 1 part of diosmetin, 5 parts of emulsifier (hydrogenated soy phosphatidyl choline), 0.2 part of antibacterial agent (Phenoxyethanol).
A kind of preparation method of moisture-keeping crease-shedding cosmetics the following steps are included:
(1) passion fruit shell extract, Moringa seed extract, Maca extract is added in pure water and is heated to 65 DEG C, stirring and dissolving is made
For A phase；
(2) polysaccharide solution is heated to 70 DEG C, stirred evenly, 20min is kept the temperature, as B phase；
(3) prinsepia utilis royle oil, walnut oil, diosmetin and emulsifier are merged and is added and stirs to is completely dissolved, it is mutually mixed to form oil
Close object C phase；
(4) B is added in A phase, keeps the temperature 70 DEG C after mixing evenly for use；
(5) oil mixture C is added in A phase again, lasting to stir, temperature is down to 45 DEG C, continues insulated and stirred 2h, cooling
Antibacterial agent is added afterwards to stir evenly, discharges when room temperature and obtains a kind of moisture-keeping crease-shedding cosmetics.
Embodiment 5
A kind of moisture-keeping crease-shedding cosmetics, by weight, including following components: 10 parts of passion fruit shell extract, moringa seeds extract
3 parts of object, 4 parts of Maca extract, 80 parts of polysaccharide (potassium alginate) aqueous solution, 8 parts of prinsepia utilis royle oil, 5 parts of walnut oil, diosmetin 2
Part, 2 parts of emulsifier (hydrogenated soy phosphatidyl choline), 0.3 part of antibacterial agent (Phenoxyethanol).
A kind of preparation method of moisture-keeping crease-shedding cosmetics the following steps are included:
(1) passion fruit shell extract, Moringa seed extract, Maca extract is added in pure water and is heated to 70 DEG C, stirring and dissolving is made
For A phase；
(2) polysaccharide solution is heated to 70 DEG C, stirred evenly, 10min is kept the temperature, as B phase；
(3) prinsepia utilis royle oil, walnut oil, diosmetin and emulsifier are merged and is added and stirs to is completely dissolved, it is mutually mixed to form oil
Close object C phase；
(4) B is added in A phase, keeps the temperature 75 DEG C after mixing evenly for use；
(5) oil mixture C is added in A phase, lasting to stir, temperature is down to 50 DEG C, insulated and stirred 1h, adds after cooling
Enter antibacterial agent to stir evenly, discharging obtains a kind of moisture-keeping crease-shedding cosmetics when room temperature.
Embodiment 6
A kind of moisture-keeping crease-shedding cosmetics, by weight, including following components: 12 parts of passion fruit shell extract, moringa seeds extract
3 parts of object, 3 parts of Maca extract, 40 parts of polysaccharide (hemicellulose) aqueous solution, 6 parts of prinsepia utilis royle oil, 3 parts of walnut oil, diosmetin 1
Part, 2 parts of emulsifier (hemicellulose), 0.3 part of antibacterial agent (Phenoxyethanol).
A kind of preparation method of moisture-keeping crease-shedding cosmetics the following steps are included:
(1) passion fruit shell extract, Moringa seed extract, Maca extract is added in pure water and is heated to 70 DEG C, stirring and dissolving is made
For A phase；
(2) polysaccharide solution is heated to 70 DEG C, stirred evenly, 10min is kept the temperature, as B phase；
(3) prinsepia utilis royle oil, walnut oil, diosmetin and emulsifier are merged and is added and stirs to is completely dissolved, it is mutually mixed to form oil
Close object C phase；
(4) B is added in A phase, keeps the temperature 75 DEG C after mixing evenly for use；
(5) oil mixture C is added in A phase, lasting to stir, temperature is down to 50 DEG C, insulated and stirred 1h, adds after cooling
Enter antibacterial agent to stir evenly, discharging obtains a kind of moisture-keeping crease-shedding cosmetics when room temperature.
Moringa seed extract uses volume fraction of ethanol 70%, 75 DEG C of extraction temperature, solid-liquid ratio 1: 10g/ in above-described embodiment
ML, extraction time 1.5h are prepared.
Maca extract is prepared using following steps in above-described embodiment:
(1) maca fresh root crush after low temperature drying, cross 60 meshes and obtain pueraria root powder；
(2) using pueraria root powder in above-mentioned step 1) as raw material, solid-to-liquid ratio 1:20 water
It extracts, is decocted at 80 DEG C and extract 80min；
(3) by above-mentioned steps 2) in filtrate filtered again through cryogenic freezing centrifuge, revolving speed 2000r/min, centrifugation time 5min,
Supernatant is collected to get Maca extract.
Diosmetin is prepared using following steps in above-described embodiment:
(1) using aurantiamarin as raw material, pyridine is solvent, the mass ratio of aurantiamarin and solvent are as follows: auxiliary material iodine, carbonic acid is added in 1:10
Sodium, 10% potassium hydroxide solution, the mass ratio with auxiliary material are 1:0.03:0.03:0.1, and reaction temperature is 90 DEG C, reaction time
8h；
(2) it is concentrated under reduced pressure with diosmetin reaction solution in above-mentioned step 1), purified water is added and is sufficiently stirred, filters, filter cake adds again
Purified water stirs into paste, precipitates, and filtering obtains wet diosmetin crude product；
(3) by above-mentioned steps 2) in solvent is added in dissolution kettle, be added with stirring diosmetin crude product, stirring and dissolving is added and lives
Property carbon decoloring, filtering obtains stand-by after filtrate；
(4) by above-mentioned steps 3) in the wet filtrate of diosmetin be adjusted to neutrality with glacial acetic acid after precipitate 8h, filters pressing, filter cake purifying
Water washing is filtered dry；
(5) by above-mentioned steps 4) in diosmetin wet cake be transferred in double conic rotary vacuum dryer after 75 DEG C of dryings of temperature
Up to diosmetin.
Claims (8)
1. a kind of moisture-keeping crease-shedding cosmetics, which is characterized in that by weight, including following components: passion fruit shell extract 5~
15 parts, 1~5 part of Moringa seed extract, 1~5 part of Maca extract, 20~100 parts of polysaccharide solution, 2~10 parts of prinsepia utilis royle oil,
1~5 part of walnut oil, 1~3 part of diosmetin, 1~6 part of emulsifier, 0.1~0.3 part of antibacterial agent.
2. a kind of moisture-keeping crease-shedding cosmetics according to claim 1, which is characterized in that the passion fruit shell extract is adopted
It is prepared with following steps:
(1) it is cleaned after peeling passion fruit shell, the passion fruit shell cleaned is placed in crusher and carries out pulverization process；
(2) Extraction solvent ethyl alcohol is added in the passion fruit shell crushed, carries out immersion treatment, is then added on ultrasonator
Carry out ultrasonication processing；
(3) warm water immersion treatment is carried out to the passion fruit shell by ultrasonication processing, is then centrifuged, filtration treatment obtains
Supernatant carries out concentration filtrate to gained supernatant and handles to obtain passion fruit shell extract.
3. a kind of moisture-keeping crease-shedding cosmetics according to claim 1, which is characterized in that the Moringa seed extract uses
Volume fraction of ethanol 60~80%, 70~80 DEG C of extraction temperature, 1: 10~15 g/mL of solid-liquid ratio, extraction time 0.5~1.5h system
It is standby to obtain.
4. a kind of moisture-keeping crease-shedding cosmetics according to claim 1, which is characterized in that the Maca extract is using such as
Lower step preparation:
(1) maca fresh root crush after low temperature drying, cross 40~60 meshes and obtain pueraria root powder；(2) with pueraria root powder in above-mentioned step 1)
For raw material, solid-to-liquid ratio 1:10~20 are extracted with water, and are decocted at 70~90 DEG C and are extracted 60~80min；
(3) by above-mentioned steps 2) in filtrate filtered again through cryogenic freezing centrifuge, revolving speed is 1000~2000r/min, when centrifugation
Between 5~10min, collect supernatant to get Maca extract.
5. a kind of moisture-keeping crease-shedding cosmetics according to claim 1, which is characterized in that the diosmetin is using as follows
Step preparation:
(1) using aurantiamarin as raw material, pyridine is solvent, the mass ratio of aurantiamarin and solvent are as follows: auxiliary material iodine, carbon is added in 1:5~15
Sour sodium, 5~15% potassium hydroxide solutions, the mass ratio with auxiliary material are 1:0.01~0.05:0.02~0.05:0.1~0.2, instead
Answering temperature is 90~100 DEG C, 5~12h of reaction time；
(2) it is concentrated under reduced pressure with diosmetin reaction solution in above-mentioned step 1), purified water is added and is sufficiently stirred, filters, filter cake adds again
Purified water stirs into paste, precipitates, and filtering obtains wet diosmetin crude product；
(3) by above-mentioned steps 2) in solvent is added in dissolution kettle, be added with stirring diosmetin crude product, stirring and dissolving is added and lives
Property carbon decoloring, filtering obtains stand-by after filtrate；
(4) by above-mentioned steps 3) in the wet filtrate of diosmetin be adjusted to neutrality with glacial acetic acid after precipitate 5~10h, filters pressing, filter cake
With purifying water washing, it is filtered dry；
(5) by above-mentioned steps 4) in diosmetin wet cake be transferred in double conic rotary vacuum dryer it is dry at 70~80 DEG C of temperature
Up to diosmetin after dry.
6. a kind of moisture-keeping crease-shedding cosmetics according to claim 1, which is characterized in that the polysaccharide solution is will be saturating
One of bright matter acid, sodium alginate, potassium alginate, carboxymethyl cellulose, hemicellulose or mixture are dissolved in water acquisition.
7. a kind of moisture-keeping crease-shedding cosmetics according to claim 1, which is characterized in that the emulsifier can use hemicellulose
Element substitution.
8. a kind of moisture-keeping crease-shedding cosmetics according to claim 6, which is characterized in that the hemicellulose molecule amount is not
Greater than 10000.
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Cited By (1)
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