CN1096433A - The extraction process of the effective-part of Gynostemma pentaphyllum and drink made from gynostemma - Google Patents
The extraction process of the effective-part of Gynostemma pentaphyllum and drink made from gynostemma Download PDFInfo
- Publication number
- CN1096433A CN1096433A CN 93106940 CN93106940A CN1096433A CN 1096433 A CN1096433 A CN 1096433A CN 93106940 CN93106940 CN 93106940 CN 93106940 A CN93106940 A CN 93106940A CN 1096433 A CN1096433 A CN 1096433A
- Authority
- CN
- China
- Prior art keywords
- gynostemma
- gynostemma pentaphylla
- extraction process
- effective ingredient
- drink made
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
Landscapes
- Coloring Foods And Improving Nutritive Qualities (AREA)
- Non-Alcoholic Beverages (AREA)
Abstract
The present invention relates to the effective-part of Gynostemma pentaphyllum extraction process and drink made from gynostemma.It is gynostemma pentaphylla to be immersed heat lixiviate in the weak alkaline medium or immerse lixiviate under the effect of enzyme in the acid medium, adds the gynostemma pentaphyllum extracting solution that precipitation filter aid sedimentation and filtration must contain saponin, natural complex C again.Its drink made from gynostemma then is that the adding auxiliary material is formulated in this extract.The present invention compares with existing technology, recovery rate height, time weak point, removal of impurities, removes tannin debitterize efficient height.The beverage of being made has pure taste, delicate fragrance, clarification, and every index all meets GB GB2759.
Description
The present invention relates to gynostemma pentaphylla is mainly contained the extraction process of effective constituent, and the drink made from gynostemma of making by this extraction process.
Gynostemma pentaphylla [Gynostemma pentuphyllum(Thurb) Makino] be the herbaceous perennial vine plant of Cucurbitales Curcurbitaceae gynostemma pentaphyllum genus (Gynostemma BI), have another name called seven leaf courages ginseng, China's fecund wide geographic area on the south the Changjiang river, because of containing abundant panaxoside, be described as " southern genseng ".
From gynostemma pentaphylla, extracted 80 surplus kind of gynosaponin, all belong to Dammar alkanols structure.Total saponin content of gynostemma pentaphyllum is 3 times of genseng, but excessive use does not have the side effect of genseng excessive use.Prove through pharmacological research: gynostemma pentaphylla has effects such as clearing heat and detoxicating, cough-relieving apophlegmatic, reducing blood lipid, tranquilizing and allaying excitement, anti arteriosclerosis, multiple cancer cell there is inhibitory action, diseases such as hepatitis B, bronchitis, diabetes, gastroenteritis are had curative effect preferably.Also has the effect that improves body's immunity, hypnosis and treatment alopecia senilis and graying of hair.
Be worth because gynostemma pentaphylla has higher medicinal and health care, doing many research aspect the extraction gynosaponin both at home and abroad in recent years, and proposing some extracting methods thus.For example:
In the clear 61-104772 of Japan's special permission communique, disclose under the condition in non-alkalescence, adopted 5 times water or moisture lower alcohol that gynostemma pentaphylla is extracted, made the saponin composition in the solvent of alkali-free, be extracted out as far as possible.
Improved technical solution to the clear 61-104772 of Japan's special permission communique is disclosed in Chinese patent 89103598.2, its major technique feature is with poach or the gynostemma pentaphylla concentrate that extracts with 20～60% ethanol heating, filtration, evaporation and concentration, in concentrate, add hydrochloric acid or phosphoric acid acidifying then, add the sodium carbonate neutralization again, eliminate blue or green stink, astringent taste in the concentrate with this, thereby reach requirement as beverage.
After this, Hangzhou pharmaceutical factory, Guangxi Gold show food factory and the Ankang pharmaceutical factory of traditional Chinese medicine etc. successively adopt similar techniques to be used for Development and Production to go out the medicinal or health-care nutritional foods of multiple gynostemma pentaphylla such as gynostemma pentaphylla concentrate, gynostemium pentaphylla oral liquid, Herb Gynostemmae Pentaphylli total glycosides tablet, gynostemma pentaphylla health-care tea and Gynostemma wine.
Above-mentioned prior art has obtained gratifying achievement on extraction gynostemma pentaphylla effective ingredient, avoided separating out of tannin to a certain extent, removed the part bitter taste, but because of in extraction, having used a large amount of ethanol and other organic solvents, reclaim complexity of technology to making, production scale is little, and process conditions are wayward, and operation easier is big.Though the decocting extraction method is simple than ethanol extraction method technology, but exist recovery rate not high.Particularly prior art is advocated and should be extracted saponin in non-alkaline medium.
For this reason, it is simple to the objective of the invention is to develop a kind of technology, consuming time few, not only need not ethanol but also be different from decocting method, and can make effective ingredient saponin recovery rate height and the high gynostemma pentaphylla effective ingredient extraction process of vitamin C recovery rate, and the drink made from gynostemma made of the gynostemma pentaphyllum extracting solution that utilizes this technology to extract.
Technical solution of the present invention relates to the prescription of gynostemma pentaphylla effective ingredient extraction process and drink made from gynostemma, and existing division is as follows:
Gynostemma pentaphylla effective ingredient extraction process of the present invention is divided into following two kinds:
One, adopt the gynostemma pentaphylla aerial part, add water, add alkali and regulate the alkalescent of pH value to 7.5～8.5, be heated to the lixiviate 10～15 minutes of boiling, adding edible acid for adjusting pH value again is 4.5～5.0, and adds the precipitation filter aid by 0.01～1% amount, through staticly settling filtration, get supernatant and be the extract that contains the gynostemma pentaphylla effective ingredient.
They are two years old, get gynostemma pentaphylla partly on the ground, add water, with edible acid for adjusting pH value is 3.9～4.5, and the control temperature is below 40 ℃, and add the enzyme insulated and stirred lixiviate that mixes with any ratio by hemicellulase and pectase in 0.04～0.1% amount, and add in leaching liquor by 0.01～1% amount again and precipitate filter aid, promptly get and be rich in the ascorbic extract that contains the gynostemma pentaphylla effective ingredient through staticly settling filtration.
Used precipitation filter aid is meant that CTS wadding agent (being produced by Chinese Academy of Sciences ecological environment center), PACS synergy flocculant (converging eastern new technology affiliated company by Beijing produces), ST flocculant (being produced by chemical plant, Yuyao, Zhejiang) and main composition are any in the diatomaceous precipitation filter aid in above-mentioned " one ", " its two " technology.
Drink made from gynostemma of the present invention is the drink made from gynostemma that a kind of extract that utilizes gynostemma pentaphylla effective ingredient extraction process of the present invention to extract to contain the gynostemma pentaphylla effective ingredient is made, the technical solution of this drink formula includes each component content prescription in raw material proportioning and the drink made from gynostemma, wherein:
Described raw material proportioning (by weight) is: gynostemma pentaphylla is 0.1～4:3～10 with the ratio of auxiliary material.
Each component content prescription (by wt%) is in the described drink made from gynostemma: gynostemma pentaphylla 0.052%, auxiliary material 1.53～5.2%.
Described gynostemma pentaphylla is the ground part of gynostemma pentaphylla.
Described auxiliary material is meant one or more the auxiliary material that comprises in Radix Glycyrrhizae, natural acid, the natural sweetener.Wherein, the consumption of Radix Glycyrrhizae, natural acid, natural sweetener should not surpass respectively: 0.08%, 0.06%, 5.2%.
So far, the present invention has reached its intended purposes, because extraction process of the present invention has adopted the unexistent weak alkaline medium hot water extracting of prior art to add the technology that precipitates filter aid, so compared with prior art have following characteristics at least:
Saponin content in one, the extract made by technology of the present invention and dissolution rate all is higher than existing decocting method and alcohol extracting is followed the example of, and be rich in natural complex C.
Its two, the required lixiviate of technology of the present invention, the sedimentation time is less than decocting method far away and alcohol extracting is followed the example of, and can improve work efficiency greatly.
Also improve the removal of impurity when three, the adding of precipitation filter aid is accelerated settling velocity and removed the efficient of tannin debitterize, and can partly eliminate the oxygen in the extract, be beneficial to the preservation of extract.
Four, technology of the present invention is applicable to the continuity production in enormous quantities.
With technology of the present invention and drink made from gynostemma of the present invention prescription, the drink made from gynostemma finished product of making has gynostemma pentaphylla delicate fragrance, and pure taste, clarification pale green.Every index all meets national GB2759 standard.
Example 1: the gynostemma pentaphylla of getting equivalent is followed the example of by decocting method, the alcohol extracting of prior art respectively and technology of the present invention is extracted experiment, saponin amount, dissolution rate that extraction presentation of results technology of the present invention extracts are the highest, alcohol extracting follows the example of the second, and decocting method is minimum, sees following table for details.
| Extraction process | Total saponin content (g/100ml) | Dissolution rate (%) |
| Decocting method | 0.81 | 15.21 |
| Alcohol extracting | 3.40 | 63.85 |
| The present invention | 3.75 | 70.42 |
Example 2: get gynostemma pentaphylla 6kg(wherein 1kg, bright 5kg), Radix Glycyrrhizae 300g, citric acid 500g, white sugar 25kg, honey 500g by the raw material proportioning of the above-mentioned drink made from gynostemma of the present invention, carry out lixiviate earlier by the above-mentioned gynostemma pentaphylla effective ingredient of the present invention extraction process, dried gynostemma pentaphyllum extracting solution that subsequently extraction is obtained and bright gynostemma pentaphyllum extracting solution and auxiliary material (Radix Glycyrrhizae, acid, sweetener) merging is deployed into 1000kg and prepares liquid, promptly gets the gynostemma pentaphylla healthy beverage after centrifugation filtration, sterilization.Every after testing quality, sanitary index all meet GB GB2759 standard.
Claims (6)
1, a kind of gynostemma pentaphylla effective ingredient extraction process, it is characterized in that, be in the pH value is 7.5～8.5 weak alkaline medium, to be heated to the lixiviate of boiling, adding edible acid for adjusting pH again is 4.5～5.0, and add the precipitation filter aid by 0.01～1% amount, through staticly settling filtration, get supernatant for containing gynostemma pentaphylla effective ingredient extract.
2, a kind of gynostemma pentaphylla effective ingredient extraction process, it is characterized in that, be under 3.9～4.5 the acid condition in the pH value, temperature is below 40 ℃, and add in 0.04～0.1% amount and to carry out insulated and stirred with the enzyme that pectase mixes with any ratio by hemicellulase, lixiviate adds the precipitation filter aid by 0.01～1% amount subsequently, promptly gets and is rich in ascorbic gynostemma pentaphylla effective ingredient extract through staticly settling filtration.
3,, it is characterized in that wherein said precipitation filter aid is meant that CTS flocculant, PACS synergy flocculant, ST flocculant and main composition are any in the diatomaceous precipitation filter aid according to the extraction process of claim 1 or claim 2.
4, a kind of extraction process of utilizing claim 1 or claim 2 extracts and contains the drink made from gynostemma that the gynostemma pentaphylla effective ingredient is made, and it is characterized in that the prescription of each component content in the raw material proportioning of this beverage and the drink made from gynostemma is respectively:
Raw material proportioning (by weight) is: gynostemma pentaphylla is 0.1～4:3～10 with the ratio of auxiliary material;
The prescription of each component content (by wt%) is in the drink made from gynostemma: gynostemma pentaphylla 0.05～2%, auxiliary material 1.53～5.2%.
5, drink made from gynostemma according to claim 4 is characterized in that wherein said auxiliary material is meant one or more the auxiliary material that comprises in Radix Glycyrrhizae, natural acid, the natural sweetener.
6, extraction process according to claim 1 is characterized in that, alkalescent is to be to use Na
2CO
3Or NaOH modulation forms.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 93106940 CN1096433A (en) | 1993-06-15 | 1993-06-15 | The extraction process of the effective-part of Gynostemma pentaphyllum and drink made from gynostemma |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 93106940 CN1096433A (en) | 1993-06-15 | 1993-06-15 | The extraction process of the effective-part of Gynostemma pentaphyllum and drink made from gynostemma |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN1096433A true CN1096433A (en) | 1994-12-21 |
Family
ID=4986495
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN 93106940 Pending CN1096433A (en) | 1993-06-15 | 1993-06-15 | The extraction process of the effective-part of Gynostemma pentaphyllum and drink made from gynostemma |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN1096433A (en) |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1317295C (en) * | 2003-01-16 | 2007-05-23 | 北京大学安康药物研究院 | Preparation method of gynostemma pentaphylia total saponin |
| CN100438781C (en) * | 2004-12-10 | 2008-12-03 | 何建强 | Health-care beverage and its prepn. method |
| CN105748563A (en) * | 2015-09-21 | 2016-07-13 | 北京大学安康药物研究院 | Preparation method of gypenosides |
| CN113893276A (en) * | 2021-11-11 | 2022-01-07 | 北华大学 | Composition for improving sleep and preparation method and application thereof |
-
1993
- 1993-06-15 CN CN 93106940 patent/CN1096433A/en active Pending
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1317295C (en) * | 2003-01-16 | 2007-05-23 | 北京大学安康药物研究院 | Preparation method of gynostemma pentaphylia total saponin |
| CN100438781C (en) * | 2004-12-10 | 2008-12-03 | 何建强 | Health-care beverage and its prepn. method |
| CN105748563A (en) * | 2015-09-21 | 2016-07-13 | 北京大学安康药物研究院 | Preparation method of gypenosides |
| CN105748563B (en) * | 2015-09-21 | 2019-12-13 | 北京大学安康药物研究院 | Method for preparing gypenoside |
| CN113893276A (en) * | 2021-11-11 | 2022-01-07 | 北华大学 | Composition for improving sleep and preparation method and application thereof |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN1066055C (en) | Production method for extracting flavonoid compound extract or powder from bamboo leaf | |
| CN106243172B (en) | A method of extracting black fruit fructus lycii anthocyanin | |
| CN101073433A (en) | Blackthorn pear fruit-juice solid product and its production | |
| CN105030878A (en) | Method for extracting multiple active ingredients of blueberry fruits | |
| CN101496854A (en) | Chinese medicine sobering-up composition and Chinese medicine sobering-up beverage | |
| CN1425643A (en) | Extracting and purifying method for chlorogenic acid in honeysuckle | |
| CN103992876A (en) | Extraction method of passionflower seed oil | |
| CN101288465A (en) | Mushroom oral liquid | |
| CN102860549A (en) | Functional beverage having functions of beautifying and detoxification and preparation method thereof | |
| CN102178004B (en) | Health-care Puer tea drink | |
| CN103767011B (en) | A kind of plant beverage and preparation method thereof | |
| CN107496490B (en) | A kind of Herba Epimedii rhodiola rosea formulated product and preparation method thereof | |
| CN1096433A (en) | The extraction process of the effective-part of Gynostemma pentaphyllum and drink made from gynostemma | |
| CN1557382A (en) | Glucoside compound preparation and its preparing process | |
| CN1288168C (en) | Polysaccharides compound preparation and method for preparing the same | |
| CN101228958A (en) | Method of extracting amylose and red-yellow pigment from medlar as accretion used for rhodiola rosea beverage | |
| CN106578218A (en) | Method for extraction of Camellia nitidissima effective ingredients with small molecular group water and use | |
| CN109430645A (en) | A kind of novel honeysuckle compound beverage and preparation method thereof | |
| CN114431470A (en) | Astragalus stem and leaf decoction and preparation method thereof | |
| CN114404517A (en) | Composition for gout and reducing uric acid and application and preparation method thereof | |
| CN106937718A (en) | A kind of pair of marine alga pollen plant composite beverage and preparation method thereof | |
| CN1472207A (en) | Extracting method of polyphenol from lotus root | |
| CN1068379C (en) | Preparation method for high grade Chinese wolfberry fruit wine | |
| CN102210368B (en) | Health-care coffee beverage | |
| CN108782870A (en) | A kind of anti-tumor healthcare tea and preparation method thereof |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C01 | Deemed withdrawal of patent application (patent law 1993) | ||
| WD01 | Invention patent application deemed withdrawn after publication |