CN109529766A - A kind of environmentally friendly moisture absorption PVC desiccant and preparation method thereof by force - Google Patents
A kind of environmentally friendly moisture absorption PVC desiccant and preparation method thereof by force Download PDFInfo
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- CN109529766A CN109529766A CN201811501622.7A CN201811501622A CN109529766A CN 109529766 A CN109529766 A CN 109529766A CN 201811501622 A CN201811501622 A CN 201811501622A CN 109529766 A CN109529766 A CN 109529766A
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- B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
- B01J20/02—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material
- B01J20/20—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material comprising free carbon; comprising carbon obtained by carbonising processes
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D53/00—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
- B01D53/26—Drying gases or vapours
- B01D53/28—Selection of materials for use as drying agents
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- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
- B01J20/02—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
- B01J20/02—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material
- B01J20/04—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material comprising compounds of alkali metals, alkaline earth metals or magnesium
- B01J20/041—Oxides or hydroxides
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- B—PERFORMING OPERATIONS; TRANSPORTING
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- B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
- B01J20/02—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material
- B01J20/06—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material comprising oxides or hydroxides of metals not provided for in group B01J20/04
- B01J20/08—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material comprising oxides or hydroxides of metals not provided for in group B01J20/04 comprising aluminium oxide or hydroxide; comprising bauxite
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- B—PERFORMING OPERATIONS; TRANSPORTING
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- B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
- B01J20/02—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material
- B01J20/10—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material comprising silica or silicate
- B01J20/103—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material comprising silica or silicate comprising silica
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
- B01J20/02—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material
- B01J20/10—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material comprising silica or silicate
- B01J20/12—Naturally occurring clays or bleaching earth
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D2253/00—Adsorbents used in seperation treatment of gases and vapours
- B01D2253/10—Inorganic adsorbents
- B01D2253/102—Carbon
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D2253/00—Adsorbents used in seperation treatment of gases and vapours
- B01D2253/10—Inorganic adsorbents
- B01D2253/104—Alumina
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D2253/00—Adsorbents used in seperation treatment of gases and vapours
- B01D2253/10—Inorganic adsorbents
- B01D2253/106—Silica or silicates
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D2253/00—Adsorbents used in seperation treatment of gases and vapours
- B01D2253/10—Inorganic adsorbents
- B01D2253/106—Silica or silicates
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- B—PERFORMING OPERATIONS; TRANSPORTING
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- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2220/00—Aspects relating to sorbent materials
- B01J2220/40—Aspects relating to the composition of sorbent or filter aid materials
- B01J2220/42—Materials comprising a mixture of inorganic materials
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
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- B01J2220/00—Aspects relating to sorbent materials
- B01J2220/40—Aspects relating to the composition of sorbent or filter aid materials
- B01J2220/48—Sorbents characterised by the starting material used for their preparation
- B01J2220/4806—Sorbents characterised by the starting material used for their preparation the starting material being of inorganic character
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- B—PERFORMING OPERATIONS; TRANSPORTING
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- B01J2220/00—Aspects relating to sorbent materials
- B01J2220/40—Aspects relating to the composition of sorbent or filter aid materials
- B01J2220/48—Sorbents characterised by the starting material used for their preparation
- B01J2220/4812—Sorbents characterised by the starting material used for their preparation the starting material being of organic character
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2220/00—Aspects relating to sorbent materials
- B01J2220/40—Aspects relating to the composition of sorbent or filter aid materials
- B01J2220/48—Sorbents characterised by the starting material used for their preparation
- B01J2220/4812—Sorbents characterised by the starting material used for their preparation the starting material being of organic character
- B01J2220/4825—Polysaccharides or cellulose materials, e.g. starch, chitin, sawdust, wood, straw, cotton
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Abstract
The present invention provides a kind of environmentally friendly moisture absorption PVC desiccant and preparation method thereof by force, and the PVC desiccant includes the ingredient of following parts by weight: iron powder: 20 ~ 30 parts, bamboo charcoal: 10 ~ 15 parts, silica: 15 ~ 20 parts, benzotriazole: 10 ~ 15 parts, hollow glass microbead: 15 ~ 25 parts, bentonite: 5 ~ 10 parts, attapulgite: 5 ~ 10 parts, carboxymethyl cellulose: 5 ~ 10 parts, calcium oxide: 5 ~ 10 parts, quartz sand: 10 ~ 15 parts, binder: 1 ~ 5 part, nanometer mildew proofing agent: 1 ~ 5 part, deoxidier: 1 ~ 5 part.Rationally, production technology is environmentally friendly for the desiccant ingredient design, and production gained desiccant is environmentally friendly, and asepsis environment-protecting, long service life, production cost is low, good in economic efficiency.
Description
Technical field
The invention belongs to desiccant production technical fields, and in particular, to a kind of environmentally friendly moisture absorption PVC desiccant and its system by force
Preparation Method.
Background technique
Desiccant refers to the substance that can remove moisture in moist substance, is often divided into two classes: chemical drier, such as calcium sulfate and
Calcium chloride etc. is dried by generating hydrate in conjunction with water;Physical dryness agent, such as silica gel and activated alumina, pass through
Physical absorption water is dried.
It is closely bound up that the control of moisture, which is with the yield of product,.For food, under temperature and humidity appropriate,
Bacterium and mould in food will breed at an amazing speed, make food spoilage, cause dampness and discoloration.Electronic product also can
Because metal aoxidizes caused by humidity is excessively high, generate bad.The use of desiccant is just intended to extra moisture is avoided to cause bad
The generation of product.
For desiccant, the Chinese patent of Publication No. CN103506068B discloses a kind of New Mineral titanium dioxide silicon wafer
The preparation method of shape desiccant and Novel mineral silicon dioxide flake desiccant obtained by this method.The method includes
Following steps: 1) mineral silica desiccant powder with water is granulated;2) particle being dried to obtain;3) to dried
Grain sieving;4) by the particle compression moulding after sieving;5) particle of dry compression moulding, is made New Mineral silica sheet
Desiccant.It uses mineral silica powder for raw material, on Mechanical pressing molding machine, the mold of different size specification can be used,
Suppress the product of different-thickness specification;Novel mineral silicon dioxide flake desiccant obtained, compared with prior art, in consubstantiality
In product situation, total hygroscopic capacity is higher, and moisture pick-up properties is stablized;Can be consistent with use space size, safety and environmental protection;It is able to achieve
Automated production has huge application prospect and economic value.However, desiccant provided by the patent, is mineral dioxy
SiClx desiccant is not particularly suited for PVC use.
Summary of the invention
It is above-mentioned to solve the problems, such as, the purpose of the present invention is to provide a kind of strong moisture absorption PVC desiccant of environmental protection and its
Preparation method, rationally, production technology is environmentally friendly for the desiccant ingredient design, and production gained desiccant is environmentally friendly,
Asepsis environment-protecting, long service life, production cost is low, good in economic efficiency.
In order to achieve the above objectives, the technical scheme is that
A kind of strong moisture absorption PVC desiccant of environmental protection, the PVC desiccant includes the ingredient of following parts by weight: iron powder: 20 ~ 30 parts, bamboo
Charcoal: 10 ~ 15 parts, silica: 15 ~ 20 parts, benzotriazole: 10 ~ 15 parts, hollow glass microbead: 15 ~ 25 parts, bentonite: 5 ~
10 parts, attapulgite: 5 ~ 10 parts, carboxymethyl cellulose: 5 ~ 10 parts, calcium oxide: 5 ~ 10 parts, quartz sand: 10 ~ 15 parts, binder:
1 ~ 5 part, nanometer mildew proofing agent: 1 ~ 5 part, deoxidier: 1 ~ 5 part.
Further, the PVC desiccant includes the ingredient of following parts by weight: iron powder: 25 ~ 30 parts, bamboo charcoal: and 13 ~ 15 parts,
Silica: 15 ~ 18 parts, benzotriazole: 10 ~ 13 parts, hollow glass microbead: 20 ~ 25 parts, bentonite: 5 ~ 8 parts, concave convex rod
Soil: 5 ~ 7 parts, carboxymethyl cellulose: 6 ~ 10 parts, calcium oxide: 7 ~ 10 parts, quartz sand: 10 ~ 12 parts, binder: 1 ~ 3 part, nanometer is anti-
Mould dose: 1 ~ 4 part, deoxidier: 2 ~ 5 parts.
Further, the PVC desiccant includes the ingredient of following parts by weight: iron powder: 25 parts, bamboo charcoal: and 13 parts, titanium dioxide
Silicon: 17 parts, benzotriazole: 13 parts, hollow glass microbead: 20 parts, bentonite: 7 parts, attapulgite: 6 parts, carboxymethyl cellulose
Element: 7 parts, calcium oxide: 8 parts, quartz sand: 12 parts, binder: 3 parts, nanometer mildew proofing agent: 4 parts, deoxidier: 3 parts.
Further, the deoxidier is nano silica or aluminium oxide.
Further, the nanometer mildew proofing agent is Nano-Zinc, nano silver or silver nitrate.
Further, the binder is sodium metasilicate.
Meanwhile the present invention also provides a kind of preparation method of the strong moisture absorption PVC desiccant of environmental protection, the preparation method includes such as
Lower step: according to the proportion by the iron powder, bamboo charcoal, silica, benzotriazole, hollow glass microbead, bentonite, concave convex rod
It is crushed, is crushed after soil, carboxymethyl cellulose, calcium oxide, quartz sand, binder, nanometer mildew proofing agent and deoxidier mixing
Compound particles granularity afterwards is in 0.5mm hereinafter, smashed mixture is roasted, and maturing temperature is 600 ~ 800 DEG C, roasting
Burning the time is 40 ~ 50 minutes, is subsequently placed in high speed disperser and disperses 2 ~ 3 hours, and rate of dispersion is 2200 ~ 2500 revs/min,
It is placed in drying box, dries 2 ~ 3 hours in 100 ~ 110 DEG C to get finished product, obtain the strong moisture absorption PVC desiccant of the environmental protection.
The beneficial effects of the present invention are:
Rationally, production technology is environmentally friendly for the desiccant ingredient design, and production gained desiccant is environmentally friendly, no poison ring
It protects, long service life, production cost is low, good in economic efficiency.
Specific embodiment
The strong moisture absorption PVC desiccant of a kind of environmental protection of the present invention, the PVC desiccant include following parts by weight at
Point: iron powder: 20 ~ 30 parts, bamboo charcoal: 10 ~ 15 parts, silica: 15 ~ 20 parts, benzotriazole: 10 ~ 15 parts, hollow glass is micro-
Pearl: 15 ~ 25 parts, bentonite: 5 ~ 10 parts, attapulgite: 5 ~ 10 parts, carboxymethyl cellulose: 5 ~ 10 parts, calcium oxide: 5 ~ 10 parts, stone
Sand: 10 ~ 15 parts, binder: 1 ~ 5 part, nanometer mildew proofing agent: 1 ~ 5 part, deoxidier: 1 ~ 5 part.
Further, the PVC desiccant includes the ingredient of following parts by weight: iron powder: 25 ~ 30 parts, bamboo charcoal: and 13 ~ 15 parts,
Silica: 15 ~ 18 parts, benzotriazole: 10 ~ 13 parts, hollow glass microbead: 20 ~ 25 parts, bentonite: 5 ~ 8 parts, concave convex rod
Soil: 5 ~ 7 parts, carboxymethyl cellulose: 6 ~ 10 parts, calcium oxide: 7 ~ 10 parts, quartz sand: 10 ~ 12 parts, binder: 1 ~ 3 part, nanometer is anti-
Mould dose: 1 ~ 4 part, deoxidier: 2 ~ 5 parts.
Further, the PVC desiccant includes the ingredient of following parts by weight: iron powder: 25 parts, bamboo charcoal: and 13 parts, titanium dioxide
Silicon: 17 parts, benzotriazole: 13 parts, hollow glass microbead: 20 parts, bentonite: 7 parts, attapulgite: 6 parts, carboxymethyl cellulose
Element: 7 parts, calcium oxide: 8 parts, quartz sand: 12 parts, binder: 3 parts, nanometer mildew proofing agent: 4 parts, deoxidier: 3 parts.
Further, the deoxidier is nano silica or aluminium oxide.
Further, the nanometer mildew proofing agent is Nano-Zinc, nano silver or silver nitrate.
Further, the binder is sodium metasilicate.
Meanwhile the present invention also provides a kind of preparation method of the strong moisture absorption PVC desiccant of environmental protection, the preparation method includes such as
Lower step: according to the proportion by the iron powder, bamboo charcoal, silica, benzotriazole, hollow glass microbead, bentonite, concave convex rod
It is crushed, is crushed after soil, carboxymethyl cellulose, calcium oxide, quartz sand, binder, nanometer mildew proofing agent and deoxidier mixing
Compound particles granularity afterwards is in 0.5mm hereinafter, smashed mixture is roasted, and maturing temperature is 600 ~ 800 DEG C, roasting
Burning the time is 40 ~ 50 minutes, is subsequently placed in high speed disperser and disperses 2 ~ 3 hours, and rate of dispersion is 2200 ~ 2500 revs/min,
It is placed in drying box, dries 2 ~ 3 hours in 100 ~ 110 DEG C to get finished product, obtain the strong moisture absorption PVC desiccant of the environmental protection.
It should be noted that the above examples are only used to illustrate the technical scheme of the present invention and are not limiting.Although referring to compared with
Good embodiment describes the invention in detail, those skilled in the art should understand that, it can be to the technology of invention
Scheme is modified or replaced equivalently, and without departing from the range of technical solution of the present invention, should all be covered in power of the invention
In sharp claimed range.
Claims (7)
1. a kind of strong moisture absorption PVC desiccant of environmental protection, which is characterized in that the PVC desiccant includes the ingredient of following parts by weight: iron
Powder: 20 ~ 30 parts, bamboo charcoal: 10 ~ 15 parts, silica: 15 ~ 20 parts, benzotriazole: 10 ~ 15 parts, hollow glass microbead: 15 ~
25 parts, bentonite: 5 ~ 10 parts, attapulgite: 5 ~ 10 parts, carboxymethyl cellulose: 5 ~ 10 parts, calcium oxide: 5 ~ 10 parts, quartz sand:
10 ~ 15 parts, binder: 1 ~ 5 part, nanometer mildew proofing agent: 1 ~ 5 part, deoxidier: 1 ~ 5 part.
2. the strong moisture absorption PVC desiccant of environmental protection according to claim 1, which is characterized in that the PVC desiccant includes as follows
The ingredient of parts by weight: iron powder: 25 ~ 30 parts, bamboo charcoal: 13 ~ 15 parts, silica: 15 ~ 18 parts, benzotriazole: 10 ~ 13 parts, in
Empty glass microballoon: 20 ~ 25 parts, bentonite: 5 ~ 8 parts, attapulgite: 5 ~ 7 parts, carboxymethyl cellulose: 6 ~ 10 parts, calcium oxide: 7 ~
10 parts, quartz sand: 10 ~ 12 parts, binder: 1 ~ 3 part, nanometer mildew proofing agent: 1 ~ 4 part, deoxidier: 2 ~ 5 parts.
3. the strong moisture absorption PVC desiccant of environmental protection according to claim 1, which is characterized in that the PVC desiccant includes as follows
The ingredient of parts by weight: iron powder: 25 parts, bamboo charcoal: 13 parts, silica: 17 parts, benzotriazole: 13 parts, hollow glass microbead:
20 parts, bentonite: 7 parts, attapulgite: 6 parts, carboxymethyl cellulose: 7 parts, calcium oxide: 8 parts, quartz sand: 12 parts, binder: 3
Part, nanometer mildew proofing agent: 4 parts, deoxidier: 3 parts.
4. the strong moisture absorption PVC desiccant of environmental protection according to claim 1, which is characterized in that the deoxidier is nano-silica
SiClx or aluminium oxide.
5. the strong moisture absorption PVC desiccant of environmental protection according to claim 1, which is characterized in that the nanometer mildew proofing agent is nanometer
Zinc, nano silver or silver nitrate.
6. the strong moisture absorption PVC desiccant of environmental protection according to claim 1, which is characterized in that the binder is sodium metasilicate.
7. a kind of preparation method of the strong moisture absorption PVC desiccant of environmental protection as described in any one of claim 1 ~ 6, feature exist
Include the following steps: according to the proportion in, the preparation method by the iron powder, bamboo charcoal, silica, benzotriazole, hollow
Glass microballoon, bentonite, attapulgite, carboxymethyl cellulose, calcium oxide, quartz sand, binder, nanometer mildew proofing agent and deoxidation
Crushed after agent mixing, smashed compound particles granularity in 0.5mm hereinafter, smashed mixture is roasted,
Maturing temperature is 600 ~ 800 DEG C, and calcining time is 40 ~ 50 minutes, is subsequently placed in high speed disperser and disperses 2 ~ 3 hours, is dispersed
Speed is 2200 ~ 2500 revs/min, is placed in drying box, dries 2 ~ 3 hours in 100 ~ 110 DEG C to get finished product, obtains described
Environmentally friendly strong moisture absorption PVC desiccant.
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Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
WO2021113367A1 (en) * | 2019-12-02 | 2021-06-10 | Ingevity South Carolina, Llc | Low emission adsorbent |
Citations (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN103638785A (en) * | 2013-11-12 | 2014-03-19 | 刘臣宇 | Drying agent with mildew-proof effect and preparation method thereof |
CN106914110A (en) * | 2017-04-11 | 2017-07-04 | 安徽博硕科技有限公司 | A kind of degerming drier and preparation method thereof |
CN107930603A (en) * | 2017-11-21 | 2018-04-20 | 王小艳 | A kind of dried flower protects drier used and preparation method thereof in prepared by color drying plate |
-
2018
- 2018-12-10 CN CN201811501622.7A patent/CN109529766A/en active Pending
Patent Citations (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN103638785A (en) * | 2013-11-12 | 2014-03-19 | 刘臣宇 | Drying agent with mildew-proof effect and preparation method thereof |
CN106914110A (en) * | 2017-04-11 | 2017-07-04 | 安徽博硕科技有限公司 | A kind of degerming drier and preparation method thereof |
CN107930603A (en) * | 2017-11-21 | 2018-04-20 | 王小艳 | A kind of dried flower protects drier used and preparation method thereof in prepared by color drying plate |
Cited By (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
WO2021113367A1 (en) * | 2019-12-02 | 2021-06-10 | Ingevity South Carolina, Llc | Low emission adsorbent |
CN114746174A (en) * | 2019-12-02 | 2022-07-12 | 英格维蒂南卡罗来纳有限责任公司 | Low emission sorbent |
US11938461B2 (en) | 2019-12-02 | 2024-03-26 | Ingevity South Carolina, Llc | Low emission adsorbent |
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