CN109468173A - Quick-fried pearl base oil and preparation method thereof with natural cream perfume (or spice) note - Google Patents
Quick-fried pearl base oil and preparation method thereof with natural cream perfume (or spice) note Download PDFInfo
- Publication number
- CN109468173A CN109468173A CN201811372408.6A CN201811372408A CN109468173A CN 109468173 A CN109468173 A CN 109468173A CN 201811372408 A CN201811372408 A CN 201811372408A CN 109468173 A CN109468173 A CN 109468173A
- Authority
- CN
- China
- Prior art keywords
- perfume
- quick
- spice
- note
- base oil
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
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- 239000002304 perfume Substances 0.000 title claims abstract description 49
- 239000002199 base oil Substances 0.000 title claims abstract description 32
- 239000006071 cream Substances 0.000 title claims abstract description 31
- 235000013599 spices Nutrition 0.000 title claims abstract description 30
- 238000002360 preparation method Methods 0.000 title claims abstract description 12
- 239000000463 material Substances 0.000 claims abstract description 20
- 239000002994 raw material Substances 0.000 claims abstract description 16
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 claims abstract description 14
- 241001060310 Styracaceae Species 0.000 claims abstract description 11
- 235000001361 Styrax officinalis Nutrition 0.000 claims abstract description 11
- 235000019382 gum benzoic Nutrition 0.000 claims abstract description 11
- NXMUXTAGFPJGTQ-UHFFFAOYSA-N decanoic acid;octanoic acid Chemical compound CCCCCCCC(O)=O.CCCCCCCCCC(O)=O NXMUXTAGFPJGTQ-UHFFFAOYSA-N 0.000 claims abstract description 7
- 235000011187 glycerol Nutrition 0.000 claims abstract description 7
- 150000005691 triesters Chemical class 0.000 claims abstract description 7
- 238000002604 ultrasonography Methods 0.000 claims abstract description 7
- 239000012535 impurity Substances 0.000 claims abstract description 6
- 230000000284 resting effect Effects 0.000 claims abstract description 3
- GHVNFZFCNZKVNT-UHFFFAOYSA-N Decanoic acid Natural products CCCCCCCCCC(O)=O GHVNFZFCNZKVNT-UHFFFAOYSA-N 0.000 claims description 3
- 239000005632 Capric acid (CAS 334-48-5) Substances 0.000 claims description 2
- 235000019504 cigarettes Nutrition 0.000 abstract description 12
- 239000003205 fragrance Substances 0.000 abstract description 10
- 238000000465 moulding Methods 0.000 abstract description 5
- 235000015511 Liquidambar orientalis Nutrition 0.000 abstract description 4
- 241000736148 Styrax Species 0.000 abstract description 4
- 239000004870 Styrax Substances 0.000 abstract description 4
- 235000000126 Styrax benzoin Nutrition 0.000 abstract description 4
- 241000411851 herbal medicine Species 0.000 abstract description 3
- 239000003921 oil Substances 0.000 abstract description 2
- 239000000654 additive Substances 0.000 abstract 1
- 230000000996 additive effect Effects 0.000 abstract 1
- 238000001914 filtration Methods 0.000 abstract 1
- 230000000052 comparative effect Effects 0.000 description 4
- 150000001875 compounds Chemical class 0.000 description 4
- 238000000034 method Methods 0.000 description 4
- NIPNSKYNPDTRPC-UHFFFAOYSA-N N-[2-oxo-2-(2,4,6,7-tetrahydrotriazolo[4,5-c]pyridin-5-yl)ethyl]-2-[[3-(trifluoromethoxy)phenyl]methylamino]pyrimidine-5-carboxamide Chemical compound O=C(CNC(=O)C=1C=NC(=NC=1)NCC1=CC(=CC=C1)OC(F)(F)F)N1CC2=C(CC1)NN=N2 NIPNSKYNPDTRPC-UHFFFAOYSA-N 0.000 description 2
- 230000007812 deficiency Effects 0.000 description 2
- 235000009508 confectionery Nutrition 0.000 description 1
- 235000013399 edible fruits Nutrition 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 239000004519 grease Substances 0.000 description 1
- 239000000383 hazardous chemical Substances 0.000 description 1
- 230000002045 lasting effect Effects 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 230000001737 promoting effect Effects 0.000 description 1
- 238000012797 qualification Methods 0.000 description 1
- 230000000391 smoking effect Effects 0.000 description 1
- 230000006641 stabilisation Effects 0.000 description 1
- 238000011105 stabilization Methods 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 238000009210 therapy by ultrasound Methods 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/02—Recovery or refining of essential oils from raw materials
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/28—Treatment of tobacco products or tobacco substitutes by chemical substances
- A24B15/30—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/28—Treatment of tobacco products or tobacco substitutes by chemical substances
- A24B15/30—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances
- A24B15/302—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances by natural substances obtained from animals or plants
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B3/00—Preparing tobacco in the factory
- A24B3/12—Steaming, curing, or flavouring tobacco
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/02—Recovery or refining of essential oils from raw materials
- C11B9/022—Refining
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/02—Recovery or refining of essential oils from raw materials
- C11B9/025—Recovery by solvent extraction
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/02—Recovery or refining of essential oils from raw materials
- C11B9/027—Recovery of volatiles by distillation or stripping
Landscapes
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Life Sciences & Earth Sciences (AREA)
- Organic Chemistry (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Engineering & Computer Science (AREA)
- Health & Medical Sciences (AREA)
- General Health & Medical Sciences (AREA)
- Toxicology (AREA)
- General Chemical & Material Sciences (AREA)
- Agronomy & Crop Science (AREA)
- Botany (AREA)
- Fats And Perfumes (AREA)
Abstract
The present invention provides a kind of quick-fried pearl base oil and preparation method thereof with natural cream perfume (or spice) note.The quick-fried pearl base oil with natural cream perfume (or spice) note, it is specific the preparation method is as follows: taking storax according to the ratio of weight ratio 1~3: 1~3, perfume material of resting in peace, and it clays into power, it is mixed and is uniformly configured to natural perfume material mixed raw material, then it is added the Glycerin, mixed triester with caprylic acid capric acid of 50~300 times of its weight, impregnates 8 under room temperature~for 24 hours, then 1~4h of ultrasound under conditions of 50~60 DEG C of temperature, filtering removal impurity and insoluble matter are to get the quick-fried pearl base oil for arriving the natural cream perfume (or spice) note.Storax, two kinds of the styrax Chinese herbal medicines rich in cream perfume (or spice) note are applied in the quick-fried pearl of cigarette by the present invention, its additive amount is minimum, but significant cream perfume (or spice) note can be brought, it gives off a strong fragrance, is comfortable natural, the basic oil nature of allotment is stablized, it will not react with wall material, well solve synthetic perfume and be added that brought fragrance in quick-fried pearl base oil is thin, molding instability problem.
Description
Technical field
The present invention relates to essence spice for cigarette fields, and in particular to a kind of quick-fried pearl base oil with natural cream perfume (or spice) note and
Preparation method.
Background technique
Quick-fried pearl is a kind of cigarette added material having compared with high technology content.As a kind of new cigarette flavoring and casing side
Formula is not involved in cigarette burning, does not generate new hazardous substance, quantitative accurate.Meanwhile safety is inhaled meeting consumer's cigarette product
Property, except the functional requirements such as abundant cigarette product fragrance, moist-keeping flavouring, reducing tar and reducing harm, also innovatively realize " can touch, can
It is broken, can ring, releasably " functional characteristics.
Essence for quick-fried pearl base oil is essentially compound essence, it enriches the side such as cigarette perfume in the aroma quality for promoting quick-fried pearl
Face plays an important role.However compound essence fragrance is more thin, and chemical property is active, easily with base oil, wall material
Etc. reacting, lead to occur unstable state in the online forming process of quick-fried pearl, to influence quick-fried pearl molding.Natural perfume material
Fragrance is comfortable pure naturally, lasting fragrance stabilization, can make up various deficiencies of synthetic perfume well.
Summary of the invention
It is an object of the invention to solve the above-mentioned deficiency of the prior art, a kind of quick-fried pearl with natural cream perfume (or spice) note is provided
The preparation method of base oil, this method simple process and low cost, raw material sources are stablized, and not only cream is fragrant for manufactured base oil
Gas is sent out thoroughly, is comfortable naturally, and machine molding effect is preferable on quick-fried pearl.
A kind of quick-fried pearl base oil with natural cream perfume (or spice) note provided by the invention, it is characterised in that mixed by natural perfume material
It closes raw material and Glycerin, mixed triester with caprylic acid capric acid is mixed according to 1: 50~300 weight ratio, wherein the natural perfume material mixed raw material is
It is formulated by storax and styrax according to the ratio of weight ratio 1~3: 1~3.
The preparation method of a kind of quick-fried pearl base oil with natural cream perfume (or spice) note provided by the invention, it is characterised in that specific
Steps are as follows:
(1) storax is taken according to the ratio of weight ratio 1~3: 1~3, perfume material of resting in peace, and clayed into power, be mixed
It is even to be configured to natural perfume material mixed raw material；
(2) Glycerin, mixed triester with caprylic acid capric acid of 50~300 times of its weight is added in the natural perfume material mixed raw material in step (1),
Impregnate 8 under room temperature~for 24 hours, then 1~4h of ultrasound under the conditions of 50~60 DEG C of temperature；
(3) removal impurity and insoluble matter are filtered after ultrasound to it to get the quick-fried pearl base of the natural cream perfume (or spice) note is arrived
Plinth oil.
The present invention preferably technical solution: the supersonic frequency in the step (2) is 25~35kHz.
Storax, styrax in the present invention are a kind of resinae Chinese herbal medicines after tentatively extracting, and aroma strength is big,
For the product directly bought.
Storax, two kinds of the styrax Chinese herbal medicines rich in cream perfume (or spice) note are applied in the quick-fried pearl of cigarette by the present invention, are added
It measures minimum, can but bring significant cream perfume (or spice) note, give off a strong fragrance, is comfortable naturally, be directly appended in Glycerin, mixed triester with caprylic acid capric acid,
And after ultrasonic treatment, its fragrance is made to can be good at merging, and property is stablized, and will not react with wall material；Well
It solves synthetic perfume and is added that brought fragrance in quick-fried pearl base oil is thin, molding instability problem.
Specific embodiment
The present invention is described in further detail below with reference to embodiment, it is necessary to it is pointed out here that implementing in detail below
Example does not represent limiting the scope of the invention only to further explanation of the invention.Other people make according to the present invention
Some nonessential modifications and adjustment, still fall within protection scope of the present invention.
A kind of quick-fried pearl base oil with natural cream perfume (or spice) note that embodiment 1 provides, preparation method are as follows: taking storax
Raw material 50g, rest in peace perfume material 50g, is uniformly mixed after claying into power respectively, and it is sweet that 150 times of mixed raw material weight of pungent capric acid is added
Grease impregnates 12h at normal temperature, then ultrasound 4h under conditions of 45 DEG C of temperature, supersonic frequency 30kHz, mistake after ultrasound
Filter removes impurity and insoluble matter, stands 24 hours, the as described quick-fried pearl base oil with natural cream perfume (or spice) note.
A kind of quick-fried pearl base oil with natural cream perfume (or spice) note that embodiment 2 provides, preparation method are as follows:
It takes that storax raw material 100g, rest in peace perfume material 50g, is uniformly mixed after claying into power respectively, addition accounts for mixed raw material
The Glycerin, mixed triester with caprylic acid capric acid that 200 times of weight impregnates for 24 hours under room temperature, then surpasses under conditions of 50 DEG C of temperature, supersonic frequency 27kHz
Sound 3h is filtered after ultrasonic, removes impurity and insoluble matter, stands 24 hours, as described quick-fried with natural cream perfume (or spice) note
Pearl base oil.
A kind of quick-fried pearl base oil with natural cream perfume (or spice) note that embodiment 3 provides, preparation method are as follows:
It takes that storax raw material 50g, rest in peace perfume material 150g, is uniformly mixed after claying into power respectively, addition accounts for mixed raw material
The Glycerin, mixed triester with caprylic acid capric acid that 100 times of weight, after impregnating 12h under room temperature, then under conditions of 60 DEG C of temperature, supersonic frequency 35kHz
Ultrasonic 2h is filtered after ultrasonic, removes impurity and insoluble matter, stands 24 hours, as the base oil.
Application Example 1: the cream perfume (or spice) note base oil that Example 1-3 is obtained, and meanwhile it is fragrant with the cream of compound essence allotment
Note base oil is comparative example, and respectively by machine molded test on quick-fried pearl, the results are shown in Table 1 for molded test；
Application Example 2: the cream perfume (or spice) note base oil that Example 1-3 is obtained, and meanwhile it is fragrant with the cream of compound essence allotment
Note base oil is comparative example, and quick-fried pearl is made by technical need respectively, is added in cigarette filter tip and smokes panel test, smoking result is shown in Table 1:
It the molding of the quick-fried pearl of quick-fried pearl base oil and the base oil in comparative example and cigarette is added smokes panel test knot in 1 embodiment 1-3 of table
Fruit
Table 1 the result shows that: the quick-fried pearl base oil of cream perfume (or spice) note in embodiment 1-3 is preferable to quick-fried pearl forming stability, finished product
Qualification rate will be substantially better than comparative example；And the cream perfume (or spice) note base oil that will be prepared, quick-fried pearl is made by technical need, volume is added
In cigarette holder stick, there is significant cream perfume (or spice) note in when suction, gives off a strong fragrance, is comfortable naturally, pure free from extraneous odour, will not form quick-fried pearl steady
Surely it impacts.
Claims (3)
1. a kind of quick-fried pearl base oil with natural cream perfume (or spice) note, it is characterised in that be by natural perfume material mixed raw material and pungent capric acid
Glyceride is mixed according to 1: 50~300 weight ratio, wherein the natural perfume material mixed raw material be by storax with rest in peace
Perfume (or spice) is formulated according to the ratio of weight ratio 1~3: 1~3.
2. a kind of preparation method of the quick-fried pearl base oil described in claim 1 with natural cream perfume (or spice) note, it is characterised in that
Specific step is as follows:
(1) storax is taken according to the ratio of weight ratio 1~3: 1~3, perfume material of resting in peace, and clayed into power, be mixed and uniformly match
Natural perfume material mixed raw material is made；
(2) Glycerin, mixed triester with caprylic acid capric acid of 50~300 times of its weight, room temperature are added in the natural perfume material mixed raw material in step (1)
It is lower impregnate 8~for 24 hours, then 1~4h of ultrasound under conditions of 50~60 DEG C of temperature；
(3) removal impurity and insoluble matter are filtered after ultrasound to it to get the quick-fried pearl base oil of the natural cream perfume (or spice) note is arrived.
3. a kind of preparation method of quick-fried pearl base oil with natural cream perfume (or spice) note according to claim 2, feature exist
In: the supersonic frequency in the step (2) is 25~35kHz.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201811372408.6A CN109468173A (en) | 2018-11-16 | 2018-11-16 | Quick-fried pearl base oil and preparation method thereof with natural cream perfume (or spice) note |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201811372408.6A CN109468173A (en) | 2018-11-16 | 2018-11-16 | Quick-fried pearl base oil and preparation method thereof with natural cream perfume (or spice) note |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN109468173A true CN109468173A (en) | 2019-03-15 |
Family
ID=65672666
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201811372408.6A Pending CN109468173A (en) | 2018-11-16 | 2018-11-16 | Quick-fried pearl base oil and preparation method thereof with natural cream perfume (or spice) note |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN109468173A (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110804497A (en) * | 2019-11-18 | 2020-02-18 | 湖北中烟工业有限责任公司 | Preparation method of saffron extract for tobacco bead blasting |
| CN111040876A (en) * | 2019-12-19 | 2020-04-21 | 云南瑞升烟草技术（集团）有限公司 | Preparation method of natural spice suitable for cigarette bead blasting |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1579259A (en) * | 2003-09-23 | 2005-02-16 | 欧发辉 | Cigarette of using leaf vegetable to replace to bacco leaf and production method thereof |
| CN105029692A (en) * | 2015-06-01 | 2015-11-11 | 湖北中烟工业有限责任公司 | Cigarette with fragrant lap adhesive colored tape and manufacturing method of cigarette |
| CN107927901A (en) * | 2017-11-22 | 2018-04-20 | 湖北中烟工业有限责任公司 | It is a kind of that the method for tobacco aromaticss and its application in the quick-fried pearl of cigarette are prepared using Glycerin, mixed triester with caprylic acid capric acid |
-
2018
- 2018-11-16 CN CN201811372408.6A patent/CN109468173A/en active Pending
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1579259A (en) * | 2003-09-23 | 2005-02-16 | 欧发辉 | Cigarette of using leaf vegetable to replace to bacco leaf and production method thereof |
| CN105029692A (en) * | 2015-06-01 | 2015-11-11 | 湖北中烟工业有限责任公司 | Cigarette with fragrant lap adhesive colored tape and manufacturing method of cigarette |
| CN107927901A (en) * | 2017-11-22 | 2018-04-20 | 湖北中烟工业有限责任公司 | It is a kind of that the method for tobacco aromaticss and its application in the quick-fried pearl of cigarette are prepared using Glycerin, mixed triester with caprylic acid capric acid |
Non-Patent Citations (1)
| Title |
|---|
| 边照阳等: "《烟草农药残留分析技术》", 31 January 2015, 中国轻工业出版社 * |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110804497A (en) * | 2019-11-18 | 2020-02-18 | 湖北中烟工业有限责任公司 | Preparation method of saffron extract for tobacco bead blasting |
| CN111040876A (en) * | 2019-12-19 | 2020-04-21 | 云南瑞升烟草技术（集团）有限公司 | Preparation method of natural spice suitable for cigarette bead blasting |
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| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| RJ01 | Rejection of invention patent application after publication | ||
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Application publication date: 20190315 |