CN109431963B - Transparent oil bead suspension essence water and preparation method thereof - Google Patents

Transparent oil bead suspension essence water and preparation method thereof Download PDF

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CN109431963B
CN109431963B CN201811588140.XA CN201811588140A CN109431963B CN 109431963 B CN109431963 B CN 109431963B CN 201811588140 A CN201811588140 A CN 201811588140A CN 109431963 B CN109431963 B CN 109431963B
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percent
water
extract
bead suspension
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CN109431963A (en
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董明生
王丽辉
彭瑜瑜
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Beiyouqing Guangdong Health Technology Co ltd
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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/99Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from microorganisms other than algae or fungi, e.g. protozoa or bacteria
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • A61K8/9728Fungi, e.g. yeasts
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • A61K8/9783Angiosperms [Magnoliophyta]
    • A61K8/9789Magnoliopsida [dicotyledons]
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • A61K8/9783Angiosperms [Magnoliophyta]
    • A61K8/9794Liliopsida [monocotyledons]
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • A61Q19/02Preparations for care of the skin for chemically bleaching or whitening the skin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • A61Q19/08Anti-ageing preparations
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/20Chemical, physico-chemical or functional or structural properties of the composition as a whole
    • A61K2800/26Optical properties
    • A61K2800/262Transparent; Translucent
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/80Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
    • A61K2800/85Products or compounds obtained by fermentation, e.g. yoghurt, beer, wine

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Abstract

The invention discloses transparent oil bead suspension essence water and a preparation method thereof. The essence water disclosed by the invention uniformly suspends a large number of transparent oil droplets in the water phase, so that coexistence of oil and water is realized, the moisture of skin can be effectively supplemented, and the essence water has an excellent long-acting moisturizing effect. The essence water is compounded by the aesculus hippocastanum seed extract, the yeast/rice bran fermentation product, the pseudoalteromonas fermentation product extract and the lettuce extract, so that a synergistic effect is generated, the skin color can be effectively brightened, the melanin is lightened, and the essence water has the performances of oxidation resistance and long-acting moisture retention.

Description

Transparent oil bead suspension essence water and preparation method thereof
Technical Field
The invention relates to the technical field of skin care products, and particularly relates to transparent oil bead suspension essence water and a preparation method thereof.
Background
Because people's irregular life leads to, facial skin extremely lacks moisture, can lead to facial water oil unbalance like this, and the skin produces the wrinkle easily, and ageing serious, and in summer interim, fragile skin exposes under the sunlight, leads to the dark yellow of complexion, dull luster, and the skin care product of present conventional, single efficiency has not been able to satisfy people's demand, and the consumer has had higher requirement to the skin care product, and the cosmetics that have functions such as accuse oil, whitening, ageing resistance, skin of releiving receive more and more oriental women's favor.
In addition, the conventional essence or essence water is usually added with an oil phase in a water phase, so that moisture and certain oil can be stored in the skin after the skin is used, the skin looks glossy, soft and smooth, and the oil can form a closed environment in the skin, so that the moisture is not easy to evaporate. However, mixing oil and water together can form two immiscible phases. The existing essence is mainly added with an emulsifier, so that an oil phase and a water phase are uniformly mixed through emulsification, but the phenomenon of oil-water stratification is easily caused after long-time storage, and the using effect is influenced.
Disclosure of Invention
The invention aims to overcome the defects of the prior art and provide the transparent oil bead suspension essence water and the preparation method thereof, the large amount of irregular transparent oil bead suspension essence water is prepared, the rheological property and the stability are good, the coexistence of oil and water can be realized, the addition amount of the emulsifier is reduced, the product is easier to absorb, and the essence water has good effects of moisturizing, ageing resistance, brightening skin color and relieving skin.
In order to achieve the purpose, the technical scheme adopted by the invention is as follows:
a transparent oil bead suspension essence water comprises Aesculus hippocastanum seed extract, yeast/rice bran fermentation product, pseudoalteromonas fermentation product extract and lettuce extract.
The European horse chestnut seed extract has good antioxidant activity, and is beneficial to improving the free radical scavenging effect and the anti-inflammatory effect of the product; the yeast/rice bran fermentation product takes rice as a raw material, and filtrate obtained by yeast fermentation is rich in glutamine, glutamic acid, proline and other amino acids, and can promote the expression of aquaporin AQP-3 and semi-light asparaginase-14, so that the yeast/rice bran fermentation product has the effects of moisturizing, brightening the skin, and homogenizing the skin color, and simultaneously improves the whitening effect of the product; the pseudoalteromonas fermentation product extract is an extracellular polymeric substance (ECPS) obtained from the marine pseudoalteromonas through a biotechnology, can reduce the protein level of MC5-R (related to the differentiation of sebaceous gland cells), reduce the maturation and lipid peroxidation of the sebaceous gland cells, and simultaneously can greatly increase the synthesis of type I collagen, thereby relieving the skin symptoms of oily and mixed skin and tightening the skin; the lettuce extract is rich in polyphenols and flavonoids, and has good effect of eliminating superoxide anions and hydroxyl free radicals. According to the invention, the European horse chestnut seed extract and the lettuce extract are compounded to realize synergistic antioxidation, so that the compound skin care product has a skin soothing effect and can effectively relieve discomfort of the skin caused by various external factors. The yeast/rice bran fermentation product and the pseudoalteromonas fermentation product extract can effectively supplement moisture required by skin by compounding, and have good effects of controlling oil, lightening melanin and brightening skin color.
The preferred embodiment of the transparent oil bead suspension essence water comprises the following components in percentage by mass: 0.1-10% of European horse chestnut seed extract, 0.1-10% of yeast/rice bran fermentation product, 0.01-10% of pseudoalteromonas fermentation product extract and 0.3-10% of lettuce extract.
The preferred embodiment of the transparent oil bead suspension essence water comprises the following components in percentage by mass: 1 to 5 percent of European horse chestnut seed extract, 2 to 6 percent of yeast/rice bran fermentation product, 0.5 to 4 percent of pseudoalteromonas fermentation product extract and 1 to 5 percent of lettuce extract.
According to the invention, by adjusting the compounding ratio of the aesculus hippocastanum seed extract, the yeast/rice bran fermentation product, the pseudoalteromonas fermentation product extract and the lettuce extract, the essential water can rapidly supplement moisture required by skin, the water locking effect is obvious, the generation of free radicals is prevented, and the skin color brightening effect is enhanced.
The preferred embodiment of the transparent oil bead suspension essence water comprises the following components in percentage by mass: 3% of European horse chestnut seed extract, 3% of yeast/rice bran fermentation product, 2% of pseudoalteromonas fermentation product extract and 3% of lettuce extract.
The preferred embodiment of the transparent oil bead suspension essence water comprises the following components in percentage by mass:
phase A: 1-6% of diphenyl siloxy phenyl trimethyl siloxane, 1-5% of diphenyl dimethyl siloxane and 0.2-3% of spherical powder;
phase B: the balance of water, 2 to 15 percent of butanediol, 1 to 8 percent of trehalose, 0.01 to 0.4 percent of methyl hydroxybenzoate, 60.1 to 0.4 percent of polyacrylate cross-linked polymer and 0.05 to 3 percent of sodium hyaluronate;
and C phase: 0.1 to 10 percent of European horse chestnut seed extract, 0.1 to 10 percent of yeast/rice bran fermentation product, 0.01 to 10 percent of pseudoalteromonas fermentation product extract and 0.3 to 10 percent of lettuce extract;
phase D: 0.01 to 1 percent of preservative.
The preferred embodiment of the transparent oil bead suspension essence water comprises the following components in percentage by mass:
phase A: 4% of diphenylsiloxy phenyl trimethyl siloxane, 2% of diphenyl dimethyl polysiloxane and 1% of spherical powder;
phase B: the balance of water, 5 percent of butanediol, 3 percent of trehalose, 0.1 percent of methyl hydroxybenzoate, 60.15 percent of polyacrylate cross-linked polymer and 0.3 percent of sodium hyaluronate;
and C phase: 1 to 5 percent of European horse chestnut seed extract, 2 to 6 percent of yeast/rice bran fermentation product, 0.5 to 4 percent of pseudoalteromonas fermentation product extract and 1 to 5 percent of lettuce extract;
phase D: 0.3 percent of preservative.
The preferred embodiment of the transparent oil bead suspension essence water comprises the following components in percentage by mass:
phase A: 4% of diphenylsiloxy phenyl trimethyl siloxane, 2% of diphenyl dimethyl polysiloxane and 1% of spherical powder;
phase B: the balance of water, 5 percent of butanediol, 3 percent of trehalose, 0.1 percent of methyl hydroxybenzoate, 60.15 percent of polyacrylate cross-linked polymer and 0.3 percent of sodium hyaluronate;
and C phase: 3% of European horse chestnut seed extract, 3% of yeast/rice bran fermentation product, 2% of pseudoalteromonas fermentation product extract and 3% of lettuce extract;
phase D: 0.3 percent of preservative.
According to the invention, through compounding, the suspension stability of the grease is further improved, the grease is uniformly suspended in a water phase, and the water replenishing effect is improved.
As a preferred embodiment of the transparent oil bead suspension essence water, the essence water further contains panthenol and silanediol salicylate, and comprises the following components in percentage by mass:
phase A: 1-6% of diphenyl siloxy phenyl trimethyl siloxane, 1-5% of diphenyl dimethyl siloxane and 0.2-3% of spherical powder;
phase B: the balance of water, 2 to 15 percent of butanediol, 1 to 8 percent of trehalose, 2 percent of panthenol, 0.01 to 0.4 percent of methyl hydroxybenzoate, 60.1 to 0.4 percent of polyacrylate cross-linked polymer and 0.05 to 3 percent of sodium hyaluronate;
and C phase: 3 percent of silanediol salicylate, 0.1 to 10 percent of European horse chestnut seed extract, 0.1 to 10 percent of yeast/rice bran fermentation product, 0.01 to 10 percent of pseudoalteromonas fermentation product extract and 0.3 to 10 percent of lettuce extract;
phase D: 0.01 to 1 percent of preservative.
As a preferred embodiment of the transparent oil bead suspension essence water, the spherical powder is at least one of tapioca starch and polymethylsilsesquioxane.
As a preferable embodiment of the transparent oil bead suspension essence water of the present invention, the preservative is at least one of phenoxyethanol, methylparaben, ethylparaben, and ethylhexylglycerin.
The invention also provides a preparation method of the transparent oil bead suspension essence water, which comprises the following steps:
(1) adding the phase A component into an oil pan, heating to 85-90 ℃, and stirring for dissolving;
(2) adding water in the phase B into a main pot, heating to 85-90 ℃, sequentially adding the phase B components, and homogenizing and stirring for 25-30 min;
(3) adding the phase B into the phase A, and uniformly stirring;
(4) and naturally cooling to 42-45 ℃, adding the phase C and the phase D, and uniformly stirring to obtain the transparent oil bead suspension essence water.
Compared with the prior art, the invention has the beneficial effects that:
the essence water disclosed by the invention uniformly suspends a large number of transparent oil droplets in the water phase, so that coexistence of oil and water is realized, the moisture of skin can be effectively supplemented, and the essence water has an excellent long-acting moisturizing effect. The essence water is compounded by the aesculus hippocastanum seed extract, the yeast/rice bran fermentation product, the pseudoalteromonas fermentation product extract and the lettuce extract, so that a synergistic effect is generated, the skin color can be effectively brightened, the melanin is lightened, and the essence water has the performances of oxidation resistance and long-acting moisture retention.
Detailed Description
To better illustrate the objects, aspects and advantages of the present invention, the present invention will be further described with reference to specific examples. It will be understood by those skilled in the art that the specific embodiments described herein are merely illustrative of the invention and are not intended to limit the invention.
In the examples, the experimental methods used were all conventional methods unless otherwise specified, and the materials, reagents and the like used were commercially available without otherwise specified.
Example 1
The transparent oil bead suspension essence water comprises the following components in percentage by mass:
phase A: 4% of diphenyl siloxy phenyl trimethyl siloxane, 2% of diphenyl dimethyl siloxane and 1% of cassava starch;
phase B: the balance of water, 5 percent of butanediol, 3 percent of trehalose, 2 percent of panthenol, 0.1 percent of methyl hydroxybenzoate, 60.15 percent of polyacrylate cross-linked polymer and 0.3 percent of sodium hyaluronate;
and C phase: 3% of silanediol salicylate, 3% of aesculus hippocastanum seed extract, 3% of yeast/rice bran fermentation product, 2% of pseudoalteromonas fermentation product extract and 3% of lettuce extract;
phase D: 0.3 percent of phenoxyethanol.
The preparation method of the transparent oil bead suspension essence water comprises the following steps:
(1) adding the phase A component into an oil pan, heating to 85-90 ℃, and stirring for dissolving;
(2) adding water in the phase B into a main pot, heating to 85-90 ℃, sequentially adding the phase B components, and homogenizing and stirring for 25-30 min;
(3) adding the phase B into the phase A, and uniformly stirring;
(4) and naturally cooling to 42-45 ℃, adding the phase C and the phase D, and uniformly stirring to obtain the transparent oil bead suspension essence water.
Example 2
The transparent oil bead suspension essence water comprises the following components in percentage by mass:
phase A: 4% of diphenyl siloxy phenyl trimethyl siloxane, 2% of diphenyl dimethyl siloxane and 1% of cassava starch;
phase B: the balance of water, 5 percent of butanediol, 3 percent of trehalose, 2 percent of panthenol, 0.1 percent of methyl hydroxybenzoate, 60.15 percent of polyacrylate cross-linked polymer and 0.3 percent of sodium hyaluronate;
and C phase: 3% of silanediol salicylate, 1% of aesculus hippocastanum seed extract, 6% of yeast/rice bran fermentation product, 3% of pseudoalteromonas fermentation product extract and 1% of lettuce extract;
phase D: 0.3 percent of phenoxyethanol.
The preparation method of the transparent oil bead suspension essence water comprises the following steps:
(1) adding the phase A component into an oil pan, heating to 85-90 ℃, and stirring for dissolving;
(2) adding water in the phase B into a main pot, heating to 85-90 ℃, sequentially adding the phase B components, and homogenizing and stirring for 25-30 min;
(3) adding the phase B into the phase A, and uniformly stirring;
(4) and naturally cooling to 42-45 ℃, adding the phase C and the phase D, and uniformly stirring to obtain the transparent oil bead suspension essence water.
Example 3
The transparent oil bead suspension essence water comprises the following components in percentage by mass:
phase A: 4% of diphenyl siloxy phenyl trimethyl siloxane, 2% of diphenyl dimethyl siloxane and 1% of cassava starch;
phase B: the balance of water, 5 percent of butanediol, 3 percent of trehalose, 2 percent of panthenol, 0.1 percent of methyl hydroxybenzoate, 60.15 percent of polyacrylate cross-linked polymer and 0.3 percent of sodium hyaluronate;
and C phase: 3% of silanediol salicylate, 5% of aesculus hippocastanum seed extract, 2% of yeast/rice bran fermentation product, 0.5% of pseudoalteromonas fermentation product extract and 3.5% of lettuce extract;
phase D: 0.3 percent of phenoxyethanol.
The preparation method of the transparent oil bead suspension essence water comprises the following steps:
(1) adding the phase A component into an oil pan, heating to 85-90 ℃, and stirring for dissolving;
(2) adding water in the phase B into a main pot, heating to 85-90 ℃, sequentially adding the phase B components, and homogenizing and stirring for 25-30 min;
(3) adding the phase B into the phase A, and uniformly stirring;
(4) and naturally cooling to 42-45 ℃, adding the phase C and the phase D, and uniformly stirring to obtain the transparent oil bead suspension essence water.
Example 4
The transparent oil bead suspension essence water comprises the following components in percentage by mass:
phase A: 4% of diphenyl siloxy phenyl trimethyl siloxane, 2% of diphenyl dimethyl siloxane and 1% of cassava starch;
phase B: the balance of water, 5 percent of butanediol, 3 percent of trehalose, 2 percent of panthenol, 0.1 percent of methyl hydroxybenzoate, 60.15 percent of polyacrylate cross-linked polymer and 0.3 percent of sodium hyaluronate;
and C phase: 3% of silanediol salicylate, 1% of aesculus hippocastanum seed extract, 2% of yeast/rice bran fermentation product, 4% of pseudoalteromonas fermentation product extract and 5% of lettuce extract;
phase D: 0.3 percent of phenoxyethanol.
The preparation method of the transparent oil bead suspension essence water comprises the following steps:
(1) adding the phase A component into an oil pan, heating to 85-90 ℃, and stirring for dissolving;
(2) adding water in the phase B into a main pot, heating to 85-90 ℃, sequentially adding the phase B components, and homogenizing and stirring for 25-30 min;
(3) adding the phase B into the phase A, and uniformly stirring;
(4) and naturally cooling to 42-45 ℃, adding the phase C and the phase D, and uniformly stirring to obtain the transparent oil bead suspension essence water.
Example 5
The transparent oil bead suspension essence water comprises the following components in percentage by mass:
phase A: 1% of diphenyl siloxy phenyl trimethyl siloxane, 4% of diphenyl dimethyl polysiloxane, and 0.2% of polymethylsilsesquioxane;
phase B: the balance of water, 15 percent of butanediol, 2 percent of trehalose, 2 percent of panthenol, 0.01 percent of methyl hydroxybenzoate, 60.1 percent of polyacrylate cross-linked polymer and 3 percent of sodium hyaluronate;
and C phase: 3% of silanediol salicylate, 0.1% of aesculus hippocastanum seed extract, 2.8% of yeast/rice bran fermentation product, 10% of pseudoalteromonas fermentation product extract and 0.3% of lettuce extract;
phase D: 1 percent of phenoxyethanol.
The preparation method of the transparent oil bead suspension essence water comprises the following steps:
(1) adding the phase A component into an oil pan, heating to 85-90 ℃, and stirring for dissolving;
(2) adding water in the phase B into a main pot, heating to 85-90 ℃, sequentially adding the phase B components, and homogenizing and stirring for 25-30 min;
(3) adding the phase B into the phase A, and uniformly stirring;
(4) and naturally cooling to 42-45 ℃, adding the phase C and the phase D, and uniformly stirring to obtain the transparent oil bead suspension essence water.
Example 6
The transparent oil bead suspension essence water comprises the following components in percentage by mass:
phase A: 4% of diphenylsiloxy phenyl trimethyl polysiloxane, 5% of diphenyl polydimethylsiloxane, and 3% of polymethylsilsesquioxane;
phase B: the balance of water, 2 percent of butanediol, 8 percent of trehalose, 2 percent of panthenol, 0.08 percent of methyl hydroxybenzoate, 60.2 percent of polyacrylate cross-linked polymer and 0.2 percent of sodium hyaluronate;
and C phase: 3% of silanediol salicylate, 10% of aesculus hippocastanum seed extract, 0.1% of yeast/rice bran fermentation product, 0.1% of pseudoalteromonas fermentation product extract and 10% of lettuce extract;
phase D: 0.8 percent of phenoxyethanol.
The preparation method of the transparent oil bead suspension essence water comprises the following steps:
(1) adding the phase A component into an oil pan, heating to 85-90 ℃, and stirring for dissolving;
(2) adding water in the phase B into a main pot, heating to 85-90 ℃, sequentially adding the phase B components, and homogenizing and stirring for 25-30 min;
(3) adding the phase B into the phase A, and uniformly stirring;
(4) and naturally cooling to 42-45 ℃, adding the phase C and the phase D, and uniformly stirring to obtain the transparent oil bead suspension essence water.
Example 7
The transparent oil bead suspension essence water comprises the following components in percentage by mass:
phase A: 6% of diphenylsiloxy phenyl trimethyl siloxane, 1% of diphenyl polydimethylsiloxane, and 1.6% of polymethylsilsesquioxane;
phase B: the balance of water, 12 percent of butanediol, 3 percent of trehalose, 2 percent of panthenol, 0.4 percent of methyl hydroxybenzoate, 60.4 percent of polyacrylate cross-linked polymer and 0.05 percent of sodium hyaluronate;
and C phase: 3% of silanediol salicylate, 3.5% of aesculus hippocastanum seed extract, 10% of yeast/rice bran fermentation product, 0.01% of pseudoalteromonas fermentation product extract and 4.5% of lettuce extract;
phase D: 0.01 percent of phenoxyethanol.
The preparation method of the transparent oil bead suspension essence water comprises the following steps:
(1) adding the phase A component into an oil pan, heating to 85-90 ℃, and stirring for dissolving;
(2) adding water in the phase B into a main pot, heating to 85-90 ℃, sequentially adding the phase B components, and homogenizing and stirring for 25-30 min;
(3) adding the phase B into the phase A, and uniformly stirring;
(4) and naturally cooling to 42-45 ℃, adding the phase C and the phase D, and uniformly stirring to obtain the transparent oil bead suspension essence water.
Comparative example 1
The transparent oil bead suspension essence water comprises the following components in percentage by mass:
phase A: 4% of diphenyl siloxy phenyl trimethyl siloxane, 2% of diphenyl dimethyl siloxane and 1% of cassava starch;
phase B: the balance of water, 5 percent of butanediol, 3 percent of trehalose, 2 percent of panthenol, 0.1 percent of methyl hydroxybenzoate, 60.15 percent of polyacrylate cross-linked polymer and 0.3 percent of sodium hyaluronate;
and C phase: 3% of silanediol salicylate, 6% of aesculus hippocastanum seed extract and 5% of pseudoalteromonas fermentation product extract;
phase D: 0.3 percent of phenoxyethanol.
The preparation method of the transparent oil bead suspension essence water comprises the following steps:
(1) adding the phase A component into an oil pan, heating to 85-90 ℃, and stirring for dissolving;
(2) adding water in the phase B into a main pot, heating to 85-90 ℃, sequentially adding the phase B components, and homogenizing and stirring for 25-30 min;
(3) adding the phase B into the phase A, and uniformly stirring;
(4) and naturally cooling to 42-45 ℃, adding the phase C and the phase D, and uniformly stirring to obtain the transparent oil bead suspension essence water.
The formula (mass percentage) of the essence liquid of examples 1 to 7 and comparative example 1 is shown in table 1.
TABLE 1
Figure BDA0001919707070000091
Performance testing
Tyrosinase activity inhibition assay
Solutions of example 1-7 and comparative example essence water at a concentration of 0.2mg/mL were prepared as sample solutions, respectively, using 0.2mol/L Phosphate Buffered Saline (PBS) having a pH of 6.8 as a solvent.
0.9mL of the sample solution having the above concentration of 0.2mg/mL was taken, 1mL of L-tyrosine (0.3mol) and 1mL of Phosphate Buffer (PBS) having a pH of 6.8 were added, the mixture was preheated in a constant temperature water bath at 37 ℃ for 10min, 0.1mL of an aqueous solution of tyrosinase (1.0mg/mL, mcllains buffer) was added thereto, the mixture was sufficiently stirred, and after a reaction at 37 ℃ for 15min, the absorbance at 475nm (D) was measured1). Further, the same reaction was carried out using the above-mentioned phosphate buffer solution in place of the sample solution having the concentration of 0.2mg/mL, and the absorbance (D) was measured2). For comparison, the absorbance (D) was measured without adding the sample solution and tyrosinase3). The tyrosinase activity inhibition rate was calculated by the following formula.
Tyrosinase activity inhibition ratio (%) - (D)2-D1)/(D2-D3)×100
The results are shown in table 2:
TABLE 2
Tyrosinase activity inhibition ratio (%)
Example 1 37%
Example 2 28%
Example 3 25%
Example 4 23%
Example 5 20%
Example 6 20%
Example 7 18%
Comparative example 1 20%
Superoxide anion scavenging assay
The essence liquids prepared in examples 1 to 7 and comparative example 1 were respectively prepared into aqueous solutions with a concentration of 100 mg/mL. To 0.1mL of the mixture were added 1mL of 16mmol/L Tris-HCl (pH 8.0) containing 557. mu. mol/L NaOH, 1mL of 16mmol/L Tris-HCl (pH 8.0) containing 45. mu. mol/L PMS, and 16mmol/L Tris-HCl (pH 8.0) containing 108. mu. mol/L NBT, respectively, and the mixture was incubated at 25 ℃ for 5 minutes, and the absorbance at 560nm was measured and recorded as A1(ii) a The same volume of solvent was used as a control instead of the sample solution and is denoted as A2The superoxide anion removal rate was calculated according to the following formula, and the results are shown in Table 3.
Superoxide anion scavenging rate ═ 1-A1/A2)×100%
TABLE 3
Superoxide anion scavenging ratio (%)
Example 1 35%
Example 2 30%
Example 3 25%
Example 4 23%
Example 5 20%
Example 6 18%
Example 7 18%
Comparative example 1 25%
Hydroxyl radical scavenging assay
The essence liquids prepared in examples 1 to 7 and comparative example 1 were respectively prepared into solutions with a concentration of 100 mg/mL. 0.6mL of a reaction buffer (0.2 mol/L phosphate buffer pH 7.4 containing 2.67mmol/L deoxyribose and 0.13mmol/L EDTA), 0.2mL of 0.4mmol/L ferrous sulfate, 0.05mL of 2.0mmol/L ascorbic acid, and 20mmol/L H were added to 0.1mL of each2O20.05mL, warm bath at 37 ℃ for 15min, taking out, adding 1mL of 1% thiobarbituric acid and 1mL of 2% trichloroacetic acid, boiling in water bath for 15min, taking out, cooling on ice, measuring absorbance at 532nm in an enzyme-linked immunosorbent assay, and recording as A1(ii) a By replacing with solvent of the same volumeThe control was a for the sample solution2(ii) a The hydroxyl radical scavenging rate was calculated according to the following formula, and the results are shown in table 4.
Hydroxy radical scavenging rate ═ 1-A1/A2)×100%
TABLE 4
Figure BDA0001919707070000111
Figure BDA0001919707070000121
Test of moisturizing Effect
The essence water prepared in the examples 1-7 and the comparative example 1 is selected as a test sample, and 20 subjects are randomly divided into 8 groups of 160 subjects. After each day of cleansing, the skin was applied to the facial skin and the skin moisture content was measured by a skin moisture tester CM825 from CK, Germany, after one month of use, and the results are shown in Table 5.
TABLE 5
Figure BDA0001919707070000122
In conclusion, the essence water is compounded by the aesculus hippocastanum seed extract, the yeast/rice bran fermentation product, the pseudoalteromonas fermentation product extract and the lettuce extract, so that a synergistic effect is generated, the skin color can be effectively brightened, the melanin can be lightened, and the essence water has the performances of oxidation resistance and long-acting moisture retention.
Finally, it should be noted that the above embodiments are only used for illustrating the technical solutions of the present invention and not for limiting the protection scope of the present invention, and although the present invention is described in detail with reference to the preferred embodiments, it should be understood by those skilled in the art that modifications or equivalent substitutions can be made on the technical solutions of the present invention without departing from the spirit and scope of the technical solutions of the present invention.

Claims (3)

1. The transparent oil bead suspension essence is characterized by comprising the following components in percentage by mass:
phase A: 4% of diphenylsiloxy phenyl trimethyl siloxane, 2% of diphenyl dimethyl polysiloxane and 1% of spherical powder; the spherical powder is at least one of tapioca starch and polymethylsilsesquioxane;
phase B: the balance of water, 5 percent of butanediol, 3 percent of trehalose, 0.1 percent of methyl hydroxybenzoate, 60.15 percent of polyacrylate cross-linked polymer and 0.3 percent of sodium hyaluronate;
and C phase: 3% of European horse chestnut seed extract, 3% of yeast/rice bran fermentation product, 2% of pseudoalteromonas fermentation product extract and 3% of lettuce extract;
phase D: 0.3 percent of preservative.
2. The essential water of claim 1, wherein the preservative is at least one of phenoxyethanol, methylparaben, ethylparaben, and ethylhexylglycerin.
3. The method for preparing the essence water of transparent oil bead suspension according to claim 1, comprising the steps of:
(1) adding the phase A component into an oil pan, heating to 85-90 ℃, and stirring for dissolving;
(2) adding water in the phase B into a main pot, heating to 85-90 ℃, sequentially adding the phase B components, and homogenizing and stirring for 25-30 min;
(3) adding the phase B into the phase A, and uniformly stirring;
(4) and naturally cooling to 42-45 ℃, adding the phase C and the phase D, and uniformly stirring to obtain the transparent oil bead suspension essence water.
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