CN110721120A - Multifunctional skin care cream and preparation method thereof - Google Patents

Multifunctional skin care cream and preparation method thereof Download PDF

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Publication number
CN110721120A
CN110721120A CN201911058151.1A CN201911058151A CN110721120A CN 110721120 A CN110721120 A CN 110721120A CN 201911058151 A CN201911058151 A CN 201911058151A CN 110721120 A CN110721120 A CN 110721120A
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skin
percent
phase
polydimethylsiloxane
stirring
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邝月红
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Guangzhou Natural Biotechnology Co Ltd
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Guangzhou Natural Biotechnology Co Ltd
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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/98Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin
    • A61K8/987Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin of species other than mammals or birds
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/92Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
    • A61K8/922Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • A61K8/9783Angiosperms [Magnoliophyta]
    • A61K8/9789Magnoliopsida [dicotyledons]
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • A61Q19/008Preparations for oily skin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • A61Q19/02Preparations for care of the skin for chemically bleaching or whitening the skin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • A61Q19/08Anti-ageing preparations

Abstract

The invention discloses a multifunctional skin cream and a preparation method thereof, wherein the ingredients of the multifunctional skin cream comprise caprylic/capric triglyceride, beeswax, pentaerythritol tetraisostearate, titanium dioxide, isononyl isononanoate, petrolatum, polydimethylsiloxane, ethylhexyl palmitate, phenylisopropyl polydimethylsiloxane, shea butter, undecylenoyl phenylalanine, cetyl PEG/PPG-10/1 polydimethylsiloxane, lipid complex, sturgeon caviar extract, Glycyrrhiza glabra root extract, emblic leafflower fruit extract and the like. According to the skin care product, natural active ingredients such as sturgeon caviar extract, shea butter, glabrous licorice root extract, emblic leafflower fruit extract and lipid complex are added in a compounding manner, so that on the basis of improving the skin glossiness, a plurality of effects such as lifting, moisturizing, elasticity, tightening, whitening and anti-wrinkle are added, and the problems of skin darkness and yellowing, dryness and roughness, skin aging, blemishes and the like in the prior art are solved.

Description

Multifunctional skin care cream and preparation method thereof
Technical Field
The invention relates to the technical field of cosmetics, in particular to a multifunctional skin care cream and a preparation method thereof.
Background
The skin, one of the most important organs of the human body, can gradually have aging conditions along with the increase of the age, such as loss of elasticity, darkness and yellowing, generation of wrinkles, color spots and the like; or the skin is dry and rough, pores become large and the like under the influence of the external environment; or, some people's natural skin is in the condition of black and yellow skin, blemishes, dull and dull, and uneven skin. These skin conditions can negatively affect people's work and life. Although various skin care products appear in the market at present, such as some skin care creams like the Guifu cream, etc., are claimed to have the effects of whitening, lightening spots or improving skin glossiness, etc., the skin care products have different qualities, or have very high cost or are easy to be allergic.
Therefore, it is necessary to research a pure natural multifunctional skin care cream with good effects of resisting wrinkles, preventing aging, whitening and repairing skin.
Disclosure of Invention
The invention aims to provide a multifunctional skin care cream and a preparation method thereof, natural active ingredients such as sturgeon caviar extract, shea butter fruit resin, glabrous licorice root extract, emblic leafflower fruit extract and lipid complex are added in a compounding manner, and on the basis of improving the skin glossiness, the multifunctional skin care cream increases a plurality of effects such as lifting, moisture retention, elasticity, firmness, oil control, whitening, wrinkle resistance and the like, and solves the problems of dark and yellow skin, dry and rough skin, skin aging, blemishes and the like in the prior art.
In order to achieve the purpose, the invention adopts the following technical scheme:
in a first aspect, the invention provides a multifunctional skin care cream which is prepared from the following raw materials in percentage by weight:
phase A: 14 to 16 percent of caprylic/capric triglyceride, 5 to 7 percent of beeswax, 5 to 7 percent of pentaerythritol tetraisostearate, 5 to 7 percent of titanium dioxide, 2.5 to 3.5 percent of isononyl isononanoate, 2.5 to 3.5 percent of petrolatum, 2 to 3 percent of silica, 1 to 3 percent of polydimethylsiloxane, 1 to 3 percent of ethylhexyl palmitate, 1 to 2 percent of phenylisopropyl polydimethylsiloxane, 0.8 to 1.2 percent of shea butter, 0.4 to 0.6 percent of undecylenoyl phenylalanine, EasyovTM0.4-0.6% of NEW water-in-oil emulsifier, 0.2-0.6% of cetyl PEG/PPG-10/1 polydimethylsiloxane, 180.3-0.6% of quaternary ammonium salt and 0.4-0.6% of lipid complex;
phase B:
Figure BDA0002257108880000021
PE 9010 liquid preservative 0.3% -0.6%, bisabolol 0.01% -0.04%, farnesol 0.01% -0.04%, sturgeon caviar extract 0.02% -0.08%, glycyrrhiza glabra root extract 0.001%, phyllanthus emblica fruit extract 0.001%, lemon yellow 0.001% -0.003%, sunset yellow 0.001%;
and C phase: SEPIPLUSTM0.4 to 0.6 percent of 400 percent of emulsifier;
phase D: glycerin polyether-262-4%, propylene glycol 1.5-2.5%, butanediol 0.5-1.5%, methyl hydroxybenzoate 0.1-0.3%, sodium polyacrylate 0.05-0.15%, and water in balance.
The formula of the multifunctional skin care cream achieves better effects of resisting aging, whitening and fading spots and reducing fine lines through a scientific proportion, effectively improves the skin darkness and yellowing, conceals blemishes and pores, improves the skin glossiness, and enables the skin to be elastic and bright.
The shea butter of the invention has the functions of locking water and keeping moisture, and also can promote the capillary vessel circulation and cell regeneration of skin, thereby reducing wrinkles and delaying senility. The shea butter contains abundant glyceric acid, protein and vitamin, is moist but not greasy, is a natural antioxidant anti-aging agent, can soften and moisten skin, can shrink pores, can form a milky isolating layer on the surface of the skin, can effectively resist sunlight irradiation, and can prevent suntan and sunburn; the rich cinnamate can also prevent skin injury and anaphylactic reaction caused by ultraviolet irradiation, and has certain effect on preventing sunburn and sunburn. In addition, the shea butter contains abundant vitamin E, magnesium, linoleic acid and essential fatty acid, is helpful for strengthening and toughening cell membranes, has soft and exquisite texture, and delays the aging speed of epidermal cells.
The glycyrrhiza glabra root extract has the effects of resisting bacteria, diminishing inflammation, resisting oxidation, resisting aging, preventing ultraviolet rays, whitening and brightening skin, removing freckles and the like. The glycyrrhiza glabra root extract used in the invention is purchased from baihabo ltd, guangzhou, and has the following model: the oil soluble licorice extract BIO-OSLP contains glabridin as powerful whitening factor in the content not lower than 40%. Has strong inhibiting effect on tyrosinase activity, and has better effect of inhibiting melanin synthesis of cells and lower cytotoxicity compared with hydroquinone, arbutin and MAP. In addition, the whitening anti-inflammatory cream can inhibit the activity of lipoxygenase, remove free radicals and achieve the effects of whitening and resisting inflammation.
The emblic leafflower fruit extract has the effects of resisting inflammation, resisting oxidation and resisting aging. The fructus Phyllanthi contains various vitamins, microelements, amino acids, organic acids, proteins and saccharides, and also contains a large amount of superoxide dismutase (SOD). SOD is free radical scavenger capable of scavenging free radical O2 -(superoxide anion radical), SOD in natural extracts is more easily absorbed by the skin. The emblic extract used in the invention is purchased from Baihabo Co Ltd, Guangzhou, type: emblicaTM(130165)。
The sturgeon caviar extract disclosed by the invention is rich in protein, fatty acid and vitamin, so that the sturgeon caviar extract brings rich nutrient substances to the skin, promotes skin metabolism, supplements lipid components to the skin, resists oxidation and regeneration, helps to inhibit skin aging, and has the effects of resisting aging, fading wrinkles, repairing damaged skin, moisturizing and the like. The sturgeon caviar extract is extracted from roe of deep-sea sturgeon, is rich in protein, nucleic acid, water-soluble vitamins, minerals, etc., has cell structure similar to human skin structure, is easy to be absorbed by skin, and can accelerate synthesis of collagen and increase skin elasticity. The sturgeon caviar extract used in the present invention is purchased from baihaobo limited company, guangzhou, with the type: caviar extract (300130).
The caprylic/capric triglyceride is easy to be absorbed by the skin, plays a good role in the uniformity and fineness of cosmetics, and enables the skin to be smooth and glossy. The caprylic/capric triglyceride can be used as base material of moisturizing factor, and has emollient effect.
The beeswax provided by the invention has the effect of improving the skin and has the function of an emollient.
The pentaerythritol tetraisostearate is high molecular weight liquid grease, is insoluble in water, is fresh and moist and not greasy, provides very moist and not greasy skin feel for skin, plays a role of an emollient, and is suitable for being applied to cream products.
The isononyl isononanoate of the invention has a unique multi-methyl branched chain structure, has silky feel, dry and comfortable and extremely soft hand feeling, and is an excellent emollient.
The petrolatum, also called vaseline, can ensure that moisture is not easy to evaporate and dissipate, can keep the skin in a moist state, has the effects of moisturizing, moistening and relieving the dryness of the skin, is mainly used for skin problems such as skin chap, skin dryness and pruritus and the like, and plays a role of a moisturizer.
The ethylhexyl palmitate disclosed by the invention has excellent penetrating, moistening and softening effects on skin and plays a role of an emollient.
The phenyl isopropyl polydimethylsiloxane has the effects of lubricating performance and ultraviolet resistance, is good in air permeability, has an obvious dustproof function, and plays a role of an emollient.
The titanium dioxide has a good ultraviolet screening effect and plays a role of a physical whitening agent and a sunscreen agent.
The silica of the present invention acts as a skin conditioner, providing lubrication.
The polydimethylsiloxane provided by the invention is used as a skin conditioner, has the functions of lubricating property and ultraviolet resistance, and is good in air permeability, obvious in dustproof function and good in skin care function.
The undecylenoyl phenylalanine provided by the invention is used as a conditioning agent, can inhibit the activity of melanocytes and reduce the generation of melanin.
Easyov described by the inventionTMThe NEW water-in-oil emulsifier is taken as an emulsifier, has emulsification and dispersion effects and is purchased from French Saibox company.
The cetyl PEG/PPG-10/1 polydimethylsiloxane provided by the invention has the functions of a skin conditioner, an emulsifier and a penetration enhancer. As a silicone, it can have lubricating and water-holding capabilities, making the skin silky; it can avoid water-oil separation in emulsion, and has good compatibility to prolong release of active molecules, especially pigment; it also has effects in caring skin, and making skin smooth and soft without generating sticky feeling.
The quaternary ammonium salt-18 is called dihydrotallow dimethyl chloride, CAS (CAS) accession number is 61789-80-8, EINECS accession number is 263-090-2, and has the functions of a gel and a stabilizer.
The lipid complex disclosed by the invention plays a role of an emollient and a conditioner, can simulate human sebum (SSLs) by using plant-derived lipids, can provide the same functions as skin surface lipids, has the functions of improving skin barrier function, self-recovery and maintenance function and antibacterial function, and can increase the water retention, viscoelasticity and firmness of skin. The lipid complex used in the present invention was purchased from Floratech international fu roller science ltd, model number: lipid complex L22.
According to the invention
Figure BDA0002257108880000061
The PE 9010 liquid preservative has the antibacterial and preservative effects and is purchased from German Shumei Co, Ltd, and the type is as follows:
Figure BDA0002257108880000062
PE 9010 cosmetic preservative.
The bisabolol provided by the invention is used as a bacteriostatic and skin conditioner, has the effects of protecting and curing skin, preventing the skin from being affected by daily tension and accelerating the skin curing process, can protect and care allergic skin, is green and safe due to the fact that the bisabolol is derived from natural plants, and is suitable for people with sensitive muscles. Bisabolol used in the present invention was purchased from akuran chemical limited, guangzhou city.
The farnesol provided by the invention is used as an antibacterial and skin conditioner, can be used for mildly inhibiting bacteria, only inhibiting microorganisms causing skin problems such as tinea corporis, dermatophytosis, body odor, acne and the like, does not damage a natural protective layer of the skin, maintains the natural ecology of the skin, and promotes the health of the skin. Farnesol used in the present invention was purchased from akuran chemical company, guangzhou.
The lemon yellow pigment of the invention plays a role of a color agent, and is purchased from Shanghai dye research institute Co., Ltd, and has the following model: the "lion head" food color CI 19140.
The sunset yellow pigment provided by the invention plays a role of a color agent, and is purchased from Shanghai dye research institute Co., Ltd, and has the following types: the "Shitou brand" food color CI 15985.
The SEPIPLUS of the inventionTMThe 400 emulsifier plays roles of emulsification and dispersion and is purchased from French Saibox company.
The glyceryl polyether-26 provided by the invention plays a role of a humectant and a spreader.
The propylene glycol is a transparent, colorless, viscous and hygroscopic straight-chain fatty alcohol liquid, has a hydrophilic moisturizing effect, can help active ingredients to permeate and absorb, and plays a role of a humectant.
The butanediol plays a role of a humectant and a solvent, and also has a certain bacteriostatic action.
The methyl hydroxybenzoate provided by the invention is used as a preservative, and has the effects of inhibiting and smoothing skin and the like.
The sodium polyacrylate provided by the invention has the functions of thickening, dispersing, suspending, stabilizing and the like, and is beneficial to the performance of thickening, foaming, stabilizing, emulsifying, dispersing, bonding, film forming, water retention and the like of cosmetics.
The water according to the invention acts as a solvent.
Further, the multifunctional skin care cream is prepared from the following raw materials in percentage by weight:
phase A: caprylic/capric triglyceride 15%, beeswax 6%, pentaerythritol tetraisostearate 6%, titanium dioxide 6%, isononyl isononanoate 3%, petrolatum 3%, silica 2.5%, polydimethylsiloxane 2%, ethylhexyl palmitate 2%, phenylisopropyl polydimethylsiloxane 1.5%, shea butter 1%, undecylenoyl phenylalanine 0.5%, EasynovTM0.5% of NEW water-in-oil emulsifier, 0.5% of cetyl PEG/PPG-10/1 polydimethylsiloxane, 180.5% of quaternary ammonium salt and 0.5% of lipid complex;
phase B:PE 9010 liquid preservative 0.5%, bisabolol 0.025%, farnesol 0.025%, sturgeon caviar extract 0.05%, glycyrrhiza glabra root extract 0.001%, emblic leafflower fruit extract 0.001%, lemon yellow 0.002%, sunset yellow 0.001%;
and C phase: SEPIPLUSTM0.5% of 400% of emulsifier;
phase D: glycerol polyether-263%, propylene glycol 2%, butanediol 1%, methyl hydroxybenzoate 0.2%, sodium polyacrylate 0.1%, and water in balance.
The multifunctional skin care cream has the advantages that the proportion is optimized, the action advantages of single components can be fully exerted, the effect performance of functional components can be fully exerted and enhanced, the optimal effects of resisting aging, whitening and fading spots and fading fine lines are achieved, the skin is effectively improved, the skin is dark and yellow, the skin is covered with blemishes, pores are refined, the skin glossiness is improved, and the skin is elastic, smooth and bright.
Preferably, the lipid complex consists of tocopherol acetate, triglyceride C18-36, jojoba esters, squalene, macadamia phytosterin oleate, phytosterols and tocopherol, wherein the weight ratio of the tocopherol acetate, triglyceride C18-36, jojoba esters, squalene, macadamia phytosterin oleate, phytosterols and tocopherol is 1: 1: 1: 1: 1: 1: 1.
the squalene has antiinflammatory, antibacterial, and repairing effects. The antioxidant has very strong inoxidizability, can supply a large amount of oxygen to cells to restore cell activity and improve the self-healing capability of skin, so the antioxidant is suitable for being used in beauty cosmetics. Firstly, the squalene has the same components as sebum, can help skin to establish a natural protective barrier, can lock skin moisture inwards, can resist dry, cold and harmful substance invasion outwards, keeps skin with good glossiness, is natural and safe, is suitable for various skin types, and has excellent affinity. And moreover, the squalene can regulate the metabolism of skin cells, promote the renewal of skin and repair skin injury, has a good improving effect on rough, uneven and uneven skin with uneven color, and enables the skin to be neat and smooth. In addition, it is also most important that squalene has an anti-radical effect, can scavenge free radicals causing skin aging, and can effectively inhibit skin relaxation, wrinkles, etc., thereby making skin young and active.
The plant sterol macadamia nut oleate has the effects of repairing and supplementing skin nutrition, is extracted from macadamia beans, has high skin permeation speed, leaves smooth and non-greasy feeling on the skin, has excellent dispersion, emulsification, lubrication, anti-inflammation and oxidation resistance, and can be used as a skin softening agent.
Tocopherol, also called vitamin E, is a fat-soluble vitamin, has antioxidant effect, is beneficial to skin, can eliminate the deposition of lipofuscin in cells, improves the normal functions of the cells, slows down the aging process of tissue cells, and has the anti-aging effect.
Tocopherol acetate is also called vitamin E acetate, is a compound produced by esterification of tocopherol (or vitamin E) and acetic acid, and is used as skin regulator and antioxidant for protecting skin from damage caused by ultraviolet rays.
The C18-36 acid triglyceride has effect in softening skin.
The jojoba esters are used as skin conditioners, can effectively relieve skin sensitivity and improve skin resistance.
Phytosterols have high permeability to skin, and can maintain skin surface moisture, promote skin metabolism, and prevent erythema solare and skin aging.
Preferably, the EasyovTMThe NEW water-in-oil emulsifier consists of octyl dodecanol, octyl dodecanol xyloside and PEG-30 dipolyhydroxystearate, wherein the weight ratio of the octyl dodecanol to the octyl dodecanol xyloside to the PEG-30 dipolyhydroxystearate is 1: 1: 1.
octyl dodecanol can improve transdermal speed, and has transdermal promoting effect; octyl dodecanol xyloside has excellent emulsifying and dispersing ability; PEG-30 dipolyhydroxystearate is a multifunctional water-in-oil emulsifier with the special properties of producing a very stable, flowable, low viscosity emulsion that spreads easily on the skin and gives a light, non-greasy skin feel.
Preferably, the SEPIPLUSTMThe 400 emulsifier consists of polyacrylate-13, polyisobutylene and polysorbate-20, wherein the weight ratio of the polyacrylate-13 to the polyisobutylene to the polysorbate-20 is 1: 1: 1.
the polyacrylate-13 plays a role in emulsification and stabilization; the polyisobutene can form a water-resistant film and has strong moisture retention; the polysorbate-20 has emulsifying effect and can increase smoothness of product.
Preferably, the
Figure BDA0002257108880000101
The PE 9010 liquid preservative consists of phenoxyethanol and ethylhexyl glycerol, wherein the weight ratio of the phenoxyethanol to the ethylhexyl glycerol is 1: 1.
phenoxyethanol is a colorless oily liquid, has antibacterial effect, and can be used in skin cream and sunscreen cream as antiseptic.
The ethylhexyl glycerin is used as a preservative-free additive of a cosmetic system, has the effects of bacteriostasis, antisepsis, skin moistening, moisture retention and the like, can enhance the traditional preservative so as to reduce the using amount of substances in the cosmetic, improve the antibacterial effect of multifunctional cosmetic additives such as glycols, fatty acid esters and the like, inhibit the unpleasant odor generated by sebum in human sweat, desquamated epidermal cells and the like under the action of gram-positive bacteria, simultaneously can improve the moisturizing effect of a formula, has smooth skin feel and overcomes the defects of certain cream in skin feel such as stickiness, white coating and the like.
In a second aspect, the invention also provides a preparation method of the multifunctional skin care cream, which comprises the following steps:
s1, weighing the raw materials according to the proportion;
s2, mixing the phase D raw materials, stirring and heating to 90 ℃ to obtain a mixture A;
s3, mixing the phase A raw materials, stirring, homogenizing, dispersing uniformly, stirring and heating to 85 ℃, and stirring at the speed of 50-70 r/min to obtain a mixture B;
s4, slowly adding the mixture B in the step S3 into the mixture A in the step S2, homogenizing for 5 minutes, keeping stirring, and obtaining a mixture C, wherein the stirring speed is 40-60 revolutions per minute;
s5, cooling the mixture C in the step S4 to 60 ℃, adding the phase B raw material, mixing, and stirring uniformly at the stirring speed of 40-60 r/min to obtain a mixture D;
s6, cooling the mixture D in the step S5 to 50 ℃, adding the C-phase raw material, mixing, and stirring uniformly at the speed of 40-60 r/min;
and S7, discharging after the inspection is qualified, filling, packaging and warehousing.
Compared with the prior art, the invention has the following beneficial effects:
according to the invention, natural extracts with functions of resisting aging, whitening and brightening skin, resisting oxidation and reducing wrinkles, such as sturgeon caviar extract, shea butter fruit resin, glabrous licorice root extract, emblic leafflower fruit extract, lipid complex and the like, are selected, and then the extracts are compounded and used, and the compounding ratio is limited, so that the skin darkness and yellowing can be improved, the skin glossiness can be improved, the moisture can be maintained for a long time, the dry and rough skin can be repaired, the skin can be moistened, whitened and softened, the skin aging can be delayed, pores can be reduced, the skin can be tightened, and the skin elasticity can be enhanced; it can be used for improving natural black and yellow skin, blemish, coarse and black skin, dull and dull skin, and uneven skin.
Compared with the traditional skin care cream, the multifunctional skin care cream disclosed by the invention has the advantages that the components for resisting aging, whitening and brightening the skin, resisting oxidation and reducing wrinkles are natural extracts, no irritant component is contained, the multifunctional skin care cream cannot damage the skin after long-term use, the skin is not sensitive, and the safety is good.
Detailed Description
The technical solutions of the present invention will be described clearly and completely with reference to the following embodiments, and it should be understood that the described embodiments are only a part of the embodiments of the present invention, and not all of the embodiments. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.
Description of the raw materials used:
the shea butter is purchased from Guangzhou Cheng Jiya Biotechnology Gmby; glycyrrhiza glabra root extract was purchased from Baihaobo, Inc., Guangzhou, model number: BIO-OSLP extracted from oil soluble Glycyrrhrizae radix; the emblic extract is purchased from baihaobo limited, guangzhou, model: emblicaTM(130165); sturgeon caviar extract was purchased from baihaobo ltd, guangzhou, type: caviar extract (300130); caprylic/capric triglyceride is available from Poa, UK; beeswax was purchased from Cheng Yuan bee limited, Chang Ge City; pentaerythritol tetraisostearate was purchased from Guangzhou Star science Inc.; isononyl isononanoate was purchased from sepbec corporation (SEPPIC); petrolatum was purchased from the riverside flying petrochemical group, ltd; ethylhexyl palmitate was purchased from Taiwan co-chemical Panjin, Inc; the phenylisopropylpolydimethylsiloxanes were obtained from Siltech, Canada; titanium dioxide was purchased from champion chemical technology ltd, guangzhou; silica was purchased from Guangzhou Ruiping chemical Co., Ltd; polydimethylsiloxane is available from the dow chemical company; undecylenoylphenylalanine was purchased from the french seebeck company (SEPPIC); easyovTMNEW water-in-oil emulsifiers were purchased from Seabic, France (SEPPIC); cetyl PEG/PPG-10/1 Dimethicone available from Yongchu specialty Chemicals (Shanghai) Co., Ltd; quaternary ammonium salt-18 was purchased from Olympic commerce, Guangzhou; lipid complexes were purchased from Floratech international fu roller technologies ltd, model: lipid complex L22;
Figure BDA0002257108880000121
PE 9010 liquid preservative was purchased from sumei ltd, germany, type:
Figure BDA0002257108880000122
PE 9010 cosmetic preservative; bisabolol was purchased from akuran chemical company, guangzhou city; farnesol was purchased from akuran chemical ltd, guangzhou city; lemon yellow pigment was purchased from shanghai dye research institute, ltd, model: lionBrand name "food color CI 19140; sunset yellow was purchased from shanghai dye research institute, ltd, model number: lion head brand food color CI 15985; SEPIPLUSTM400 emulsifiers were purchased from seibic, france (SEPPIC); glycopolyether-26 was obtained from clariant chemical (china) ltd; propylene glycol was purchased from SKC corporation, korea; butanediol was purchased from Guangzhou Congress chemical technology, Inc.; methylparaben was purchased from shanghai light industrial research institute; sodium polyacrylate was purchased from NlPPON corporation, japan; the water is self-made.
Example 1
The embodiment provides a multifunctional skin care cream which is prepared from the following raw materials in percentage by weight:
phase A: caprylic/capric triglyceride 15%, beeswax 6%, pentaerythritol tetraisostearate 6%, titanium dioxide 6%, isononyl isononanoate 3%, petrolatum 3%, silica 2.5%, polydimethylsiloxane 2%, ethylhexyl palmitate 2%, phenylisopropyl polydimethylsiloxane 1.5%, shea butter 1%, undecylenoyl phenylalanine 0.5%, EasynovTM0.5% of NEW water-in-oil emulsifier, 0.5% of cetyl PEG/PPG-10/1 polydimethylsiloxane, 180.5% of quaternary ammonium salt and 0.5% of lipid complex;
phase B:
Figure BDA0002257108880000131
PE 9010 liquid preservative 0.5%, bisabolol 0.025%, farnesol 0.025%, sturgeon caviar extract 0.05%, glycyrrhiza glabra root extract 0.001%, emblic leafflower fruit extract 0.001%, lemon yellow 0.002%, sunset yellow 0.001%;
and C phase: SEPIPLUSTM0.5% of 400% of emulsifier;
phase D: glycerol polyether-263%, propylene glycol 2%, butanediol 1%, methyl hydroxybenzoate 0.2%, sodium polyacrylate 0.1%, and water in balance.
The preparation method of the multifunctional skin cream comprises the following steps:
s1, weighing the raw materials according to the proportion;
s2, mixing the phase D raw materials, stirring and heating to 90 ℃ to obtain a mixture A;
s3, mixing the phase A raw materials, stirring, homogenizing, dispersing uniformly, stirring and heating to 85 ℃, and stirring at the speed of 50-70 r/min to obtain a mixture B;
s4, slowly adding the mixture B in the step S3 into the mixture A in the step S2, homogenizing for 5 minutes, keeping stirring, and obtaining a mixture C, wherein the stirring speed is 40-60 revolutions per minute;
s5, cooling the mixture C in the step S4 to 60 ℃, adding the phase B raw material, mixing, and stirring uniformly at the stirring speed of 40-60 r/min to obtain a mixture D;
s6, cooling the mixture D in the step S5 to 50 ℃, adding the C-phase raw material, mixing, and stirring uniformly at the speed of 40-60 r/min;
and S7, discharging after the inspection is qualified, filling, packaging and warehousing.
Example 2
The embodiment provides a multifunctional skin care cream which is prepared from the following raw materials in percentage by weight:
phase A: 14% caprylic/capric triglyceride, 5% beeswax, 5% pentaerythritol tetraisostearate, 5% titanium dioxide, 2.5% isononyl isononanoate, 2.5% petrolatum, 2% silica, 1% polydimethylsiloxane, 1% ethylhexyl palmitate, 1% phenylisopropyl polydimethylsiloxane, 0.8% shea butter, 0.4% undecylenoyl phenylalanine, EasyovTM0.4% of NEW water-in-oil emulsifier, 0.2% of cetyl PEG/PPG-10/1 polydimethylsiloxane, 180.3% of quaternary ammonium salt and 0.4% of lipid complex;
phase B:PE 9010 liquid preservative 0.3%, bisabolol 0.01%, farnesol 0.01%, sturgeon caviar extract 0.02%, Glycyrrhiza glabra root extract 0.001%, Emblica officinalis fruit extract 0.001%, lemon yellow 0.001%, sunset yellow 0.001%;
and C phase: SEPIPLUSTM0.4% of 400% of emulsifier;
phase D: glycerol polyether-262%, propylene glycol 1.5%, butanediol 0.5%, methyl hydroxybenzoate 0.1%, sodium polyacrylate 0.05%, and water in balance.
The preparation method of the multifunctional skin cream comprises the following steps:
s1, weighing the raw materials according to the proportion;
s2, mixing the phase D raw materials, stirring and heating to 90 ℃ to obtain a mixture A;
s3, mixing the phase A raw materials, stirring, homogenizing, dispersing uniformly, stirring and heating to 85 ℃, and stirring at the speed of 50-70 r/min to obtain a mixture B;
s4, slowly adding the mixture B in the step S3 into the mixture A in the step S2, homogenizing for 5 minutes, keeping stirring, and obtaining a mixture C, wherein the stirring speed is 40-60 revolutions per minute;
s5, cooling the mixture C in the step S4 to 60 ℃, adding the phase B raw material, mixing, and stirring uniformly at the stirring speed of 40-60 r/min to obtain a mixture D;
s6, cooling the mixture D in the step S5 to 50 ℃, adding the C-phase raw material, mixing, and stirring uniformly at the speed of 40-60 r/min;
and S7, discharging after the inspection is qualified, filling, packaging and warehousing.
Example 3
The embodiment provides a multifunctional skin care cream which is prepared from the following raw materials in percentage by weight:
phase A: caprylic/capric triglyceride 16%, beeswax 7%, pentaerythritol tetraisostearate 7%, titanium dioxide 7%, isononyl isononanoate 3.5%, petrolatum 3.5%, silica 3%, polydimethylsiloxane 3%, ethylhexyl palmitate 3%, phenylisopropyl polydimethylsiloxane 2%, shea butter 1.2%, undecylenoyl phenylalanine 0.6%, EasyovTM0.6% of NEW water-in-oil emulsifier, 0.6% of cetyl PEG/PPG-10/1 polydimethylsiloxane, 180.6% of quaternary ammonium salt and 0.6% of lipid complex;
phase B:
Figure BDA0002257108880000161
PE 9010 liquid preservative 0.6%, bisabolol 0.04%, farnesol 0.04%, sturgeon caviar extract 0.08%, glycyrrhiza glabra root extract 0.001%, emblic leafflower fruit extract 0.001%, lemon yellow 0.003%, sunset yellow 0.001%;
and C phase: SEPIPLUSTM0.6 percent of 400 percent of emulsifier;
phase D: glyceryl polyether-264%, propylene glycol 2.5%, butanediol 1.5%, methyl hydroxybenzoate 0.3%, sodium polyacrylate 0.15%, and water in balance.
The preparation method of the multifunctional skin cream comprises the following steps:
s1, weighing the raw materials according to the proportion;
s2, mixing the phase D raw materials, stirring and heating to 90 ℃ to obtain a mixture A;
s3, mixing the phase A raw materials, stirring, homogenizing, dispersing uniformly, stirring and heating to 85 ℃, and stirring at the speed of 50-70 r/min to obtain a mixture B;
s4, slowly adding the mixture B in the step S3 into the mixture A in the step S2, homogenizing for 5 minutes, keeping stirring, and obtaining a mixture C, wherein the stirring speed is 40-60 revolutions per minute;
s5, cooling the mixture C in the step S4 to 60 ℃, adding the phase B raw material, mixing, and stirring uniformly at the stirring speed of 40-60 r/min to obtain a mixture D;
s6, cooling the mixture D in the step S5 to 50 ℃, adding the C-phase raw material, mixing, and stirring uniformly at the speed of 40-60 r/min;
and S7, discharging after the inspection is qualified, filling, packaging and warehousing.
Comparative example 1
Comparative example 1 differs from example 1 in that shea butter is not included, the corresponding amount is replaced with water, and the preparation method is the same as that of example 1, and therefore, the detailed description is omitted.
Comparative example 2
Comparative example 2 differs from example 1 in that it does not contain a lipid complex, and the corresponding amount is replaced with water, and the preparation method is the same as that of example 1, and thus, the description thereof is omitted.
Comparative example 3
Comparative example 3 differs from example 1 in that the sturgeon caviar extract was not included, and the corresponding content was replaced with water, and the preparation method was the same as that of example 1, and thus, no further description is given herein.
Comparative example 4
Comparative example 4 differs from example 1 in that it does not contain glycyrrhiza glabra root extract and emblic leafflower fruit extract, and the corresponding contents are replaced by water, and the preparation method is the same as that of example 1, and thus, the detailed description thereof is omitted.
To verify the beneficial effects of the multifunctional skin cream of the present invention, the following tests were conducted.
First, anti-wrinkle and anti-aging efficacy test
Testing the population: the multifunctional skin care cream prepared in the embodiment 1 of the invention is used twice in the morning and at night every day in the test of 50 persons and female testers of 40-65 years old.
Testing parameters: wrinkle depth, skin firmness, skin elasticity. The results of the test using the skin elasticity tester MAP580 after two consecutive months are shown in table 1 below.
Table 1: skin change in anti-wrinkle and anti-aging efficacy tests
Skin Properties Compared with before use
Wrinkle depth reduction 15.7%
Increased skin firmness 18.2%
Skin elasticity increasingAdding 7.6%
As can be seen from the results in Table 1, the multifunctional skin care cream provided by the invention can be used for keeping moisture for a long time, repairing dry and rough skin, moistening and softening skin, delaying skin aging, tightening skin, enhancing skin elasticity and reducing wrinkles.
Test two, whitening efficacy test
50 female volunteers aged 20-40 years are selected for testing, the indoor temperature is kept at 25 ℃, the relative humidity is kept at 55%, the multifunctional skin care cream prepared by the invention is coated on the bent parts of the left and right forearms of the volunteers and is continuously used for 28 days, the melanin indexes MI of the test positions at the initial, 7, 14 and 28 days of the test are respectively measured by a skin melanin and heme tester (Mexameter MX18), and the average value is calculated, and the results are shown in Table 2.
Table 2: melanin index MI test result condition in whitening efficacy test
Figure BDA0002257108880000181
As can be seen from the results in Table 2, compared with comparative examples 1 to 4, the melanin index MI tested in examples 1 to 3 is lower, and therefore, the multifunctional skin care cream has a better whitening effect. The whitening effect of the multifunctional skin care cream is the best in example 1, and the whitening effect of the multifunctional skin care cream obtained finally is poor due to the fact that the active ingredients are not partially contained in the comparative examples 1-4, and the fact that the sturgeon caviar extract, the shea butter, the glycyrrhiza glabra root extract, the emblic leafflower fruit extract and the lipid complex are used in a specific ratio shows that the multifunctional skin care cream has a synergistic effect and the whitening effect is improved.
Third test, skin repairing efficacy test
Taking 7 groups of samples of the multifunctional skin care cream prepared in the examples 1-3 and the comparative examples 1-4, selecting 70 female testers with sensitive skin to carry out the effect use evaluation of sensitive skin repair, wherein 7 female testers in each group of samples are scored and averaged, the score is 10, the score of 10 is the best sensitive repair effect, the score of 9 is the lowest, and the score of 1 is the worst sensitive repair effect. The composition was administered twice daily for 10 consecutive days, and the results are shown in Table 3 below.
Table 3: sensitive skin repair evaluation score condition in skin repair efficacy test
Sample (I) Scoring the effect of repairing sensitive skin
Example 1 10
Example 2 8
Example 3 9
Comparative example 1 4
Comparative example 2 2
Comparative example 3 2
Comparative example 4 3
From the results in table 3, it can be seen that the multifunctional skin care cream prepared according to the technical scheme provided by the invention in the embodiments 1-3 has good repairing effect on sensitive skin. The multifunctional skin care cream has the best repairing effect in example 1, the score reaches 10 points, and the multifunctional skin care cream obtained in comparative examples 1-4 is lack of partial active ingredients, so that the repairing sensitive skin effect of the multifunctional skin care cream is poor, and the multifunctional skin care cream has a synergistic interaction effect and an effect of repairing sensitive skin by using sturgeon caviar extract, shea butter, glabrous licorice root extract, emblic leafflower fruit extract and lipid complex in a specific ratio.
The above description is only for the purpose of illustrating the preferred embodiments of the present invention and is not to be construed as limiting the invention, and any modifications, equivalents, improvements and the like that fall within the spirit and principle of the present invention are intended to be included therein.
Furthermore, it should be understood that although the present description refers to embodiments, not every embodiment may contain only a single embodiment, and such description is for clarity only, and those skilled in the art should integrate the description, and the embodiments may be combined as appropriate to form other embodiments understood by those skilled in the art.

Claims (7)

1. The multifunctional skin cream is characterized by comprising the following raw materials in percentage by weight:
phase A: 14 to 16 percent of caprylic/capric triglyceride, 5 to 7 percent of beeswax, 5 to 7 percent of pentaerythritol tetraisostearate, 5 to 7 percent of titanium dioxide, 2.5 to 3.5 percent of isononyl isononanoate, 2.5 to 3.5 percent of petrolatum, 2 to 3 percent of silica, 1 to 3 percent of polydimethylsiloxane, 1 to 3 percent of ethylhexyl palmitate, 1 to 2 percent of phenylisopropyl polydimethylsiloxane, 0.8 to 1.2 percent of shea butter, 0.4 to 0.6 percent of undecylenoyl phenylalanine, EasyovTM0.4-0.6% of NEW water-in-oil emulsifier, 0.2-0.6% of cetyl PEG/PPG-10/1 polydimethylsiloxane, 180.3-0.6% of quaternary ammonium salt and 0.4-0.6% of lipid complex;
phase B:
Figure FDA0002257108870000011
PE 9010 liquid preservative 0.3% -0.6%, bisabolol 0.01% -0.04%, farnesol 0.01% -0.04%, sturgeon caviar extract 0.02% -0.08%, glycyrrhiza glabra root extract 0.001%, phyllanthus emblica fruit extract 0.001%, lemon yellow 0.001% -0.003%, sunset yellow 0.001%;
and C phase: SEPIPLUSTM0.4 to 0.6 percent of 400 percent of emulsifier;
phase D: glycerin polyether-262-4%, propylene glycol 1.5-2.5%, butanediol 0.5-1.5%, methyl hydroxybenzoate 0.1-0.3%, sodium polyacrylate 0.05-0.15%, and water in balance.
2. The multifunctional skin cream according to claim 1, which is characterized by comprising the following raw materials in percentage by weight:
phase A: caprylic/capric triglyceride 15%, beeswax 6%, pentaerythritol tetraisostearate 6%, titanium dioxide 6%, isononyl isononanoate 3%, petrolatum 3%, silica 2.5%, polydimethylsiloxane 2%, ethylhexyl palmitate 2%, phenylisopropyl polydimethylsiloxane 1.5%, shea butter 1%, undecylenoyl phenylalanine 0.5%, EasyvTM0.5% of NEW water-in-oil emulsifier, 0.5% of cetyl PEG/PPG-10/1 polydimethylsiloxane, 180.5% of quaternary ammonium salt and 0.5% of lipid complex;
phase B:
Figure FDA0002257108870000021
PE 9010 liquid preservative 0.5%, bisabolol 0.025%, farnesol 0.025%, sturgeon caviar extract 0.05%, glycyrrhiza glabra root extract 0.001%, emblic leafflower fruit extract 0.001%, lemon yellow 0.002%, sunset yellow 0.001%;
and C phase: SEPIPLUSTM0.5% of 400% of emulsifier;
phase D: glycerol polyether-263%, propylene glycol 2%, butanediol 1%, methyl hydroxybenzoate 0.2%, sodium polyacrylate 0.1%, and water in balance.
3. The multifunctional skin cream of claim 1 or 2, wherein the lipid complex is composed of tocopherol acetate, triglycerides of C18-36 acids, jojoba esters, squalene, macadamia phytosterin oleate, phytosterols and tocopherols, and the weight ratio of the tocopherol acetate, triglycerides of C18-36 acids, jojoba esters, squalene, macadamia phytosterin oleate, phytosterols and tocopherols is 1: 1: 1: 1: 1: 1: 1.
4. the multifunctional skin cream as claimed in claim 1 or 2, wherein EasyovTMThe NEW water-in-oil emulsifier consists of octyl dodecanol, octyl dodecanol xyloside and PEG-30 dipolyhydroxystearate, wherein the weight ratio of the octyl dodecanol to the octyl dodecanol xyloside to the PEG-30 dipolyhydroxystearate is 1: 1: 1.
5. the multifunctional skin cream as claimed in claim 1 or 2, wherein the SEPIPLUS is prepared byTMThe 400 emulsifier consists of polyacrylate-13, polyisobutylene and polysorbate-20, wherein the weight ratio of the polyacrylate-13 to the polyisobutylene to the polysorbate-20 is 1: 1: 1.
6. the multifunctional skin cream according to claim 1 or 2, wherein said multifunctional skin cream is characterized in that
Figure FDA0002257108870000031
The PE 9010 liquid preservative consists of phenoxyethanol and ethylhexyl glycerol, wherein the weight ratio of the phenoxyethanol to the ethylhexyl glycerol is 1: 1.
7. the method for preparing a multifunctional skin cream according to claim 1 or 2, comprising the steps of:
s1, weighing the raw materials according to the proportion;
s2, mixing the phase D raw materials, stirring and heating to 90 ℃ to obtain a mixture A;
s3, mixing the phase A raw materials, stirring, homogenizing, dispersing uniformly, stirring and heating to 85 ℃, and stirring at the speed of 50-70 r/min to obtain a mixture B;
s4, slowly adding the mixture B in the step S3 into the mixture A in the step S2, homogenizing for 5 minutes, keeping stirring, and obtaining a mixture C, wherein the stirring speed is 40-60 revolutions per minute;
s5, cooling the mixture C in the step S4 to 60 ℃, adding the phase B raw material, mixing, and stirring uniformly at the stirring speed of 40-60 r/min to obtain a mixture D;
s6, cooling the mixture D in the step S5 to 50 ℃, adding the C-phase raw material, mixing, and stirring uniformly at the speed of 40-60 r/min;
and S7, discharging after the inspection is qualified, filling, packaging and warehousing.
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Cited By (4)

* Cited by examiner, † Cited by third party
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CN113230198A (en) * 2021-06-02 2021-08-10 上海佩威化妆品有限公司 Anti-wrinkle anti-aging freeze-dried essence and preparation method thereof
CN114522112A (en) * 2021-12-20 2022-05-24 广州市瑞芬化妆品有限公司 Instant brightening physical concealer long-acting composition, cream and preparation method
CN115487095A (en) * 2022-09-02 2022-12-20 广东粤港澳大湾区国家纳米科技创新研究院 Cosmetic composition containing nano-liposome, preparation method and application thereof
CN115770267A (en) * 2021-09-07 2023-03-10 广州赞誉化妆品有限公司 Infantile eczema ointment and preparation method thereof

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN113230198A (en) * 2021-06-02 2021-08-10 上海佩威化妆品有限公司 Anti-wrinkle anti-aging freeze-dried essence and preparation method thereof
CN115770267A (en) * 2021-09-07 2023-03-10 广州赞誉化妆品有限公司 Infantile eczema ointment and preparation method thereof
CN114522112A (en) * 2021-12-20 2022-05-24 广州市瑞芬化妆品有限公司 Instant brightening physical concealer long-acting composition, cream and preparation method
CN115487095A (en) * 2022-09-02 2022-12-20 广东粤港澳大湾区国家纳米科技创新研究院 Cosmetic composition containing nano-liposome, preparation method and application thereof

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