CN109384956A - A kind of production method of gum filler silicon powder - Google Patents

A kind of production method of gum filler silicon powder Download PDF

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Publication number
CN109384956A
CN109384956A CN201710656185.5A CN201710656185A CN109384956A CN 109384956 A CN109384956 A CN 109384956A CN 201710656185 A CN201710656185 A CN 201710656185A CN 109384956 A CN109384956 A CN 109384956A
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CN
China
Prior art keywords
silicon powder
grinder
sent
gum filler
grinding
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Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201710656185.5A
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Chinese (zh)
Inventor
郭涛
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Jiangsu Tin Yi High Tech Zone Technology Development Co Ltd
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Jiangsu Tin Yi High Tech Zone Technology Development Co Ltd
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Priority to CN201710656185.5A priority Critical patent/CN109384956A/en
Publication of CN109384956A publication Critical patent/CN109384956A/en
Pending legal-status Critical Current

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    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08KUse of inorganic or non-macromolecular organic substances as compounding ingredients
    • C08K3/00Use of inorganic substances as compounding ingredients
    • C08K3/34Silicon-containing compounds
    • C08K3/36Silica

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  • Chemical & Material Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Organic Chemistry (AREA)
  • Silicon Compounds (AREA)

Abstract

The invention discloses a kind of production method of gum filler silicon powder, which finishes field;The present invention is using high-quality high purity quartz block as raw material, gum filler silicon powder is produced by techniques such as broken, magnetic separation, two-stage grinding, classifications, the production method includes the gum filler silicon powder that equipment investment is few, production cost is low, discharges without sewage exhaust gas, can be mass out high quality, and product is mainly used as filler when rubber production.

Description

A kind of production method of gum filler silicon powder
Technical field
The invention belongs to quartz finishing field more particularly to a kind of production methods of gum filler silicon powder.
Background technique
Vitreous silica is the amorphous state of silica, and the content of silica must not be less than 99.8%, and when production will be smart The natural stone diamond stone of choosing is melted in furnace high-temperature, and melting temperature is 1800 DEG C -1900 DEG C, becomes molten after about 12 hours melting times Melt state, become solid-state vitreous silica after cooling, vitreous silica have using temperature is high, thermal expansion coefficient is low, wear-resisting property is good, The series of advantages such as hardness is high, light transparent refractive is good, piezoelectric property is excellent.The product of vitreous silica has: various specifications and difference Tekite sand, vitreous silica block and the vitreous silica silicon powder of purposes.Vitreous silica silicon powder is by tekite diamond stone through broken The silicon powder that the multiple tracks technique such as broken, magnetic separation, grinding, classification is process is a kind of nontoxic, tasteless, free of contamination inorganic non-gold Belong to material, gum filler silicon powder is that a kind of granularity is a kind of special between normal melt silicon powder and ultra-fine melting silicon powder It is used as the silicon powder of gum filler, in production because it is thinner compared with ordinary silicon powder size, is ground in production using increase level-one Grinding process keeps product granularity thinner.The present invention is a kind of gum filler silicon powder, the content of silica 99.9% or more, For granularity at 2-10 microns, which selects high-purity natural quartz, and through high melt, the vitreous silica block formed after cooling is carried out Micro mist made of attrition process twice has many advantages, such as that purity is high, thermal expansion coefficient is small, low-activity, resistant to chemical etching, outside Seeing is white powder, and bulk density is 200-250 kilograms per cubic meter, widely used.The present invention using high-quality high purity quartz block as raw material, It is process by techniques such as broken, magnetic separation, two-stage grinding, classifications, the major advantage of the process flow is: simple process, nothing The gum filler silicon powder that toxic and harmful gas and liquid discharge, can be mass and produce high quality.
Summary of the invention
Present invention mainly solves the problem of be to provide the production method of gum filler silicon powder a kind of, this method is with high-quality height Pure quartz wedge is raw material, produces gum filler silicon powder by techniques such as broken, magnetic separation, two-stage grinding, classifications.
The present invention can be achieved through the following technical solutions:
(1) high-quality high purity quartz block is sent into broken crusher machine, obtains tekite sand of the diameter less than 3 millimeters.
(2) tekite sand is sent into magnetic separator, will be divided containing magnetic, the tekite sand containing metal and metal oxide It leaves away and removes, the magnetic separation time is 0.3-0.4 hours.
(3) the tekite sand after magnetic separation is sent to grinder to grind, controls charging and the discharging speed of grinder Equilibrium, keeping milling time is 2.5-3.0 hours.
(4) powder after the grinding of first order grinder, which is sent to second level grinder, is ground, milling time 1.5- 2.0 hours, vibrating screen is sent to be sieved after grinding, the biggish return second level grinder of granularity repeats to grind, and granularity conforms to Ask the discharging of silicon powder.
Preferably, the granularity of the gum filler silicon powder is 2-10 microns.
The beneficial effects of the present invention are: providing a kind of production method of gum filler silicon powder, which is included The gum filler silicon powder that equipment investment is few, production cost is low, discharges without sewage exhaust gas, can be mass out high quality, product It is mainly used as filler when rubber production.
Specific embodiment
Below with reference to specific embodiment, the present invention is described in further detail.
Embodiment 1
High-quality high purity quartz block is sent into broken crusher machine, obtains tekite sand of the diameter less than 3 millimeters;By tekite sand It is sent into magnetic separator, separation removal will be carried out containing magnetic, the tekite sand containing metal and metal oxide, the magnetic separation time is 0.3 small When;Tekite sand after magnetic separation is sent to grinder to grind, charging and the discharging speed for controlling grinder are balanced, keep Milling time is 2.5 hours;Powder after the grinding of first order grinder, which is sent to second level grinder, to be ground, milling time It is 2.0 hours, send vibrating screen to be sieved after grinding, the biggish return second level grinder of granularity repeats to grind, and granularity meets It is required that the discharging of silicon powder.
Embodiment 2
High-quality high purity quartz block is sent into broken crusher machine, obtains tekite sand of the diameter less than 3 millimeters;By tekite sand It is sent into magnetic separator, separation removal will be carried out containing magnetic, the tekite sand containing metal and metal oxide, the magnetic separation time is 0.35 small When;Tekite sand after magnetic separation is sent to grinder to grind, charging and the discharging speed for controlling grinder are balanced, keep Milling time is 2.75 hours;Powder after the grinding of first order grinder send to second level grinder and is ground, when grinding Between be 1.75 hours, send vibrating screen to be sieved after grinding, biggish the returns second level grinder of granularity repeats to grind, and granularity accords with Close the discharging for requiring silicon powder.
Embodiment 3
High-quality high purity quartz block will be sent into broken crusher machine, obtain tekite sand of the diameter less than 3 millimeters;By vitreous silica Sand is sent into magnetic separator, will carry out separation removal containing magnetic, the tekite sand containing metal and metal oxide, the magnetic separation time is 0.4 Hour;Tekite sand after magnetic separation is sent to grinder to grind, charging and the discharging speed for controlling grinder are balanced, protect Holding milling time is 3.0 hours;Powder after the grinding of first order grinder send to second level grinder and is ground, when grinding Between be 1.5 hours, send vibrating screen to be sieved after grinding, biggish the returns second level grinder of granularity repeats to grind, and granularity accords with Close the discharging for requiring silicon powder.

Claims (2)

1. a kind of production method of gum filler silicon powder, this method passes through broken, magnetic using high-quality high purity quartz block as raw material The techniques such as choosing, two-stage grinding, classification produce normal melt quartz silicon powder, it is characterized in that:
(1) high-quality high purity quartz block is sent into broken crusher machine, obtains tekite sand of the diameter less than 3 millimeters;
(2) tekite sand is sent into magnetic separator, will be separated containing magnetic, the tekite sand containing metal and metal oxide It removes, the magnetic separation time is 0.3-0.4 hours;
(3) the tekite sand after magnetic separation grinder being sent to grind, charging and the discharging speed for controlling grinder are balanced, Keeping milling time is 2.5-3.0 hours;
(4) powder after the grinding of first order grinder, which is sent to second level grinder, is ground, and milling time is that 1.5-2.0 is small When, send vibrating screen to be sieved after grinding, the biggish return second level grinder of granularity repeats to grind, and the granularity silicon that meets the requirements is micro- The discharging of powder.
2. the production method of a kind of gum filler silicon powder according to claim 1, it is characterized in that: the gum filler The granularity of silicon powder is 2-10 microns.
CN201710656185.5A 2017-08-03 2017-08-03 A kind of production method of gum filler silicon powder Pending CN109384956A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201710656185.5A CN109384956A (en) 2017-08-03 2017-08-03 A kind of production method of gum filler silicon powder

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201710656185.5A CN109384956A (en) 2017-08-03 2017-08-03 A kind of production method of gum filler silicon powder

Publications (1)

Publication Number Publication Date
CN109384956A true CN109384956A (en) 2019-02-26

Family

ID=65412259

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201710656185.5A Pending CN109384956A (en) 2017-08-03 2017-08-03 A kind of production method of gum filler silicon powder

Country Status (1)

Country Link
CN (1) CN109384956A (en)

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Application publication date: 20190226