CN109355136A - A kind of preparation method and its handmade soap of lily feet flower essential oil - Google Patents
A kind of preparation method and its handmade soap of lily feet flower essential oil Download PDFInfo
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- CN109355136A CN109355136A CN201811309089.4A CN201811309089A CN109355136A CN 109355136 A CN109355136 A CN 109355136A CN 201811309089 A CN201811309089 A CN 201811309089A CN 109355136 A CN109355136 A CN 109355136A
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/02—Recovery or refining of essential oils from raw materials
- C11B9/025—Recovery by solvent extraction
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/48—Medical, disinfecting agents, disinfecting, antibacterial, germicidal or antimicrobial compositions
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/02—Compositions of detergents based essentially on soap on alkali or ammonium soaps
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/04—Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
- C11D9/22—Organic compounds, e.g. vitamins
- C11D9/26—Organic compounds, e.g. vitamins containing oxygen
- C11D9/262—Organic compounds, e.g. vitamins containing oxygen containing carbohydrates
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/04—Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
- C11D9/22—Organic compounds, e.g. vitamins
- C11D9/26—Organic compounds, e.g. vitamins containing oxygen
- C11D9/265—Organic compounds, e.g. vitamins containing oxygen containing glycerol
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/04—Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
- C11D9/22—Organic compounds, e.g. vitamins
- C11D9/26—Organic compounds, e.g. vitamins containing oxygen
- C11D9/267—Organic compounds, e.g. vitamins containing oxygen containing free fatty acids
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/04—Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
- C11D9/22—Organic compounds, e.g. vitamins
- C11D9/38—Products in which the composition is not well defined
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Abstract
The invention belongs to plants essential oil technical fields, and in particular to a kind of preparation method and its handmade soap of lily feet flower essential oil.The preparation method of the lily feet flower essential oil is easy, mild, and chemical reagent is not added in extraction process, and safety and environmental protection, obtained trollflower extraction of essential oil rate is high, and property is stablized, and quality is good.Lily feet flower essential oil produced by the present invention can be used for preparing handmade soap, the handmade soap includes that following parts by weight prepare raw material: 3~5 parts of lily feet flower essential oil, 5~10 parts of palmitoleic acid sodium, 8~15 parts of Sodium myristate, 10~20 parts of sodium carboxymethyl starch, 4~8 parts of glycerol, 2~6 parts of antioxidant, 0.3~1 part of essence and 45~55 parts of deionized water, with good performance of keeping humidity, the drying property and gloss of skin are significantly improved, and has achieved the effect that smoothing wrinkle and anti-aging.
Description
Technical field
The invention belongs to plants essential oil technical fields, and in particular to a kind of preparation method and its craft of lily feet flower essential oil
Soap.
Background technique
Trollflower is drying flower and alabastrum also known as nonirrigated farmland lotus, globe-flower of ranunculaceae plant trollflower etc., is a kind of history
Long traditional mongolian medicine is mainly distributed on the ground such as east Inner Mongolia, Technique in Western Jilin Province and Liaoning.It is trollflower bitter, cold in nature, nontoxic,
The diseases such as aphtha, mesh pain, ear pain, superficial heat pingival atrophy can be controlled, have preferable treatment for tonsillitis, pharyngitis and the infection of the upper respiratory tract
Effect, it is civil to be drunk extensively for tea bubble in treating the lighter infection of the upper respiratory tract and cold and dressed with sauce edible with trollflower.Currently on the market
There is the product of many serial Chinese globeflowers, as globeflower capsule and trollius chinensis granular are used to treat the infection of the upper respiratory tract, pharyngitis
With tonsillitis etc..
Plants essential oil is that one kind refines out from flower, leaf, root, bark, fruit, seed, resin extraction in plant
Highly concentrated liquid with volatile, molecular weight is low, therefore is easy to be absorbed by the body, and can permeate people's intracorporeal organ rapidly,
Extra ingredient is excreted, and the fragrance of plant itself, also directly stimulate the secretion of pituitary gland, ferment and hormone point
It secretes, function in balanced body plays the role of beauty and skin care.Natural plant essential oils have can promote cytothesis, bactericidal antiphlogistic,
Pacify calm and strengthen immunity function.At present due to the limitation in the source of natural essential oil, essence is extracted from plants
Concern of the oil by more and more people.Studies have shown that the main active substances of trollflower are alkaloid, flavones and volatility essence
Oil, wherein alkaloid and flavones ingredient are studied more mature, and volatile essential oil ingredient gradually obtains science in recent years and grinds
The attention for the person of studying carefully.The antioxidant activity of lily feet flower essential oil is studied for example, Wei Yongjiang, beam will are remote etc., is steamed by vapor
The method of evaporating is extracted to obtain lily feet flower essential oil, then studies its antioxidant activity, but the recovery rate of obtained lily feet flower essential oil
It is very low, only 0.11%, the waste of effective component is caused, the development and utilization of lily feet flower essential oil, and gained gold are unfavorable for
The antioxidant activity of lotus flower essential oil is bad, it may be possible to since prolonged high temperature causes the effective component in essential oil to be decomposed,
Influence activity.
Therefore, based on current lily feet flower essential oil is low in the prevalence of extraction efficiency, product quality is bad and organic reagent
The problems such as residual, it is good and safe without organic reagent residual to need to provide a kind of high, obtained product quality of extraction efficiency for people
Lily feet flower essential oil preparation method and applications.
Summary of the invention
The present invention is directed to overcome the shortcomings of the prior art, the preparation method and its craft of a kind of lily feet flower essential oil are provided
Soap, the trollflower extraction of essential oil which extracts is high-efficient, product quality is good and safety is remained without organic reagent, preparation
Lily feet flower essential oil be added in handmade soap by a certain percentage, have good performance of keeping humidity, hence it is evident that improve the drying of skin
Property and gloss, and achieved the effect that smoothing wrinkle and anti-aging.
To achieve the goals above, technical scheme is as follows:
A kind of preparation method of lily feet flower essential oil, comprising the following steps:
S1, the fresh trollflower of picking is placed in baking oven, the dry 4h at 50 DEG C, and is crushed to 10~40 mesh, be made
Lily feet pollen；
S2, lily feet pollen obtained in step S1 is fitted into extraction column, is compacted, installs；
S3, cooling tower and cold are first opened, opens CO afterwards2Extraction kettle water tank temperature 50~60 is arranged in overcritical equipment
DEG C, 60~65 DEG C of second level extraction-container water tank temperature, 30~40 DEG C of three-level extraction-container water tank temperature opens each valve step by step and gets through gas
Body circulation simultaneously carries out air-discharging；
S4, CO is opened2Force (forcing) pump, the frequency for adjusting force (forcing) pump is 18~z for 24 hours；
S5, extraction kettle dump valve is adjusted, keeping pressure in extraction kettle is 25~30MPa, second level extraction-container dump valve is adjusted,
Keeping pressure in kettle is 6~10MPa, adjusts three-level extraction-container dump valve, and keeping pressure in kettle is 5MPa or hereinafter, extraction 2.5h
~3h；
S6, CO is closed2Force (forcing) pump collects lily feet flower essential oil from second level extraction-container product dump valve, is heated to 48 DEG C~52
DEG C, the boiling water that oil weighs 3~5% is added, quickly stirs 10~20min, is warming up to 78 DEG C~80 DEG C, stops stirring, heat preservation stands 5
~8h takes supernatant through 12000r/min high speed centrifugation 15min, takes supernatant to get lily feet flower essential oil.
Further, the preparation method of the lily feet flower essential oil, comprising the following steps:
S1, the fresh trollflower of picking is placed in baking oven, the dry 4h at 50 DEG C, and is crushed to 30 mesh, lily feet is made
Pollen；
S2, lily feet pollen obtained in step S1 is fitted into extraction column, is compacted, installs；
S3, cooling tower and cold are first opened, opens CO afterwards2Overcritical equipment, 55 DEG C of extraction kettle water tank temperature of setting, two
62 DEG C of water tank temperature of extraction-container of grade, 35 DEG C of three-level extraction-container water tank temperature open each valve step by step and get through gas and recycle and carry out
Air-discharging；
S4, CO is opened2Force (forcing) pump, the frequency for adjusting force (forcing) pump is 20hz；
S5, extraction kettle dump valve is adjusted, keeping pressure in extraction kettle is 28MPa, adjusts second level extraction-container dump valve, keeps
Pressure is 8MPa in kettle, adjusts three-level extraction-container dump valve, and keeping pressure in kettle is 4MPa, extracts 3h；
S6, CO is closed2Force (forcing) pump collects lily feet flower essential oil from second level extraction-container product dump valve, is heated to 50 DEG C, is added
The boiling water of oily weight 4%, quickly stirs 15min, is warming up to 80 DEG C, stops stirring, and heat preservation stands 7h, takes supernatant through 12000r/
Min high speed centrifugation 15min, takes supernatant to get lily feet flower essential oil.
A kind of lily feet flower essential oil handmade soap prepares raw material including following parts by weight: lily feet anthosin produced by the present invention
Oil 3~5 parts, 5~10 parts of palmitoleic acid sodium, 8~15 parts of Sodium myristate, 10~20 parts of sodium carboxymethyl starch, 4~8 parts of glycerol,
2~6 parts of antioxidant, 0.3~1 part of essence and 45~55 parts of deionized water.
Further, the lily feet flower essential oil handmade soap prepares raw material including following parts by weight: produced by the present invention
4 parts of lily feet caul-fat, 8 parts of palmitoleic acid sodium, 12 parts of Sodium myristate, 15 parts of sodium carboxymethyl starch, 6 parts of glycerol, antioxidant 4
Part, 0.7 part of essence and 50.3 parts of deionized water.
Further, the antioxidant is the composition of gallic acid and GINKGO BILOBA EXTRACT, the gallic acid and ginkgo
The weight ratio of flavones is (0.2~0.6): 1.
Further, the weight ratio of the gallic acid and GINKGO BILOBA EXTRACT is 0.33:1.
The preparation method of the lily feet flower essential oil handmade soap, comprising the following steps:
S1, by palmitoleic acid sodium, Sodium myristate, sodium carboxymethyl starch, glycerol, antioxidant, essence and deionized water
It mixes in proportion, 70~75 DEG C of heating water baths stir to being completely dissolved, are cooled to 50~55 DEG C of heat preservations, and mixed liquor A is made；
S2, lily feet flower essential oil is added into the mixed liquor, stirs evenly, mixed liquid B is made；
S3, the mixed liquid B is poured into mold to solidification 12~for 24 hours, is demoulded after soap lye solidification, it is dry is placed in shady and cool ventilation
After repairing packaging, lily feet flower essential oil handmade soap is made in dry place 3~5 days.
In the inventive solutions, by supercritical CO2The lily feet flower essential oil that extraction obtains have antibacterial anti-inflammatory,
Anti-oxidant, blackhead of dispelling, desalination melanin effect；Sodium carboxymethyl starch is a kind of water soluble anionic high-molecular compound,
With stronger water imbibition and dilatancy, good moisture absorption and performance of keeping humidity are shown, acts synergistically, reaches with lily feet flower essential oil
Excellent performance of keeping humidity.
Gallic acid is a kind of polyphenol compound, and scientific name is Gallic Acid, and it is big to be widely present in palm leaf
In the plants such as Huang, great Ye amine, mainly there are the various biologicals such as anti-inflammatory, anti-mutation, anti-oxidant, free radical resisting active；GINKGO BILOBA EXTRACT
It is the active principle extracted from ginkgo, there are expansion blood vessel, adjustment body processes, improve metabolism and eliminate the function of fatigue
Effect, the two are synergistic, and interact with the other ingredients of the present invention, can be obviously improved the gloss of skin, reach smoothing wrinkle and
The effect of anti-aging.In addition, gallic acid is compounded with GINKGO BILOBA EXTRACT, ratio is suitable for showing good antibacterial effect.
Compared with prior art, the invention has the following advantages:
(1) lily feet flower essential oil preparation method provided by the invention is easy, mild, through supercritical CO2One step of extraction is made,
Chemical reagent is not added in extraction process, safety and environmental protection, obtained trollflower extraction of essential oil rate is high, and property is stablized, and quality is good.
(2) handmade soap of the flower essential oil provided by the invention containing lily feet is safe and non-stimulating, sodium carboxymethyl starch, glycerol and lily feet
Flower essential oil synergistic effect, has good performance of keeping humidity, hence it is evident that improves the drying property of skin, gallic acid and GINKGO BILOBA EXTRACT association
Same synergy, and interact with other ingredients, it can be obviously improved the gloss of skin, achieve the effect that smoothing wrinkle and anti-aging,
Also there is good antibiotic property simultaneously.
Specific embodiment
It is as described below, it is merely preferred embodiments of the present invention, but scope of protection of the present invention is not limited thereto,
Anyone skilled in the art in the technical scope disclosed by the present invention, according to the technique and scheme of the present invention and its
Inventive concept is subject to equivalent substitution or change, should be covered by the protection scope of the present invention.
Gallic acid CAS 149-91-7 of the present invention, GINKGO BILOBA EXTRACT CAS 481-46-9, other raw materials are conventional city
Sell product.
The preparation method of embodiment 1, lily feet flower essential oil of the present invention
The preparation method of 1 lily feet flower essential oil of the embodiment of the present invention, comprising the following steps:
S1, the fresh trollflower of picking is placed in baking oven, the dry 4h at 50 DEG C, and is crushed to 20 mesh, lily feet is made
Pollen；
S2, lily feet pollen obtained in step S1 is fitted into extraction column, is compacted, installs；
S3, cooling tower and cold are first opened, opens CO afterwards2Overcritical equipment, 50 DEG C of extraction kettle water tank temperature of setting, two
60 DEG C of water tank temperature of extraction-container of grade, 30 DEG C of three-level extraction-container water tank temperature open each valve step by step and get through gas and recycle and carry out
Air-discharging；
S4, CO is opened2Force (forcing) pump, the frequency for adjusting force (forcing) pump is 18hz；
S5, extraction kettle dump valve is adjusted, keeping pressure in extraction kettle is 25MPa, adjusts second level extraction-container dump valve, keeps
Pressure is 6MPa in kettle, adjusts three-level extraction-container dump valve, and keeping pressure in kettle is 3MPa, extracts 2.5h；
S6, CO is closed2Force (forcing) pump collects lily feet flower essential oil from second level extraction-container product dump valve, is heated to 48 DEG C, is added
The boiling water of oily weight 3%, quickly stirs 10min, is warming up to 78 DEG C, stops stirring, and heat preservation stands 5h, takes supernatant through 12000r/
Min high speed centrifugation 15min, takes supernatant to get lily feet flower essential oil.
The recovery rate of prepared lily feet flower essential oil is 2%.
The preparation method of embodiment 2, lily feet flower essential oil of the present invention
The preparation method of 2 lily feet flower essential oil of the embodiment of the present invention, comprising the following steps:
S1, the fresh trollflower of picking is placed in baking oven, the dry 4h at 50 DEG C, and is crushed to 30 mesh, lily feet is made
Pollen；
S2, lily feet pollen obtained in step S1 is fitted into extraction column, is compacted, installs；
S3, cooling tower and cold are first opened, opens CO afterwards2Overcritical equipment, 55 DEG C of extraction kettle water tank temperature of setting, two
62 DEG C of water tank temperature of extraction-container of grade, 35 DEG C of three-level extraction-container water tank temperature open each valve step by step and get through gas and recycle and carry out
Air-discharging；
S4, CO is opened2Force (forcing) pump, the frequency for adjusting force (forcing) pump is 20hz；
S5, extraction kettle dump valve is adjusted, keeping pressure in extraction kettle is 28MPa, adjusts second level extraction-container dump valve, keeps
Pressure is 8MPa in kettle, adjusts three-level extraction-container dump valve, and keeping pressure in kettle is 4MPa, extracts 3h；
S6, CO is closed2Force (forcing) pump collects lily feet flower essential oil from second level extraction-container product dump valve, is heated to 50 DEG C, is added
The boiling water of oily weight 4%, quickly stirs 15min, is warming up to 80 DEG C, stops stirring, and heat preservation stands 6h, takes supernatant through 12000r/
Min high speed centrifugation 15min, takes supernatant to get lily feet flower essential oil.
The recovery rate of prepared lily feet flower essential oil is 3%.
The preparation method of embodiment 3, lily feet flower essential oil of the present invention
The preparation method of 3 lily feet flower essential oil of the embodiment of the present invention, comprising the following steps:
S1, the fresh trollflower of picking is placed in baking oven, the dry 4h at 50 DEG C, and is crushed to 40 mesh, lily feet is made
Pollen；
S2, lily feet pollen obtained in step S1 is fitted into extraction column, is compacted, installs；
S3, cooling tower and cold are first opened, opens CO afterwards2Overcritical equipment, 60 DEG C of extraction kettle water tank temperature of setting, two
65 DEG C of water tank temperature of extraction-container of grade, 40 DEG C of three-level extraction-container water tank temperature open each valve step by step and get through gas and recycle and carry out
Air-discharging；
S4, CO is opened2Force (forcing) pump adjusts the frequency of force (forcing) pump as z for 24 hours；
S5, extraction kettle dump valve is adjusted, keeping pressure in extraction kettle is 30MPa, adjusts second level extraction-container dump valve, keeps
Pressure is 10MPa in kettle, adjusts three-level extraction-container dump valve, and keeping pressure in kettle is 5MPa, extracts 3.5h；
S6, CO is closed2Force (forcing) pump collects lily feet flower essential oil from second level extraction-container product dump valve, is heated to 52 DEG C, is added
The boiling water of oily weight 5%, quickly stirs 20min, is warming up to 80 DEG C, stops stirring, and heat preservation stands 8h, takes supernatant through 12000r/
Min high speed centrifugation 15min, takes supernatant to get lily feet flower essential oil.
The recovery rate of prepared lily feet flower essential oil is 2.4%.
Embodiment 4, lily feet flower essential oil handmade soap of the present invention
4 lily feet flower essential oil handmade soap of the embodiment of the present invention, is made of the raw material for preparing of following weight: lily feet flower essential oil 3kg,
Palmitoleic acid sodium 10kg, Sodium myristate 15kg, sodium carboxymethyl starch 20kg, glycerol 4kg, gallic acid 0.4kg, GINKGO BILOBA EXTRACT
1.6kg, essence 0.3kg and deionized water 45.7kg.
The weight ratio of the gallic acid and GINKGO BILOBA EXTRACT is 0.25:1.
The preparation method of the lily feet flower essential oil handmade soap, comprising the following steps:
S1, by palmitoleic acid sodium, Sodium myristate, sodium carboxymethyl starch, glycerol, gallic acid, GINKGO BILOBA EXTRACT, essence and
Deionized water mixes in proportion, and 72 DEG C of heating water baths stir to being completely dissolved, are cooled to 52 DEG C of heat preservations, and mixed liquor A is made；
S2, lily feet flower essential oil is added into the mixed liquor, stirs evenly, mixed liquid B is made；
S3, the mixed liquid B poured into solidify 20h in mold, demoulded after soap lye solidification, be placed in shady and cool ventilation it is dry at
4 days, lily feet flower essential oil handmade soap is made after repairing packaging.
Wherein lily feet flower essential oil is made by 2 preparation method of embodiment.
Embodiment 5, lily feet flower essential oil handmade soap of the present invention
5 lily feet flower essential oil handmade soap of the embodiment of the present invention, is made of the raw material for preparing of following weight: lily feet flower essential oil 4kg,
Palmitoleic acid sodium 8kg, Sodium myristate 12kg, sodium carboxymethyl starch 15kg, glycerol 6kg, gallic acid 1kg, GINKGO BILOBA EXTRACT
3kg, essence 0.7kg and deionized water 50.3kg.
The weight ratio of the gallic acid and GINKGO BILOBA EXTRACT is 0.33:1.
The preparation method of the lily feet flower essential oil handmade soap, comprising the following steps:
S1, by palmitoleic acid sodium, Sodium myristate, sodium carboxymethyl starch, glycerol, gallic acid, GINKGO BILOBA EXTRACT, essence and
Deionized water mixes in proportion, and 72 DEG C of heating water baths stir to being completely dissolved, are cooled to 52 DEG C of heat preservations, and mixed liquor A is made；
S2, lily feet flower essential oil is added into the mixed liquor, stirs evenly, mixed liquid B is made；
S3, the mixed liquid B poured into solidify 20h in mold, demoulded after soap lye solidification, be placed in shady and cool ventilation it is dry at
4 days, lily feet flower essential oil handmade soap is made after repairing packaging.
Wherein lily feet flower essential oil is made by 2 preparation method of embodiment.
Embodiment 6, lily feet flower essential oil handmade soap of the present invention
6 lily feet flower essential oil handmade soap of the embodiment of the present invention, is made of the raw material for preparing of following weight: lily feet flower essential oil 5kg,
Palmitoleic acid sodium 5kg, Sodium myristate 8kg, sodium carboxymethyl starch 12kg, glycerol 8kg, gallic acid 2.2kg, GINKGO BILOBA EXTRACT
3.8kg, essence 1kg and deionized water 55kg.
The weight ratio of the gallic acid and GINKGO BILOBA EXTRACT is 0.58:1.
The preparation method of the lily feet flower essential oil handmade soap, comprising the following steps:
S1, by palmitoleic acid sodium, Sodium myristate, sodium carboxymethyl starch, glycerol, gallic acid, GINKGO BILOBA EXTRACT, essence and
Deionized water mixes in proportion, and 72 DEG C of heating water baths stir to being completely dissolved, are cooled to 52 DEG C of heat preservations, and mixed liquor A is made；
S2, lily feet flower essential oil is added into the mixed liquor, stirs evenly, mixed liquid B is made；
S3, the mixed liquid B poured into solidify 20h in mold, demoulded after soap lye solidification, be placed in shady and cool ventilation it is dry at
4 days, lily feet flower essential oil handmade soap is made after repairing packaging.
Wherein lily feet flower essential oil is made by 2 preparation method of embodiment.
Comparative example 1
Compared with Example 2, the difference of this comparative example is only that: extraction kettle water tank temperature is 65 DEG C in the step S3,
Extracting pressure is 35Mpa.
The recovery rate of prepared lily feet flower essential oil is 1.5%.
Comparative example 2
Compared with Example 5, the difference of this comparative example is only that: replacing lily feet flower essential oil using peony seed oil.
Comparative example 3
Compared with Example 5, the difference of this comparative example is only that: not adding sodium carboxymethyl starch.
Comparative example 4
Compared with Example 5, the difference of this comparative example is only that: the weight ratio of the gallic acid and GINKGO BILOBA EXTRACT is
0.8:1.
Comparative example 5
Compared with Example 5, the difference of this comparative example is only that: not adding gallic acid.
Comparative example 6
Compared with Example 5, the difference of this comparative example is only that: not adding GINKGO BILOBA EXTRACT.
The moistening effect test of test example one, lily feet flower essential oil handmade soap
1, test material: control group (commercially available common handmade soap), lily feet flower essential oil handmade soap, right prepared by embodiment 4~6
Lily feet flower essential oil handmade soap prepared by peony seed oil handmade soap and comparative example 3 prepared by ratio 2.
2, test method: moisture-keeping efficacy evaluation uses external weight method, imitates the biological material such as cuticula, epidermis using adhesive tape
Material, in the peony seed oil handmade soap that adhesive tape uses the lily feet flower essential oil handmade soap of the preparation of embodiment 4~6, comparative example 2 to prepare respectively
It is dried after the lily feet flower essential oil handmade soap cleaning prepared with comparative example 3, the application situation of practical handmade soap is simulated, in constant temperature and humidity
Under conditions of after a certain period of time, weigh sample and place the of poor quality of front and back, find out the loss of sample size, calculate moisturizing ingredient moisturizing
Effect；
3, test result is as shown in table 1 below.
1 moisture-keeping efficacy test result of table
| Project | 0h | 1h | 6h |
| Control group | 33 ± 1.2% | 47 ± 2.1% | 33 ± 1.2% |
| Embodiment 4 | 32 ± 3.6% | 73 ± 3.6% | 65 ± 3.6% |
| Embodiment 5 | 32 ± 2.7% | 77 ± 2.5% | 70 ± 2.7% |
| Embodiment 6 | 33 ± 3.5% | 72 ± 2.2% | 62 ± 3.1% |
| Comparative example 2 | 34 ± 4.2% | 52 ± 3.6% | 38 ± 3.9% |
| Comparative example 3 | 32 ± 1.6% | 58 ± 1.7% | 36 ± 1.1% |
From upper table 1:
(1) control group is poor using the moistening effect of commercially available common handmade soap, substantially without moisture-keeping function after 6h.
(2) compared with the control group, the moistening effect for the lily feet flower essential oil handmade soap that prepared by the embodiment of the present invention 4~6 is significant,
Using after 6h, still there is good moistening effect, be of the invention best wherein best with the moistening effect of embodiment 2
Embodiment；
(3) compared with Example 5, lily feet flower essential oil prepared by the peony seed oil handmade soap and comparative example 3 that prepared by comparative example 2
The moistening effect of handmade soap is decreased obviously after using 6h, illustrates lily feet flower essential oil of the present invention and sodium carboxymethyl starch and glycerol
Synergy, and raw material interaction is prepared with other, there is good moistening effect.
The anti-aging effect test of test example two, lily feet flower essential oil handmade soap
1, test material: lily feet flower essential oil handmade soap, right prepared by control group (commercially available common handmade soap), embodiment 4~6
Lily feet flower essential oil handmade soap prepared by peony seed oil handmade soap and comparative example 3~6 prepared by ratio 2；
2, tested crowd: 90 women, the age 28~38 years old, a crease in the skin, drying, obscure, no skin disease allergies, by
Examination person's aspiration is selected；
3, test method: selection hand is recipient site, does not smear any external drug and cosmetics during test, early
It is late to be used continuously three weeks respectively using primary, with it is excellent, good, in, difference evaluate anti-aging performance；
4, test result: as shown in table 2 below.
2 anti-aging test result of table
| Project | Anti-wrinkle | Bright color |
| Control group | Difference | Difference |
| Embodiment 4 | It is good | It is excellent |
| Embodiment 5 | It is excellent | It is excellent |
| Embodiment 6 | It is excellent | It is good |
| Comparative example 2 | Difference | Difference |
| Comparative example 3 | In | In |
| Comparative example 4 | Difference | In |
| Comparative example 5 | Difference | Difference |
| Comparative example 6 | Difference | Difference |
From upper table 2:
(1) control group is poor using the anti-aging effect of commercially available common handmade soap, a crease in the skin after user's use
It is poor with colour of skin improvement；
(2) compared with the control group, the anti-aging for the lily feet flower essential oil handmade soap that prepared by the embodiment of the present invention 4~6 is obvious,
A crease in the skin and the colour of skin after user's use are obviously improved；Compared with Example 5, peony seed oil hand prepared by comparative example 2
After user's use, a crease in the skin and the colour of skin delay senescence and imitate lily feet flower essential oil handmade soap prepared by work soap and comparative example 3
Fruit is unobvious；Comparative example 4~6 change respectively gallic acid and GINKGO BILOBA EXTRACT ratio, be used alone GINKGO BILOBA EXTRACT and individually
Using gallic acid, after user's use, a crease in the skin and the colour of skin delay senescence and imitate the lily feet flower essential oil handmade soap of preparation
Fruit is unobvious, illustrates that gallic acid and GINKGO BILOBA EXTRACT ratio of the present invention is reasonable, synergistic with lily feet flower essential oil, and and other
Raw material interaction is prepared, has the effect of delaying senescence well.
The anti-microbial property test of test example three, lily feet flower essential oil handmade soap
According to QB/T 2738 " the anti-fungistatic effect evaluation method of daily chemical products " suspension quantitative method to lily feet flower essential oil handmade soap
Carry out anti-microbial property test, wherein test concentrations 1:100, action time 20min, test strain are Staphylococcus aureus
Bacterium ATCC6538, Escherichia coli 8099 and Candida albicans 98001, as a result see the table below 3.
3 lily feet flower essential oil handmade soap anti-microbial property test result of table
| Group | Staphylococcus aureus inhibiting rate (%) | Escherichia coli inhibiting rate (%) | Candida albicans inhibiting rate (%) |
| Embodiment 4 | 94.72 | 95.52 | 93.04 |
| Embodiment 5 | 97.21 | 98.21 | 95.52 |
| Embodiment 6 | 93.89 | 94.74 | 93.64 |
| Comparative example 4 | 85.42 | 82.65 | 81.78 |
| Comparative example 5 | 48.41 | 45.16 | 50.26 |
| Comparative example 6 | 62.78 | 64.98 | 65.21 |
The result shows that lily feet flower essential oil handmade soap prepared by the embodiment of the present invention 4~6 is to staphylococcus aureus, large intestine
The bacteriostasis rate of bacillus and Candida albicans reaches 90% or more, and fungistatic effect is preferable, and trollflower made from comparative example 4~6
Essential oil handmade soap changes the ratio of gallic acid and GINKGO BILOBA EXTRACT respectively, GINKGO BILOBA EXTRACT is used alone and is used alone and does not eat
Sub- acid, fungistatic effect obviously weaken, and illustrate gallic acid and GINKGO BILOBA EXTRACT synergistic effect of the present invention, and compound proportion is suitable for table
Good antibacterial effect is revealed.
The above-described embodiments merely illustrate the principles and effects of the present invention, and is not intended to limit the present invention.It is any ripe
The personage for knowing this technology all without departing from the spirit and scope of the present invention, carries out modifications and changes to above-described embodiment.Cause
This, institute is complete without departing from the spirit and technical ideas disclosed in the present invention by those of ordinary skill in the art such as
At all equivalent modifications or change, should be covered by the claims of the present invention.
Claims (8)
1. a kind of preparation method of lily feet flower essential oil, which comprises the following steps:
S1, the fresh trollflower of picking is placed in baking oven, the dry 4h at 50 DEG C, and is crushed to 10~40 mesh, lily feet is made
Pollen；
S2, lily feet pollen obtained in step S1 is fitted into extraction column, is compacted, installs；
S3, cooling tower and cold are first opened, opens CO afterwards2Overcritical equipment, 50~60 DEG C of extraction kettle water tank temperature of setting, two
60~65 DEG C of water tank temperature of extraction-container of grade, 30~40 DEG C of three-level extraction-container water tank temperature open each valve step by step and get through gas and follow
Ring simultaneously carries out air-discharging；
S4, CO is opened2Force (forcing) pump, the frequency for adjusting force (forcing) pump is 18~z for 24 hours；
S5, extraction kettle dump valve is adjusted, keeping pressure in extraction kettle is 25~30MPa, adjusts second level extraction-container dump valve, keeps
In kettle pressure be 6~10MPa, adjust three-level extraction-container dump valve, keep kettle in pressure be 5MPa or hereinafter, extraction 2.5h~
3h；
S6, CO is closed2Force (forcing) pump collects lily feet flower essential oil from second level extraction-container product dump valve, is heated to 48 DEG C~52 DEG C, adds
Entering the boiling water of oily weight 3~5%, quickly stir 10~20min, be warming up to 78 DEG C~80 DEG C, stops stirring, heat preservation stands 5~8h,
It takes supernatant through 12000r/min high speed centrifugation 15min, takes supernatant to get lily feet flower essential oil.
2. the preparation method of lily feet flower essential oil as described in claim 1, which comprises the following steps:
S1, the fresh trollflower of picking is placed in baking oven, the dry 4h at 50 DEG C, and is crushed to 30 mesh, lily feet pollen is made；
S2, lily feet pollen obtained in step S1 is fitted into extraction column, is compacted, installs；
S3, cooling tower and cold are first opened, opens CO afterwards2Overcritical equipment is arranged 55 DEG C of extraction kettle water tank temperature, second level solution
62 DEG C of kettle water tank temperature of analysis, 35 DEG C of three-level extraction-container water tank temperature open each valve step by step and get through gas and recycle and emptied
Gas；
S4, CO is opened2Force (forcing) pump, the frequency for adjusting force (forcing) pump is 20hz；
S5, extraction kettle dump valve is adjusted, keeping pressure in extraction kettle is 28MPa, adjusts second level extraction-container dump valve, keeps in kettle
Pressure is 8MPa, adjusts three-level extraction-container dump valve, and keeping pressure in kettle is 4MPa, extracts 3h；
S6, CO is closed2Force (forcing) pump collects lily feet flower essential oil from second level extraction-container product dump valve, is heated to 50 DEG C, and oil weight is added
4% boiling water, quickly stirs 15min, is warming up to 80 DEG C, stops stirring, and heat preservation stands 7h, takes supernatant through 12000r/min high
Speed centrifugation 15min, takes supernatant to get lily feet flower essential oil.
3. lily feet flower essential oil prepared by the preparation method of lily feet flower essential oil as claimed in claim 1 or 2.
4. a kind of lily feet flower essential oil handmade soap, which is characterized in that the raw material for preparing including following parts by weight: claim 3 institute
3~5 parts of the lily feet flower essential oil stated, 5~10 parts of palmitoleic acid sodium, 8~15 parts of Sodium myristate, sodium carboxymethyl starch 10~20
Part, 4~8 parts of glycerol, 2~6 parts of antioxidant, 0.3~1 part of essence and 45~55 parts of deionized water.
5. lily feet flower essential oil handmade soap as claimed in claim 4, which is characterized in that prepare raw material including following parts by weight:
It is 4 parts of lily feet flower essential oil as claimed in claim 3,8 parts of palmitoleic acid sodium, 12 parts of Sodium myristate, 15 parts of sodium carboxymethyl starch, sweet
6 parts of oil, 4 parts of antioxidant, 0.7 part of essence and 50.3 parts of deionized water.
6. lily feet flower essential oil handmade soap as claimed in claim 4, which is characterized in that the antioxidant is gallic acid and ginkgo
The weight ratio of the composition of flavones, the gallic acid and GINKGO BILOBA EXTRACT is (0.2~0.6): 1.
7. lily feet flower essential oil handmade soap as claimed in claim 6, which is characterized in that the weight of the gallic acid and GINKGO BILOBA EXTRACT
Than for 0.4:1.
8. the preparation method of lily feet flower essential oil handmade soap as claimed in claim 4, which comprises the following steps:
S1, by palmitoleic acid sodium, Sodium myristate, sodium carboxymethyl starch, glycerol, antioxidant, essence and deionized water by matching
Side's amount mixing, 70~75 DEG C of heating water baths stir to being completely dissolved, are cooled to 50~55 DEG C of heat preservations, and mixed liquor A is made；
S2, lily feet flower essential oil is added into the mixed liquor A, stirs evenly, mixed liquid B is made；
S3, the mixed liquid B is poured into mold to solidification 12~for 24 hours, is demoulded after soap lye solidification, be placed in shady and cool ventilation it is dry at
3~5 days, lily feet flower essential oil handmade soap is made after repairing packaging.
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