CN109336712A - A kind of humic acid bio-fertilizer material and preparation method thereof - Google Patents
A kind of humic acid bio-fertilizer material and preparation method thereof Download PDFInfo
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- CN109336712A CN109336712A CN201811198040.6A CN201811198040A CN109336712A CN 109336712 A CN109336712 A CN 109336712A CN 201811198040 A CN201811198040 A CN 201811198040A CN 109336712 A CN109336712 A CN 109336712A
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- humic acid
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- vinegar grain
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- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
- C05G3/00—Mixtures of one or more fertilisers with additives not having a specially fertilising activity
- C05G3/80—Soil conditioners
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- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05D—INORGANIC FERTILISERS NOT COVERED BY SUBCLASSES C05B, C05C; FERTILISERS PRODUCING CARBON DIOXIDE
- C05D1/00—Fertilisers containing potassium
- C05D1/04—Fertilisers containing potassium from minerals or volcanic rocks
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- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05F—ORGANIC FERTILISERS NOT COVERED BY SUBCLASSES C05B, C05C, e.g. FERTILISERS FROM WASTE OR REFUSE
- C05F17/00—Preparation of fertilisers characterised by biological or biochemical treatment steps, e.g. composting or fermentation
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02W—CLIMATE CHANGE MITIGATION TECHNOLOGIES RELATED TO WASTEWATER TREATMENT OR WASTE MANAGEMENT
- Y02W30/00—Technologies for solid waste management
- Y02W30/40—Bio-organic fraction processing; Production of fertilisers from the organic fraction of waste or refuse
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- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Biotechnology (AREA)
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- Engineering & Computer Science (AREA)
- Biochemistry (AREA)
- Pest Control & Pesticides (AREA)
- Soil Sciences (AREA)
- General Chemical & Material Sciences (AREA)
- Health & Medical Sciences (AREA)
- Molecular Biology (AREA)
- Environmental & Geological Engineering (AREA)
- General Life Sciences & Earth Sciences (AREA)
- Geochemistry & Mineralogy (AREA)
- Geology (AREA)
- Inorganic Chemistry (AREA)
- Fertilizers (AREA)
Abstract
The invention discloses a kind of humic acid bio-fertilizer material and preparation method thereof, are related to technical field of fertilizer production；Raw material including following parts by weight: 10-15 parts of dregs of beans；10-20 parts of potassium feldspar；10-15 parts of vinegar grain；20-25 parts of humic acid；0.1-0.2 parts of magnesium sulfate；0.1-0.2 parts of zinc chloride；0.1-0.2 parts of ferric trichloride；Bacillus subtilis, existing fermentation are added after dregs of beans and vinegar grain are mixed, then magnesium sulfate, zinc chloride, ferric trichloride addition are continued to ferment, potassium feldspar is mixed with water again with humic acid addition, at the uniform velocity stirs to get the humic acid fertilizer；One aspect of the present invention solves pollution of the by-products such as the vinegar grain of generation to environment, reduce fertilizer cost, on the other hand, make full use of the effect of humic acid, it is formed and is rich in microelement, minerals and phosphorous high bio-fertilizer, the bio-fertilizer is more conducive to being absorbed and utilized for plant, and fertility is stronger.
Description
Technical field
The present invention relates to technical field of fertilizer production, and in particular to a kind of humic acid bio-fertilizer for being conducive to plant absorption
Material and preparation method thereof.
Background technique
Humic acid is a kind of natural organic monoacid, is made of fulvic acid, humic acid and ulmic acid three parts, essential element has
Carbon, hydrogen, oxygen, there are also a small amount of nitrogen and sulphur, and in addition also there are many functional groups.Root application and spraying can promote plant growth, improve agriculture
Crop yield；Root application also has the effects that improve soil texture, improvement and the absorption for optimizing Plant To Nutrient and moisture.
Meanwhile crops are during the growth process, need microelement.So once lack microelement, crops are just not
It healthy can normally grow, so needing to add certain microelement in fertilizer.The microelement applied at present is mostly with divalent
Metal ion exists, into after soil, be easy and soil in generally existing a large amount of negative divalent carbonate and negative trivalent
Phosphate radical reaction generates carbonate and phosphate not soluble in water, is not easy to be absorbed by plants.So generally can will be micro in fertilizer
Element generation chelate increases the stability of microelement, avoids generating carbonate and phosphate not soluble in water, so that micro
The fertilization effect of element greatly improves.
Humic acid can improve soil, promote the formation of soil agreegate, improve the function of soil exchange capacity.Humic acid pair
Nitrogenous fertilizer, phosphate fertilizer, potash fertilizer all have apparent synergistic effect.With various trace elements chelatropic reaction can occur for humic acid, generate
Solubility is good, the microelement chelate being easy in the humic acid absorbed by crops, is conducive to crop root part or blade face is inhaled
It receives.Humic acid can also make seed germinate ahead of time, emergence rate is high, develop the roots of the crops, the life of above-ground plant parts trophosome
Length is vigorous, and cereal crops yield is more.Humic acid is also to crops drought resisting, cold-resistant, disease and insect resistance and immunity, and there are also agricultural product
Quality is all significantly improved.
But the humic acid trace element fertilizer of these prior art preparations is in the prevalence of soil phosphorus decomposing, the activation energy of solution silicon
Power is low；Humic acid activity is low, and resistance to hard water is insufficient；Microelement be easy antagonism, so microelement kind and additive amount
It is few, the low problem of utilization rate.
Summary of the invention
The present invention overcomes the shortcomings of the prior art, provides one kind rich in nutrient and microelement, and be easier to be planted
The humic acid fertilizer that object absorbs, the present invention is achieved through the following technical solutions.
A kind of humic acid bio-fertilizer material, the raw material including following parts by weight: 10-15 parts of dregs of beans；10-20 parts of potassium feldspar；Vinegar
It is 10-15 parts poor；20-25 parts of humic acid；0.1-0.2 parts of magnesium sulfate；0.1-0.2 parts of zinc chloride；0.1-0.2 parts of ferric trichloride.
It preferably, further include 5-10 parts of rice bran.
A kind of preparation method of humic acid bio-fertilizer material, comprising the following steps:
1) bacillus subtilis is added after mixing dregs of beans and vinegar grain, fermentation obtains tunning A in 30-60 days；
2) magnesium sulfate, zinc chloride, ferric trichloride are prepared into solution to be added in A, continue fermentation 7-14 days, obtains tunning
B；
3) it is added to after being mixed after potassium feldspar being ground into powder with humic acid in tunning B, is uniformly mixing to obtain C, pressed
C is mixed according to weight ratio 1:1-2, at the uniform velocity stirring 1-3h with water, obtains the humic acid fertilizer.
Preferably, the fermentation temperature is 30-40 DEG C.
Preferably, potassium feldspar is ground to 100-200 mesh.
Preferably, the vinegar grain water content is 65%-70%.
Bacillus subtilis is conventional commercially available strain.
Phytic acid, that is, phytic acid is widely present in plant as the repository of phosphoric acid.Since minerals are incorporated in egg
In white-phytic acid-mineral element compound, therefore just reduce certain plants property food and some vegetable protein isolate Minerals
The nutrition balance of matter.Phytase (phytases) can hydrolyze phosphate moiety from phytic acid, therefore destroy phytic acid to mine
The strong affinity of matter-element element, thus phytase can increase the nutrition balance of mineral element.
Vinegar grain is the by-product during vinegar processed.The raw material of vinegar processed mainly has wheat bran, sorghum and cracks rice on a small quantity, fermented wine
It makes, extracts vinegar, remaining by-product is vinegar grain, vinegar grain 9.6%-20.4% containing thick protein, crude fibre 15.1%-28%, containing abundant
Trace elements iron, zinc, selenium, manganese etc., fermented using bacillus subtilis to vinegar grain and dregs of beans, contained in tunning
A large amount of phytase.The present invention is using the phytase generated in fermentation process to including cavings, the rice husk, rice in dregs of beans, vinegar grain
The phytic acid in plant material including chaff is decomposed, and phosphoric acid is formed, when subsequent addition magnesium sulfate, zinc chloride, ferric trichloride etc.
After raw mineral materials, corresponding phosphate is formed, phosphate further by carrying out chelating with the humic acid of addition, is formd and is easier to
The nutritional ingredient being absorbed and utilized by plant, meanwhile, P elements become the inorganic form for being easier to be absorbed and used, and improve fertilizer
Fertility and release effect.
The present invention is generated compared with the existing technology to be had the beneficial effect that.
The present invention is using bacillus subtilis by Vinegar Fermentation product --- vinegar grain carries out fermentation and generates degradable plant original
The phytase for expecting ingredient phytic acid further decomposes organic phosphorus in raw material, formation phosphoric acid, phosphoric acid and mine by the effect of phytase
The phosphate and humic acid that substance is formed form chelating body, to obtain humic acid bio-fertilizer material；One aspect of the present invention solves
Pollution of the by-products such as the vinegar grain of generation to environment, reduces fertilizer cost, on the other hand, makes full use of the effect of humic acid,
It is formed and is more conducive to being absorbed and utilized for plant rich in microelement, minerals and phosphorous high bio-fertilizer, the bio-fertilizer,
Fertility is stronger.
Specific embodiment
In order to which technical problems, technical solutions and advantages to be solved are more clearly understood, in conjunction with reality
Example is applied, the present invention will be described in further detail.It should be appreciated that specific embodiment described herein is only used to explain this
Invention, is not intended to limit the present invention.Below with reference to the embodiment technical solution that the present invention will be described in detail, but protection scope not by
This limitation.
Embodiment 1
A kind of humic acid bio-fertilizer material, including following raw material: dregs of beans 10kg, potassium feldspar 15kg, vinegar grain 15kg, humic acid 25kg,
Magnesium sulfate 0.1kg, zinc chloride 0.1kg, ferric trichloride 0.1kg, rice bran 5kg, wherein the water content of vinegar grain is 65%.
A kind of preparation method of humic acid bio-fertilizer material, comprising the following steps:
1) raw material for weighing above-mentioned weight is added bacillus subtilis after mixing dregs of beans and vinegar grain, ferments at 35 DEG C 50 days
To tunning A；Bacillus subtilis
2) mixed aqueous solution that magnesium sulfate, zinc chloride, ferric trichloride are prepared into weight ratio 30% is added in A, continues fermentation 14
It, obtains tunning B；
3) potassium feldspar is ground into after being mixed after 200 mesh powder shapes with humic acid and is added in tunning B, stirred evenly
To C, C is mixed according to weight ratio 1:1, at the uniform velocity stirring 3h with water, obtains the humic acid fertilizer.
Embodiment 2
A kind of humic acid bio-fertilizer material, including following raw material: dregs of beans 15kg, potassium feldspar 20kg, vinegar grain 10kg, humic acid 20kg,
Magnesium sulfate 0.2kg, zinc chloride 0.2kg, ferric trichloride 0.2kg, rice bran 10kg, wherein the water content of vinegar grain is 68%.
A kind of preparation method of humic acid bio-fertilizer material, comprising the following steps:
1) raw material for weighing above-mentioned weight is added bacillus subtilis after mixing dregs of beans and vinegar grain, ferments at 37 DEG C 60 days
To tunning A；
2) mixed aqueous solution that magnesium sulfate, zinc chloride, ferric trichloride are prepared into weight ratio 25% is added in A, continues fermentation 10
It, obtains tunning B；
3) potassium feldspar is ground into after being mixed after 100 mesh powder shapes with humic acid and is added in tunning B, stirred evenly
To C, C is mixed according to weight ratio 1:2, at the uniform velocity stirring 2h with water, obtains the humic acid fertilizer.
Embodiment 3
A kind of humic acid bio-fertilizer material, including following raw material: dregs of beans 12kg, potassium feldspar 10kg, vinegar grain 12kg, humic acid 22kg,
Magnesium sulfate 0.15kg, zinc chloride 0.2kg, ferric trichloride 0.1kg, rice bran 7kg, wherein the water content of vinegar grain is 70%.
A kind of preparation method of humic acid bio-fertilizer material, comprising the following steps:
1) raw material for weighing above-mentioned weight is added bacillus subtilis after mixing dregs of beans and vinegar grain, ferments at 40 DEG C 30 days
To tunning A；
2) mixed aqueous solution that magnesium sulfate, zinc chloride, ferric trichloride are prepared into weight ratio 20% is added in A, continues fermentation 7
It, obtains tunning B；
3) potassium feldspar is ground into after being mixed after 200 mesh powder shapes with humic acid and is added in tunning B, stirred evenly
To C, C is mixed according to weight ratio 1:1.5, at the uniform velocity stirring 1h with water, obtains the humic acid fertilizer.
Bacillus subtilis described in above-described embodiment is purchased in Xingtai Si Beite Biotechnology Co., Ltd, gemma number
>=500 hundred million/gram.
The above content is combine specific preferred embodiment to the further description done of the present invention, and it cannot be said that
A specific embodiment of the invention is only limitted to this, for those of ordinary skill in the art to which the present invention belongs, is not taking off
Under the premise of from the present invention, several simple deduction or replace can also be made, all shall be regarded as belonging to the present invention by being submitted
Claims determine scope of patent protection.
Claims (6)
1. a kind of humic acid bio-fertilizer material, which is characterized in that the raw material including following parts by weight: 10-15 parts of dregs of beans；Potassium feldspar
10-20 parts；10-15 parts of vinegar grain；20-25 parts of humic acid；0.1-0.2 parts of magnesium sulfate；0.1-0.2 parts of zinc chloride；Ferric trichloride
0.1-0.2 parts.
2. a kind of humic acid bio-fertilizer material according to claim 1, which is characterized in that further include 5-10 parts of rice bran.
3. a kind of preparation method of humic acid bio-fertilizer material as described in claim 1, which comprises the following steps:
1) bacillus subtilis is added after mixing dregs of beans and vinegar grain, fermentation obtains tunning A in 30-60 days；
2) magnesium sulfate, zinc chloride, ferric trichloride are prepared into solution to be added in A, continue fermentation 7-14 days, obtains tunning
B；
3) it is added to after being mixed after potassium feldspar being ground into powder with humic acid in tunning B, is uniformly mixing to obtain C, pressed
C is mixed according to weight ratio 1:1-2, at the uniform velocity stirring 1-3h with water, obtains the humic acid fertilizer.
4. a kind of preparation method of humic acid bio-fertilizer material according to claim 3, which is characterized in that the fermentation temperature
Degree is 30-40 DEG C.
5. a kind of preparation method of humic acid bio-fertilizer material according to claim 3, which is characterized in that grind potassium feldspar
To 100-200 mesh.
6. a kind of preparation method of humic acid bio-fertilizer material according to claim 3, which is characterized in that the vinegar grain contains
Water is 65%-70%.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201811198040.6A CN109336712A (en) | 2018-10-15 | 2018-10-15 | A kind of humic acid bio-fertilizer material and preparation method thereof |
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| CN201811198040.6A CN109336712A (en) | 2018-10-15 | 2018-10-15 | A kind of humic acid bio-fertilizer material and preparation method thereof |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN116784231A (en) * | 2023-08-02 | 2023-09-22 | 河北农业大学 | Seedling raising method capable of rapidly screening stress-resistant varieties of crops |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN116784231A (en) * | 2023-08-02 | 2023-09-22 | 河北农业大学 | Seedling raising method capable of rapidly screening stress-resistant varieties of crops |
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