CN109331536A - Cementing slurry is thickened experiment useless conduction oil recovering and purifying system - Google Patents

Cementing slurry is thickened experiment useless conduction oil recovering and purifying system Download PDF

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Publication number
CN109331536A
CN109331536A CN201811340256.1A CN201811340256A CN109331536A CN 109331536 A CN109331536 A CN 109331536A CN 201811340256 A CN201811340256 A CN 201811340256A CN 109331536 A CN109331536 A CN 109331536A
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CN
China
Prior art keywords
grease
oil
conduction oil
coarse separator
thickened
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201811340256.1A
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Chinese (zh)
Inventor
王良才
姚勇
何雨轩
黄琛
蒋卓颖
刘强
罗鸿
杜培伟
罗龙
罗翰
周泉
邓天安
焦建芳
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Sinopec Oilfield Service Corp
Sinopec Southwest Petroleum Engineering Co Ltd Cementing Branch
Original Assignee
Sinopec Oilfield Service Corp
Sinopec Southwest Petroleum Engineering Co Ltd Cementing Branch
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Sinopec Oilfield Service Corp, Sinopec Southwest Petroleum Engineering Co Ltd Cementing Branch filed Critical Sinopec Oilfield Service Corp
Priority to CN201811340256.1A priority Critical patent/CN109331536A/en
Publication of CN109331536A publication Critical patent/CN109331536A/en
Pending legal-status Critical Current

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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D36/00Filter circuits or combinations of filters with other separating devices
    • B01D36/003Filters in combination with devices for the removal of liquids

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  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Filtration Of Liquid (AREA)

Abstract

The invention discloses a kind of cementing slurries to be thickened experiment useless conduction oil recovering and purifying system, including the trash eliminator for being in upstream and the absolute oil storage bin for being in downstream, being linked in sequence between the trash eliminator and absolute oil storage bin has grease coarse separator and grease fine seperator, the water-oil separating element of the grease coarse separator is ceramic filter web frame, the water-oil separating element of the grease fine seperator is ceramic filter web frame, and the filtering accuracy of grease fine seperator is greater than the filtering accuracy of grease coarse separator.The present invention can either effectively remove the solid impurity in useless conduction oil, the moisture impurity in useless conduction oil can be effectively removed again, so that the purity is high of purification conduction oil obtained, reliably can directly be reused in the multiviscosity meter of cementing slurry thickening experiment, turn waste into wealth, good economy performance.

Description

Cementing slurry is thickened experiment useless conduction oil recovering and purifying system
Technical field
The present invention relates to waste oil reclaiming clean technology, the useless conduction oil of specifically a kind of cementing slurry thickening experiment is returned Receive purification system.
Background technique
The thickening time of cement slurry is the important parameter that well cementing operation is related to, and is had to well cementing operation important Influence.The measuring of cement slurry thickening time is realized by multiviscosity meter.In the thickening experiment of cement slurry, multiviscosity meter Corresponding heating, thickening processing are carried out to cement slurry come simulated formation temperature, strata pressure by conduction oil, to obtain water Thickening time of the mud under specific formation temperature and strata pressure.
In the thickening experiment of cement slurry, conduction oil is contaminated due to the heating to cement slurry, so that multiviscosity meter can generate Largely contain the oil liquid of various solid impurities and moisture impurity, these oil liquid are cannot to be directly used as multiviscosity meter again to cement slurry Heating, thickening, it will usually make waste treatment, this certainly will by directly increase cement slurry thickening test experimental cost.
In order to turn waste into wealth, the experimental cost of cement slurry thickening experiment is reduced, attempting in the industry will be containing impurity Discarded conduction oil carries out reclaiming clean, the conduction oil of reclaiming clean is repeated to recycle into multiviscosity meter, such as Chinese patent " a kind of pressurizing multiviscosity meter conduction oil filter device " disclosed in document (publication number CN 207463441, publication date 06 month 2018 08 day), " a kind of thermally conductive oil treatment provisions of Portable high-temperature high-pressure multiviscosity meter " (publication number CN 207463440, publication date 2018 Year 08 day 06 month), " a kind of multiviscosity meter conduction oil reuse means " (publication number CN 207680159, publication date 08 month 2018 03 day) etc..Presently disclosed these carry out the technology of reclaiming clean to cement slurry thickening experiment with useless conduction oil, though it can go Solid impurity in degreasing fluid, but it cannot remove the moisture impurity in degreasing fluid, purify oil liquid obtained because miscellaneous containing moisture Matter and purity is relatively low, still cannot reliably repeat recycle into the multiviscosity meter as precision instrument.If by time that purity is relatively low It receives purification conduction oil to be reused in multiviscosity meter reluctantly, then the accurate operation stability of multiviscosity meter can be impacted, based on thick Change involving great expense for instrument, the operation stability of multiviscosity meter is sacrificed with the conduction oil inferior of reclaiming clean, it is real in economic cost It is losing more than gain.
Summary of the invention
Technical purpose of the invention is: testing for the particularity and existing thickening of the thickening experiment of above-mentioned cementing slurry With the deficiency of useless conduction oil reclaiming clean technology, a kind of solid impurity that can either be effectively removed in useless conduction oil, and energy are provided The moisture impurity in useless conduction oil is enough effectively removed, so that the purity is high, thick in cementing slurry of purification conduction oil obtained Change the useless conduction oil recovering and purifying system that reliably can directly recycle in the multiviscosity meter of experiment.
The present invention realizes that technical solution used by its technical purpose is: a kind of cementing slurry thickening experiment is thermally conductive with giving up Oily recovering and purifying system, the recovering and purifying system include the absolute oil storage for being in the trash eliminator of upstream and being in downstream Case, being linked in sequence between the trash eliminator and absolute oil storage bin has grease coarse separator and grease fine seperator, the oil The water-oil separating element of water coarse separator is ceramic filter web frame, and the water-oil separating element of the grease fine seperator is ceramics Filter screen structure, the filtering accuracy of the grease fine seperator are greater than the filtering accuracy of the grease coarse separator, the thickening Useless conduction oil in the multiviscosity meter of experiment is first after trash eliminator removes granule foreign, then through grease coarse separator and grease After fine seperator removes moisture removal, obtains pure, recycling conduction oil and recycle.
One of preferably, the cabinet of the grease coarse separator is sealing structure, in the grease coarse separator Pressure be 02MPa, be provided with waste water discharge opening in the grease coarse separator.Further, in the grease coarse separator It is connected with pressurizing device.
Waste water discharge opening is provided on the grease fine seperator.
One of preferably, impurity crude separating layer and impurity are equipped with by upstream and downstream sequence in the trash eliminator Smart separating layer, the impurity crude separating layer are 80 mesh filter screen structures, and the impurity essence separating layer is 200 mesh filter screen structures, described The filtering accuracy of impurity essence separating layer is greater than the filtering accuracy of the impurity crude separating layer.
One of preferably, the cabinet of the trash eliminator is the uncovered structure of top end opening, the impurity point Cabinet top from device is used as injection useless conduction oil.
One of preferably, the fuel-displaced port of the trash eliminator passes through the first petroleum pipeline and grease coarse separator Oil inlet port connection.
One of preferably, the fuel-displaced port of the grease coarse separator is separated by the second petroleum pipeline with grease essence The oil inlet port of device connects.
One of preferably, the fuel-displaced port of the grease fine seperator passes through third petroleum pipeline and absolute oil storage bin Oil inlet port connection.
The method have the benefit that:
1. the present invention is for the particularity of cementing slurry thickening experiment, with the characteristic of liquid flowing in the sequence of upstream and downstream In be provided with corresponding trash eliminator and oil water separator, so that the solid impurity in useless conduction oil can either be effectively removed, The moisture impurity in useless conduction oil can be effectively removed again, so that the purity is high of purification conduction oil obtained, it can be reliably It is directly reused in the multiviscosity meter of cementing slurry thickening experiment, will not influence the stability of multiviscosity meter operation, turn waste into wealth, The experimental cost of cement slurry thickening experiment, good economy performance is greatly reduced;
2. grease coarse separator of the invention is while ensuring filtering, disintegrate-quality, filter efficiency with higher.
Detailed description of the invention
Fig. 1 is a kind of structural schematic diagram of the invention.
Code name meaning in figure: 1-trash eliminator;11-impurity crude separating layers;12-impurity essence separating layers;2-greases Coarse separator;3-grease fine seperators;4-absolute oil storage bins;5-the first petroleum pipeline;6-the second petroleum pipeline;7-thirds are defeated Oil pipe.
Specific embodiment
The present invention relates to waste oil reclaiming clean technology, the useless conduction oil of specifically a kind of cementing slurry thickening experiment is returned Purification system is received, agent technology content of the invention is described in detail with multiple embodiments below.Wherein, 1 knot of embodiment It closes Figure of description-i.e. Fig. 1 and detailed, specific description is carried out to the contents of the present invention, other embodiments do not draw attached drawing individually, But its main structure still can refer to the attached drawing of embodiment 1.Herein it should be strongly noted that attached drawing of the invention is schematic , in order to which technical purpose clearly of the invention has been simplified for unnecessary details, contributed to avoid the present invention has been obscured The technical solution of the prior art.
Embodiment 1
Shown in Figure 1, the present invention includes the trash eliminator 1 being sequentially connected with by upstream and downstream, grease coarse separator 2, oil Crystal's separator 3 and absolute oil storage bin 4.
Wherein, the cabinet of trash eliminator 1 is the uncovered structure of top end opening, and the cabinet top of trash eliminator 1 is used as Inject useless conduction oil.Impurity crude separating layer 11 and impurity essence separating layer are equipped with by upstream and downstream sequence in foregoing impurities separator 1 12, impurity crude separating layer 11 is 80 mesh filter screen structures, and impurity essence separating layer 12 is 200 mesh filter screen structures, impurity crude separating layer 11 It is transversely arranged in the cabinet of trash eliminator 1 and keeps in the up-down direction spacing distance respectively with impurity essence separating layer 12, The filtering accuracy of impurity essence separating layer 12 is greater than the filtering accuracy of impurity crude separating layer 11.The cabinet bottom of foregoing impurities separator 1 Portion is provided with fuel-displaced port, and the fuel-displaced port of trash eliminator 1 is connect with the upstream end of the first petroleum pipeline 5.
The cabinet of grease coarse separator 2 is sealing structure.The top of the box of grease coarse separator 2 is provided with oil inlet port, The oil inlet port of grease coarse separator 2 is connect with the downstream of the first petroleum pipeline 5;The bottom of box of grease coarse separator 2 is arranged There are waste water discharge opening and fuel-displaced port, is connected with valve on waste water discharge opening, the fuel-displaced port of grease coarse separator 2 and second defeated The upstream end of oil pipe 6 connects.Water-oil separating element is provided in grease coarse separator 2, which is ceramic filter Web frame.It is connected with pressurizing device in aforementioned grease coarse separator 2, which is used as control grease crude separation Pressure in device 2, the pressure in grease coarse separator 2 remain 0.2MPa.
The top of the box of grease fine seperator 3 is provided with oil inlet port, the oil inlet port of grease fine seperator 3 and second defeated The downstream of oil pipe 6 connects;The bottom of box of grease fine seperator 3 is provided with waste water discharge opening and fuel-displaced port, waste water discharge It is connected with valve on mouthful, the fuel-displaced port of grease fine seperator 3 is connect with the upstream end of third petroleum pipeline 7.Grease fine seperator 3 It is inside provided with water-oil separating element, which is ceramic filter web frame.The filtering essence of aforementioned grease fine seperator 3 Degree is greater than the filtering accuracy of above-mentioned grease coarse separator 2.
Absolute oil storage bin 4 is used as the high-purity that storage is separated with moisture through impurity separation and obtained and purifies oil.Absolute oil storage The top of the box of case 4 is provided with oil inlet port, and the oil inlet port of absolute oil storage bin 4 is connect with the downstream of third petroleum pipeline 7;Only The bottom of box of oily storage bin 4 is provided with fuel-displaced port, is connected with valve on the fuel-displaced port.
The course of work of the invention is:
It is introduced in trash eliminator 1 from the useless conduction oil being discharged in multiviscosity meter;Oil liquid is separated by filtration through impurity crude separating layer 11, Large granular impurity contained in oil liquid is obstructed, little particle impurity and moisture is allowed to flow through and enter impurity essence separating layer 12;Oil Liquid is separated by filtration through impurity essence separating layer 12, and little particle impurity contained in oil liquid is obstructed, moisture is allowed to flow through;
The oil liquid containing moisture is introduced in grease coarse separator 2 out of trash eliminator 1 through the first petroleum pipeline 5;Oil liquid is through oil The water-oil separating element of water coarse separator 2 isolates most of moisture barrier, and small part moisture is allowed to flow through;
It will be introduced in grease fine seperator 3 containing the oil liquid of small part moisture out of grease coarse separator 2 through the second petroleum pipeline 6; Oil liquid isolates all moisture barriers through the water-oil separating element of grease fine seperator 3;
High-purity oil liquid obtained will be purified out of grease fine seperator 3 through third petroleum pipeline 7 to introduce in absolute oil storage bin 4; So far, the useless conduction oil in the multiviscosity meter of experiment is thickened first after the removal granule foreign of trash eliminator 1, then through grease rough segmentation After removing moisture removal from device 2 and grease fine seperator 3, obtains pure, recycling conduction oil and recycle.
Embodiment 2
The present invention includes the trash eliminator being sequentially connected with by upstream and downstream, grease coarse separator, grease fine seperator and net Oily storage bin.
Wherein, the cabinet of trash eliminator is the uncovered structure of top end opening, and the cabinet top of trash eliminator is used as note Enter useless conduction oil.It is equipped with impurity crude separating layer and impurity essence separating layer by upstream and downstream sequence in foregoing impurities separator, impurity Rough segmentation absciss layer is 80 mesh filter screen structures, and impurity essence separating layer is 200 mesh filter screen structures, impurity crude separating layer and impurity essence separating layer It is transversely arranged in the cabinet of trash eliminator respectively and keeps spacing distance, the mistake of impurity essence separating layer in the up-down direction Filter the filtering accuracy that precision is greater than impurity crude separating layer.The bottom of box of foregoing impurities separator is provided with fuel-displaced port.
The cabinet of grease coarse separator is sealing structure.The top of the box of grease coarse separator is provided with oil inlet port, oil The oil inlet port of water coarse separator is connected directly between on the fuel-displaced port of trash eliminator;The bottom of box of grease coarse separator is set It is equipped with waste water discharge opening and fuel-displaced port, is connected with valve on waste water discharge opening.Water-oil separating is provided in grease coarse separator Element, the water-oil separating element are ceramic filter web frame.It is connected with pressurizing device in aforementioned grease coarse separator, pressurization dress The pressure being used as in control grease coarse separator is set, the pressure in grease coarse separator remains 0.2MPa.
The top of the box of grease fine seperator is provided with oil inlet port, and the oil inlet port of grease fine seperator is connected directly between On the fuel-displaced port of grease coarse separator;The bottom of box of grease fine seperator is provided with waste water discharge opening and fuel-displaced port, gives up Valve is connected on water outlet.Water-oil separating element is provided in grease fine seperator, which is ceramic mistake Filter structure.The filtering accuracy of aforementioned grease fine seperator is greater than the filtering accuracy of above-mentioned grease coarse separator.
Absolute oil storage bin is used as the high-purity that storage is separated with moisture through impurity separation and obtained and purifies oil.Absolute oil storage bin Top of the box be provided with oil inlet port, the oil inlet port of absolute oil storage bin is connected directly between the fuel-displaced of above-mentioned grease fine seperator On port;The bottom of box of absolute oil storage bin is provided with fuel-displaced port, is connected with valve on the fuel-displaced port.
The course of work of the invention is:
It is introduced in trash eliminator from the useless conduction oil being discharged in multiviscosity meter;Oil liquid is separated by filtration through impurity crude separating layer, will be oily The barrier of large granular impurity contained in liquid, allows little particle impurity and moisture to flow through and enter impurity essence separating layer;Oil liquid is through miscellaneous Matter essence separating layer is separated by filtration, and little particle impurity contained in oil liquid is obstructed, moisture is allowed to flow through;
Oil liquid be discharged out of trash eliminator, containing moisture introduces in grease coarse separator;Oil liquid is through grease coarse separator Resolution element by most of moisture barrier isolate, allow small part moisture to flow through;
Oil liquid be discharged out of grease coarse separator, containing small part moisture introduces in grease fine seperator;Oil liquid is through grease The resolution element of fine seperator isolates all moisture barriers;
Be discharged out of grease fine seperator, purification high-purity oil liquid obtained introduces in absolute oil storage bin;So far, it is thickened Useless conduction oil in the multiviscosity meter of experiment is first after trash eliminator removes granule foreign, then through grease coarse separator and grease After fine seperator removes moisture removal, obtains pure, recycling conduction oil and recycle.
The above various embodiments is only to illustrate the present invention, rather than its limitations;Although referring to the various embodiments described above to this hair It is bright to be described in detail, those skilled in the art should understand that: the present invention still can be to the various embodiments described above In specific technical solution modify perhaps equivalent replacement of some of the technical features and these modifications or replace It changes, the spirit and scope of the present invention that it does not separate the essence of the corresponding technical solution.

Claims (9)

1. a kind of cementing slurry is thickened experiment useless conduction oil recovering and purifying system, the recovering and purifying system includes being in The trash eliminator (1) of trip and the absolute oil storage bin (4) for being in downstream, it is characterised in that: the trash eliminator (1) and absolute oil Being linked in sequence between storage bin (4) has grease coarse separator (2) and grease fine seperator (3), the grease coarse separator (2) Water-oil separating element is ceramic filter web frame, and the water-oil separating element of the grease fine seperator (3) is foam ceramic filter knot Structure, the filtering accuracy of the grease fine seperator (3) are greater than the filtering accuracy of the grease coarse separator (2), and the thickening is real The useless conduction oil in multiviscosity meter tested first after trash eliminator (1) removes granule foreign, then through grease coarse separator (2) and After grease fine seperator (3) removes moisture removal, obtains pure, recycling conduction oil and recycle.
2. cementing slurry is thickened experiment useless conduction oil recovering and purifying system according to claim 1, it is characterised in that: institute The cabinet for stating grease coarse separator (2) is sealing structure, and the pressure in the grease coarse separator (2) is 0.2MPa, the oil Water coarse separator is provided with waste water discharge opening on (2).
3. cementing slurry is thickened experiment useless conduction oil recovering and purifying system according to claim 2, it is characterised in that: institute It states and is connected with pressurizing device on grease coarse separator (2).
4. cementing slurry is thickened experiment useless conduction oil recovering and purifying system according to claim 1, it is characterised in that: institute It states and is provided with waste water discharge opening on grease fine seperator (3).
5. cementing slurry is thickened experiment useless conduction oil recovering and purifying system according to claim 1, it is characterised in that: institute It states in trash eliminator (1) and is equipped with impurity crude separating layer (11) and impurity essence separating layer (12) by upstream and downstream sequence, it is described miscellaneous Matter rough segmentation absciss layer (11) is 80 mesh filter screen structures, and the impurity essence separating layer (12) is 200 mesh filter screen structures, the impurity essence point The filtering accuracy of absciss layer (12) is greater than the filtering accuracy of the impurity crude separating layer (11).
6. according to claim 1 or 5 cementing slurries are thickened experiment useless conduction oil recovering and purifying system, feature exists In: the cabinet of the trash eliminator (1) is the uncovered structure of top end opening, and the cabinet top of the trash eliminator (1) is used Make injection useless conduction oil.
7. cementing slurry is thickened experiment useless conduction oil recovering and purifying system according to claim 1, it is characterised in that: institute The fuel-displaced port for stating trash eliminator (1) is connect by the first petroleum pipeline (5) with the oil inlet port of grease coarse separator (2).
8. cementing slurry is thickened experiment useless conduction oil recovering and purifying system according to claim 1, it is characterised in that: institute The fuel-displaced port for stating grease coarse separator (2) is connect by the second petroleum pipeline (6) with the oil inlet port of grease fine seperator (3).
9. cementing slurry is thickened experiment useless conduction oil recovering and purifying system according to claim 1, it is characterised in that: institute The fuel-displaced port for stating grease fine seperator (3) is connect by third petroleum pipeline (7) with the oil inlet port of absolute oil storage bin (4).
CN201811340256.1A 2018-11-12 2018-11-12 Cementing slurry is thickened experiment useless conduction oil recovering and purifying system Pending CN109331536A (en)

Priority Applications (1)

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CN201811340256.1A CN109331536A (en) 2018-11-12 2018-11-12 Cementing slurry is thickened experiment useless conduction oil recovering and purifying system

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Application Number Priority Date Filing Date Title
CN201811340256.1A CN109331536A (en) 2018-11-12 2018-11-12 Cementing slurry is thickened experiment useless conduction oil recovering and purifying system

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Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN201670832U (en) * 2010-04-29 2010-12-15 陈蓉 Oil purification device
CN203754654U (en) * 2013-12-31 2014-08-06 西安理工大学 Diesel or gasoline dehydrator based on micro-nano fiber membrane
CN204246948U (en) * 2014-11-24 2015-04-08 卫辉市化工有限公司 Pressurizing multiviscosity meter conduction oil filter
CN206434933U (en) * 2017-01-20 2017-08-25 天津开发区四达科工贸发展有限公司 A kind of pressurizing multiviscosity meter anti-overflow conduction oil filter
CN207169227U (en) * 2017-09-15 2018-04-03 黄茂灿 Apparatus for purifying oil products
CN207838444U (en) * 2017-11-30 2018-09-11 西安市永鑫科技有限公司 A kind of oil filter

Patent Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN201670832U (en) * 2010-04-29 2010-12-15 陈蓉 Oil purification device
CN203754654U (en) * 2013-12-31 2014-08-06 西安理工大学 Diesel or gasoline dehydrator based on micro-nano fiber membrane
CN204246948U (en) * 2014-11-24 2015-04-08 卫辉市化工有限公司 Pressurizing multiviscosity meter conduction oil filter
CN206434933U (en) * 2017-01-20 2017-08-25 天津开发区四达科工贸发展有限公司 A kind of pressurizing multiviscosity meter anti-overflow conduction oil filter
CN207169227U (en) * 2017-09-15 2018-04-03 黄茂灿 Apparatus for purifying oil products
CN207838444U (en) * 2017-11-30 2018-09-11 西安市永鑫科技有限公司 A kind of oil filter

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