CN109251998A - A kind of particle glucose production method - Google Patents
A kind of particle glucose production method Download PDFInfo
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- CN109251998A CN109251998A CN201811373709.0A CN201811373709A CN109251998A CN 109251998 A CN109251998 A CN 109251998A CN 201811373709 A CN201811373709 A CN 201811373709A CN 109251998 A CN109251998 A CN 109251998A
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- C—CHEMISTRY; METALLURGY
- C13—SUGAR INDUSTRY
- C13K—SACCHARIDES OBTAINED FROM NATURAL SOURCES OR BY HYDROLYSIS OF NATURALLY OCCURRING DISACCHARIDES, OLIGOSACCHARIDES OR POLYSACCHARIDES
- C13K1/00—Glucose; Glucose-containing syrups
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- C—CHEMISTRY; METALLURGY
- C13—SUGAR INDUSTRY
- C13B—PRODUCTION OF SUCROSE; APPARATUS SPECIALLY ADAPTED THEREFOR
- C13B40/00—Drying sugar
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- C—CHEMISTRY; METALLURGY
- C13—SUGAR INDUSTRY
- C13B—PRODUCTION OF SUCROSE; APPARATUS SPECIALLY ADAPTED THEREFOR
- C13B50/00—Sugar products, e.g. powdered, lump or liquid sugar; Working-up of sugar
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- C—CHEMISTRY; METALLURGY
- C13—SUGAR INDUSTRY
- C13K—SACCHARIDES OBTAINED FROM NATURAL SOURCES OR BY HYDROLYSIS OF NATURALLY OCCURRING DISACCHARIDES, OLIGOSACCHARIDES OR POLYSACCHARIDES
- C13K1/00—Glucose; Glucose-containing syrups
- C13K1/06—Glucose; Glucose-containing syrups obtained by saccharification of starch or raw materials containing starch
- C13K1/08—Purifying
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- C—CHEMISTRY; METALLURGY
- C13—SUGAR INDUSTRY
- C13K—SACCHARIDES OBTAINED FROM NATURAL SOURCES OR BY HYDROLYSIS OF NATURALLY OCCURRING DISACCHARIDES, OLIGOSACCHARIDES OR POLYSACCHARIDES
- C13K1/00—Glucose; Glucose-containing syrups
- C13K1/10—Crystallisation
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- Biochemistry (AREA)
- Emergency Medicine (AREA)
- General Health & Medical Sciences (AREA)
- Health & Medical Sciences (AREA)
- Crystallography & Structural Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Food Science & Technology (AREA)
- Medicinal Preparation (AREA)
- Coloring Foods And Improving Nutritive Qualities (AREA)
- Saccharide Compounds (AREA)
Abstract
The invention discloses a kind of particle glucose production methods, and the glucose syrup of a certain concentration and DX value is placed in container, then add crystal seed and are crystallized, and then drying is dry after sieving or sieving, and obtain finished product.Particle dextran particles degree size produced by the invention is controllable, and bulk density is small, and dissolubility is good, can apply in multiple field of food, as the auxiliary material of sweetener or in instant food；International market demand is vigorous, and product consumption is big, can bring considerable economic benefit.
Description
Technical field
The invention belongs to starch sugar production technical fields, more particularly to a kind of particle glucose production method.
Background technique
Currently, the universal crystallization mode production crystal diabetin of starch sugar processing enterprise, Dextrose Monohydrate and DEXTROSE ANHYDROUS.?
It in this production technology, requires horizontal crystallizer, vertical crystallizer or open pan and is crystallized, then produced through drying
The Icing Sugar of different-grain diameter is screened by screening plant.But as current foreign customers are in the development of food deep processing,
The crystal sugar particle that there is an urgent need to a kind of partial sizes between 100~10 mesh, specific gravity are small compared with a water crystallization sugar particle, rough surface,
The high glucose of dissolubility, is called particle glucose.A kind of production method being exclusively used in particle glucose currently not yet, therefore
It cannot meet customer need, there is an urgent need to a kind of production methods that can satisfy this market.
The existing starch sugar technological process of production: starch milk → primary injection (105~110 DEG C) → pillar liquefier → secondary
Injection (135~145 DEG C) → pillar liquefier (laminar flow pipe) → saccharification → albumen deslagging filtering → decoloration → ion-exchange → evaporation →
Crystallize (horizontal crystallizer, vertical crystallizer or open pan) → centrifugation → drying → packaging → finished product.
Summary of the invention
The technical problems to be solved by the present invention are: providing a kind of particle glucose production method.This method is simple, to matching
Set production equipment requirement is low, and the particle glucose that can produce different-grain diameter size within the scope of 100 mesh~10 mesh as needed produces
Product meet market needs.
Process flow of the invention: starch milk → primary injection (105~110 DEG C) → pillar liquefier → secondary injection
(135~145 DEG C) → pillar liquefier → saccharification → albumen deslagging filtering → decoloration → ion-exchange → evaporation → particle glucose system
Work → drying → screening (or screening → drying) → packaging → finished product.
In order to solve the above technical problems, the technical scheme is that
A kind of particle glucose production method, comprising the following steps:
A. the glucose syrup of a certain concentration and DX value is placed in container, and adds the 0~15% of its mass percentage
Crystal seed, stand 1~100h；
B. it dries after the particle glucose after crystallization being sieved, or is sieved again after drying；
C. it is classified as between 100~10 mesh as needed, packed products.
Preferably, the container in the step a is square or bulge, and material is that stainless steel or plastics etc. are free of
The material of harmful substance.
Preferably, the concentration of glucose syrup is 60~90% in the step a.
Preferably, the DX value of glucose syrup is 75~99.8 in the step a.
Preferably, in the step a in the container of glucose syrup with a thickness of 0.1~100cm.
Preferably, crystal seed is a water crystallization glucose or DEXTROSE ANHYDROUS in the step a.
Preferably, the drying of particle glucose uses ebullated bed, fluidized bed or airflow drying drying side in the step b
Formula.
Preferably, particle glucose is sieved by multistage in the step b.
By adopting the above-described technical solution, the beneficial effects of the present invention are:
1. production method of the present invention is different from traditional crystallization processes, particle glucose production reduce horizontal crystallizer or
The cold crystallization link of vertical crystallizer decreases whiz scheming link, first is that equipment investment is saved, second is that the energy is saved,
Power consumption is greatly saved.Wherein the cold crystallization link of horizontal crystallizer or vertical crystallizer needs chilled water, this method
Steam consumption is greatly saved in the use for reducing refrigeration machine；
2. particle dextran particles degree size produced by the invention is controllable, bulk density is small, and dissolubility is good, can apply
Multiple field of food, as the auxiliary material of sweetener or in instant food；International market demand is vigorous, product consumption
Greatly, considerable economic benefit can be brought.
Specific embodiment
Below with reference to embodiment, the present invention is further explained.
Embodiment one:
Glucose syrup after taking 50kg to evaporate, concentration 60%, DX value are 75, are placed in square container, then add
Add 5% crystal seed (crystal seed for crystallization Dextrose Monohydrate), in container then liquid glucose thickness is wanted meeting food and medicine grade in 10cm
It asks and stands 20h in clean rooms, there are a small amount of dextran particles to occur in liquid glucose at this time, remain as liquid.
Conclusion, illustrates concentration 60%, under the conditions of DX value 75, when standing 20h, although seed load 5% quantity,
But crystallization rate is still too slow, if being further continued for addition crystal seed amount, production cost can increase significantly.
Embodiment two:
Glucose syrup after taking 50kg to evaporate, concentration 60%, DX value are 75, are placed in bulge, then add
Add 5% crystal seed (crystal seed is DEXTROSE ANHYDROUS), in container then liquid glucose thickness is meeting the requirement of food and medicine grade only in 10cm
Change and stand 30h in room, there is the appearance of part glucose crystalline solid in liquid glucose at this time, overall performance is thick massecuite.
Conclusion, illustrates concentration 60%, under the conditions of DX value 75, when standing 30h, although seed load 5% quantity,
But crystallization rate is still too slow, and crystallization time is longer, if being further continued for addition crystal seed amount, producing liter, this can rise higher greatly
It is high.
Embodiment three:
Glucose syrup after taking 50kg to evaporate, concentration 60%, DX value are 75, are placed in square container, then add
Add 5% crystal seed (crystal seed for crystallization Dextrose Monohydrate), in container then liquid glucose thickness is wanted meeting food and medicine grade in 10cm
It asks and stands 40h in clean rooms, whole at this time to condense into blocks, volume does not change, and the blocks is solid, and hardness is big, leads to
It crosses after being crushed and dries, obtained particle is smaller.
Illustrated by embodiment one to three, concentration 60%, is not suitable for that particle grape is mass produced under the conditions of DX value 75
Sugar.
Example IV:
Glucose syrup after taking 50kg to evaporate, concentration 70%, DX value are 85, are placed in bulge, do not add
Crystal seed, then liquid glucose thickness requires to stand 30h in clean rooms meeting food and medicine grade, at this time liquid glucose in 10cm in container
In there is the original clear liquid variation to be opaque turbid state, but it is whole be rendered as more sticky dilute massecuite shape, can not have
Broken state needs to extend crystallization time again if needed to reach preferable crystalline state.
Conclusion, illustrates concentration 70%, under the conditions of DX value 85, when standing 30h, and in the case where not adding crystal seed, crystallization time
Too long, production cost can increase significantly, be not suitable for that particle glucose is mass produced.
Embodiment five:
Glucose syrup after taking 50kg to evaporate, concentration 70%, DX value are 85, are placed in square container, then add
Add 1% crystal seed (crystal seed for crystallization Dextrose Monohydrate), in container then liquid glucose thickness is wanted meeting food and medicine grade in 10cm
It asks and stands 20h in clean rooms, having original clear liquid variation in liquid glucose at this time is opaque turbid state, but entirety is rendered as
More sticky dilute massecuite shape, can not have broken state, if needed to reach preferable crystalline state, when needing to extend crystallization again
Between.
Embodiment six:
Glucose syrup after taking 50kg to evaporate, concentration 70%, DX value are 85, are placed in square container, then add
Add 1% crystal seed (crystal seed for crystallization Dextrose Monohydrate), in container then liquid glucose thickness is wanted meeting food and medicine grade in 10cm
It asks and stands 30h in clean rooms, liquid glucose integrally condenses into blocks at this time, and blocks sugar volume is unchanged, the blocks sugar knot
Real, hardness is big, by drying after being crushed, obtains 40~20 mesh particles compared with yield 10%, irregular impurity is more, and micro mist is more, raw
It produces at high cost.
Illustrated by example IV to six, concentration 70%, is not suitable for production particle glucose under the conditions of DX value 85.
Embodiment seven:
Glucose syrup after taking 50kg to evaporate, concentration 75%, DX value are 95, are placed in square container, then not
Crystal seed is added, then liquid glucose thickness requires to stand 20h in clean rooms meeting food and medicine grade, at this time in 10cm in container
Puffy blocks is presented in container, volume becomes larger compared with liquid glucose to 1.08 times, easily crush, after drying particle diameter distribution mainly 40~
Between 80 mesh, granularity is somewhat smaller.
Embodiment eight:
Glucose syrup after taking 50kg to evaporate, concentration 75%, DX value are 95, are placed in square container, then not
Crystal seed is added, then liquid glucose thickness requires to stand 30h in clean rooms meeting food and medicine grade, at this time in 10cm in container
Puffy blocks is presented in container, volume becomes larger compared with liquid glucose volume to 1.12 times, easily crushes, and granule is uniform after crushing, dries
Particle diameter distribution is between 30~80 mesh after dry, and crystallization time is slightly long, and granularity is somewhat smaller.
Embodiment nine:
Glucose syrup after taking 50kg to evaporate, concentration 75%, DX value are 95, are placed in square container, then not
Crystal seed is added, then liquid glucose thickness requires to stand 40h in clean rooms meeting food and medicine grade, at this time in 10cm in container
Puffy blocks is presented in container, volume becomes larger to 1.13 times, easily crushes, and granule is uniform after crushing, partial size point after drying
For cloth between 20~60 mesh, effect is preferable, but crystallization time is slightly long.
Embodiment ten:
Glucose syrup after taking 50kg to evaporate, concentration 75%, DX value are 95, are placed in square container, then add
Add 1% crystal seed (crystal seed for crystallization Dextrose Monohydrate), then require to stand 20h in clean rooms meeting food and medicine grade,
Puffy blocks is presented in container at this time, volume becomes larger to 1.03 times compared with liquid glucose, is not easy to crush, after crushing drying, grape
Sugared particle diameter distribution mainly between 40~80 mesh, can achieve 55% or more.
Embodiment 11:
Glucose syrup after taking 50kg to evaporate, concentration 75%, DX value are 95, are placed in square container, then add
Add 2% crystal seed (crystal seed for crystallization Dextrose Monohydrate), in container then liquid glucose thickness is wanted meeting food and medicine grade in 10cm
It asks and stands 20h in clean rooms, whole at this time to condense into blocks, blocks sugar volume is unchanged, and the blocks sugar is solid, firmly
Degree is big, is not easy to crush, and after crushing drying, mainly the high production cost between 50~100 mesh, market need glucose particle diameter distribution
Ask small.
Illustrated by embodiment seven to ten one, concentration 75%, the particle Portugal of different-grain diameter can be produced under the conditions of DX value 95
Grape sugar, but production cycle and production cost can also continue to optimize.
Embodiment 12:
Glucose syrup after taking 50kg to evaporate, concentration 85%, DX value are 99, are placed in square container, then not
Crystal seed is added, then liquid glucose thickness requires to stand 10h in clean rooms meeting food and medicine grade, at this time in 10cm in container
The obvious glucose paste turbid of liquid glucose presentation, constancy of volume, viscosity are big in container.
Embodiment 13:
Glucose syrup after taking 50kg to evaporate, concentration 85%, DX value are 99, are placed in square container, then not
Crystal seed is added, then liquid glucose thickness requires to stand 20h in clean rooms meeting food and medicine grade, at this time in 10cm in container
Puffy blocks is presented in container, volume becomes larger compared with liquid glucose volume to 1.16 times, easily crushes, and granule is uniform after crushing, dries
Partial size is largely distributed between 10~40 mesh after dry, can achieve 63% or more, wherein 10~20 mesh reach 19%, 20~40
Mesh reaches 32%, and 40~60 mesh are 12%.
Embodiment 14:
Glucose syrup after taking 50kg to evaporate, concentration 85%, DX value are 99, are placed in square container, then add
Add 1% crystal seed (crystal seed for crystallization Dextrose Monohydrate), in container then liquid glucose thickness is wanted meeting food and medicine grade in 10cm
Ask and stand 10h in clean rooms, blocks is presented in container liquid glucose at this time, hardness is big, be not easy to crush, after crushing granule compared with
Small, after crushing drying, mainly high production cost, the market demand are small between 50~80 mesh for glucose particle diameter distribution.
Embodiment 15:
Glucose syrup after taking 50kg to evaporate, concentration 85%, DX value are 99, are placed in square container, then add
Add 0.5% crystal seed (crystal seed is crystallization Dextrose Monohydrate), in container then liquid glucose thickness is meeting food and medicine grade in 10cm
It is required that stand 10h in clean rooms, liquid glucose is presented obvious dextran particles body in container at this time, volume compared with liquid glucose volume become larger to
1.14, easily crush, granule is uniform after crushing, and particle diameter distribution can achieve 58% or more between 10~60 mesh after drying,
In 10~20 mesh reach 13%, 20~40 mesh reach 29%, and 40~60 mesh reach 16% or more.
Conclusion comparative analysis:
1, it is told the truth by embodiment one to three bright, concentration 60% under the conditions of DX value 75, is not suitable for large-scale production particle Portugal
Grape sugar.
2, illustrated by example IV to six, concentration 70%, under the conditions of DX value 85, be able to produce out particle glucose, but
Yield is low, and impurity is more, and the production time is long, high production cost, is not suitable for large-scale production.
3, illustrated by embodiment seven to ten one, concentration 75%, the particle of different-grain diameter can be produced under the conditions of DX value 95
Glucose reduces production cost it is also possible to optimize crystallization processes according to seed load and sugar concentration and DX value.
4, illustrated by embodiment ten two to ten five, when it is 99 that sugar concentration, which is 85%, DX value, scale can be carried out
Production:
1) crystal seed, is not added, effect is relatively good when standing time 20h, and partial size is largely distributed in 10~40 mesh after drying
Between, it can achieve 63% or more, wherein 10~20 mesh reach 19%, 20~40 mesh reach 32%, and 40~60 mesh are 12%.
2), addition crystal seed amount is 0.5%, and effect is preferable when standing time 10h, and can be shortened crystallization time, wherein 10~
20 mesh reach 13%, and 20~40 mesh reach 29%, and 40~60 mesh reach 16% or more.
It should be understood that these examples are only for illustrating the present invention and are not intended to limit the scope of the present invention.In addition, it should also be understood that,
After reading the content taught by the present invention, those skilled in the art can make various modifications or changes to the present invention, these
Equivalent form is also fallen within the scope of the appended claims of the present application.
Claims (7)
1. a kind of particle glucose production method, which comprises the following steps:
A. the glucose syrup of a certain concentration and DX value is placed in container, and adds 0~15% crystalline substance of its mass percentage
Kind, stand 1~100h；
B. it dries after the particle glucose after crystallization being sieved, or is sieved again after drying；
C. it is classified as between 100~10 mesh as needed, packed products.
2. particle glucose production method as described in claim 1, it is characterised in that: glucose syrup is dense in the step a
Degree is 60~90%.
3. particle glucose production method as described in claim 1, it is characterised in that: the DX of glucose syrup in the step a
Value is 75~99.8.
4. particle glucose production method as described in claim 1, it is characterised in that: the thickness in the container of the glucose syrup
Degree is 0.1~100cm.
5. particle glucose production method as described in claim 1, it is characterised in that: the crystal seed is a water crystallization glucose
Or DEXTROSE ANHYDROUS.
6. particle glucose production method as described in claim 1, it is characterised in that: particle glucose dries in the step b
It is dry to use ebullated bed, fluidized bed or airflow drying drying mode.
7. particle glucose production method as described in claim 1, it is characterised in that: particle glucose is logical in the step b
Cross multistage sieved.
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201811373709.0A CN109251998A (en) | 2018-11-19 | 2018-11-19 | A kind of particle glucose production method |
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| Application Number | Priority Date | Filing Date | Title |
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| CN201811373709.0A CN109251998A (en) | 2018-11-19 | 2018-11-19 | A kind of particle glucose production method |
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| CN109251998A true CN109251998A (en) | 2019-01-22 |
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| CN201811373709.0A Pending CN109251998A (en) | 2018-11-19 | 2018-11-19 | A kind of particle glucose production method |
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Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1063903A (en) * | 1991-02-06 | 1992-08-26 | 轻工部食品发酵工业科学研究所 | Preparation of fructose by crystallization |
| CN102816876A (en) * | 2012-09-19 | 2012-12-12 | 广西贝拓糖业生物科技有限公司 | Solid fructose glucose and production method thereof |
| CN103397111A (en) * | 2013-07-11 | 2013-11-20 | 广西贝拓糖业生物科技有限公司 | Preparation method of granulated crystal sugar |
| CN104829446A (en) * | 2015-04-17 | 2015-08-12 | 山东西王糖业有限公司 | Method for extracting sodium gluconate without generating mother liquor |
| CN107746900A (en) * | 2017-11-14 | 2018-03-02 | 王鑫 | Continuous crystallisation equipment and technique in a kind of glucose production |
| CN108251569A (en) * | 2018-01-23 | 2018-07-06 | 山东兆光色谱分离技术有限公司 | A kind of DEXTROSE ANHYDROUS preparation process |
-
2018
- 2018-11-19 CN CN201811373709.0A patent/CN109251998A/en active Pending
Patent Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1063903A (en) * | 1991-02-06 | 1992-08-26 | 轻工部食品发酵工业科学研究所 | Preparation of fructose by crystallization |
| CN102816876A (en) * | 2012-09-19 | 2012-12-12 | 广西贝拓糖业生物科技有限公司 | Solid fructose glucose and production method thereof |
| CN103397111A (en) * | 2013-07-11 | 2013-11-20 | 广西贝拓糖业生物科技有限公司 | Preparation method of granulated crystal sugar |
| CN104829446A (en) * | 2015-04-17 | 2015-08-12 | 山东西王糖业有限公司 | Method for extracting sodium gluconate without generating mother liquor |
| CN107746900A (en) * | 2017-11-14 | 2018-03-02 | 王鑫 | Continuous crystallisation equipment and technique in a kind of glucose production |
| CN108251569A (en) * | 2018-01-23 | 2018-07-06 | 山东兆光色谱分离技术有限公司 | A kind of DEXTROSE ANHYDROUS preparation process |
Non-Patent Citations (1)
| Title |
|---|
| 刘宝家等: "《食品加工技术、工艺和配方大全（精选版下）》", 30 September 2005, 科学技术文献出版社 * |
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Application publication date: 20190122 |