CN109247627A - A kind of preparation method of Chinese medicine antibacterial underwear fabric - Google Patents
A kind of preparation method of Chinese medicine antibacterial underwear fabric Download PDFInfo
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- CN109247627A CN109247627A CN201811226839.1A CN201811226839A CN109247627A CN 109247627 A CN109247627 A CN 109247627A CN 201811226839 A CN201811226839 A CN 201811226839A CN 109247627 A CN109247627 A CN 109247627A
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- chinese medicine
- antibacterial
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Classifications
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- A—HUMAN NECESSITIES
- A41—WEARING APPAREL
- A41B—SHIRTS; UNDERWEAR; BABY LINEN; HANDKERCHIEFS
- A41B17/00—Selection of special materials for underwear
-
- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
- D01F1/00—General methods for the manufacture of artificial filaments or the like
- D01F1/02—Addition of substances to the spinning solution or to the melt
- D01F1/10—Other agents for modifying properties
- D01F1/103—Agents inhibiting growth of microorganisms
-
- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
- D01F2/00—Monocomponent artificial filaments or the like of cellulose or cellulose derivatives; Manufacture thereof
-
- D—TEXTILES; PAPER
- D02—YARNS; MECHANICAL FINISHING OF YARNS OR ROPES; WARPING OR BEAMING
- D02G—CRIMPING OR CURLING FIBRES, FILAMENTS, THREADS, OR YARNS; YARNS OR THREADS
- D02G3/00—Yarns or threads, e.g. fancy yarns; Processes or apparatus for the production thereof, not otherwise provided for
- D02G3/02—Yarns or threads characterised by the material or by the materials from which they are made
- D02G3/04—Blended or other yarns or threads containing components made from different materials
-
- D—TEXTILES; PAPER
- D02—YARNS; MECHANICAL FINISHING OF YARNS OR ROPES; WARPING OR BEAMING
- D02G—CRIMPING OR CURLING FIBRES, FILAMENTS, THREADS, OR YARNS; YARNS OR THREADS
- D02G3/00—Yarns or threads, e.g. fancy yarns; Processes or apparatus for the production thereof, not otherwise provided for
- D02G3/44—Yarns or threads characterised by the purpose for which they are designed
- D02G3/449—Yarns or threads with antibacterial properties
-
- A—HUMAN NECESSITIES
- A41—WEARING APPAREL
- A41B—SHIRTS; UNDERWEAR; BABY LINEN; HANDKERCHIEFS
- A41B2400/00—Functions or special features of shirts, underwear, baby linen or handkerchiefs not provided for in other groups of this subclass
- A41B2400/34—Functions or special features of shirts, underwear, baby linen or handkerchiefs not provided for in other groups of this subclass antimicrobial or antibacterial
-
- D—TEXTILES; PAPER
- D10—INDEXING SCHEME ASSOCIATED WITH SUBLASSES OF SECTION D, RELATING TO TEXTILES
- D10B—INDEXING SCHEME ASSOCIATED WITH SUBLASSES OF SECTION D, RELATING TO TEXTILES
- D10B2201/00—Cellulose-based fibres, e.g. vegetable fibres
- D10B2201/20—Cellulose-derived artificial fibres
- D10B2201/22—Cellulose-derived artificial fibres made from cellulose solutions
-
- D—TEXTILES; PAPER
- D10—INDEXING SCHEME ASSOCIATED WITH SUBLASSES OF SECTION D, RELATING TO TEXTILES
- D10B—INDEXING SCHEME ASSOCIATED WITH SUBLASSES OF SECTION D, RELATING TO TEXTILES
- D10B2401/00—Physical properties
- D10B2401/02—Moisture-responsive characteristics
- D10B2401/021—Moisture-responsive characteristics hydrophobic
-
- D—TEXTILES; PAPER
- D10—INDEXING SCHEME ASSOCIATED WITH SUBLASSES OF SECTION D, RELATING TO TEXTILES
- D10B—INDEXING SCHEME ASSOCIATED WITH SUBLASSES OF SECTION D, RELATING TO TEXTILES
- D10B2401/00—Physical properties
- D10B2401/13—Physical properties anti-allergenic or anti-bacterial
-
- D—TEXTILES; PAPER
- D10—INDEXING SCHEME ASSOCIATED WITH SUBLASSES OF SECTION D, RELATING TO TEXTILES
- D10B—INDEXING SCHEME ASSOCIATED WITH SUBLASSES OF SECTION D, RELATING TO TEXTILES
- D10B2501/00—Wearing apparel
- D10B2501/02—Underwear
Landscapes
- Engineering & Computer Science (AREA)
- Textile Engineering (AREA)
- Chemical & Material Sciences (AREA)
- Mechanical Engineering (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Manufacturing & Machinery (AREA)
- Materials Engineering (AREA)
- Chemical Or Physical Treatment Of Fibers (AREA)
- Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)
Abstract
The invention belongs to the separation and extraction technologies of biology and the natural products effective ingredient of light industry and chemical industry biology skill in new medicine, are related to active skull cap components extraction and application field, specially a kind of preparation method of Chinese medicine antibacterial underwear fabric.The invention firstly uses the ethyl alcohol extractive techniques of ultrasonic wave added, and Antibacterial Constituents are extracted from Chinese medicine；Then natural antibacterial ingredient encapsulate using mesoporous silicon oxide/chitosan complexes and the chitosan for carrying medicine/mesoporous silicon dioxide nano particle is made；After finally bamboo fibre, the chitosan/mesoporous silicon dioxide nano particle for carrying medicine, natural, water, spin finish aid are mixed, through electrostatic spinning handle after Chinese medicine antibacterial fiber, by the cotton fiber of Chinese medicine antibacterial fiber and hydrophobically modified carry out it is blended after to get Chinese medicine antibacterial underwear fabric.Not only have effects that antibiotic health care fruit through Chinese medicine antibacterial underwear fabric prepared by the present invention, but also have skin-friendly good, sucting wet air permeability it is strong wear experience sense.
Description
Technical field
The invention belongs to the separation and Extractions of biology and the natural products effective ingredient of light industry and chemical industry biology skill in new medicine
Technology is related to active skull cap components extraction and application field, specially a kind of Chinese medicine antibacterial underwear fabric and preparation method thereof.
Background technique
With the raising of the development of modern textile technology and living standards of the people and health perception, abundance, production
Process warm and environmental protection, the comfortable fiber textile of fabric have been favored by people gradually.Personal clothing of the underwear as people, disappears
The person of expense requires its comfort and security performance higher.The long-term antibacterial effect of traditional fabric is bad, it is difficult to prevent bacterium sense
Dye.Market antibacterial fabric is mostly antibacterial agent and the antibacterial silver nanoparticle of addition synthesis to promote the antibiotic property of fabric, but is synthesized
Antibacterial agent can stimulate skin, and antibacterial silver nanoparticle can be then rapidly absorbed by a human into human body by skin pore, influence consumer's
Health.Based on this, before the Chinese medicine antibacterial underwear fabric of safe and efficient antibacterial provided by the invention will have huge market to apply
Scape.
Summary of the invention
It is bad in order to solve the long-term antibacterial effect of traditional fabric, it is difficult to bacterium infection is prevented, and it is anti-in antibacterial fabric
There is security risk in bacterium ingredient.It is of the invention to provide a kind of Chinese medicine antibacterial underwear fabric and preparation method thereof.In order to
Realize that above-mentioned target, the present invention will use following technology:
A kind of Chinese medicine antibacterial underwear fabric and preparation method thereof, which comprises the following steps:
(1) traditional Chinese medicine powder is mixed to obtain after 60 meshes being crushed respectively after folium artemisiae argyi, radix scutellariae, kuh-seng drying, by traditional Chinese medicine powder microwave treatment
After being mixed with ethanol-water mixture by the mass volume ratio (g/mL) of 1:15-25 after 20-35min 300-500W ultrasonic power,
It is filtered after ultrasound 20-30min under the conditions of 45-60 DEG C, the residue merging filtrate after ultrasonic extraction-filtration step repeats 2-3 times again,
Filtrate is crossed after ultrafiltration membrane to be concentrated to be evaporated, natural antibacterial agent is prepared；
(2) after natural antibacterial agent being dissolved in n-hexane, after meso-porous titanium dioxide Si powder is added, after ultrasonic disperse is uniform, in 300-
After stirring 3-5h under the conditions of 500rpm, solution is centrifuged, saves supernatant, dry centrifugation product obtains being adsorbed with natural antibacterial
It is added it in chitosan acetic acid solution after mesoporous silicon dioxide nano particle of ingredient, at room temperature in 300-500rpm condition
After lower magnetic agitation 20-36 h, after centrifuge separation precipitating, precipitating is washed with deionized and is dried afterwards twice, obtains carrying medicine
Chitosan/mesoporous silicon dioxide nano particle；
(3) after impregnating 20-30h in hydrogen peroxide/urea liquid processing after bamboo is sliced, broken, water-washing drying-machine tool
Disperse that bamboo fibre is made；Bamboo fibre is placed in high energy ball mill, using dehydrated alcohol as decentralized medium, carries out ball-milling treatment
After 25-30min, after the sample after ball milling is impregnated 4-5h in citric acid-trisodium citrate buffer solution, through washing filtering point
Bamboo fibre is separated out, solid bamboo fibre is obtained after freeze-drying；
(4) solid bamboo fibre, chitosan/mesoporous silicon dioxide nano particle for carrying medicine, natural, water, spinning are helped
Fiber spinning solution is prepared in agent after mixing, dry after electrostatic spinning is handled, and Chinese medicine antibacterial fiber is obtained, by Chinese medicine antibacterial
To get Chinese medicine antibacterial underwear fabric after the progress of the cotton fiber of fiber and hydrophobically modified is blended.
Preferably, folium artemisiae argyi in traditional Chinese medicine powder as described in step (1), radix scutellariae, kuh-seng mass ratio be 1:0.5-1.5:1-2.
Preferably, the volume fraction of ethyl alcohol is 35-50% in ethanol-water mixture as described in step (1)；Described is super
The molecular cut off of filter membrane is 5000.
Preferably, concentration of the natural antibacterial agent in n-hexane described in step (2) is 0.2-0.35g/mL;Mesoporous two
The partial size of silica is not more than 100nm in silicon oxide powder;Mesoporous diameter is not less than 10nm;The mesoporous silicon oxide adds
Enter the 80-120% that amount is natural antibacterial agent quality.
Preferably, the pH of chitosan acetic acid solution described in step (2) is adjusted to 5-7 with NaOH solution；The shell
The concentration of glycan is 0.08-0.1g/mL.
Preferably, the concentration of hydrogen peroxide is 2-4mol/L, urine in hydrogen peroxide/urea liquid described in step (3)
Plain concentration is 1-3mol/L;The temperature when immersion is 35-45 DEG C；Ratio of grinding media to material is 1:1.5-2 when ball-milling treatment.
Preferably, citric acid concentration is 0.15- in citric acid described in step (3)-trisodium citrate buffer solution
0.2g/mL, trisodium citrate concentration are 0.25-0.3g/mL;The temperature when immersion is 45-50 DEG C.
Preferably, natural inhibitor described in step (4) is tea polyphenols；The auxiliary agent polyacrylamide, poly- carbonic acid
One of rouge；Chitosan/mesoporous silicon dioxide nano particle, natural, the water, spinning of the bamboo fibre, load medicine
Auxiliary agent is figured by mass parts is followed successively by 20-35 parts, 3-5 parts, 0.5-1 parts, 65-85 parts, 5-8 parts.
Preferably, mass ratio is 1- when Chinese medicine antibacterial fiber described in step (4) and hydrophobically modified cotton fiber are blended
0.5-0.8。
In addition, Chinese medicine antibacterial underwear fabric of the invention is as prepared by above-mentioned preparation method.
Compared with prior art, a kind of preparation method of Chinese medicine antibacterial underwear fabric of the present invention has with following
Beneficial effect, the present invention extract antibacterial agent of the antimicrobial component as underwear fabric in Chinese medicine using ethyl alcohol, not only ensure that underwear
Antibacterial effect, and artificial synthesized antibacterial agent is not used, product is safer；The present invention utilizes mesoporous silicon oxide/shell
Glycan microballoon encapsulates Chinese medicine antimicrobial component, and the encapsulation rate for improving active ingredient of Chinese herbs connect activity at fiber
It is closer to fall off, enable fabric durable antibiotic；The chitosan of addition makes fabric have good antibacterial effect；This
Outside, the cotton fiber of Chinese medicine antibacterial fiber and hydrophobically modified is blended so that fabric skin-friendly is good, sucting wet air permeability is strong.Through the present invention
The Chinese medicine antibacterial underwear fabric of preparation not only has antibiotic health care function, but also has skin-friendly good, and sucting wet air permeability is strong to be worn
Experience sense.
Specific embodiment
[embodiment 1]
A kind of Chinese medicine antibacterial underwear fabric and preparation method thereof, which comprises the following steps:
(1) crushed after being separately dried folium artemisiae argyi, radix scutellariae, kuh-seng and mix to obtain traditional Chinese medicine powder by 1:1:1 mass ratio after 60 meshes, will in
In 400W after being mixed with 40% ethanol-water mixture by the mass volume ratio (g/mL) of 1:20 after medicinal powder microwave treatment 20-35min
Ultrasonic power is filtered after ultrasound 25min under the conditions of 50 DEG C, and residue merges filter after ultrasonic extraction-filtration step is repeated 3 times again
Filtrate is crossed molecular cut off and natural antibacterial agent is prepared to be concentrated to be evaporated after 5000 ultrafiltration membrane by liquid；
(2) after natural antibacterial agent system to be dissolved in the solution for obtaining 0.25g/mL after n-hexane, mesoporous silicon oxide is added into solution
After powder, after ultrasonic disperse is uniform, after stirring 4h under 400rpm piece, solution is centrifuged, saves supernatant, dry centrifugation
Product adds it to the 0.08g/mL that pH is 5-7 after obtaining mesoporous silicon dioxide nano particle of absorption natural antibacterial ingredient
In chitosan acetic acid solution, at room temperature under the conditions of 400rpm after 24 h of magnetic agitation, product centrifuge separation is washed with deionized water
It washs and dries afterwards twice, obtain chitosan/mesoporous silicon dioxide nano particle for carrying medicine；
(3) after bamboo is sliced, broken in 2.5mol/L hydrogen peroxide, 1.5mol/L urea liquid, under the conditions of 40 DEG C, leaching
After steeping 20h, water-washing drying-machine tool disperses that bamboo fibre is made；Bamboo fibre is placed in high energy ball mill, is 1:1.5 item in ratio of grinding media to material
Under part, using dehydrated alcohol as decentralized medium, after ball-milling treatment 25-min, by the sample after ball milling in 0.15-0.2g/mL lemon
Acid in 0.25-0.3g/mL trisodium citrate buffer solution, after impregnating 4h under the conditions of 45-50 DEG C, is isolated through washing filtering
Bamboo fibre obtains solid bamboo fibre after freeze-drying；
(4) 25 parts of solid bamboo fibres, 4.5 parts are carried to chitosan/mesoporous silicon dioxide nano particle, the 0.5 part of tea polyphenols, 65 parts of medicine
Fiber spinning solution is prepared in water, 5 parts of polyacrylamides after mixing, dry that Chinese medicine antibacterial is fine after electrostatic spinning is handled
After dimension, to get in Chinese medicine antibacterial after the mass ratio progress that the cotton fiber of Chinese medicine antibacterial fiber and hydrophobically modified is pressed 1:0.5 is blended
Clothing fabric.
[embodiment 2]
A kind of preparation method of Chinese medicine antibacterial underwear fabric, which comprises the following steps:
(1) will folium artemisiae argyi, radix scutellariae, kuh-seng it is dry after crushed mix to obtain traditional Chinese medicine powder by 1:1.5:2 mass ratio after 60 meshes respectively, will
After being mixed with 35% ethanol-water mixture by the mass volume ratio (g/mL) of 1:25 after traditional Chinese medicine powder microwave treatment 20-35min
400W ultrasonic power is filtered after ultrasound 30min under the conditions of 45 DEG C, and residue merges after ultrasonic extraction-filtration step is repeated 3 times again
Filtrate is crossed molecular cut off and natural antibacterial agent is prepared to be concentrated to be evaporated after 5000 ultrafiltration membrane by filtrate；
(2) after natural antibacterial agent system to be dissolved in the solution for obtaining 0.2g/mL after n-hexane, meso-porous titanium dioxide silicon powder is added into solution
It is last, after ultrasonic disperse is uniform, after stirring 4h under the conditions of 400rpm, solution is centrifuged, saves supernatant, dry centrifugation produces
Object obtains adding it to the 0.1g/mL shell that pH is 5-7 after mesoporous silicon dioxide nano particle of absorption natural antibacterial ingredient poly-
In sugared acetic acid solution, at room temperature under the conditions of 400rpm after 24 h of magnetic agitation, product centrifuge separation, deionized water is washed twice
After dry, obtain carry medicine chitosan/mesoporous silicon dioxide nano particle；
(3) it after bamboo is sliced, broken in 3mol/L hydrogen peroxide, 1.5mol/L urea liquid, under the conditions of 40 DEG C, impregnates
After 20h, water-washing drying-machine tool disperses that bamboo fibre is made；Bamboo fibre is placed in high energy ball mill, is 1:1.2 condition in ratio of grinding media to material
Under, using dehydrated alcohol as decentralized medium, after ball-milling treatment 25-min, by the sample after ball milling in 0.15-0.2g/mL lemon
Acid in 0.25-0.3g/mL trisodium citrate buffer solution, after impregnating 4h under the conditions of 45-50 DEG C, is isolated through washing filtering
Bamboo fibre obtains solid bamboo fibre after freeze-drying；
(4) 23 parts of solid bamboo fibres, 3.5 parts are carried to chitosan/mesoporous silicon dioxide nano particle, the 0.5 part of tea polyphenols, 68 parts of medicine
Fiber spinning solution is prepared in water, 5 parts of polycarbonate after mixing, dry the Chinese medicine antibacterial fiber after electrostatic spinning is handled
Afterwards, to get Chinese medicine antibacterial underwear after the mass ratio progress for the cotton fiber of Chinese medicine antibacterial fiber and hydrophobically modified being pressed 1:0.8 is blended
Fabric.
For the ordinary skill in the art, specific embodiment is only exemplarily described the present invention,
Obviously the present invention specific implementation is not subject to the restrictions described above, as long as use the inventive concept and technical scheme of the present invention into
The improvement of capable various unsubstantialities, or not improved the conception and technical scheme of the invention are directly applied to other occasions
, it is within the scope of the present invention.
Claims (10)
1. a kind of preparation method of Chinese medicine antibacterial underwear fabric, which comprises the following steps:
(1) traditional Chinese medicine powder is mixed to obtain after 60 meshes being crushed respectively after folium artemisiae argyi, radix scutellariae, kuh-seng drying, by traditional Chinese medicine powder microwave treatment
After being mixed with ethanol-water mixture by the mass volume ratio (g/mL) of 1:15-25 after 20-35min 300-500W ultrasonic power,
It is filtered after ultrasound 20-30min under the conditions of 45-60 DEG C, the residue merging filtrate after ultrasonic extraction-filtration step repeats 2-3 times again,
Filtrate is crossed after ultrafiltration membrane to be concentrated to be evaporated, natural antibacterial agent is prepared；
(2) after natural antibacterial agent being dissolved in n-hexane, after meso-porous titanium dioxide Si powder is added, after ultrasonic disperse is uniform, in 300-
After stirring 3-5h under the conditions of 500rpm, solution is centrifuged, saves supernatant, dry centrifugation product obtains being adsorbed with natural antibacterial
It is added it in chitosan acetic acid solution after mesoporous silicon dioxide nano particle of ingredient, at room temperature in 300-500rpm condition
After lower magnetic agitation 20-36 h, after centrifuge separation precipitating, precipitating is washed with deionized and is dried afterwards twice, obtains carrying medicine
Chitosan/mesoporous silicon dioxide nano particle；
(3) after impregnating 20-30h in hydrogen peroxide/urea liquid processing after bamboo is sliced, broken, water-washing drying-machine tool
Disperse that bamboo fibre is made；Bamboo fibre is placed in high energy ball mill, using dehydrated alcohol as decentralized medium, carries out ball-milling treatment
After 25-30min, after the sample after ball milling is impregnated 4-5h in citric acid-trisodium citrate buffer solution, through washing filtering point
Bamboo fibre is separated out, solid bamboo fibre is obtained after freeze-drying；
(4) solid bamboo fibre, chitosan/mesoporous silicon dioxide nano particle for carrying medicine, natural, water, spinning are helped
Fiber spinning solution is prepared in agent after mixing, dry after electrostatic spinning is handled, and Chinese medicine antibacterial fiber is obtained, by Chinese medicine antibacterial
To get Chinese medicine antibacterial underwear fabric after the progress of the cotton fiber of fiber and hydrophobically modified is blended.
2. a kind of preparation method of Chinese medicine antibacterial underwear fabric according to claim 1, which is characterized in that in step (1)
Folium artemisiae argyi in the traditional Chinese medicine powder, radix scutellariae, kuh-seng mass ratio be 1:0.5-1.5:1-2.
3. a kind of preparation method of Chinese medicine antibacterial underwear fabric according to claim 2, which is characterized in that in step (1)
The volume fraction of ethyl alcohol is 35-50% in the ethanol-water mixture；The molecular cut off of the ultrafiltration membrane is 5000.
4. a kind of preparation method of Chinese medicine antibacterial underwear fabric according to claim 1, which is characterized in that in step (2)
Concentration of the natural antibacterial agent in n-hexane is 0.2-0.35g/mL;The grain of silica in meso-porous titanium dioxide Si powder
Diameter is not more than 100nm;Mesoporous diameter is not less than 10nm;The additional amount of the mesoporous silicon oxide is natural antibacterial agent quality
80-120%。
5. a kind of preparation method of Chinese medicine antibacterial underwear fabric according to claim 1, which is characterized in that in step (2)
The pH of the chitosan acetic acid solution is adjusted to 5-7 with NaOH solution；The concentration of the chitosan is 0.08-0.1g/mL.
6. a kind of preparation method of Chinese medicine antibacterial underwear fabric according to claim 1, it is characterised in that institute in step (3)
The concentration of hydrogen peroxide is 2-4mol/L, urea concentration 1-3mol/L in the hydrogen peroxide/urea liquid stated;The immersion
When temperature be 35-45 DEG C；Ratio of grinding media to material is 1:1.5-2 when ball-milling treatment.
7. a kind of preparation method of Chinese medicine antibacterial underwear fabric according to claim 1, it is characterised in that institute in step (3)
Citric acid concentration is 0.15-0.2g/mL in the citric acid stated-trisodium citrate buffer solution, and trisodium citrate concentration is 0.25-
0.3g/mL;The temperature when immersion is 45-50 DEG C.
8. a kind of preparation method of Chinese medicine antibacterial underwear fabric according to claim 1, it is characterised in that institute in step (4)
The natural inhibitor stated is tea polyphenols；One of the auxiliary agent polyacrylamide, polycarbonate；The bamboo fibre carries
Chitosan/mesoporous silicon dioxide nano particle, natural, water, the spin finish aid of medicine are figured by mass parts is followed successively by 20-35
Part, 3-5 parts, 0.5-1 parts, 65-85 parts, 5-8 parts.
9. a kind of preparation method of Chinese medicine antibacterial underwear fabric according to claim 1, it is characterised in that institute in step (4)
Mass ratio is 1-0.5-0.8 when the Chinese medicine antibacterial fiber and hydrophobically modified cotton fiber stated are blended.
10. a kind of Chinese medicine antibacterial underwear fabric, prepared by the preparation method as described in -9 any one according to claim 1.
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| CN201811226839.1A CN109247627A (en) | 2018-10-22 | 2018-10-22 | A kind of preparation method of Chinese medicine antibacterial underwear fabric |
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|---|---|---|---|---|
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| CN109943893A (en) * | 2019-02-27 | 2019-06-28 | 唐卫兵 | A kind of preparation method of the warming natural nano bamboo fibre/cotton fiber composite material of long acting antibiotic |
| CN110079919A (en) * | 2019-05-11 | 2019-08-02 | 唐卫兵 | One kind containing nano-quantum point antibiotic cotton fiber fabric and preparation method thereof |
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Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103920153A (en) * | 2014-05-06 | 2014-07-16 | 中国科学院上海硅酸盐研究所 | Chitosan-modified pH responsive medicine-loading controlled release material and preparation method thereof |
| CN107557880A (en) * | 2017-11-08 | 2018-01-09 | 唐卫兵 | A kind of preparation method of antiallergy face liber |
| CN108251903A (en) * | 2018-03-08 | 2018-07-06 | 唐卫兵 | A kind of preparation method of the cellulose nano-fibrous spinning solution of super-hydrophobicity |
| CN108330558A (en) * | 2018-03-08 | 2018-07-27 | 唐卫兵 | A kind of preparation method of the hydrophobic fibre element chitosan nano fiber spinning solution of antibacterial functions |
| CN108456966A (en) * | 2018-06-14 | 2018-08-28 | 张秀仙 | A kind of preparation method of the soft tencel fabric of environmental protection parent |
| CN108560246A (en) * | 2018-05-05 | 2018-09-21 | 汕头市雪果制衣实业有限公司 | A kind of preparation method of the water-fastness bamboo fibre fabric of the pro-skin of children |
-
2018
- 2018-10-22 CN CN201811226839.1A patent/CN109247627A/en active Pending
Patent Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103920153A (en) * | 2014-05-06 | 2014-07-16 | 中国科学院上海硅酸盐研究所 | Chitosan-modified pH responsive medicine-loading controlled release material and preparation method thereof |
| CN107557880A (en) * | 2017-11-08 | 2018-01-09 | 唐卫兵 | A kind of preparation method of antiallergy face liber |
| CN108251903A (en) * | 2018-03-08 | 2018-07-06 | 唐卫兵 | A kind of preparation method of the cellulose nano-fibrous spinning solution of super-hydrophobicity |
| CN108330558A (en) * | 2018-03-08 | 2018-07-27 | 唐卫兵 | A kind of preparation method of the hydrophobic fibre element chitosan nano fiber spinning solution of antibacterial functions |
| CN108560246A (en) * | 2018-05-05 | 2018-09-21 | 汕头市雪果制衣实业有限公司 | A kind of preparation method of the water-fastness bamboo fibre fabric of the pro-skin of children |
| CN108456966A (en) * | 2018-06-14 | 2018-08-28 | 张秀仙 | A kind of preparation method of the soft tencel fabric of environmental protection parent |
Cited By (13)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
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| CN115323778B (en) * | 2022-08-16 | 2023-07-18 | 汕头市润丰纺织科技实业有限公司 | Chitosan-I type collagen amino acid composite antibacterial finishing liquid, preparation method thereof and antibacterial fabric |
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Application publication date: 20190122 |