CN109096866A - A kind of water-base epoxy dumb light floor coatings and preparation method thereof - Google Patents
A kind of water-base epoxy dumb light floor coatings and preparation method thereof Download PDFInfo
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- CN109096866A CN109096866A CN201810608749.2A CN201810608749A CN109096866A CN 109096866 A CN109096866 A CN 109096866A CN 201810608749 A CN201810608749 A CN 201810608749A CN 109096866 A CN109096866 A CN 109096866A
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- water
- epoxy
- dumb light
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D163/00—Coating compositions based on epoxy resins; Coating compositions based on derivatives of epoxy resins
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/60—Additives non-macromolecular
- C09D7/61—Additives non-macromolecular inorganic
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K3/00—Use of inorganic substances as compounding ingredients
- C08K3/30—Sulfur-, selenium- or tellurium-containing compounds
- C08K2003/3045—Sulfates
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K3/00—Use of inorganic substances as compounding ingredients
- C08K3/34—Silicon-containing compounds
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K3/00—Use of inorganic substances as compounding ingredients
- C08K3/34—Silicon-containing compounds
- C08K3/36—Silica
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- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Paints Or Removers (AREA)
Abstract
The invention discloses a kind of water-base epoxy dumb light floor coatings and preparation method thereof, the water-base epoxy dumb light floor coatings include that according to the mass fraction following group is grouped as: component A: 30-50 parts of epoxy hardener, 10-20 parts of deionized water, 0.1-0.3 parts of defoaming agent, 0.1-0.4 parts of dispersing agent, 0.1-0.3 parts of anti-floating agent, 2-5 parts of talcum powder, 0.1-0.5 parts of white carbon black, 10-20 parts of barium sulfate, 0.2-0.6 parts of substrate wetting agents, 15-25 parts of CY-100；B component: 85-95 parts of epoxy resin, 5-15 parts of aliphatic glycidyl ether.VOC content of the present invention is low, has good skid resistance, and the paint film adhesion of formation is strong, has excellent resistance to deionization aqueous and solvent resistance.
Description
Technical field
The present invention relates to functional environment-friendly paint fields, and in particular to a kind of water-base epoxy dumb light floor coatings and its preparation
Method.
Background technique
Water-base epoxy dumb light floor coatings refer to that coating has matte effect, and have hardness height, wearability good, excellent
Non-skid property, can be suitable for requiring the decoration on ground very well.
And requirement of the people to coating at this stage is higher and higher, it is also more and more diversified, it is therefore desirable to provide a kind of aqueous
Epoxy dumb light floor coatings, can make up for it this vacancy, solve the problems, such as that ground floor brick gloss is high and it is anti-skidding not have and
The problem of some poor quality wood floors long-term release formaldehydes, make ground environment that can also there is good decorative performance and skid resistance
Can, however the gloss at lapping defect of dumb light floor coatings on the market is substantially higher at non-lapping defect, overall surface effect is poor.Cause
This researches and develops a novel dumb light floor coatings, to reach the personalization and art up requirement of people's finishing.
Summary of the invention
Regarding the issue above, the present invention provides one kind can solve dumb light floor coatings in construction very well
It waits, the water-base epoxy dumb light floor coatings and preparation method thereof of gloss difference problem at lapping defect.
In order to achieve the above objectives, present invention employs following technical proposals: a kind of water-base epoxy dumb light terrace of the invention
Coating, the water-base epoxy dumb light floor coatings include that according to the mass fraction following group is grouped as:
Wherein aliphatic contracting deionized water glycerin ether must meet the following requirement: (1) viscosity: 40 DEG C of (mpa.s) 3~7,
(2) epoxide equivalent: g/eq 290~310.
Further, the water-base epoxy dumb light floor coatings include that according to the mass fraction following group is grouped as:
Further, the dispersing agent is 750W, and the substrate wetting agents are BYK346, the WET510 of Digao or elder generation
One of PW336 of wound or a variety of combinations；The epoxy resin is low-molecular-weight epoxy resin, the epoxy resin
Concentration be 85-95%.
Further, the defoaming agent is the SN154 of BYK-028, BYK-024, Nuo Puke or the A10 of BASF
One or more of combination.
Further, the ratio of the epoxy resin and epoxy hardener is 6:1.
Further, the anti-flood and anti-float agent is hyper-dispersant, and the epoxy hardener is 8B.
Further, the CY-100 is not flatting silica.
The preparation method of water-base epoxy dumb light floor coatings of the present invention, includes the following steps:
(1) deionized water, defoaming agent, the anti-floating agent of dispersing agent and substrate wetting agents are uniformly mixed and obtain slurries A；
(2) talcum powder, white carbon black, barium sulfate, CY-100 are added into slurries A, is uniformly mixed and obtains slurries B；
(3) epoxy hardener and levelling agent, uniformly mixed slurries C, as component A are added into slurries B；
(4) epoxy resin is opened in the container of no deionized water cleaning with aliphatic contracting deionized water glycerin ether dilute, mixed
It closes and uniformly obtains B component.
The utility model has the advantages that the present invention has the function of absorbing harmful organic substance, VOC content is low, has good skid resistance, shape
At paint film adhesion it is strong, with excellent resistance to deionization is aqueous and solvent resistance, therefore reached the environmental protection of people's promotion
The art up requirement with individual character.
Compared with prior art, the present invention has the advantage that
(1) present invention has the reference area of very little, to reach the left and right of delustring.And it is able to solve flatting silica going
Dynamic in ion aqueous epoxy floor coating is floated black.And it does not need special dispersing agent and (flatting silica is arranged to CY-100
This needs special dispersing agent to be arranged).
It (2), can be with the variation of gloss, i.e., especially at 10 minutes or more lapping defects when traditional mute powder is early constructed
Semi-gloss is become from dumb light.Cause coating film gloss inconsistent, to influence beauty.
(3) paint film that the present invention is formed can be good at solving current floor brick without dumb light gloss and floor tile belongs to
Highly energy-consuming high pollution industry, floor inferior finishing the problems such as causing formaldehyde again.
Specific embodiment
It should be understood that it is to describe special embodiment that heretofore described term, which is only, it is not intended to limit this hair
It is bright.In addition, for the numberical range in the present invention, it is thus understood that it is also specifically disclosed that between the upper limit value and lower limit value of the range
Each median.Median and any other statement value in any statement value or stated ranges or in the range
Lesser range is also included in the present invention each of between interior median.These small range of upper limit values and lower limit value can
Independently include or exclude in range.
In addition, in order to better illustrate the present invention, being given in specific embodiment below numerous specific
Details.It will be appreciated by those skilled in the art that without certain details, the present invention equally be can be implemented.In other reality
It applies in example, method well known to those skilled in the art, means is not described in detail, in order to highlight purport of the invention.
In the present invention, indicate that the unit of material content is based on parts by weight meter, unless otherwise stated.In addition, about technology of the invention
The measuring method of index is in the art using standard method, and for details, reference can be made to newest national standards, unless otherwise stated.
In an embodiment of the present invention, the adhesive force of paint film is preferably according to GB/T1720-1979 standard testing, paint film it is resistance to
Deionization is aqueous preferably according to GB/T1733-1993 standard testing, and VOC content is preferably according to GB18582-2008 standard testing.
Embodiment 1
A kind of water-base epoxy dumb light floor coatings of the invention, the water-base epoxy dumb light floor coatings include pressing quality
Following group of number meter is grouped as:
In certain embodiments of the present invention, the composition principle of the low-molecular-weight epoxy resin is as follows:
Ring-opening reaction:
Condensation reaction:
Ring-opening reaction:
Ring-closure reaction:
So carry out open loop, the cyclic process of closed loop, final reaction at epoxy resin macromolecular.
The epoxy resin is low-molecular-weight epoxy resin, and the concentration of the epoxy resin is 85%.The ring
The ratio of oxygen resin and epoxy hardener is 6:1.The CY-100 is not flatting silica.
The dispersing agent is 750W, and the substrate wetting agents are BYK346.
The defoaming agent is BYK-028.
The anti-flood and anti-float agent is hyper-dispersant, and the epoxy hardener is 8B.
Water-base epoxy dumb light floor coatings of the present invention, due to containing function monomer amido therein by epoxy resin
It can reduce or eliminate the organic pollutant in air, therefore indoor air quality can be improved and VOC is extremely low.The present invention
Described in epoxy resin and epoxy hardener blend proportion be it is optimal, have good hardness and solvent resistance.
Heretofore described various auxiliary agents, the auxiliary agent that can be used using any this field, can directly be bought
It obtains, it can also oneself preparation.
The preparation method of water-base epoxy dumb light floor coatings of the present invention, includes the following steps:
(1) 13 parts of deionized waters, 0.2 part of 750W dispersing agent and 0.2 part of defoaming agent are uniformly mixed, are slowly added to talcum powder
3 parts, 0.3 part of white carbon black, 15 parts of barium sulfate, 15 parts of CY-100, fineness of grind≤35um obtain slurries A；
(2) 30 portions of epoxy hardeners, 0.2 part of anti-flood and anti-float agent, 0.5 part of substrate wetting agents are added into slurries A, mix
It closes and uniformly obtains slurries B.(spare toning)
(3) 15% mill base is added into slurries B, modulates different colors.The as A of water-base epoxy dumb light floor coatings
Component.
(4) epoxy resin is opened into dilute open with aliphatic contracting deionized water glycerin ether in the container of no deionized water cleaning
It is dilute.(wherein the concentration of epoxy resin is 90%), which is uniformly mixed, obtains B component.(A:B=6:1)
Embodiment 2
Embodiment 2 the difference from embodiment 1 is that:
A kind of water-base epoxy dumb light floor coatings of the invention, the water-base epoxy dumb light floor coatings include pressing quality
Following group of number meter is grouped as:
The epoxy resin is low-molecular-weight epoxy resin, and the concentration of the epoxy resin is 90%.
The dispersing agent is BYK190, and the substrate wetting agents are BYK346, the WET510 of Digao and are first created
Three kinds of combination in PW336.
The defoaming agent is two kinds of combination in the SN154 of BYK-024 and Nuo Puke.
The preparation method of water-base epoxy dumb light floor coatings of the present invention, includes the following steps:
In step (1), 13 parts of deionized waters, 0.2 part of 750W dispersing agent and 0.2 part of defoaming agent are uniformly mixed, slowly
3 parts of talcum powder, 0.3 part of white carbon black, 15 parts of barium sulfate, 20 parts of CY-100, fineness of grind≤35um is added and obtains slurries A；
In step (2), 30 portions of epoxy hardeners, 0.2 part of anti-flood and anti-float agent, 0.5 part of substrate profit are added into slurries A
Humectant is uniformly mixed and obtains slurries B.(spare toning)
In step (3), 15% mill base is added into slurries B, modulates different colors, as water-base epoxy dumb light
The component A of level ground coating.
In step (4), by epoxy resin with aliphatic contracting deionized water glycerol in the container of no deionized water cleaning
Ether open it is dilute open it is dilute.(wherein the concentration of resin is 90%), which is uniformly mixed, obtains B component.(A:B=6:1)
Embodiment 3
Embodiment 3 the difference from embodiment 1 is that:
A kind of water-base epoxy dumb light floor coatings of the invention, the water-base epoxy dumb light floor coatings include pressing quality
Following group of number meter is grouped as:
The dispersing agent is 750W or BYK190, and the substrate wetting agents are the WET510 of Digao and first create
Two kinds of combination in PW336；The epoxy resin is low-molecular-weight epoxy resin, and the concentration of the epoxy resin is
95%.
The defoaming agent is two kinds of combination in the SN154 of Nuo Puke and the A10 of BASF.
The epoxy resin is low-molecular-weight epoxy resin, and the concentration of the epoxy resin is 90%.
The preparation method of water-base epoxy dumb light floor coatings of the present invention, includes the following steps:
In step (1), 13 parts of deionized waters, 0.2 part of 750W dispersing agent and 0.2 part of defoaming agent are uniformly mixed, slowly
3 parts of talcum powder, 0.3 part of white carbon black, 15 parts of barium sulfate, 15 parts of CY-100, fineness of grind≤35um is added and obtains slurries A；
In step (2), 30 portions of epoxy hardeners, 0.2 part of anti-flood and anti-float agent, 0.5 part of substrate profit are added into slurries A
Humectant is uniformly mixed and obtains slurries B.(spare toning)
In step (3), 15% mill base is added into slurries B, modulates different colors.As water-base epoxy dumb light
The component A of level ground coating.
In step (4), by epoxy resin with aliphatic contracting deionized water glycerol in the container of no deionized water cleaning
Ether open it is dilute open it is dilute.(wherein the concentration of resin is 90%), which is uniformly mixed, obtains B component.(A:B=10:1)
Embodiment 4
Embodiment 4 the difference from embodiment 1 is that: a kind of water-base epoxy dumb light floor coatings of the invention, the water
Property epoxy dumb light floor coatings include that according to the mass fraction following group is grouped as:
The preparation method of water-base epoxy dumb light floor coatings of the present invention, includes the following steps:
In step (1), 13 parts of deionized waters, 0.2 part of 750W dispersing agent and 0.2 part of defoaming agent are uniformly mixed, slowly
3 parts of talcum powder, 0.3 part of white carbon black, 15 parts of barium sulfate, 15 parts of CY-100, fineness of grind≤35um is added and obtains slurries A；
In step (2), 30 portions of epoxy hardeners, 0.2 part of anti-flood and anti-float agent, 0.5 part of substrate profit are added into slurries A
Humectant is uniformly mixed and obtains slurries B.(spare toning)
In step (3), 15% mill base is added into slurries B, modulates different colors.As water-base epoxy dumb light
The component A of level ground coating.
In step (4), by epoxy resin with aliphatic contracting deionized water glycerol in the container of no deionized water cleaning
Ether open it is dilute open it is dilute.(wherein the concentration of resin is 90%), which is uniformly mixed, obtains B component.(A:B=3:1)
Embodiment 5
Embodiment 5 the difference from embodiment 1 is that: a kind of water-base epoxy dumb light floor coatings of the invention, the water
Property epoxy dumb light floor coatings include that according to the mass fraction following group is grouped as:
The preparation method of water-base epoxy dumb light floor coatings of the present invention, includes the following steps:
In step (1), 13 parts of deionized waters, 0.2 part of FX365 dispersing agent or 731A and 0.2 part of defoaming agent are mixed
Uniformly, it is slowly added to 3 parts of talcum powder, 0.3 part of white carbon black, 15 parts of barium sulfate, CY-100,15 parts, fineness of grind≤35um obtains
Slurries A；
In step (2), 30 portions of epoxy hardeners, 0.2 part of anti-flood and anti-float agent, 0.5 part of substrate profit are added into slurries A
Humectant is uniformly mixed and obtains slurries B.(spare toning)
In step (3), 15% mill base is added into slurries B, modulates different colors.As water-base epoxy dumb light
The component A of level ground coating.
In step (4), by epoxy resin with aliphatic contracting deionized water glycerol in the container of no deionized water cleaning
Ether open it is dilute open it is dilute.(wherein the concentration of resin is 90%), which is uniformly mixed, obtains B component.(A:B=6:1).
Embodiment 6
Embodiment 6 the difference from embodiment 1 is that: a kind of water-base epoxy dumb light floor coatings of the invention, the water
Property epoxy dumb light floor coatings include that according to the mass fraction following group is grouped as:
The preparation method of water-base epoxy dumb light floor coatings of the present invention, includes the following steps:
In step (1), 10 parts of deionized waters, 0.2 part of FX365 dispersing agent and 0.2 part of defoaming agent are uniformly mixed, slowly
3 parts of talcum powder, 0.3 part of white carbon black, 15 parts of barium sulfate, 20 parts of CY-100, fineness of grind≤35um is added and obtains slurries A；
In step (2), 40 portions of epoxy hardeners, 0.1 part of anti-flood and anti-float agent, 0.5 part of substrate profit are added into slurries A
Humectant is uniformly mixed and obtains slurries B；(spare toning)
In step (3), 15% mill base is added into slurries B, modulates different colors, as water-base epoxy dumb light
The component A of level ground coating；
In step (4), by epoxy resin with aliphatic contracting deionized water glycerol in the container of no deionized water cleaning
Ether open it is dilute open it is dilute.(wherein the concentration of resin is 90%), which is uniformly mixed, obtains B component.(A:B=6:1).
Embodiment 7
Embodiment 7 the difference from embodiment 1 is that: a kind of water-base epoxy dumb light floor coatings of the invention, the water
Property epoxy dumb light floor coatings include that according to the mass fraction following group is grouped as:
The preparation method of water-base epoxy dumb light floor coatings of the present invention, includes the following steps:
In step (1), 15 parts of deionized waters, 0.3 part of dispersing agent and 0.3 part of defoaming agent are uniformly mixed, are slowly added to
4 parts of talcum powder, 0.2 part of white carbon black, 20 parts of barium sulfate, 20 parts of CY-100, fineness of grind≤35um obtain slurries A；
In step (2), 35 portions of epoxy hardeners, 0.1 part of anti-flood and anti-float agent, 0.2 part of substrate profit are added into slurries A
Humectant is uniformly mixed and obtains slurries B.(spare toning)
In step (3), 15% mill base is added into slurries B, modulates different colors.As water-base epoxy dumb light
The component A of level ground coating.
In step (4), by epoxy resin with aliphatic contracting deionized water glycerol in the container of no deionized water cleaning
Ether open it is dilute open it is dilute.(wherein the concentration of resin is 90%), which is uniformly mixed, obtains B component.(A:B=6:1).
Test 1
The above case study on implementation is done contrasting detection to obtain, as shown in table 1:
Table 1
As shown in Table 1, wearability of the invention, numerical value is bigger, illustrates that wearability is better, otherwise poorer, floating, number
Value is bigger, illustrates that floating is poorer, otherwise better.
Specific embodiment described herein is only an example for the spirit of the invention.The neck of technology belonging to the present invention
The technical staff in domain can make various modifications or additions to the described embodiments or replace by a similar method
In generation, however, it does not deviate from the spirit of the invention or beyond the scope of the appended claims.
Claims (8)
1. a kind of water-base epoxy dumb light floor coatings, it is characterised in that: the water-base epoxy dumb light floor coatings include pressing matter
Following group of amount number meter is grouped as:
2. water-base epoxy dumb light floor coatings according to claim 1, it is characterised in that: the water-base epoxy dumb light
Level ground coating includes that according to the mass fraction following group is grouped as:
3. water-base epoxy dumb light floor coatings according to claim 1, it is characterised in that: the dispersing agent be 750W or
BYK190, the substrate wetting agents are BYK346, one of the WET510 of Digao or the PW336 that first creates or a variety of groups
It closes；The epoxy resin is low-molecular-weight epoxy resin, and the concentration of the epoxy resin is 85-95%.
4. water-base epoxy dumb light floor coatings according to claim 2, it is characterised in that: the defoaming agent is BYK-
028, the combination of one or more of SN154 of BYK-024, Nuo Puke or the A10 of BASF.
5. water-base epoxy dumb light floor coatings according to claim 2, it is characterised in that: the epoxy resin and epoxy
The ratio of curing agent is 6:1.
6. water-base epoxy dumb light floor coatings according to claim 2, it is characterised in that: the anti-flood and anti-float agent is
Hyper-dispersant, the epoxy hardener are 8B.
7. water-base epoxy dumb light floor coatings according to claim 2, it is characterised in that: the CY-100 is not delustring
Powder.
8. the preparation method of water-base epoxy dumb light floor coatings described in claim 1, it is characterised in that include the following steps:
(1) deionized water, defoaming agent, the anti-floating agent of dispersing agent and substrate wetting agents are uniformly mixed and obtain slurries A；
(2) talcum powder, white carbon black, barium sulfate, CY-100 are added into slurries A, is uniformly mixed and obtains slurries B；
(3) epoxy hardener and levelling agent, uniformly mixed slurries C, as component A are added into slurries B；
(4) epoxy resin is opened in the container of no deionized water cleaning with aliphatic contracting deionized water glycerin ether dilute, mixing is equal
It is even to obtain B component.
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| CN201810608749.2A CN109096866A (en) | 2018-06-13 | 2018-06-13 | A kind of water-base epoxy dumb light floor coatings and preparation method thereof |
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| Application Number | Priority Date | Filing Date | Title |
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| CN201810608749.2A CN109096866A (en) | 2018-06-13 | 2018-06-13 | A kind of water-base epoxy dumb light floor coatings and preparation method thereof |
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| CN110128867A (en) * | 2019-05-14 | 2019-08-16 | 河北晨阳工贸集团有限公司 | A kind of dedicated epoxy putty coating of aqueous terrace and preparation method thereof |
| CN110255971A (en) * | 2019-06-19 | 2019-09-20 | 河北晨阳工贸集团有限公司 | A kind of aqueous terrace phase transformation epoxy resin mortar coating and preparation method thereof |
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| CN110128867A (en) * | 2019-05-14 | 2019-08-16 | 河北晨阳工贸集团有限公司 | A kind of dedicated epoxy putty coating of aqueous terrace and preparation method thereof |
| CN110255971A (en) * | 2019-06-19 | 2019-09-20 | 河北晨阳工贸集团有限公司 | A kind of aqueous terrace phase transformation epoxy resin mortar coating and preparation method thereof |
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Application publication date: 20181228 |
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