CN108975327B - 一种制备活性炭的方法 - Google Patents
一种制备活性炭的方法 Download PDFInfo
- Publication number
- CN108975327B CN108975327B CN201811060025.5A CN201811060025A CN108975327B CN 108975327 B CN108975327 B CN 108975327B CN 201811060025 A CN201811060025 A CN 201811060025A CN 108975327 B CN108975327 B CN 108975327B
- Authority
- CN
- China
- Prior art keywords
- activated carbon
- heating
- camphor
- raw material
- raw materials
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 title claims abstract description 259
- 238000000034 method Methods 0.000 title claims abstract description 18
- 241000723346 Cinnamomum camphora Species 0.000 claims abstract description 67
- 239000002994 raw material Substances 0.000 claims abstract description 61
- 238000010438 heat treatment Methods 0.000 claims abstract description 42
- 210000003608 fece Anatomy 0.000 claims abstract description 34
- 239000010871 livestock manure Substances 0.000 claims abstract description 34
- JIAARYAFYJHUJI-UHFFFAOYSA-L zinc dichloride Chemical compound [Cl-].[Cl-].[Zn+2] JIAARYAFYJHUJI-UHFFFAOYSA-L 0.000 claims abstract description 34
- 238000001035 drying Methods 0.000 claims abstract description 29
- 238000005406 washing Methods 0.000 claims abstract description 27
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 23
- 239000011592 zinc chloride Substances 0.000 claims abstract description 17
- 235000005074 zinc chloride Nutrition 0.000 claims abstract description 17
- 238000010000 carbonizing Methods 0.000 claims abstract description 16
- 238000002791 soaking Methods 0.000 claims abstract description 15
- 239000002253 acid Substances 0.000 claims abstract description 10
- 239000000203 mixture Substances 0.000 claims abstract description 9
- 229910052799 carbon Inorganic materials 0.000 claims abstract description 8
- 238000000197 pyrolysis Methods 0.000 claims abstract description 6
- 239000007788 liquid Substances 0.000 claims abstract 2
- 230000005855 radiation Effects 0.000 claims description 26
- 238000001816 cooling Methods 0.000 claims description 25
- 238000007873 sieving Methods 0.000 claims description 25
- 238000003756 stirring Methods 0.000 claims description 15
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 claims description 13
- 238000004519 manufacturing process Methods 0.000 claims description 7
- 230000008569 process Effects 0.000 claims description 5
- 239000000463 material Substances 0.000 claims description 3
- 238000004140 cleaning Methods 0.000 claims 1
- DSSYKIVIOFKYAU-XCBNKYQSSA-N (R)-camphor Chemical compound C1C[C@@]2(C)C(=O)C[C@@H]1C2(C)C DSSYKIVIOFKYAU-XCBNKYQSSA-N 0.000 abstract description 60
- 229960000846 camphor Drugs 0.000 abstract description 36
- 229930008380 camphor Natural products 0.000 abstract description 36
- 238000001179 sorption measurement Methods 0.000 abstract description 20
- 238000002360 preparation method Methods 0.000 abstract description 5
- 239000000243 solution Substances 0.000 description 17
- 230000007935 neutral effect Effects 0.000 description 11
- 238000005303 weighing Methods 0.000 description 11
- 238000002156 mixing Methods 0.000 description 10
- 238000010298 pulverizing process Methods 0.000 description 5
- RBTBFTRPCNLSDE-UHFFFAOYSA-N 3,7-bis(dimethylamino)phenothiazin-5-ium Chemical compound C1=CC(N(C)C)=CC2=[S+]C3=CC(N(C)C)=CC=C3N=C21 RBTBFTRPCNLSDE-UHFFFAOYSA-N 0.000 description 4
- ZCYVEMRRCGMTRW-UHFFFAOYSA-N 7553-56-2 Chemical compound [I] ZCYVEMRRCGMTRW-UHFFFAOYSA-N 0.000 description 4
- 229910052740 iodine Inorganic materials 0.000 description 4
- 239000011630 iodine Substances 0.000 description 4
- 229960000907 methylthioninium chloride Drugs 0.000 description 4
- 239000002699 waste material Substances 0.000 description 4
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 3
- NBIIXXVUZAFLBC-UHFFFAOYSA-N Phosphoric acid Chemical compound OP(O)(O)=O NBIIXXVUZAFLBC-UHFFFAOYSA-N 0.000 description 2
- 230000003213 activating effect Effects 0.000 description 2
- IWOUKMZUPDVPGQ-UHFFFAOYSA-N barium nitrate Chemical compound [Ba+2].[O-][N+]([O-])=O.[O-][N+]([O-])=O IWOUKMZUPDVPGQ-UHFFFAOYSA-N 0.000 description 2
- 230000009286 beneficial effect Effects 0.000 description 2
- 238000003763 carbonization Methods 0.000 description 2
- YIXJRHPUWRPCBB-UHFFFAOYSA-N magnesium nitrate Chemical compound [Mg+2].[O-][N+]([O-])=O.[O-][N+]([O-])=O YIXJRHPUWRPCBB-UHFFFAOYSA-N 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- UXVMQQNJUSDDNG-UHFFFAOYSA-L Calcium chloride Chemical compound [Cl-].[Cl-].[Ca+2] UXVMQQNJUSDDNG-UHFFFAOYSA-L 0.000 description 1
- 241000196324 Embryophyta Species 0.000 description 1
- GRYLNZFGIOXLOG-UHFFFAOYSA-N Nitric acid Chemical compound O[N+]([O-])=O GRYLNZFGIOXLOG-UHFFFAOYSA-N 0.000 description 1
- 241000557624 Nucifraga Species 0.000 description 1
- 230000004913 activation Effects 0.000 description 1
- 229910000147 aluminium phosphate Inorganic materials 0.000 description 1
- 239000007864 aqueous solution Substances 0.000 description 1
- 239000010426 asphalt Substances 0.000 description 1
- 239000012752 auxiliary agent Substances 0.000 description 1
- 235000013361 beverage Nutrition 0.000 description 1
- 239000001110 calcium chloride Substances 0.000 description 1
- 229910001628 calcium chloride Inorganic materials 0.000 description 1
- 239000003575 carbonaceous material Substances 0.000 description 1
- 239000005539 carbonized material Substances 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 239000003245 coal Substances 0.000 description 1
- 238000009264 composting Methods 0.000 description 1
- 229910000365 copper sulfate Inorganic materials 0.000 description 1
- XTVVROIMIGLXTD-UHFFFAOYSA-N copper(II) nitrate Chemical compound [Cu+2].[O-][N+]([O-])=O.[O-][N+]([O-])=O XTVVROIMIGLXTD-UHFFFAOYSA-N 0.000 description 1
- ARUVKPQLZAKDPS-UHFFFAOYSA-L copper(II) sulfate Chemical compound [Cu+2].[O-][S+2]([O-])([O-])[O-] ARUVKPQLZAKDPS-UHFFFAOYSA-L 0.000 description 1
- 238000001514 detection method Methods 0.000 description 1
- 239000012153 distilled water Substances 0.000 description 1
- 239000003814 drug Substances 0.000 description 1
- 239000000428 dust Substances 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 230000007613 environmental effect Effects 0.000 description 1
- 238000001914 filtration Methods 0.000 description 1
- 230000006872 improvement Effects 0.000 description 1
- 239000012535 impurity Substances 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 229910017604 nitric acid Inorganic materials 0.000 description 1
- 239000002006 petroleum coke Substances 0.000 description 1
- 239000011148 porous material Substances 0.000 description 1
- 238000004537 pulping Methods 0.000 description 1
- 238000004064 recycling Methods 0.000 description 1
- 239000005060 rubber Substances 0.000 description 1
- 239000010902 straw Substances 0.000 description 1
- 238000012795 verification Methods 0.000 description 1
- 239000002023 wood Substances 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B32/00—Carbon; Compounds thereof
- C01B32/30—Active carbon
- C01B32/312—Preparation
- C01B32/318—Preparation characterised by the starting materials
- C01B32/324—Preparation characterised by the starting materials from waste materials, e.g. tyres or spent sulfite pulp liquor
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B32/00—Carbon; Compounds thereof
- C01B32/30—Active carbon
- C01B32/312—Preparation
- C01B32/342—Preparation characterised by non-gaseous activating agents
- C01B32/348—Metallic compounds
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Environmental & Geological Engineering (AREA)
- Materials Engineering (AREA)
- Carbon And Carbon Compounds (AREA)
- Solid-Sorbent Or Filter-Aiding Compositions (AREA)
Abstract
Description
Claims (6)
Priority Applications (1)
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CN201811060025.5A CN108975327B (zh) | 2018-09-12 | 2018-09-12 | 一种制备活性炭的方法 |
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CN201811060025.5A CN108975327B (zh) | 2018-09-12 | 2018-09-12 | 一种制备活性炭的方法 |
Publications (2)
Publication Number | Publication Date |
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CN108975327A CN108975327A (zh) | 2018-12-11 |
CN108975327B true CN108975327B (zh) | 2022-04-22 |
Family
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Family Applications (1)
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CN201811060025.5A Active CN108975327B (zh) | 2018-09-12 | 2018-09-12 | 一种制备活性炭的方法 |
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CN (1) | CN108975327B (zh) |
Families Citing this family (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN111408349A (zh) * | 2020-04-30 | 2020-07-14 | 南阳师范学院 | 一种秸秆基磁性多孔生物炭的制备方法 |
CN111874905A (zh) * | 2020-07-13 | 2020-11-03 | 宁夏新龙蓝天科技股份有限公司 | 一种新型活性炭工艺 |
CN111924823A (zh) * | 2020-07-30 | 2020-11-13 | 盐城工学院 | 一种基于鸟粪的电极材料的制备 |
CN113877479A (zh) * | 2021-09-15 | 2022-01-04 | 西南科技大学 | 一种基于不同基因型梁山慈竹制备水热炭的方法及吸附应用 |
Citations (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN101618871A (zh) * | 2009-03-27 | 2010-01-06 | 新疆大学 | 一种用杏核壳制备活性炭的方法 |
CN108190884A (zh) * | 2018-01-30 | 2018-06-22 | 武汉科技大学 | 一种以树叶为模板制备多级孔活性炭的方法 |
Family Cites Families (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN104803383B (zh) * | 2015-04-13 | 2017-08-22 | 中南大学 | 一种利用樟树叶制备超级电容器活性炭的方法 |
CN108264044B (zh) * | 2018-04-26 | 2019-11-01 | 济南大学 | 一种碱蓬基超微粉压块活性炭及其制备方法 |
-
2018
- 2018-09-12 CN CN201811060025.5A patent/CN108975327B/zh active Active
Patent Citations (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN101618871A (zh) * | 2009-03-27 | 2010-01-06 | 新疆大学 | 一种用杏核壳制备活性炭的方法 |
CN108190884A (zh) * | 2018-01-30 | 2018-06-22 | 武汉科技大学 | 一种以树叶为模板制备多级孔活性炭的方法 |
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CN108975327A (zh) | 2018-12-11 |
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TR01 | Transfer of patent right |
Effective date of registration: 20221107 Address after: 237011 Jingliu Road, Lu'an Economic and Technological Development Zone, Anhui Province Patentee after: Anhui Chuangyu New Material Technology Co.,Ltd. Address before: No. 1638 Wolong Road, Wolong District, Nanyang City, Henan Province Patentee before: Nanyang Normal University |
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PE01 | Entry into force of the registration of the contract for pledge of patent right |
Denomination of invention: A method for preparing activated carbon Granted publication date: 20220422 Pledgee: Huishang Bank Co.,Ltd. Lu'an Gaocheng road sub branch Pledgor: Anhui Chuangyu New Material Technology Co.,Ltd. Registration number: Y2024980005350 |
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