CN108968165A - A method of improving electronic cigarette and aspirates strength - Google Patents
A method of improving electronic cigarette and aspirates strength Download PDFInfo
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- CN108968165A CN108968165A CN201811179290.5A CN201811179290A CN108968165A CN 108968165 A CN108968165 A CN 108968165A CN 201811179290 A CN201811179290 A CN 201811179290A CN 108968165 A CN108968165 A CN 108968165A
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- China
- Prior art keywords
- cotinine
- nicotine
- sense
- cigarette
- alkaloids
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- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
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- 239000003571 electronic cigarette Substances 0.000 title claims abstract description 29
- 238000000034 method Methods 0.000 title claims abstract description 19
- 241000208125 Nicotiana Species 0.000 claims abstract description 60
- 229930013930 alkaloid Natural products 0.000 claims abstract description 54
- UIKROCXWUNQSPJ-VIFPVBQESA-N (-)-cotinine Chemical compound C1CC(=O)N(C)[C@@H]1C1=CC=CN=C1 UIKROCXWUNQSPJ-VIFPVBQESA-N 0.000 claims abstract description 49
- UIKROCXWUNQSPJ-UHFFFAOYSA-N Cotinine Natural products C1CC(=O)N(C)C1C1=CC=CN=C1 UIKROCXWUNQSPJ-UHFFFAOYSA-N 0.000 claims abstract description 49
- 229950006073 cotinine Drugs 0.000 claims abstract description 49
- SNICXCGAKADSCV-JTQLQIEISA-N (-)-Nicotine Chemical compound CN1CCC[C@H]1C1=CC=CN=C1 SNICXCGAKADSCV-JTQLQIEISA-N 0.000 claims abstract description 45
- SNICXCGAKADSCV-UHFFFAOYSA-N nicotine Natural products CN1CCCC1C1=CC=CN=C1 SNICXCGAKADSCV-UHFFFAOYSA-N 0.000 claims abstract description 45
- 229960002715 nicotine Drugs 0.000 claims abstract description 45
- 235000019504 cigarettes Nutrition 0.000 claims abstract description 33
- 230000014860 sensory perception of taste Effects 0.000 claims abstract description 32
- 239000000779 smoke Substances 0.000 claims abstract description 29
- 235000002637 Nicotiana tabacum Nutrition 0.000 claims abstract description 27
- 235000011389 fruit/vegetable juice Nutrition 0.000 claims abstract description 20
- 239000003795 chemical substances by application Substances 0.000 claims abstract description 11
- 238000006467 substitution reaction Methods 0.000 claims abstract description 5
- 238000004458 analytical method Methods 0.000 claims abstract description 3
- 239000000654 additive Substances 0.000 claims description 20
- 230000000996 additive effect Effects 0.000 claims description 20
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 claims description 15
- DNIAPMSPPWPWGF-UHFFFAOYSA-N Propylene glycol Chemical compound CC(O)CO DNIAPMSPPWPWGF-UHFFFAOYSA-N 0.000 claims description 15
- 238000004445 quantitative analysis Methods 0.000 claims description 6
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 5
- 238000006243 chemical reaction Methods 0.000 claims description 3
- 230000005611 electricity Effects 0.000 claims description 2
- 239000000796 flavoring agent Substances 0.000 abstract description 2
- 235000019634 flavors Nutrition 0.000 abstract description 2
- 230000006872 improvement Effects 0.000 abstract description 2
- 230000008569 process Effects 0.000 abstract description 2
- DPNGWXJMIILTBS-UHFFFAOYSA-N myosmine Chemical compound C1CCN=C1C1=CC=CN=C1 DPNGWXJMIILTBS-UHFFFAOYSA-N 0.000 description 6
- MYKUKUCHPMASKF-VIFPVBQESA-N (S)-nornicotine Chemical compound C1CCN[C@@H]1C1=CC=CN=C1 MYKUKUCHPMASKF-VIFPVBQESA-N 0.000 description 5
- MYKUKUCHPMASKF-UHFFFAOYSA-N Nornicotine Natural products C1CCNC1C1=CC=CN=C1 MYKUKUCHPMASKF-UHFFFAOYSA-N 0.000 description 5
- RYFOJXFXERAMLS-UHFFFAOYSA-N Nicotyrine Chemical compound CN1C=CC=C1C1=CC=CN=C1 RYFOJXFXERAMLS-UHFFFAOYSA-N 0.000 description 4
- 239000003513 alkali Substances 0.000 description 4
- 235000019658 bitter taste Nutrition 0.000 description 4
- 235000009508 confectionery Nutrition 0.000 description 4
- 238000002290 gas chromatography-mass spectrometry Methods 0.000 description 4
- 230000000638 stimulation Effects 0.000 description 3
- SOPPBXUYQGUQHE-JTQLQIEISA-N Anatabine Chemical compound C1C=CCN[C@@H]1C1=CC=CN=C1 SOPPBXUYQGUQHE-JTQLQIEISA-N 0.000 description 2
- SOPPBXUYQGUQHE-UHFFFAOYSA-N Anatabine Natural products C1C=CCNC1C1=CC=CN=C1 SOPPBXUYQGUQHE-UHFFFAOYSA-N 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 238000005516 engineering process Methods 0.000 description 2
- 239000003205 fragrance Substances 0.000 description 2
- 238000004519 manufacturing process Methods 0.000 description 2
- 235000019640 taste Nutrition 0.000 description 2
- 235000019505 tobacco product Nutrition 0.000 description 2
- MTXSIJUGVMTTMU-JTQLQIEISA-N (S)-anabasine Chemical compound N1CCCC[C@H]1C1=CC=CN=C1 MTXSIJUGVMTTMU-JTQLQIEISA-N 0.000 description 1
- 206010007269 Carcinogenicity Diseases 0.000 description 1
- 208000024172 Cardiovascular disease Diseases 0.000 description 1
- 206010012335 Dependence Diseases 0.000 description 1
- 241000195955 Equisetum hyemale Species 0.000 description 1
- 150000003797 alkaloid derivatives Chemical class 0.000 description 1
- 229930014345 anabasine Natural products 0.000 description 1
- 230000003542 behavioural effect Effects 0.000 description 1
- 230000008901 benefit Effects 0.000 description 1
- 210000004556 brain Anatomy 0.000 description 1
- 230000007670 carcinogenicity Effects 0.000 description 1
- 231100000260 carcinogenicity Toxicity 0.000 description 1
- 238000011156 evaluation Methods 0.000 description 1
- 238000001727 in vivo Methods 0.000 description 1
- 239000004615 ingredient Substances 0.000 description 1
- 238000002156 mixing Methods 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 210000005036 nerve Anatomy 0.000 description 1
- 230000001766 physiological effect Effects 0.000 description 1
- 230000035790 physiological processes and functions Effects 0.000 description 1
- 229930010796 primary metabolite Natural products 0.000 description 1
- 238000005086 pumping Methods 0.000 description 1
- 230000011514 reflex Effects 0.000 description 1
- 235000019605 sweet taste sensations Nutrition 0.000 description 1
Classifications
-
- A24F47/008—
Landscapes
- Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
- Other Investigation Or Analysis Of Materials By Electrical Means (AREA)
Abstract
The present invention provides a kind of method of improvement electronic cigarette suction strength, and the content data that means obtain conventional cigarette nicotiana alkaloids is determined by analysis；Then, the related alkaloids in addition to nicotine are substituted using cotinine, the sense of taste contribution margin of cotinine after substituting is made to be equal to the sum of related alkaloids sense of taste contribution margin；Finally, electronic smoke agent is added in nicotine and cotinine, tobacco juice for electronic smoke is made.The present invention takes into account contribution of all nicotiana alkaloids to electronic cigarette suction strength, and the tobacco juice for electronic smoke of allotment reaches the suction strength of conventional cigarette, can improve the flavor of electronic cigarette；The present invention realizes the substitution of cotinine and other nicotiana alkaloids according to sense of taste contribution margin, and using only nicotine and cotinine when allotment, process is easy to operate.
Description
Technical field
The present invention relates to tobacco product fragrance field, specifically a kind of method for improving electronic cigarette suction strength.
Background technique
Nicotiana alkaloids is important tobacco and smoke chemistry ingredient, including nicotine, nornicotine, anatabine, false scouring rush
Alkali, myosmine, cotinine, nicotyrine, nicotimine etc..Nicotiana alkaloids is not only to measure the key factor of quality of tobacco, together
When be also tobacco product pleasant feeling and satisfaction source (Tobacco:Production, chemistry and
Technology, Blackwell Science, Oxford, 1999).Nicotine and nornicotine have an alkaline breath, but nornicotine
Intensity is low.Nicotine has peppery sense, and the peppery sense of nornicotine is lowered and with faint bitter taste.Anatabine, anabasine and myosmine have
Tingle and bitter taste.Cotinine, nicotyrine and nicotimine have bitter taste but without peppery senses, and cotinine then has weak sweet taste, such as table 1
Shown (tobacco science and technology, 2016,49,36).
The taste characteristics of 1 nicotiana alkaloids of table and perceive threshold value
In order to make the suction strength of electronic cigarette be close to or up to the suction strength of cigarette, often added in tobacco juice for electronic smoke
Nicotiana alkaloids.However, the type and content of nicotiana alkaloids are widely different in commercially available electronic cigarette, lead to electronic cigarette
Suction strength has very big difference, and nicotiana alkaloids such as nornicotine has ill effect to the suction quality of electronic cigarette；In addition, tobacco
The source of alkaloid and purity are different, and there are also carcinogenicities, such as myosmine for some.In recent years, it has been found that cotinine is not only
Satisfaction with similar nicotine stimulation nerve；In addition, cotinine does not cause cardiovascular disease not only and causes addiction compared with nicotine
Property, also with antidepression and the curative effect (Behavioural Brain Research, 2014,268,55) relieved stress.
The present inventor has found after study in the implementation of the present invention: having strong alkaline breath and peppery in view of nicotine
Sense, cotinine does not have peppery sense but has bitter taste, and the physiological function with nicotine, therefore deploys electronic cigarette with nicotine and cotinine
The nicotiana alkaloids used, and the related alkaloids except nicotine are substituted with cotinine, the suction strength of electronic cigarette can not only be improved
Head additionally aids the standardization production of tobacco juice for electronic smoke.
Summary of the invention
The object of the present invention is to provide a kind of methods of improvement electronic cigarette suction strength, are adjusted using nicotine and cotinine
The related alkaloids in addition to nicotine are substituted with nicotiana alkaloids used in electronic cigarette, and with cotinine, to eliminate biological tobacco
Bad fragrance and the sense of taste caused by alkali reduce harmful components, improve the suction strength of electronic cigarette, while electronic cigarette being kept to aspirate strength
Head has stability.
Above-mentioned purpose of the present invention is achieved by the following technical programs:
A method of improving electronic cigarette and aspirate strength, includes the following steps: to obtain often firstly, means are determined by analysis
Advise the content of nicotiana alkaloids in cigarette；Then, the related alkaloids in addition to nicotine are substituted using cotinine, making can after substituting
It is equal to the sum of the related alkaloids sense of taste contribution margin in addition to nicotine for peaceful sense of taste contribution margin；Finally, by nicotine and cotinine
Electronic smoke agent is added, tobacco juice for electronic smoke is made.
Further, specific step is as follows for the method:
(1) quantitative analysis method is used, determines that the content of nicotiana alkaloids in conventional cigarette, content unit are defined as micro-
Gram/cigarette (mg/cig)；
(2) ratio that threshold value is perceived according to the content and the sense of taste of sense of taste contribution margin namely nicotiana alkaloids, uses cotinine
The related alkaloids in addition to nicotine are substituted, the sense of taste for making the sense of taste contribution margin of cotinine after substituting be equal to related alkaloids is contributed
The sum of value, using the cotinine amount after conversion as the foundation of additive amount；
(3) additive amount that above-mentioned cotinine is deducted from the nicotine content of conventional cigarette, as nicotine in tobacco juice for electronic smoke
The foundation of additive amount；
C(nicotine in electronic cigarette)=C(Nicotine from Cigarette)-C(conversion cotinine)
Cotinine equally causes suction strength with nicotine, in addition, primary metabolite of the cotinine as nicotine in vivo, tool
There is the identical physiological activity of nicotine.Human physiological reaction caused by nicotine is mainly caused by cotinine, in order to keep electronic cigarette with
The consistency of conventional cigarette strength, therefore operation in this way.
(4) by glycerol, propylene glycol and water mix, electronic smoke agent is made, by step (3) determine nicotine additive amount and
Electronic smoke agent is added in the cotinine additive amount that step (2) determines, the tobacco juice for electronic smoke of 10-15mg/mL is made into, by above-mentioned electricity
Sub- cigarette tobacco juice is added in electronic cigarette, balances 0.5-1h at room temperature, then perfumer evaluates.
Tune of the present invention has the advantage that
1, the present invention takes into account contribution of all nicotiana alkaloids to electronic cigarette suction strength, and the tobacco juice for electronic smoke of allotment reaches
The suction strength of conventional cigarette, can improve the flavor of electronic cigarette；
2, the present invention realizes the substitution of cotinine and other nicotiana alkaloids according to sense of taste contribution margin, using only cigarette when allotment
Alkali and cotinine, process are easy to operate.
Specific embodiment
The present invention is described further with reference to embodiments, but is not limited the scope of the invention in any way.
Embodiment 1
By GC-MS quantitative analysis method measure #1 conventional cigarette in nicotiana alkaloids content, unit be defined as microgram/
Cigarette (mg/cig)；The ratio that threshold value is perceived by the content and the sense of taste that calculate nicotiana alkaloids, obtains the taste of nicotiana alkaloids
Feel contribution margin, as shown in table 2.In addition to nicotine, the sense of taste contribution margin of related alkaloids is 210+68+130+160=568.It can
When for peaceful substitution related alkaloids, additive amount is 568/2=284 times of cotinine, therefore cotinine additive amount is 0.001mg
× 284=0.284mg, nicotine additive amount are 0.716mg.Nicotine and cotinine are added to glycerol, propylene glycol and water in proportion
It is mixed in electronic smoke agent, is made into the tobacco juice for electronic smoke of 10mg/mL, above-mentioned tobacco juice for electronic smoke is added in electronic cigarette,
0.5h is balanced at room temperature, and then 5 perfumers evaluate.Compared with cigarette, all valuation officers think no obvious stimulation, nothing
Sweet sense, suction strength reach the suction strength of cigarette.
The content and sense of taste contribution margin of nicotiana alkaloids in table 2#1 cigarette
Embodiment 2
The content of nicotiana alkaloids in #2 conventional cigarette is measured by GC-MS quantitative analysis method；Calculate nicotiana alkaloids
Content and the sense of taste perceive the ratio of threshold value, obtain the sense of taste contribution margin of nicotiana alkaloids, be shown in Table 3.In addition to nicotine, other lifes
The sense of taste contribution margin of alkaloids is 253+52+150+200+10=665.When cotinine substitutes related alkaloids, additive amount is can
For peaceful 665/2=333 times, therefore cotinine additive amount is 0.001mg × 328=0.333mg, and nicotine additive amount is
0.767mg.Nicotine and cotinine are added to glycerol, propylene glycol and water to be mixed in electronic smoke agent in proportion, are made into
Above-mentioned tobacco juice for electronic smoke is added in electronic cigarette, balances 0.5h at room temperature, then 5 perfumers by the tobacco juice for electronic smoke of 12mg/mL
It is evaluated.Compared with cigarette, all valuation officers think that no obvious stimulation, no sweet sense, suction strength reach the pumping of cigarette
Inhale strength.
The content and sense of taste contribution margin of nicotiana alkaloids in table 3#2 cigarette
Embodiment 3
The content of nicotiana alkaloids in #3 conventional cigarette is measured by GC-MS quantitative analysis method, calculates nicotiana alkaloids
Content and the sense of taste perceive the ratio of threshold value, obtain their sense of taste contribution margin, as shown in table 4.In addition to nicotine, other biological
The sense of taste contribution margin of alkali is 293+48+180+110+10=641.When cotinine substitutes related alkaloids, additive amount is that can replace
Peaceful 641/4=160 times, therefore cotinine additive amount is 0.002mg × 160=0.641mg, nicotine additive amount is 0.459mg.
Nicotine and cotinine are added in proportion in electronic smoke agent, the tobacco juice for electronic smoke of 10mg/mL is made into, then 5 blending
Shi Jinhang evaluation.Compared with cigarette, all valuation officers think that no sweet sense, suction strength reach the suction strength of cigarette.
The content and sense of taste contribution margin of nicotiana alkaloids in table 4#3 cigarette
Embodiment 4
The content that nicotiana alkaloids in #4 conventional cigarette is measured by GC-MS quantitative analysis method, it is raw by calculating tobacco
The content and the sense of taste of alkaloids perceive the ratio of threshold value, obtain the sense of taste contribution margin of nicotiana alkaloids, as shown in table 5.Except nicotine it
Outside, the sense of taste contribution margin of related alkaloids is 283+87+160+180=710.When cotinine substitutes related alkaloids, addition
Amount is 710/2=350 times of cotinine, therefore cotinine additive amount is 0.001mg × 350=0.350mg, and nicotine additive amount is
0.850mg.Nicotine and cotinine are added to glycerol, propylene glycol and water to be mixed in electronic smoke agent in proportion, are made into
Above-mentioned tobacco juice for electronic smoke is added in electronic cigarette, balances 0.5h at room temperature, then 5 perfumers by the tobacco juice for electronic smoke of 12mg/mL
It is evaluated.Compared with cigarette, all valuation officers think that no sweet sense, suction strength reach the suction strength of cigarette.
The content and sense of taste contribution margin of nicotiana alkaloids in table 5#4 cigarette
The above description is merely a specific embodiment, but scope of protection of the present invention is not limited thereto, any
Belong to those skilled in the art in the technical scope disclosed by the present invention, any changes or substitutions that can be easily thought of, all answers
It is included within the scope of the present invention.Therefore, protection scope of the present invention should be subject to the protection scope in claims.
Claims (2)
1. a kind of method for improving electronic cigarette suction strength, it is characterised in that include the following steps: that means, which are determined by analysis, to be obtained
Obtain the content data of conventional cigarette nicotiana alkaloids；Then, the related alkaloids in addition to nicotine are substituted using cotinine, makes to replace
It is equal to the sum of related alkaloids sense of taste contribution margin for the sense of taste contribution margin of rear cotinine；Finally, electricity is added in nicotine and cotinine
Sub- smog agent, is made tobacco juice for electronic smoke.
2. the method according to claim 1 for improving electronic cigarette suction strength, it is characterised in that: the specific step of the method
It is rapid as follows:
(1) quantitative analysis method is used, determines that the content of nicotiana alkaloids in conventional cigarette, content unit are defined as microgram/cigarette
Branch；
(2) ratio that threshold value is perceived according to the content and the sense of taste of sense of taste contribution margin namely nicotiana alkaloids, is substituted using cotinine
Related alkaloids in addition to nicotine, make substitution after cotinine sense of taste contribution margin be equal to related alkaloids sense of taste contribution margin it
With using the cotinine amount after conversion as the foundation of additive amount；
(3) additive amount that above-mentioned cotinine is deducted from the nicotine content of conventional cigarette is added as nicotine in tobacco juice for electronic smoke
The foundation of amount；
(4) glycerol, propylene glycol and water are mixed, electronic smoke agent is made, the nicotine additive amount and step that step (3) are determined
(2) electronic smoke agent is added in the cotinine additive amount determined, the tobacco juice for electronic smoke of 10-15mg/mL is made into, by above-mentioned electronic cigarette
Tobacco juice is added in electronic cigarette, balances 0.5-1h at room temperature.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201811179290.5A CN108968165A (en) | 2018-10-10 | 2018-10-10 | A method of improving electronic cigarette and aspirates strength |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201811179290.5A CN108968165A (en) | 2018-10-10 | 2018-10-10 | A method of improving electronic cigarette and aspirates strength |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN108968165A true CN108968165A (en) | 2018-12-11 |
Family
ID=64543431
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
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| CN201811179290.5A Pending CN108968165A (en) | 2018-10-10 | 2018-10-10 | A method of improving electronic cigarette and aspirates strength |
Country Status (1)
| Country | Link |
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Cited By (3)
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| GB2595967A (en) * | 2020-05-01 | 2021-12-15 | Exhale Tech Ltd | Composition and use thereof |
| CN114732148A (en) * | 2022-04-18 | 2022-07-12 | 汪冶 | Application of anabasine in heating non-combustion electron delivery product, solid-state slice and preparation method thereof |
| CN114831335A (en) * | 2022-04-15 | 2022-08-02 | 汪冶 | Application of anabasine in atomized electronic delivery product |
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