CN101856144A - Method for improving quality of cigarette tobacco shreds - Google Patents
Method for improving quality of cigarette tobacco shreds Download PDFInfo
- Publication number
- CN101856144A CN101856144A CN 201010196979 CN201010196979A CN101856144A CN 101856144 A CN101856144 A CN 101856144A CN 201010196979 CN201010196979 CN 201010196979 CN 201010196979 A CN201010196979 A CN 201010196979A CN 101856144 A CN101856144 A CN 101856144A
- Authority
- CN
- China
- Prior art keywords
- tobacco
- cigarette
- malate
- tobacco leaf
- shreds
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 241000208125 Nicotiana Species 0.000 title claims abstract description 64
- 235000002637 Nicotiana tabacum Nutrition 0.000 title claims abstract description 64
- 235000019504 cigarettes Nutrition 0.000 title claims abstract description 40
- 238000000034 method Methods 0.000 title claims abstract description 24
- BJEPYKJPYRNKOW-UHFFFAOYSA-N malic acid Chemical compound OC(=O)C(O)CC(O)=O BJEPYKJPYRNKOW-UHFFFAOYSA-N 0.000 claims abstract description 22
- 239000001630 malic acid Substances 0.000 claims abstract description 16
- 235000011090 malic acid Nutrition 0.000 claims abstract description 16
- BJEPYKJPYRNKOW-REOHCLBHSA-N (S)-malic acid Chemical compound OC(=O)[C@@H](O)CC(O)=O BJEPYKJPYRNKOW-REOHCLBHSA-N 0.000 claims abstract description 15
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 12
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims abstract description 8
- 229940049920 malate Drugs 0.000 claims abstract description 8
- 239000011259 mixed solution Substances 0.000 claims abstract description 6
- 239000000243 solution Substances 0.000 claims description 12
- PXHVJJICTQNCMI-UHFFFAOYSA-N Nickel Chemical compound [Ni] PXHVJJICTQNCMI-UHFFFAOYSA-N 0.000 claims description 8
- WHXSMMKQMYFTQS-UHFFFAOYSA-N Lithium Chemical compound [Li] WHXSMMKQMYFTQS-UHFFFAOYSA-N 0.000 claims description 7
- 229910052744 lithium Inorganic materials 0.000 claims description 7
- 239000011575 calcium Substances 0.000 claims description 5
- 239000010949 copper Substances 0.000 claims description 5
- 239000000126 substance Substances 0.000 claims description 5
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 claims description 4
- 229910052791 calcium Inorganic materials 0.000 claims description 4
- 229910052802 copper Inorganic materials 0.000 claims description 4
- 125000000524 functional group Chemical group 0.000 claims description 4
- 239000011777 magnesium Substances 0.000 claims description 4
- 229910052750 molybdenum Inorganic materials 0.000 claims description 4
- 229910052759 nickel Inorganic materials 0.000 claims description 4
- 238000012545 processing Methods 0.000 claims description 4
- 239000007921 spray Substances 0.000 claims description 4
- 238000003860 storage Methods 0.000 claims description 4
- OYPRJOBELJOOCE-UHFFFAOYSA-N Calcium Chemical compound [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 claims description 3
- RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 claims description 3
- ZOKXTWBITQBERF-UHFFFAOYSA-N Molybdenum Chemical compound [Mo] ZOKXTWBITQBERF-UHFFFAOYSA-N 0.000 claims description 3
- 229910052790 beryllium Inorganic materials 0.000 claims description 3
- ATBAMAFKBVZNFJ-UHFFFAOYSA-N beryllium atom Chemical compound [Be] ATBAMAFKBVZNFJ-UHFFFAOYSA-N 0.000 claims description 3
- 229910052739 hydrogen Inorganic materials 0.000 claims description 3
- 229910052749 magnesium Inorganic materials 0.000 claims description 3
- 230000004048 modification Effects 0.000 claims description 3
- 238000012986 modification Methods 0.000 claims description 3
- 239000011733 molybdenum Substances 0.000 claims description 3
- 229910052700 potassium Inorganic materials 0.000 claims description 3
- 239000011734 sodium Substances 0.000 claims description 3
- 239000011701 zinc Substances 0.000 claims description 3
- 229910052725 zinc Inorganic materials 0.000 claims description 3
- QGZKDVFQNNGYKY-UHFFFAOYSA-O Ammonium Chemical compound [NH4+] QGZKDVFQNNGYKY-UHFFFAOYSA-O 0.000 claims description 2
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 claims description 2
- FYYHWMGAXLPEAU-UHFFFAOYSA-N Magnesium Chemical compound [Mg] FYYHWMGAXLPEAU-UHFFFAOYSA-N 0.000 claims description 2
- ZLMJMSJWJFRBEC-UHFFFAOYSA-N Potassium Chemical compound [K] ZLMJMSJWJFRBEC-UHFFFAOYSA-N 0.000 claims description 2
- HCHKCACWOHOZIP-UHFFFAOYSA-N Zinc Chemical compound [Zn] HCHKCACWOHOZIP-UHFFFAOYSA-N 0.000 claims description 2
- 239000004411 aluminium Substances 0.000 claims description 2
- 229910052782 aluminium Inorganic materials 0.000 claims description 2
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 claims description 2
- 125000004432 carbon atom Chemical group C* 0.000 claims description 2
- 239000001257 hydrogen Substances 0.000 claims description 2
- 229910052742 iron Inorganic materials 0.000 claims description 2
- WPBNNNQJVZRUHP-UHFFFAOYSA-L manganese(2+);methyl n-[[2-(methoxycarbonylcarbamothioylamino)phenyl]carbamothioyl]carbamate;n-[2-(sulfidocarbothioylamino)ethyl]carbamodithioate Chemical compound [Mn+2].[S-]C(=S)NCCNC([S-])=S.COC(=O)NC(=S)NC1=CC=CC=C1NC(=S)NC(=O)OC WPBNNNQJVZRUHP-UHFFFAOYSA-L 0.000 claims description 2
- 239000011591 potassium Substances 0.000 claims description 2
- 238000007670 refining Methods 0.000 claims description 2
- 229910052708 sodium Inorganic materials 0.000 claims description 2
- 125000004435 hydrogen atom Chemical class [H]* 0.000 claims 1
- 230000000391 smoking effect Effects 0.000 abstract description 15
- 238000012360 testing method Methods 0.000 abstract description 5
- UGFAIRIUMAVXCW-UHFFFAOYSA-N Carbon monoxide Chemical compound [O+]#[C-] UGFAIRIUMAVXCW-UHFFFAOYSA-N 0.000 description 18
- 239000003546 flue gas Substances 0.000 description 18
- 239000000523 sample Substances 0.000 description 17
- SNICXCGAKADSCV-JTQLQIEISA-N (-)-Nicotine Chemical compound CN1CCC[C@H]1C1=CC=CN=C1 SNICXCGAKADSCV-JTQLQIEISA-N 0.000 description 11
- 239000012496 blank sample Substances 0.000 description 11
- 229960002715 nicotine Drugs 0.000 description 11
- SNICXCGAKADSCV-UHFFFAOYSA-N nicotine Natural products CN1CCCC1C1=CC=CN=C1 SNICXCGAKADSCV-UHFFFAOYSA-N 0.000 description 11
- SVICABYXKQIXBM-UHFFFAOYSA-L potassium malate Chemical compound [K+].[K+].[O-]C(=O)C(O)CC([O-])=O SVICABYXKQIXBM-UHFFFAOYSA-L 0.000 description 11
- 239000011269 tar Substances 0.000 description 8
- CLWNPUARORRDFD-UHFFFAOYSA-N 2-hydroxybutanedioic acid;zinc Chemical compound [Zn].OC(=O)C(O)CC(O)=O CLWNPUARORRDFD-UHFFFAOYSA-N 0.000 description 6
- 239000001362 calcium malate Substances 0.000 description 6
- OLOZVPHKXALCRI-UHFFFAOYSA-L calcium malate Chemical compound [Ca+2].[O-]C(=O)C(O)CC([O-])=O OLOZVPHKXALCRI-UHFFFAOYSA-L 0.000 description 6
- 229940016114 calcium malate Drugs 0.000 description 6
- 235000011038 calcium malates Nutrition 0.000 description 6
- 238000005516 engineering process Methods 0.000 description 6
- 239000007864 aqueous solution Substances 0.000 description 5
- 230000008569 process Effects 0.000 description 5
- 230000001953 sensory effect Effects 0.000 description 5
- 239000011573 trace mineral Substances 0.000 description 5
- 235000013619 trace mineral Nutrition 0.000 description 5
- 230000006872 improvement Effects 0.000 description 4
- 238000004519 manufacturing process Methods 0.000 description 4
- 239000001415 potassium malate Substances 0.000 description 4
- 235000011033 potassium malate Nutrition 0.000 description 4
- 238000005303 weighing Methods 0.000 description 4
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 description 3
- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 description 3
- 239000011285 coke tar Substances 0.000 description 3
- 230000000694 effects Effects 0.000 description 3
- 238000000855 fermentation Methods 0.000 description 3
- 230000004151 fermentation Effects 0.000 description 3
- 235000013305 food Nutrition 0.000 description 3
- 238000004868 gas analysis Methods 0.000 description 3
- JFQQIWNDAXACSR-UHFFFAOYSA-L magnesium malate Chemical compound [Mg+2].[O-]C(=O)C(O)CC([O-])=O JFQQIWNDAXACSR-UHFFFAOYSA-L 0.000 description 3
- 229940096424 magnesium malate Drugs 0.000 description 3
- 239000011572 manganese Substances 0.000 description 3
- 239000000779 smoke Substances 0.000 description 3
- VZCYOOQTPOCHFL-OWOJBTEDSA-N Fumaric acid Chemical compound OC(=O)\C=C\C(O)=O VZCYOOQTPOCHFL-OWOJBTEDSA-N 0.000 description 2
- 238000004458 analytical method Methods 0.000 description 2
- 239000004567 concrete Substances 0.000 description 2
- 238000001514 detection method Methods 0.000 description 2
- 238000011156 evaluation Methods 0.000 description 2
- 239000000796 flavoring agent Substances 0.000 description 2
- 235000019634 flavors Nutrition 0.000 description 2
- 239000003517 fume Substances 0.000 description 2
- JVTAAEKCZFNVCJ-UHFFFAOYSA-N lactic acid Chemical compound CC(O)C(O)=O JVTAAEKCZFNVCJ-UHFFFAOYSA-N 0.000 description 2
- 229910052748 manganese Inorganic materials 0.000 description 2
- 150000007524 organic acids Chemical class 0.000 description 2
- 241000196324 Embryophyta Species 0.000 description 1
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 description 1
- PWHULOQIROXLJO-UHFFFAOYSA-N Manganese Chemical compound [Mn] PWHULOQIROXLJO-UHFFFAOYSA-N 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 238000005273 aeration Methods 0.000 description 1
- 229910021529 ammonia Inorganic materials 0.000 description 1
- 230000002929 anti-fatigue Effects 0.000 description 1
- 230000004888 barrier function Effects 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000008901 benefit Effects 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 229910052796 boron Inorganic materials 0.000 description 1
- 239000004566 building material Substances 0.000 description 1
- 239000000920 calcium hydroxide Substances 0.000 description 1
- 235000011116 calcium hydroxide Nutrition 0.000 description 1
- 229910052799 carbon Inorganic materials 0.000 description 1
- 230000008859 change Effects 0.000 description 1
- 229910052801 chlorine Inorganic materials 0.000 description 1
- 239000000460 chlorine Substances 0.000 description 1
- 239000002131 composite material Substances 0.000 description 1
- 235000013409 condiments Nutrition 0.000 description 1
- 230000007423 decrease Effects 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 239000003814 drug Substances 0.000 description 1
- 238000001035 drying Methods 0.000 description 1
- 238000000605 extraction Methods 0.000 description 1
- 238000011049 filling Methods 0.000 description 1
- 235000013373 food additive Nutrition 0.000 description 1
- 239000002778 food additive Substances 0.000 description 1
- 239000003205 fragrance Substances 0.000 description 1
- 239000001530 fumaric acid Substances 0.000 description 1
- 230000036541 health Effects 0.000 description 1
- 210000002216 heart Anatomy 0.000 description 1
- 210000003734 kidney Anatomy 0.000 description 1
- 239000004310 lactic acid Substances 0.000 description 1
- 235000014655 lactic acid Nutrition 0.000 description 1
- 210000004185 liver Anatomy 0.000 description 1
- 239000002932 luster Substances 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 210000000214 mouth Anatomy 0.000 description 1
- 201000008383 nephritis Diseases 0.000 description 1
- 229910052757 nitrogen Inorganic materials 0.000 description 1
- 235000005985 organic acids Nutrition 0.000 description 1
- 230000003647 oxidation Effects 0.000 description 1
- 238000007254 oxidation reaction Methods 0.000 description 1
- 229910052760 oxygen Inorganic materials 0.000 description 1
- 229910052698 phosphorus Inorganic materials 0.000 description 1
- 238000001556 precipitation Methods 0.000 description 1
- 238000003672 processing method Methods 0.000 description 1
- 238000012797 qualification Methods 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 230000007115 recruitment Effects 0.000 description 1
- 230000009467 reduction Effects 0.000 description 1
- 230000001105 regulatory effect Effects 0.000 description 1
- 238000011160 research Methods 0.000 description 1
- 150000003839 salts Chemical class 0.000 description 1
- 230000004936 stimulating effect Effects 0.000 description 1
- 230000000638 stimulation Effects 0.000 description 1
- 229910052717 sulfur Inorganic materials 0.000 description 1
- 238000003786 synthesis reaction Methods 0.000 description 1
- JBQYATWDVHIOAR-UHFFFAOYSA-N tellanylidenegermanium Chemical compound [Te]=[Ge] JBQYATWDVHIOAR-UHFFFAOYSA-N 0.000 description 1
- VZCYOOQTPOCHFL-UHFFFAOYSA-N trans-butenedioic acid Natural products OC(=O)C=CC(O)=O VZCYOOQTPOCHFL-UHFFFAOYSA-N 0.000 description 1
Landscapes
- Manufacture Of Tobacco Products (AREA)
Abstract
The invention discloses a method for improving the quality of cut tobacco of cigarettes. Dissolving 0.1-25% of malate in water or a mixed solution of ethanol and water, and adjusting the acidity to 6.0-6.8 AV by adopting malic acid; alcoholizing the tobacco leaves according to the addition ratio of 0.01-5 percent, wherein the alcoholizing time is 180-360 days; and preparing the alcoholized tobacco leaves into tobacco shreds, baking at the temperature of 120-140 ℃, for 4-6 minutes, storing the tobacco shreds for 3-5 hours, and controlling the water content of the tobacco shreds to be 10-16%, thus obtaining the required cigarette tobacco shreds. The system test data of different leaf group formulas show that the invention can effectively improve the tobacco shred quality and further improve the smoking quality of cigarettes.
Description
Technical field
The present invention relates to the processing method of pipe tobacco and tobacco leaf, more particularly, the present invention relates to a kind of method of improving quality of tobacco shreds of cigarettes.
Background technology
The control of the tar in the cigarette mainstream flue gas, nicotine and other harmful components is great research topics that whole world tobacco business is faced.Along with " (Framework Convention on Tobacco Control " in 2005 formally effective in China, it is increasing that China's tobacco business faces the pressure that the criterion of " tobacco component control and disclosure " brings.
At present, the method that reduces harmful components in the cigarette mainstream flue gas mainly adopts filter tip aeration technology and composite tip stick technology.These technology are with strong points, and use is extensive and effect is obvious, and still, the problem that also can bring simultaneously is the loss of tobacco flavor material, makes flue gas enrich degree and decreases.
Malic acid is a kind of natural organic acids, has the important physical function, has antifatigue, protects liver, kidney, heart effect, it can be developed as health drink.Be widely used in industries such as food, medicine, chemical industry, building materials at present, become the acid condiment that after citric acid, lactic acid consumption ranked third the position.At present, consume in U.S.'s year more than 1,500 ten thousand pounds, wherein 90% is used for Food ﹠ Drink processing.And Japanese scholar successfully is applied to malate to subtract in sugar, the salt-decreasing food in recent years, simultaneously can be as the salt substitute (Liu Jianjun, Food Additives Used in China, 2003) of nephritis patient.Usually, the method for extraction malic acid is the milk of lime precipitation method from natural plants.And the method for oxidation fumaric acid is mainly adopted in chemical synthesis, but the product that obtains is DL type mixture (Wang Boyan, fermentation organic acid production and an application manual).Also can adopt microbe fermentation method through a step or multistep fermentation gained.
In 92 kinds of elements that nature exists, known tobacco growing is grown essential unit and is have 17 kinds.Wherein the more unit of content have 9 kinds of C, H, O, N, S, P, K, Ca, Mg etc. in the tobacco, and trace element has 8 kinds of Fe, B, Cu, Zn, Mn, Cl, Mo, Ni etc.Indispensable element tobacco growing is grown and the formation of quality very important, it not only influences growing of tobacco and output, and can change the correlation of attributes indexs such as flammability, color and luster, elasticity, suction flavor, filling power of tobacco.The content of trace element in tobacco leaf generally maintains tens ng/g between the hundreds of μ g/g.But its trace element of the tobacco leaf of different regions growth is formed and is varied, and causes using the fluctuation of the cigarette quality that these raw materials produce to a certain extent.Studies show that in a large number: trace element as: lithium, beryllium, calcium, copper, zinc, manganese, molybdenum, nickel etc. have more significantly influence to cigarette odor-absorbing.Therefore, how improving the quality of cigarette shreds targetedly, is the technical barrier that this area waits to solve.
Summary of the invention
The objective of the invention is at the deficiencies in the prior art part, especially, provide a kind of method of improving quality of tobacco shreds of cigarettes at suction quality problems such as the flue gas drying sense that is faced in the smoking property of cigarette process, burr senses.Simultaneously, described method also has the effect that reduces harmful components such as tar, nicotine, ammonia in the cigarette mainstream flue gas.
Purpose of the present invention is achieved by following technical proposals.
* except as otherwise noted, the percentage that is adopted among the present invention is mass percent.
A. the invention provides a kind of method of improving quality of tobacco shreds of cigarettes, described method adopts following steps:
1. malate 0.1%～25% is dissolved in the mixed solution of water or second alcohol and water, and the employing malic acid is 6.0～6.8AV with its acidity adjustment;
With the described solution of step 1 by 0.01%～5% adding proportion, tobacco leaf is refined processing, the alcoholization time is 180～360 days;
3. the tobacco leaf after will refining is made pipe tobacco, and baking temperature is 120 ℃～140 ℃, and stoving time is 4～6 minutes, and the storage silk time is 3～5 hours, and the pipe tobacco moisture content is controlled to be 10%～16%, is required cigarette shreds.
Wherein, the described alcoholization processing of step 2 is to tobacco leaf surface with described spray solution; Described tobacco leaf comprises C4F, B2R, B3F, B3F, B2L, B2V, B3R, B4F, C4L, B3L, B3V, B1K, B2K, B3K, GY1, GY2 or B4L; The described cigarette of step 3 is fire-cured tobacco type or blended type cigarette.
B. malate of the present invention, chemical name are the 2-malate, and chemical structural formula is:
Wherein, the configuration of its 2 carbon atoms can be the R type, the S type, and M can independently choose wantonly from following element or functional group, or the combination of following element or functional group, or the combination of its stereoisomer, enantiomter, diastereoisomer, racemic modification.M is selected from following element:
Hydrogen (H), ammonium (NH4), sodium (Na), potassium (K), lithium (Li), beryllium (Be), magnesium (Mg), aluminium (Al), calcium (Ca), iron (Fe), copper (Cu), zinc (Zn), manganese (Mn), molybdenum (Mo), nickel (Ni).
Compared with prior art, the present invention has following beneficial effect:
System test data of different leaf combination formulae shows that described method can be improved the quality of cigarette shreds effectively, reduces the not mature sense that tobacco leaf brought, and the burr sense increases throat's moisture feeling.Make in the cigarette mainstream flue gas nicotine burst size reduce 5%～10% than blank sample, NH
3Burst size reduces 10%～13% than blank sample, and releasing content of coke tar reduces 5%～8% than blank sample, and flue gas moisture increases by 1%～9% than blank sample.Simultaneously, the moderate-element and the trace element that can replenish in the tobacco leaf to be lacked improve the soften and the fine and smooth degree of flue gas, have further improved the suction quality of cigarette.
The specific embodiment
In order to make purpose of the present invention, technical scheme and advantage clearer,, the present invention is further elaborated below in conjunction with embodiment.Should be appreciated that specific embodiment described herein only in order to explanation the present invention, and be not used in qualification the present invention.
Embodiment 1
Take by weighing 2g potassium malate, 5g zinc malate and 3g calcium malate respectively and be dissolved in the 100mL water, add the ethanol of 10mL, the acidity of aqueous solution of malic acid regulator solution with 60%, preferred acidity is: 6.7AV.Described spray solution on the B2F tobacco leaf, is preferably sprayed mass ratio and is: 0.5%, preferred leaves moisting moisture content is 12%.With the preferred time of tobacco mellowing be: 200 days.Be cut into pipe tobacco and prepare cigarette, prepare blank sample simultaneously.
Through the sample that above-mentioned treatment technology is handled, smoking result shows: its comfort level, humidity promote to some extent, and the flue gas excitant obviously descends.Conventional fume component analysis result shows: its nicotine burst size reduces 5.8% than blank sample, NH
3Burst size reduces 10.1% than blank sample, and releasing content of coke tar reduces 5.6% than blank sample, and the moisture recruitment is 1.1%.
Embodiment 2
Take by weighing 2g magnesium malate, 2g zinc malate and 3g calcium malate respectively and 3g malic acid lithium is dissolved in the 100mL water, the acidity of aqueous solution of malic acid regulator solution with 60%, preferred acidity is: 6.3AV.Described spray solution in pipe tobacco leaf group, is preferably sprayed mass ratio and is: 0.3%, preferred pipe tobacco moisture content is controlled to be 18%, and preferred baking temperature is 130 ℃, and preferred stoving time is 5min, and the preferred storage silk time is 4h.
Smoking result shows: through the sample that above-mentioned treatment technology is handled, its comfort level, humidity promote to some extent, and the flue gas excitant obviously descends.Conventional fume component analysis result shows: its nicotine burst size reduces 10.5% than blank sample, NH
3Burst size reduces 14.1% than blank sample, and releasing content of coke tar reduces 6.6% than blank sample, and flue gas moisture increases by 2.1%.
Embodiment 3
4g zinc malate, 2g calcium malate and 4g malic acid lithium being dissolved in the 80mL water, adding the ethanol of 10mL, is 60% aqueous solution of malic acid adjusting acidity with mass ratio.Under 20 ℃ of temperature, measure and write down parameters such as the diopter of above-mentioned mixed solution and density.The B2F tobacco leaf is carried out the leaf stalk separate, be cut into the square of about 35*35mm.Above-mentioned mixed solution and tobacco leaf are added according to 0.5%～2% ratio, moisture content in leaves is controlled at 12%, baking temperature is controlled at 150 ℃, seal up for safekeeping behind the baking 8min, after normal temperature alcoholization in 200 days, will roll into cigarette after the tobacco leaf chopping, obtain 1#～6# sample, to be 0# in the same old way, the fabrication process condition of all samples is identical.The result shows: TPM, tar, nicotine and NH in the cigarette smoke
3Reduction is in various degree all arranged, and flue gas moisture and cigarette smoking quality have a distinct increment, its concrete proportioning and detection data are shown in table 1～3.
Sample adds formula table in table 1 tobacco leaf
| ??0# | ??1# | ??2# | ??3# | ??4# | ??5# | ??6# | |
| Potassium malate (g) | ??- | ??2.0 | ??2.0 | ??3.0 | ??2.0 | ??- | ??5.0 |
| Zinc malate (g) | ??- | ??5.0 | ??5.0 | ??4.0 | ??5.0 | ??5.0 | ??5.0 |
| Calcium malate (g) | ??- | ??3.0 | ??3.0 | ??3.0 | ??3.0 | ??5.0 | ??- |
| 60% malic acid solution (mL) | ??- | ??10.0 | ??10.0 | ??12.5 | ??13.0 | ??9.5 | ??11.0 |
| Acidity (AV) | ??- | ??6.7 | ??6.7 | ??6.5 | ??6.3 | ??6.7 | ??6.7 |
| Adding proportion % in tobacco leaf | ??- | ??0.5 | ??1.0 | ??1.0 | ??0.5 | ??1.0 | ??3.0 |
Table 2 sample cigarette specification and flue gas analysis result
| ??0# | ??1# | ??2# | ??3# | ??4# | ??5# | ??6# | |
| Moisture in cut tobacco % | ??11.9 | ??12.3 | ??12.6 | ??12.4 | ??12.5 | ??12.4 | ??12.6 |
| Cigarette weight (g/ props up) | ??0.98 | ??0.97 | ??0.98 | ??1.00 | ??1.01 | ??1.04 | ??1.01 |
| Puff number (mouthful /) | ??7.52 | ??7.34 | ??7.53 | ??7.46 | ??7.54 | ??7.60 | ??7.55 |
| ??0# | ??1# | ??2# | ??3# | ??4# | ??5# | ??6# | |
| TPM (mg/ props up) | ??18.88 | ??17.99 | ??17.61 | ??17.35 | ??17.66 | ??17.32 | ??17.06 |
| Tar (mg/ props up) | ??14.71 | ??13.88 | ??13.43 | ??13.21 | ??13.58 | ??13.34 | ??13.00 |
| Moisture (mg/ props up) | ??2.61 | ??2.64 | ??2.80 | ??2.84 | ??2.74 | ??2.73 | ??2.80 |
| Nicotine (mg/ props up) | ??1.56 | ??1.47 | ??1.38 | ??1.30 | ??1.34 | ??1.25 | ??1.16 |
| ??NH 3(μ g/ props up) | ??13.50 | ??12.14 | ??11.24 | ??11.88 | ??11.16 | ??11.38 | ??9.96 |
Table 3 sample cigarette sensory evaluating smoking result (with the contrast of 0# sample)
*
| ??0# | ??1# | ??2# | ??3# | ??4# | ??5# | ??6# | |
| Smoking result | ??- | Excitant slightly reduces | Stimulate slightly and reduce, pleasant impression has improvement | Rich increase to some extent stimulates slightly and reduces | Rich increase to some extent stimulates slightly and reduces | Rich increase to some extent stimulates slightly and reduces | Stimulating has minimizing, the flue gas property sent out reduction thoroughly |
*Wherein, the sensory evaluating smoking of table 3 is the 7 people group's evaluation results of smokeing panel test.
Embodiment 4
Taking by weighing 2.5g potassium malate and 2.5g zinc malate respectively and be dissolved in the 40mL water, is that 60% aqueous solution of malic acid is regulated acidity to 6.7AV with mass ratio.The GY1 tobacco leaf is carried out the leaf stalk separate, be cut into the square of about 35*35mm.Above-mentioned mixed solution and tobacco leaf are added according to 0.5% mass ratio, moisture content in leaves is controlled at 18%, baking temperature is controlled at 140 ℃, seal up for safekeeping behind the baking 10min, baking back moisture in cut tobacco is controlled at 12%, after normal temperature alcoholization in 200 days, to roll into cigarette after the tobacco leaf chopping, obtain 7#, 8# sample, to be 7# in the same old way, the fabrication process condition of all samples is identical.The result shows: TPM, tar, nicotine and NH in the cigarette smoke
3Reduction is in various degree all arranged, and flue gas moisture and cigarette smoking quality have a distinct increment, it is as shown in table 4 that it detects data.
Table 4GY1 tobacco leaf is smoked panel test and conventional flue gas analysis result
| Sample | Smoking result | Tar mg/ props up | Moisture mg/ props up | Nicotine mg/ props up | ??NH 3μ g/ props up |
| ??7# | Flue gas is rich slightly poor, and pleasant impression is slightly poor | ??12.1 | ??2.60 | ??1.44 | ??12.10 |
| ??8# | The rich increase of fragrance, pleasant impression makes moderate progress | ??11.8 | ??2.67 | ??1.32 | ??11.04 |
Embodiment 5
Take by weighing 2g magnesium malate, 2g zinc malate, 3g calcium malate and 3g malic acid lithium respectively and be dissolved in the 100mL water, the acidity of the aqueous solution of malic acid regulator solution with 60% is to 6.3AV.This solution is sprayed in the pipe tobacco leaf group 1～4 with 0.3% ratio, and its treatment process condition is as shown in table 5, is prepared into 9#～15# sample, and 9# is with reference to sample, and the fabrication process condition of all samples is identical.The result shows: under the different disposal condition, and TPM, tar, nicotine and NH in the cigarette smoke
3Reduction is in various degree all arranged, and most of suction quality has a distinct increment, its concrete proportioning and detection data are shown in table 5～7.
Sample adds formula table in table 5 tobacco leaf
| ?9# | ??10# | ??11# | ??12# | ??13# | ??14# | ??15# | |
| Magnesium malate (g) | ?- | ??2.0 | ??- | ??3.0 | ??- | ??- | ??5.0 |
| Potassium malate (g) | ?- | ??- | ??2.0 | ??2.0 | ??- | ??2.0 | ??- |
| Zinc malate (g) | ?- | ??2.0 | ??5.0 | ??2.0 | ??- | ??3.0 | ??5.0 |
| Calcium malate (g) | ?- | ??3.0 | ??3.0 | ??2.0 | ??- | ??- | ??- |
| Malic acid lithium (g) | ??3.0 | ??- | ??1.0 | ??- | ??5.0 | ??- | |
| 60% malic acid solution (mL) | ?- | ??10.5 | ??10.0 | ??11.0 | ??- | ??10.0 | ??11.5 |
| Acidity (AV) | ?- | ??6.3 | ??6.3 | ??6.5 | ??- | ??6.3 | ??6.3 |
| Used leaf group | ?1 | ??1 | ??1 | ??1 | ??2 | ??2 | ??2 |
| Leaves moisting moisture content % | ?18 | ??18 | ??20 | ??20 | ??18 | ??18 | ??20 |
| ?9# | ??10# | ??11# | ??12# | ??13# | ??14# | ??15# | |
| Baking temperature (℃) | ?130 | ??130 | ??120 | ??120 | ??130 | ??130 | ??120 |
| Stoving time (min) | ?5 | ??5 | ??7 | ??7 | ??5 | ??5 | ??7 |
| The storage silk time (h) | ?4 | ??2 | ??2 | ??4 | ??2 | ??2 | ??4 |
| Adding proportion % in tobacco leaf | ?- | ??0.3 | ??0.3 | ??0.1 | ??- | ??0.3 | ??0.1 |
Table 6 sample cigarette specification and flue gas analysis result
| ??9# | ??10# | ??11# | ??12# | ??13# | ??14# | ??15# | |
| Moisture in cut tobacco % | ??11.9 | ??12.4 | ??12.5 | ??12.2 | ??12.0 | ??12.7 | ??12.5 |
| Cigarette weight (g/ props up) | ??0.97 | ??0.97 | ??1.02 | ??1.02 | ??0.99 | ??1.03 | ??1.03 |
| Puff number (mouthful /) | ??7.42 | ??7.36 | ??7.58 | ??7.49 | ??7.64 | ??7.62 | ??7.58 |
| TPM (mg/ props up) | ??18.05 | ??16.98 | ??17.37 | ??17.67 | ??22.94 | ??19.78 | ??21.43 |
| Tar (mg/ props up) | ??14.91 | ??13.92 | ??14.28 | ??14.55 | ??18.95 | ??16.49 | ??17.85 |
| Moisture (mg/ props up) | ??2.01 | ??2.05 | ??2.05 | ??2.06 | ??2.64 | ??2.11 | ??2.34 |
| Nicotine (mg/ props up) | ??1.13 | ??1.01 | ??1.04 | ??1.08 | ??1.35 | ??1.18 | ??1.24 |
| ??NH 3(μ g/ props up) | ??8.39 | ??8.07 | ??8.03 | ??8.14 | ??12.79 | ??10.22 | ??11.57 |
Table 7 sample cigarette sensory evaluating smoking result 1
*
| Sample | Smoking result |
| The 9# contrast | Excitant is bigger than normal, and comfortableness is slightly poor |
| ??10# | Stimulate slightly and reduce, comfortableness increases, and strength descends |
| ??11# | Stimulate slightly and reduce, comfortableness increases, and the oral cavity is residual better |
| ??12# | Stimulate improvement not obvious, comfortableness is slightly poor, and strength descends |
Table 8 sample cigarette sensory evaluating smoking result 2
*
| Sample | Smoking result |
| The 13# contrast | Excitant is bigger than normal |
| ?14# | Stimulate stimulation bigger than normal slightly to reduce, comfortableness increases, and strength descends |
| ?15# | Stimulate improvement not obvious, comfortableness is slightly poor, and strength descends |
*Wherein, the sensory evaluating smoking of table 7 and table 8 is the 7 people group's evaluation results of smokeing panel test.
The above only is preferred embodiment of the present invention, not in order to restriction the present invention, all any modifications of being done within the spirit and principles in the present invention, is equal to and replaces and improvement etc., all should be included within protection scope of the present invention.
Claims (5)
1. a method of improving quality of tobacco shreds of cigarettes is characterized in that, described method adopts following steps:
(1) malate 0.1%～25% is dissolved in the mixed solution of water or second alcohol and water, and the employing malic acid is 6.0～6.8AV with its acidity adjustment;
(2) with the described solution of step 1 by 0.01%～5% adding proportion, tobacco leaf is refined processing, the alcoholization time is 180～360 days;
(3) tobacco leaf after will refining is made pipe tobacco, and baking temperature is 120 ℃～140 ℃, and stoving time is 4～6 minutes, and the storage silk time is 3～5 hours, and the pipe tobacco moisture content is controlled to be 10%～16%, is required cigarette shreds.
2. method according to claim 1 is characterized in that, it is to tobacco leaf surface with described spray solution that the described alcoholization of step 2 is handled.
3. method according to claim 1 is characterized in that described tobacco leaf comprises C4F, B2R, B3F, B3F, B2L, B2V, B3R, B4F, C4L, B3L, B3V, B1K, B2K, B3K, GY1, GY2 or B4L.
4. method according to claim 1 is characterized in that, the described cigarette of step 3 is fire-cured tobacco type or blended type cigarette.
5. method according to claim 1 is characterized in that, the described malate of step 1, chemical name are the 2-malate, and chemical structural formula is:
Wherein, the configuration of its 2 carbon atoms can be the R type, the S type, and M can independently choose wantonly from following element or functional group, or the combination of following element or functional group, perhaps the combination of its stereoisomer, enantiomter, diastereoisomer, racemic modification; M is selected from following element: hydrogen, ammonium, sodium, potassium, lithium, beryllium, magnesium, aluminium, calcium, iron, copper, zinc, manganese, molybdenum, nickel.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2010101969796A CN101856144B (en) | 2010-06-10 | 2010-06-10 | Method for improving quality of cigarette tobacco shreds |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2010101969796A CN101856144B (en) | 2010-06-10 | 2010-06-10 | Method for improving quality of cigarette tobacco shreds |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN101856144A true CN101856144A (en) | 2010-10-13 |
| CN101856144B CN101856144B (en) | 2012-07-04 |
Family
ID=42942485
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN2010101969796A Active CN101856144B (en) | 2010-06-10 | 2010-06-10 | Method for improving quality of cigarette tobacco shreds |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN101856144B (en) |
Cited By (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102524950A (en) * | 2010-12-15 | 2012-07-04 | 李贵生 | Health-care cigarette containing agilawood |
| CN102823942A (en) * | 2012-09-20 | 2012-12-19 | 上海烟草集团有限责任公司 | Application of aqueous solution of salt serving as hydrous stem humectant |
| CN102835734A (en) * | 2012-09-20 | 2012-12-26 | 上海烟草集团有限责任公司 | Hydrated-salt-type tobacco humectant and preparation method thereof |
| CN105249528A (en) * | 2014-07-09 | 2016-01-20 | 江西中烟工业有限责任公司 | Moisture-retaining agent improving physical moisture retaining performance of expanded tobacco and preparation method for moisture-retaining agent |
| CN105307515A (en) * | 2013-06-19 | 2016-02-03 | 日本烟草产业株式会社 | Process for producing raw tobacco material |
| CN109288127A (en) * | 2018-10-22 | 2019-02-01 | 福建中烟工业有限责任公司 | A kind of composition and application thereof of adjustable cigarette mainstream flue gas pH value |
| CN116268540A (en) * | 2022-09-08 | 2023-06-23 | 广东中烟工业有限责任公司 | Method for improving sensory quality of heated cigarettes |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1051291A (en) * | 1989-11-01 | 1991-05-15 | 航空航天工业部第三研究院第三设计部 | tobacco treatment agent |
| CN101224040A (en) * | 2008-01-22 | 2008-07-23 | 深圳波顿香料有限公司 | Spice for tobacco and method for partially substituting Zimbabwe tobacco leaf |
| CN101356995A (en) * | 2008-09-24 | 2009-02-04 | 中国烟草总公司郑州烟草研究院 | Cure tobacco leaf roasting aroma-extracting agent and use thereof |
| CN101375735A (en) * | 2007-08-30 | 2009-03-04 | 武汉烟草(集团)有限公司 | Method for preparing burley tobacco expanded tobacco shred for low-coke tar flue-cured type cigarette |
-
2010
- 2010-06-10 CN CN2010101969796A patent/CN101856144B/en active Active
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1051291A (en) * | 1989-11-01 | 1991-05-15 | 航空航天工业部第三研究院第三设计部 | tobacco treatment agent |
| CN101375735A (en) * | 2007-08-30 | 2009-03-04 | 武汉烟草(集团)有限公司 | Method for preparing burley tobacco expanded tobacco shred for low-coke tar flue-cured type cigarette |
| CN101224040A (en) * | 2008-01-22 | 2008-07-23 | 深圳波顿香料有限公司 | Spice for tobacco and method for partially substituting Zimbabwe tobacco leaf |
| CN101356995A (en) * | 2008-09-24 | 2009-02-04 | 中国烟草总公司郑州烟草研究院 | Cure tobacco leaf roasting aroma-extracting agent and use thereof |
Cited By (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102524950A (en) * | 2010-12-15 | 2012-07-04 | 李贵生 | Health-care cigarette containing agilawood |
| CN102524950B (en) * | 2010-12-15 | 2014-08-13 | 李贵生 | Health-care cigarette containing agilawood |
| CN102823942A (en) * | 2012-09-20 | 2012-12-19 | 上海烟草集团有限责任公司 | Application of aqueous solution of salt serving as hydrous stem humectant |
| CN102835734A (en) * | 2012-09-20 | 2012-12-26 | 上海烟草集团有限责任公司 | Hydrated-salt-type tobacco humectant and preparation method thereof |
| CN102835734B (en) * | 2012-09-20 | 2014-07-16 | 上海烟草集团有限责任公司 | Hydrated-salt-type tobacco humectant and preparation method thereof |
| CN102823942B (en) * | 2012-09-20 | 2014-10-15 | 上海烟草集团有限责任公司 | Application of aqueous solution of salt serving as hydrous stem humectants, and method for keeping moisture of stem |
| CN105307515A (en) * | 2013-06-19 | 2016-02-03 | 日本烟草产业株式会社 | Process for producing raw tobacco material |
| CN105249528A (en) * | 2014-07-09 | 2016-01-20 | 江西中烟工业有限责任公司 | Moisture-retaining agent improving physical moisture retaining performance of expanded tobacco and preparation method for moisture-retaining agent |
| CN109288127A (en) * | 2018-10-22 | 2019-02-01 | 福建中烟工业有限责任公司 | A kind of composition and application thereof of adjustable cigarette mainstream flue gas pH value |
| CN116268540A (en) * | 2022-09-08 | 2023-06-23 | 广东中烟工业有限责任公司 | Method for improving sensory quality of heated cigarettes |
Also Published As
| Publication number | Publication date |
|---|---|
| CN101856144B (en) | 2012-07-04 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN101856144B (en) | Method for improving quality of cigarette tobacco shreds | |
| CN101411543A (en) | Method for preparing flavoring for cigarette and use | |
| CN104829288A (en) | Tobacco foliar fertilizer and preparation method thereof | |
| CN102415614B (en) | Method for improving tobacco stem quality by applying liquorice | |
| CN114343229B (en) | Preparation method of novel nicotine salt | |
| CN102823937A (en) | Extracting method of submerged fermentation mycelium extractive of lepista nuda and application thereof in cigarettes | |
| CN104450192A (en) | Tobacco flavor prepared by taking fructus terminaliae immaturus, dendrobium nobile, tobacco and the like as raw materials and application thereof | |
| CN103462212A (en) | Method for improving quality of tobacco leaves by adding enzyme preparation, glucose and citric acid | |
| CN107155653A (en) | A kind of engrafting method of loquat | |
| CN104673608A (en) | Preparation method for moringa oleifera health wine | |
| CN105011353A (en) | Natural bio-chemical agent used for cigar fermentation and quality improvement, preparation and application thereof | |
| CN101317692A (en) | Additive agent for jasmine fragrance type cigarette, preparation and application thereof | |
| CN104432494A (en) | Method for preparing tobacco shreds capable of improving smoking satisfaction and low tar cigarette | |
| CN101856149A (en) | Method for improving quality of cigarette filter tip | |
| CN101455442A (en) | Grape extractum and preparation method thereof and use thereof in cigarette performing | |
| CN105361238A (en) | Electronic cigarette smoke solution containing pH conditioning agent and method for improving smoking feeling of electronic cigarette smoke solution | |
| CN101342007B (en) | Citronella grass cigarette | |
| CN103947553A (en) | Passion flower tissue culture medium | |
| CN103004770A (en) | Plant growth regulator for improving upper leaf enlargement, nicotine reduction and potassium increase after topping | |
| CN102498953B (en) | Method for improving medium-grade 100 cured tobacco variety | |
| CN109328821A (en) | A kind of apocarya breeding method of high survival rate | |
| CN108887728A (en) | A kind of preparation method of selenium-rich black tea reconstituted tobacoo | |
| CN1586247A (en) | Fresh shaddock tea and its producing method | |
| CN106941844A (en) | Tobacco-rice rotation integral fertilization method | |
| CN106748324A (en) | A kind of nutrient solution for being used for the cultivation of five Fancy-leaf caladiums |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant |