CN108917397A - A kind of plasma sintering equipment of heat-resisting material - Google Patents

A kind of plasma sintering equipment of heat-resisting material Download PDF

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Publication number
CN108917397A
CN108917397A CN201810938967.2A CN201810938967A CN108917397A CN 108917397 A CN108917397 A CN 108917397A CN 201810938967 A CN201810938967 A CN 201810938967A CN 108917397 A CN108917397 A CN 108917397A
Authority
CN
China
Prior art keywords
compression bar
interior
mold
heat
wall
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Withdrawn
Application number
CN201810938967.2A
Other languages
Chinese (zh)
Inventor
贝国平
董金勇
董峰
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Zhong Ming Fu Chi (suzhou) Nanometer High Tech Materials Co Ltd
Original Assignee
Zhong Ming Fu Chi (suzhou) Nanometer High Tech Materials Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Zhong Ming Fu Chi (suzhou) Nanometer High Tech Materials Co Ltd filed Critical Zhong Ming Fu Chi (suzhou) Nanometer High Tech Materials Co Ltd
Priority to CN201810938967.2A priority Critical patent/CN108917397A/en
Publication of CN108917397A publication Critical patent/CN108917397A/en
Withdrawn legal-status Critical Current

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Classifications

    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F27FURNACES; KILNS; OVENS; RETORTS
    • F27BFURNACES, KILNS, OVENS, OR RETORTS IN GENERAL; OPEN SINTERING OR LIKE APPARATUS
    • F27B17/00Furnaces of a kind not covered by any preceding group
    • F27B17/0016Chamber type furnaces
    • F27B17/0041Chamber type furnaces specially adapted for burning bricks or pottery
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F27FURNACES; KILNS; OVENS; RETORTS
    • F27DDETAILS OR ACCESSORIES OF FURNACES, KILNS, OVENS, OR RETORTS, IN SO FAR AS THEY ARE OF KINDS OCCURRING IN MORE THAN ONE KIND OF FURNACE
    • F27D5/00Supports, screens, or the like for the charge within the furnace
    • F27D5/0031Treatment baskets for ceramic articles
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F27FURNACES; KILNS; OVENS; RETORTS
    • F27DDETAILS OR ACCESSORIES OF FURNACES, KILNS, OVENS, OR RETORTS, IN SO FAR AS THEY ARE OF KINDS OCCURRING IN MORE THAN ONE KIND OF FURNACE
    • F27D7/00Forming, maintaining, or circulating atmospheres in heating chambers
    • F27D7/06Forming or maintaining special atmospheres or vacuum within heating chambers
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F27FURNACES; KILNS; OVENS; RETORTS
    • F27DDETAILS OR ACCESSORIES OF FURNACES, KILNS, OVENS, OR RETORTS, IN SO FAR AS THEY ARE OF KINDS OCCURRING IN MORE THAN ONE KIND OF FURNACE
    • F27D9/00Cooling of furnaces or of charges therein
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F27FURNACES; KILNS; OVENS; RETORTS
    • F27DDETAILS OR ACCESSORIES OF FURNACES, KILNS, OVENS, OR RETORTS, IN SO FAR AS THEY ARE OF KINDS OCCURRING IN MORE THAN ONE KIND OF FURNACE
    • F27D7/00Forming, maintaining, or circulating atmospheres in heating chambers
    • F27D7/06Forming or maintaining special atmospheres or vacuum within heating chambers
    • F27D2007/066Vacuum
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F27FURNACES; KILNS; OVENS; RETORTS
    • F27DDETAILS OR ACCESSORIES OF FURNACES, KILNS, OVENS, OR RETORTS, IN SO FAR AS THEY ARE OF KINDS OCCURRING IN MORE THAN ONE KIND OF FURNACE
    • F27D9/00Cooling of furnaces or of charges therein
    • F27D2009/0002Cooling of furnaces
    • F27D2009/001Cooling of furnaces the cooling medium being a fluid other than a gas
    • F27D2009/0013Cooling of furnaces the cooling medium being a fluid other than a gas the fluid being water
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F27FURNACES; KILNS; OVENS; RETORTS
    • F27DDETAILS OR ACCESSORIES OF FURNACES, KILNS, OVENS, OR RETORTS, IN SO FAR AS THEY ARE OF KINDS OCCURRING IN MORE THAN ONE KIND OF FURNACE
    • F27D9/00Cooling of furnaces or of charges therein
    • F27D2009/0002Cooling of furnaces
    • F27D2009/0018Cooling of furnaces the cooling medium passing through a pattern of tubes
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F27FURNACES; KILNS; OVENS; RETORTS
    • F27MINDEXING SCHEME RELATING TO ASPECTS OF THE CHARGES OR FURNACES, KILNS, OVENS OR RETORTS
    • F27M2001/00Composition, conformation or state of the charge
    • F27M2001/03Charges containing minerals
    • F27M2001/035China
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F27FURNACES; KILNS; OVENS; RETORTS
    • F27MINDEXING SCHEME RELATING TO ASPECTS OF THE CHARGES OR FURNACES, KILNS, OVENS OR RETORTS
    • F27M2003/00Type of treatment of the charge
    • F27M2003/04Sintering

Abstract

A kind of plasma sintering equipment of heat-resisting material of the application, including vacuum discharge plasma agglomeration furnace, the cylindric outer mold being arranged in vacuum discharge plasma agglomeration furnace, the cylindric interior mold being arranged in the outer mold, the upper and lower ends of the interior mold are respectively inserted with interior compression bar and lower interior compression bar in the cylinder for playing increase pressure and sealing function;Since upper interior compression bar and lower external compression bar are respectively provided with upper projecting portion and lower convex portion, sealing effect can be preferably played, and upper and lower interior compression bar is small with the contact surface of sample, and sample is enable to obtain bigger pressure.

Description

A kind of plasma sintering equipment of heat-resisting material
Technical field
This application involves a kind of plasma sintering equipments of heat-resisting material.
Background technique
With high-tech development, the fields such as national defence, space flight and aviation, energy are to the high-strength of material, Gao Mo, high temperature resistant, resistance to Burn into is anti-oxidant, more stringent requirements are proposed for the performances such as wear-resistant.It is to utilize using the nano ceramic material that nanotechnology is developed Nano-powder is modified existing ceramics, by the way that nano-scale particle, whisker, chip fiber etc. are added or generated into ceramics, So that crystal grain, crystal boundary and the combination between them is all reached nanometer level, mentions the intensity, toughness of material and superplasticity significantly It is high.It overcomes many deficiencies of engineering ceramics, and the performances such as the mechanics to material, electricity, calorifics, magnetooptics generate important shadow It rings, to replace the application of engineering ceramics to open up frontier.With the extensive use of nanotechnology, nano ceramics generates therewith, Wish the brittleness for overcoming ceramic material with this, there are ceramics as metal is like flexibility and machinability.In terms of high temperature resistant, Nano ceramic material also has significant superior function.This invention address that the preparation process of optimization nano ceramic material, makes to grind High temperature resistance, the strength character of the nano ceramic material of system increase substantially.
Summary of the invention
The application technical problems to be solved are to provide a kind of plasma sintering equipment of heat-resisting material.
In order to solve the above-mentioned technical problem, described this application provides a kind of plasma sintering equipment of heat-resisting material Agglomerating plant include vacuum discharge plasma agglomeration furnace, the cylindric external mold that is arranged in vacuum discharge plasma agglomeration furnace The cylindric interior mold for having, being arranged in the outer mold, the upper and lower ends of the interior mold increase inserted with respectively Interior compression bar and lower interior compression bar in the cylinder of plus-pressure and sealing function;The upper and lower ends of the outer mold respectively inserted with rise Increase external compression bar and lower external compression bar in pressure and the cylinder of sealing function, the lower end of the upper external compression bar pushes against described The upper end of compression bar in upper, the upper end of the lower external compression bar push against the lower end of the lower interior compression bar, and described is upper outer The upper end of compression bar is driven by fluid head on one, and the lower end of the lower external compression bar is driven by fluid head once, and described is upper The upper end of external compression bar and the lower end of the lower external compression bar are also respectively provided with top electrode and lower electrode, the top electrode It being electrically connected with lower electrode with direct current pulse power source, the upper fluid head and the lower fluid head are driven by a hydraulic device, The upper interior compression bar includes cylindrical upper internal pressure bar body portion, set on the cylindrical of the upper internal pressure bar body subordinate The outer wall of upper projecting portion, the upper internal pressure bar body portion is in contact with the inner wall of the outer mold, the upper projecting portion The external insertion interior mold in, be in contact with the inner wall of interior mold;The lower interior compression bar includes the lower interior of cylinder Compression bar body part, the cylindrical lower convex portion in the lower internal pressure bar body portion, the lower internal pressure bar body portion Outer wall be in contact with the inner wall of the outer mold, it is and interior in the external insertion of the lower convex portion interior mold The inner wall of mold is in contact.
Preferably, the agglomerating plant further includes one for by the vacuum discharge plasma agglomeration stove evacuation Vacuum evacuation device.
Preferably, the agglomerating plant further includes cooling system, and the cooling system is wrapped in vacuum including one and puts Cooling water pipe on electric plasma agglomeration furnace outer wall, the water tank being connected with the cooling water pipe.
Preferably, the lower end of the upper interior compression bar is provided with one layer of upper graphite paper.
Preferably, the lower end of the lower interior compression bar is provided with one layer of lower graphite paper.
Preferably, the agglomerating plant further includes the water for being pumped into water in the water tank in cooling water pipe Pump.
Preferably, one layer of heat preservation layer is additionally provided on the inner wall of the vacuum discharge plasma agglomeration furnace.
The plasma sintering equipment of a kind of heat-resisting material of the application, since upper interior compression bar and lower external compression bar are respectively provided with Upper projecting portion and lower convex portion can preferably play sealing effect, and upper and lower interior compression bar is small with the contact surface of sample, makes sample Product can obtain bigger pressure.
Detailed description of the invention
Fig. 1 is a kind of structural schematic diagram of the plasma sintering equipment of heat-resisting material.
Wherein:11, upper external compression bar;12, lower external compression bar;21, upper interior compression bar;22, lower interior compression bar;3, interior mold;4, external mold Tool;51, top electrode;52, lower electrode;61, upper fluid head;62, lower fluid head;7, water tank;71, cooling water pipe;8, vacuum means It sets;9, direct current pulse power source;10, vacuum discharge plasma agglomeration furnace;101, insulating layer;100, hydraulic device.
Specific embodiment
The application is described further in the following with reference to the drawings and specific embodiments, so that those skilled in the art can be with It more fully understands the application and can be practiced, but illustrated embodiment is not as the restriction to the application.
As shown, this application provides a kind of plasma sintering equipment of heat-resisting material, the agglomerating plant packet Include vacuum discharge plasma agglomeration furnace 10, the cylindric outer mold 4 that is arranged in vacuum discharge plasma agglomeration furnace 10, setting Cylindric interior mold 3 in the outer mold 4, the upper and lower ends of the interior mold 3 increase pressure inserted with respectively Interior compression bar 21 and lower interior compression bar 22 in power and the cylinder of sealing function;The upper and lower ends of the outer mold 4 respectively inserted with External compression bar 11 and lower external compression bar 12 in the cylinder for increasing pressure and sealing function are acted, the lower end of the upper external compression bar 11 is supported The upper end of the tight interior compression bar 21, the upper end of the lower external compression bar 12 push against the lower end of the lower interior compression bar 22 Portion, the upper end of the upper external compression bar 11 are driven by fluid head 61 on one, and the lower end of the lower external compression bar 12 is by once Fluid head 62 drives, and the lower end of the upper end of the upper external compression bar 11 and the lower external compression bar 12 is also respectively provided with Electrode 51 and lower electrode 52, the top electrode 51 and lower electrode 52 are electrically connected with direct current pulse power source 9, the upper fluid head 61 are driven with the lower fluid head 62 by a hydraulic device 100, and the upper interior compression bar 21 includes cylindrical upper interior compression bar Body part, the cylindrical upper projecting portion set on the upper internal pressure bar body subordinate, the upper internal pressure bar body portion it is outer Wall is in contact with the inner wall of the outer mold 4, in the external insertion of the upper projecting portion interior mold 3, with internal model The inner wall of tool 3 is in contact;The lower interior compression bar 22 includes cylindrical lower internal pressure bar body portion, set on the lower interior compression bar Cylindrical lower convex portion on body part, the inner wall phase of the outer wall and the outer mold 4 in the lower internal pressure bar body portion Contact, the external of the lower convex portion are inserted into the interior mold 3, are in contact with the inner wall of interior mold 3.The sintering Equipment further includes a vacuum evacuation device 8 for vacuumizing the vacuum discharge plasma agglomeration furnace 10.The sintering Equipment further includes cooling system, the cooling system include one be wrapped in it is cold on 10 outer wall of vacuum discharge plasma agglomeration furnace But water pipe 71, the water tank 7 being connected with the cooling water pipe 71.The lower end of the upper interior compression bar 21 is provided on one layer Graphite paper.The lower end of the lower interior compression bar 22 is provided with one layer of lower graphite paper.The agglomerating plant further includes one being used for Water in the water tank 7 is pumped into the water pump in cooling water pipe 71.On the inner wall of the vacuum discharge plasma agglomeration furnace 10 It is additionally provided with one layer of heat preservation layer 101.
The plasma sintering equipment of a kind of heat-resisting material of the application, since upper interior compression bar 21 and lower external compression bar 12 are distinguished With upper projecting portion and lower convex portion, sealing effect can be preferably played, and the contact surface with sample of interior compression bar 22 up and down It is small, so that sample is obtained bigger pressure.
Embodiment described above is only the preferred embodiment lifted to absolutely prove the application, the protection model of the application It encloses without being limited thereto.Those skilled in the art made equivalent substitute or transformation on the basis of the application, in the application Protection scope within.The protection scope of the application is subject to claims.

Claims (7)

1. a kind of plasma sintering equipment of heat-resisting material, which is characterized in that the agglomerating plant includes vacuum discharge etc. Ion sintering furnace, is arranged in the outer mold the cylindric outer mold being arranged in vacuum discharge plasma agglomeration furnace Cylindric interior mold, the upper and lower ends of the interior mold are respectively inserted with acting the cylinder for increasing pressure and sealing function Compression bar and lower interior compression bar in upper;The upper and lower ends of the outer mold are respectively inserted with the cylinder for playing increase pressure and sealing function External compression bar and lower external compression bar in shape, the lower end of the upper external compression bar pushes against the upper end of the upper interior compression bar, described The upper end of lower external compression bar pushes against the lower end of the lower interior compression bar, and the upper end of the upper external compression bar is by fluid head on one Driving, the lower end of the lower external compression bar are driven by fluid head once, the upper end of the upper external compression bar and it is described under The lower end of external compression bar is also respectively provided with top electrode and lower electrode, the top electrode and lower electrode and direct current pulse power source electricity Connection, the upper fluid head and the lower fluid head are driven by a hydraulic device, and the upper interior compression bar includes cylinder Upper internal pressure bar body portion, the cylindrical upper projecting portion set on the upper internal pressure bar body subordinate, the upper interior compression bar The outer wall of body part is in contact with the inner wall of the outer mold, the external insertion of the upper projecting portion interior mold It is interior, it is in contact with the inner wall of interior mold;The lower interior compression bar includes cylindrical lower internal pressure bar body portion, under described Cylindrical lower convex portion in internal pressure bar body portion, the outer wall in the lower internal pressure bar body portion are interior with the outer mold Wall is in contact, and in the external insertion of the lower convex portion interior mold, is in contact with the inner wall of interior mold.
2. a kind of plasma sintering equipment of heat-resisting material as described in claim 1, which is characterized in that the sintering is set Standby further includes one for by the vacuum evacuation device of the vacuum discharge plasma agglomeration stove evacuation.
3. a kind of plasma sintering equipment of heat-resisting material as claimed in claim 2, which is characterized in that the sintering is set Standby further includes cooling system, and the cooling system includes a cooling water being wrapped on vacuum discharge plasma agglomeration furnace outer wall Pipe, the water tank being connected with the cooling water pipe.
4. a kind of plasma sintering equipment of heat-resisting material as claimed in claim 3, which is characterized in that the upper internal pressure The lower end of bar is provided with one layer of upper graphite paper.
5. a kind of plasma sintering equipment of heat-resisting material as claimed in claim 4, which is characterized in that the lower internal pressure The lower end of bar is provided with one layer of lower graphite paper.
6. a kind of plasma sintering equipment of heat-resisting material as claimed in claim 5, which is characterized in that the sintering is set Standby further includes a water pump for being pumped into water in the water tank in cooling water pipe.
7. a kind of plasma sintering equipment of heat-resisting material as claimed in claim 6, which is characterized in that the vacuum is put One layer of heat preservation layer is additionally provided on the inner wall of electric plasma agglomeration furnace.
CN201810938967.2A 2018-08-17 2018-08-17 A kind of plasma sintering equipment of heat-resisting material Withdrawn CN108917397A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201810938967.2A CN108917397A (en) 2018-08-17 2018-08-17 A kind of plasma sintering equipment of heat-resisting material

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201810938967.2A CN108917397A (en) 2018-08-17 2018-08-17 A kind of plasma sintering equipment of heat-resisting material

Publications (1)

Publication Number Publication Date
CN108917397A true CN108917397A (en) 2018-11-30

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Family Applications (1)

Application Number Title Priority Date Filing Date
CN201810938967.2A Withdrawn CN108917397A (en) 2018-08-17 2018-08-17 A kind of plasma sintering equipment of heat-resisting material

Country Status (1)

Country Link
CN (1) CN108917397A (en)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109828614A (en) * 2019-01-31 2019-05-31 青岛众志测控技术有限公司 A kind of automatic control of sintering process water-adding system

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109828614A (en) * 2019-01-31 2019-05-31 青岛众志测控技术有限公司 A kind of automatic control of sintering process water-adding system

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Application publication date: 20181130