CN108913384A - 一种长效抗菌多功能地板清洁蜡及其制备方法 - Google Patents
一种长效抗菌多功能地板清洁蜡及其制备方法 Download PDFInfo
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Abstract
本发明涉及一种长效抗菌多功能地板清洁蜡及其制备方法，其主要成分为：非离子表面活性剂1‑10份，润湿剂1‑5份，吐温201‑5份，水溶助长剂2‑10份，天然油脂0.5‑5份，巴西棕榈蜡乳液0.1‑5份，遮光剂0.1‑2份，银离子抗菌剂0.05‑5份，螯合剂0.1‑10份，流变调节剂0.1‑5份。本发明所述的一种长效抗菌多功能地板清洁蜡具有长效抗菌、清洁去污、修复细微划痕、滋润保养、光亮、除异味的多重功效，且无挥发性溶剂，pH中性，不污染室内环境，生产工艺简单、成本低，并且使用方便，可应用于家居商业各类实木地板、复合木地板、竹木地板等多种类型木地板的清洁护理打蜡。
Description
技术领域
本发明属于日用精细化工领域，具体涉及一种长效抗菌多功能地板清洁蜡及其制备方法。
背景技术
随着中国城市化进程的加快，人们生活水平及品质的日渐提高，越来越多的人群更加注重健康和自然，而木地板因其自然美观、安全舒适、保温性能好等优点成为更多消费者居家装饰的首选材质。但是木地板由于其制造工艺、硬度不足和多孔结构，在使用过程中极易造成刮花、细微划痕、干裂、漆面光泽黯淡、细菌滋生、吸潮发霉等问题，大大的影响了木地板的美观和使用寿命。因此，木地板的日常清洁和养护、打蜡就显得尤为重要。
目前市面上的木地板清洁养护打蜡用品主要包括木地板清洁剂、固体地板蜡、液体木地板护理精油等产品。现今城市生活节奏较快，方便快捷多功能的产品更能赢得消费者的青睐，传统的地板清洁养护打蜡产品在使用时需清洁、养护打蜡多种产品分步进行，虽然效果尚可，但使用费时费力。同时，抗菌功能也成为消费者关注的居家清洁护理用品的主要功能之一，但目前多数木地板清洁护理打蜡产品不具有抗菌功能，即使部分具有抗菌作用的产品，抗菌性能、安全性及抗菌时效也较有限。如：CN101514272A中描述的木地板清洗护理剂的抗菌成分为异噻唑啉酮，虽然就有一定杀菌防霉功效，但是它在空气中易于分解，对眼睛和皮肤具有刺激性；CN103275621A中所描述的中草药防虫抗菌地板蜡其抗菌成分为中草药提取物，而中草药提取物在空气中易于氧化变质，不但会降低其抗菌功效，而且更加达不到持久抗菌。且在日常生活中，人们对木地板的清洁护理周期相对较长，更加需要一种具有持续抗菌功能的产品来呵护家人健康。
基于以上情况，本发明提供了一种长效抗菌多功能地板清洁蜡及其制备方法，其具有长效抗菌、清洁去污、修复细微划痕、滋润保养、光亮、除异味的多重功效，且无挥发性溶剂，pH中性，不污染室内环境，生产工艺简单、成本低，并且使用方便，可应用于家居商业各类实木地板、复合木地板、竹木地板等多种类型木地板的清洁护理打蜡。
发明内容
本发明涉一种长效抗菌多功能地板清洁蜡及其制备方法，为实现上述发明目的，本发明采用以下技术方案予以实现：
一种长效抗菌多功能地板清洁蜡，由以下原料按重量份组成，非离子表面活性剂1-10份，润湿剂1-5份，吐温20为1-5份，水溶助长剂2-10份，天然油脂0.5-5份，巴西棕榈蜡乳液0.1-5份，遮光剂0.1-2份，银离子抗菌剂0.05-5份，螯合剂0.1-10份，流变调节剂0.1-5份，余量为软化水，总计100份。
进一步的，所述脂肪醇聚氧乙烯醚中烷基链长度为C8-C18，EO数为3-15；进一步优选，所述非离子表面活性剂选自脂肪醇聚氧乙烯醚，优选烷基链长度为C8-C12，EO数为3-10。
进一步的，所述润湿剂为烷基糖苷，碳链长度为C6-C12。
进一步的，所述水溶助长剂选择短链醇或短链醇醚，碳链长度为C6-C12，进一步优化，所述水溶助长剂优选异己二醇或丙酮缩甘油。
其中所述的天然油脂优选棕榈油和橙油，其中棕榈油中脂肪酸饱和度较高，在自然环境下不易分解，可起到长期滋养木地板而不会产生酸败等问题，而橙油是天然的清洁剂，去除顽固污渍，消除异味。
进一步的，所述天然油脂选自但不限于棕榈油、椰子油、橙油中的一种或几种。
进一步的，所述遮光剂为苯乙烯/丙烯酸乳液，选自但不限于OP301、OP3255的一种或两种。
进一步的，所述螯合剂为柠檬酸钠、甲基甘氨酸二乙酰乙酸、α-葡庚糖酸钠中的一种，进一步优化，所述螯合剂优选甲基甘氨酸二乙酰乙酸。
进一步的，所述流变调节剂选自但不限于羧甲基纤维素、羟乙基纤维素、黄原胶中的一种或几种，进一步优化，所述流变调节剂优选黄原胶。
进一步优化，所述银离子抗菌剂为高活性银离子溶液，加量优选0.1-1份。
本发明还提供了一种长效抗菌多功能地板清洁蜡的制备方法：
所述地板清洁蜡由以下重量份组成：非离子表面活性剂1-10份，润湿剂1-5份，吐温20为1-5份，水溶助长剂2-10份，天然油脂0.5-5份，巴西棕榈蜡乳液0.1-5份，遮光剂0.1-2份，银离子抗菌剂0.05-5份，螯合剂0.1-10份，流变调节剂0.1-5份，余量为软化水，总计100份。首先向反应釜加入软化水，加热至50℃，在搅拌下，加入流变调节剂0.1-5份和水溶助长剂2-10份的混合溶液，搅拌40分钟且均匀后停止加热；依次向溶液中加入非离子表面活性剂1-10份、润湿剂1-5份、吐温20为1-5份、天然油脂0.5-5份、巴西棕榈蜡乳液0.1-5份、银离子抗菌剂0.05-5份、螯合剂0.1-10份、遮光剂0.1-2份，搅拌20分钟后均匀即成。
本发明具有以下特点及优势：
1、具有长效抗菌、清洁去污、修复细微划痕、滋润保养、光亮、除异味多重功效；
2、使用时清洁打蜡一次完成，及其方便快捷，适合居家商业使用；
3、配方中复配多组分表面活性剂能够快速清除污渍；
4、小分子天然植物油脂结合较大分子量巴西棕榈蜡，渗透滋养，修复填补细微划痕，上光，且可有效隔离水分及保护地板；
5、银离子抗菌剂的加入能持续抗菌，减少地板霉变和异味；
6、遮光剂成分有效解决银离子抗菌剂在溶液中的不稳定的难题；
7、产品不含挥发性有机溶剂，不污染室内环境；
8、各种木地板均可使用，适用范围广泛。
具体实施方式
下面结合具体实施方式对本发明进行详细的说明。
本发明OP301和OP3255为苯乙烯/丙烯酸共聚物,购自于广州飞瑞化工有限公司。
实施例1
一种长效抗菌多功能地板清洁蜡，按重量份计各组分如下：
各组分的重量份数总和为100。
一种长效抗菌多功能地板清洁蜡的制备方法按以下步骤实施：
首先向反应釜加入软化水，加热至50℃，在搅拌下，加入黄原胶0.5份和异己二醇6份的混合溶液，搅拌40分钟后，均匀并停止加热；依次向溶液中加入脂肪醇聚氧乙烯醚10份、烷基糖苷1份、吐温20为1份、棕榈油1.5份、橙油0.5份、巴西棕榈蜡乳液1份、银离子抗菌剂0.5份、甲基甘氨酸二乙酰乙酸0.2份、OP301为0.1份，搅拌20分钟后均匀即成。
实施例2
一种长效抗菌多功能地板清洁蜡，按重量份计各组分如下：
各组分的重量份数总和为100。
一种长效抗菌多功能地板清洁蜡的制备方法按以下步骤实施：
首先向反应釜加入软化水，加热至50℃，在搅拌下，加入黄原胶0.3份和丙酮缩甘油4份的混合溶液，搅拌40分钟后均匀并停止加热；依次向溶液中加入脂肪醇聚氧乙烯醚5份、烷基糖苷2份、吐温20为2份、棕榈油1.5份、橙油1份、巴西棕榈蜡乳液0.5份、银离子抗菌剂0.1份、甲基甘氨酸二乙酰乙酸0.5份、遮光剂3255为0.5份，搅拌20分钟均匀即成。
实施例3
一种长效抗菌多功能地板清洁蜡，按重量份计各组分如下：
各组分的重量份数总和为100。
一种长效抗菌多功能地板清洁蜡的制备方法按以下步骤实施：
首先向反应釜加入软化水，加热至50℃，在搅拌下，加入黄原胶0.3份和丙酮缩甘油4份的混合溶液，搅拌均匀并停止加热；依次向溶液中加入脂肪醇聚氧乙烯醚1份、烷基糖苷3份、吐温20为5份、棕榈油1份、橙油0.5份、巴西棕榈蜡乳液0.5份、银离子抗菌剂0.1份、甲基甘氨酸二乙酰乙酸0.5份、遮光剂3255为0.5份，搅拌均匀即成。
实施例4
一种长效抗菌多功能地板清洁蜡，按重量份计各组分如下：
各组分的重量份数总和为100。
一种长效抗菌多功能地板清洁蜡的制备方法按以下步骤实施：首先向反应釜加入软化水，加热至50℃，在搅拌下，加入羧甲基纤维素0.3份和丙酮缩甘油2份的混合溶液，搅拌40分钟后均匀并停止加热；依次向溶液中加入脂肪醇聚氧乙烯醚5份、烷基糖苷2份、吐温20为2份、椰子油1份、橙油1份、巴西棕榈蜡乳液0.5份、银离子抗菌剂1份、柠檬酸钠1份、遮光剂3255为0.5份，搅拌20分钟均匀即成。
实施例5
一种长效抗菌多功能地板清洁蜡，按重量份计各组分如下：
各组分的重量份数总和为100。
一种长效抗菌多功能地板清洁蜡的制备方法按以下步骤实施：
首先向反应釜加入软化水，加热至50℃，在搅拌下，加入羟乙基纤维素0.5份和丙酮缩甘油4份的混合溶液，搅拌40分钟后均匀并停止加热；依次向溶液中加入脂肪醇聚氧乙烯醚6份、烷基糖苷2份、吐温20为3份、椰子油1份、橙油0.5份、巴西棕榈蜡乳液2份、银离子抗菌剂0.5份、α-葡庚糖酸钠0.5份、遮光剂3255为0.2份，搅拌20分钟均匀即成。
以下为本发明的性能测试说明：
实验1：实施例理化指标测试。
上述实施例进行理化指标测试，具体结果如下：
实验2：实施例光泽增加值的测试。
测试方法按照QB/T2991-2008《木制品上光蜡》方法执行，评价结果如下：
实验3：实施例去污性能测试。
测试方法按照QB/T4532-2013《硬质地板清洗剂》执行，评价结果如下：
| 实施例1 | 实施例2 | 实施例3 | 市售产品① | 市售产品② | 市售产品③ | |
| 去污力％ | 94.22 | 93.47 | 92.54 | 74.83 | 90.62 | 88.46 |
实验4：实施例长效抗菌性能测试。
实验方法参照《消毒技术规范》2002版中的贴膜实验方法，通过将细菌污染于抗菌样片表面，然后用塑料薄膜覆盖，使细菌与抗菌制品表面充分接触，以测定其抗菌效果。抗菌样片采用消毒后的载玻片均匀涂抹实施例样品并放置于25℃恒温箱中7天后进行实验。微生物菌种为：大肠杆菌(ATCC 8099)、金黄色葡萄球菌(ATCC 6538)，测试液体为样品原液，作用时间为5min。
根测试结果如下：
a：实施例4为不添加遮光剂的实施例2配方
本发明的内容不限于实施例所列举，本领域普通技术人员通过阅读本发明说明书而对本发明技术方案采取的任何等同替换，均为本发明的权利要求所涵盖。
Claims (10)
1.一种长效抗菌多功能地板清洁蜡，其特征在于，以下原料按重量份组成：
各组分的重量份数总和为100。
2.根据权利要求1所述的一种长效抗菌多功能地板清洁蜡，其特征在于，所述非离子表面活性剂为脂肪醇聚氧乙烯醚。
3.根据权利要求2所述的一种长效抗菌多功能地板清洁蜡，其特征在于，所述脂肪醇聚氧乙烯醚中，烷基链长度为C8-C18，EO数为3-15。
4.根据权利要求1所述的一种长效抗菌多功能地板清洁蜡，其特征在于，所述润湿剂为烷基糖苷，碳链长度为C6-C12。
5.根据权利要求1所述的一种长效抗菌多功能地板清洁蜡，其特征在于，所述水溶助长剂选自短链醇或短链醇醚，碳链长度为C6-C12。
6.根据权利要求1所述的一种长效抗菌多功能地板清洁蜡，其特征在于，所述天然油脂选自但不限于棕榈油、椰子油、橙油中的一种或几种。
7.根据权利要求1所述的一种长效抗菌多功能地板清洁蜡，其特征在于，所述遮光剂为苯乙烯/丙烯酸乳液。
8.根据权利要求1所述的一种长效抗菌多功能地板清洁蜡，其特征在于，所述螯合剂为柠檬酸钠、甲基甘氨酸二乙酰乙酸、α-葡庚糖酸钠中的一种。
9.根据权利要求1所述的一种长效抗菌多功能地板清洁蜡，其特征在于，所述流变调节剂选自但不限于羧甲基纤维素、羟乙基纤维素、黄原胶中的一种或几种。
10.一种制备权利要求1-9任意一项所述的长效抗菌多功能地板清洁蜡的方法，其特征在于，所述方法按以下步骤实施：
步骤1、按照权利要求1所述的重量份称量配料，总计100份；
步骤2、反应釜加软化水，加热至80℃，搅拌下加入流变调节剂和水溶助长剂的混合溶液，搅拌40分钟，直至无悬浮不溶物，停止加热；
步骤3、依次向步骤2得到的溶液中加入非离子表面活性剂、润湿剂、吐温20、天然油脂、巴西棕榈蜡乳液、银离子抗菌剂、螯合剂、遮光剂，添加完后搅拌20分钟，搅拌均匀即成。
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