CN108853168B - Incense with chrysanthemum fragrance and preparation method thereof - Google Patents

Incense with chrysanthemum fragrance and preparation method thereof Download PDF

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CN108853168B
CN108853168B CN201810768986.5A CN201810768986A CN108853168B CN 108853168 B CN108853168 B CN 108853168B CN 201810768986 A CN201810768986 A CN 201810768986A CN 108853168 B CN108853168 B CN 108853168B
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chrysanthemum
parts
incense
fragrance
mica powder
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CN108853168A (en
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王磊
蔡忠弟
江洁
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Chuzhou Vocational and Technical College
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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18Magnoliophyta (angiosperms)
    • A61K36/185Magnoliopsida (dicotyledons)
    • A61K36/28Asteraceae or Compositae (Aster or Sunflower family), e.g. chamomile, feverfew, yarrow or echinacea
    • A61K36/287Chrysanthemum, e.g. daisy
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K47/00Medicinal preparations characterised by the non-active ingredients used, e.g. carriers or inert additives; Targeting or modifying agents chemically bound to the active ingredient
    • A61K47/02Inorganic compounds
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K47/00Medicinal preparations characterised by the non-active ingredients used, e.g. carriers or inert additives; Targeting or modifying agents chemically bound to the active ingredient
    • A61K47/30Macromolecular organic or inorganic compounds, e.g. inorganic polyphosphates
    • A61K47/32Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds, e.g. carbomers, poly(meth)acrylates, or polyvinyl pyrrolidone
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K47/00Medicinal preparations characterised by the non-active ingredients used, e.g. carriers or inert additives; Targeting or modifying agents chemically bound to the active ingredient
    • A61K47/30Macromolecular organic or inorganic compounds, e.g. inorganic polyphosphates
    • A61K47/36Polysaccharides; Derivatives thereof, e.g. gums, starch, alginate, dextrin, hyaluronic acid, chitosan, inulin, agar or pectin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K9/00Medicinal preparations characterised by special physical form
    • A61K9/0012Galenical forms characterised by the site of application
    • A61K9/007Pulmonary tract; Aromatherapy
    • A61K9/0073Sprays or powders for inhalation; Aerolised or nebulised preparations generated by other means than thermal energy
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61PSPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
    • A61P11/00Drugs for disorders of the respiratory system
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61PSPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
    • A61P27/00Drugs for disorders of the senses
    • A61P27/02Ophthalmic agents
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61PSPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
    • A61P29/00Non-central analgesic, antipyretic or antiinflammatory agents, e.g. antirheumatic agents; Non-steroidal antiinflammatory drugs [NSAID]
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61PSPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
    • A61P9/00Drugs for disorders of the cardiovascular system
    • A61P9/12Antihypertensives

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Abstract

The invention discloses a chrysanthemum fragrance, which comprises the following raw materials in parts by weight: 50-82 parts of chrysanthemum overground part, 0-20 parts of talcum powder, 0-20 parts of chrysanthemum essence and 4-10 parts of adhesive. The invention also discloses a preparation method of the incense with chrysanthemum fragrance, which comprises the following steps: cutting the above-ground part of the chrysanthemum into segments, crushing the segments to 80-120 meshes, adding other residual raw materials, and uniformly mixing to obtain a mixture; adding water, and stirring for 45-60min to obtain dough-like material; then pressing and forming, drying in the shade to obtain the incense with chrysanthemum fragrance, wherein the weight ratio of the mixture to the water is 1: 1-1.5, drying in the shade at 20-30 deg.C for 2-3 days. The invention has the advantages of fragrance, wind dispelling, liver calming, tranquilizing, antibacterial and anti-inflammatory effects, and can effectively adsorb fine particles released in the combustion process.

Description

Incense with chrysanthemum fragrance and preparation method thereof
Technical Field
The invention relates to the technical field of incense, in particular to incense with chrysanthemum fragrance and a preparation method thereof.
Background
The traditional incense has single effect. In recent years, many kinds of perfumes having various effects such as saussurea lappa, aquilaria sinensis, a perfume having a characteristic of green tea, and the like have been researched and developed. The chrysanthemum is a composite plant used as both medicine and food, the flower and stem of the chrysanthemum mainly contain volatile oil, flavonoid, phenolic acid and other active substances, and the emitted faint scent has the effects of dispelling wind and heat, calming the liver, improving eyesight, resisting bacteria, diminishing inflammation, tranquilizing and allaying excitement. Has certain relieving effect on wind-heat type common cold, headache, dizziness, conjunctival congestion, swelling and pain, dim eyesight, hypertension and the like.
Chrysanthemum is produced in Chuzhou, is usually viewed and appreciated, is prepared into scented tea and traditional Chinese medicines, or is extracted from effective components in chrysanthemum, stems, leaves and defective flowers of the chrysanthemum are usually discarded, a large amount of waste is easily generated to pollute the environment, or the stems and leaves are simply processed to prepare pillows with health care effects, and further deep processing, development and utilization cannot be carried out.
Disclosure of Invention
Based on the technical problems in the background art, the invention provides a chrysanthemum fragrance and a preparation method thereof, the chrysanthemum fragrance is fragrant and has the effects of dispelling wind and calming the liver, tranquilizing and allaying excitement, resisting bacteria and diminishing inflammation, and the chrysanthemum fragrance can effectively adsorb fine particles released in the combustion process.
The invention provides a chrysanthemum fragrance, which comprises the following raw materials in parts by weight: 50-82 parts of chrysanthemum overground part, 0-20 parts of talcum powder, 0-20 parts of chrysanthemum essence and 4-10 parts of adhesive.
Preferably, the aerial parts of the chrysanthemum are dried by sun.
Preferably, the above-ground part of the chrysanthemum is one of a chrysanthemum stem, a mixture of chrysanthemum stem and chrysanthemum leaf, and a mixture of chrysanthemum stem, chrysanthemum leaf and chrysanthemum flower.
Preferably, the binder is at least one of starch, guar gum, sticky powder and polyacrylamide.
Preferably, the raw material further comprises pigment, wherein the pigment is bright yellow, basic orange, tea green, pinkish green, etc.
Preferably, the raw materials also comprise an adsorbent, wherein the weight ratio of the chrysanthemum stems to the adsorbent is 50-82: 10-15.
Preferably, the adsorbent is modified mica powder, straw charcoal powder and montmorillonite, wherein the weight ratio of the modified mica powder to the straw charcoal powder to the montmorillonite is 1-3: 1-2: 0.5-1.
Preferably, in the preparation process of the modified mica powder, adding the mica powder into a guar gum water solution with the mass fraction of 1-3wt% and uniformly mixing, swelling for 20-24h, cooling to-40 to-60 ℃, and carrying out freeze vacuum drying for 24-36h to obtain an intermediate material; adding the intermediate material into a borax water solution with the mass fraction of 4-6wt%, uniformly mixing, standing for 10-30min, washing with water, cooling to-40 to-60 ℃, freezing, vacuum-drying for 24-36h, and crushing to obtain the modified mica powder.
Preferably, in the preparation process of the modified mica powder, the weight ratio of the mica powder to the guar gum is 7-8: 2-3, wherein the volume ratio of the guar gum aqueous solution to the borax aqueous solution is 1-1.5: 1.
preferably, the modified mica powder is 80-120 meshes, the straw charcoal powder is 100-200 meshes, and the montmorillonite is 400-600 meshes.
The invention also provides a preparation method of the incense with chrysanthemum fragrance, which comprises the following steps: cutting the above-ground part of the chrysanthemum into segments, crushing the segments to 80-120 meshes, adding other residual raw materials, and uniformly mixing to obtain a mixture; adding water, and stirring for 45-60min to obtain dough-like material; then pressing and forming, drying in the shade to obtain the incense with chrysanthemum fragrance, wherein the weight ratio of the mixture to the water is 1: 1-1.5, drying in the shade at 20-30 deg.C for 2-3 days.
The talcum powder and the chrysanthemum essence are both food grade.
The chrysanthemum tea adopts the above-ground part of the chrysanthemum and the chrysanthemum essence to be matched with each other, so that the chrysanthemum tea has the faint scent of the chrysanthemum after burning, has the functions of dispelling wind and calming the liver, tranquilizing and allaying excitement, resisting bacteria and diminishing inflammation, increases the health-care performance of the chrysanthemum tea, and is suitable for being used in household and office occasions; the chrysanthemum stems, the chrysanthemum leaves and the chrysanthemum flowers are selected as raw materials, are cheap and easy to obtain, can relieve the pollution of the chrysanthemum stems, the chrysanthemum leaves and the chrysanthemum flowers to the environment, and change waste into valuable; in addition, at least one of starch, guar gum, sticky powder and polyacrylamide is used as a bonding agent, so that the anti-bending and anti-bending properties of the incense can be increased by tightly bonding all the substances, and the problem that the incense is easy to break is solved; because the incense is slowly combusted, fine particles are easily released in the combustion process, the health care effects of dispelling wind and calming the liver, tranquilizing and allaying excitement, resisting bacteria and diminishing inflammation are reduced, the mica powder, the straw charcoal powder and the montmorillonite all have good adsorption performance, the mica powder swells in guar gum aqueous solution, so that guar gum is coated on the surface of the mica powder and enters between layers of the mica powder, then the guar gum is crosslinked into a net structure on the surface of the mica powder and between the layers through borax, and then a porous net structure is formed on the surface of the mica powder and between the layers through freezing and vacuum drying, so that the adsorption performance of the mica powder is greatly improved, the fine particles released by combustion can be effectively adsorbed, and the health care performance of the invention is greatly improved; the modified mica powder, the straw charcoal powder and the montmorillonite are matched with each other according to a proper proportion and a proper particle size, so that the adsorption performance of the composite material can be further improved, and the composite material can be matched with an adhesive to improve the folding resistance and the bending resistance of the composite material.
Detailed Description
The technical solution of the present invention will be described in detail below with reference to specific examples.
Example 1
The incense with chrysanthemum fragrance comprises the following raw materials in parts by weight: 70 parts of chrysanthemum overground part, 10 parts of talcum powder, 10 parts of chrysanthemum essence and 10 parts of adhesive.
The preparation method of the incense with chrysanthemum fragrance comprises the following steps: cutting the above-ground part of the chrysanthemum into segments, crushing the segments to 100 meshes, adding other residual raw materials, and uniformly mixing to obtain a mixture; adding water, and stirring for 53min to obtain dough-like material; then pressing and forming, drying in the shade to obtain the incense with chrysanthemum fragrance, wherein the weight ratio of the mixture to the water is 1: 1.25, the drying temperature in the shade is 25 ℃, and the drying time in the shade is 3 days.
Example 2
The incense with chrysanthemum fragrance comprises the following raw materials in parts by weight: 58 parts of dried chrysanthemum stems, 15 parts of talcum powder, 20 parts of chrysanthemum essence and 7 parts of polyacrylamide.
The preparation method of the incense with chrysanthemum fragrance comprises the following steps: cutting dried chrysanthemum stems into segments, crushing the cut dried chrysanthemum stems into 80 meshes, adding other residual raw materials, and uniformly mixing to obtain a mixture; adding water, and stirring for 60min to obtain dough-like material; then pressing and forming, drying in the shade to obtain the incense with chrysanthemum fragrance, wherein the weight ratio of the mixture to the water is 1: 1, drying in the shade at 20 ℃ for 3 days.
Example 3
The incense with chrysanthemum fragrance comprises the following raw materials in parts by weight: 60 parts of dried chrysanthemum stems, 20 parts of dried chrysanthemum leaves, 8 parts of chrysanthemum essence, 10 parts of polyacrylamide and 2 parts of light yellow.
The preparation method of the incense with chrysanthemum fragrance comprises the following steps: cutting dried chrysanthemum stems and dried chrysanthemum leaves into segments, crushing the cut dried chrysanthemum stems and dried chrysanthemum leaves into 100 meshes, adding other residual raw materials, and uniformly mixing to obtain a mixture; adding water, and stirring for 60min to obtain dough-like material; then pressing and forming, drying in the shade to obtain the incense with chrysanthemum fragrance, wherein the weight ratio of the mixture to the water is 1: 1.2, drying in the shade at 25 ℃ for 2 days.
Example 4
The incense with chrysanthemum fragrance comprises the following raw materials in parts by weight: 36 parts of dried chrysanthemum stems, 46 parts of dried chrysanthemum leaves, 10 parts of guar gum and 4 parts of tea green essence.
The preparation method of the incense with chrysanthemum fragrance comprises the following steps: cutting dried chrysanthemum stems and dried chrysanthemum leaves into segments, crushing the cut dried chrysanthemum stems and dried chrysanthemum leaves into 120 meshes, adding other residual raw materials, and uniformly mixing to obtain a mixture; adding water and stirring for 45min to obtain a dough-like material; then pressing and forming, drying in the shade to obtain the incense with chrysanthemum fragrance, wherein the weight ratio of the mixture to the water is 1: 1.2, the drying temperature in the shade is 30 ℃, and the drying time in the shade is 2 days.
Example 5
The incense with chrysanthemum fragrance comprises the following raw materials in parts by weight: 50 parts of dried chrysanthemum stems, 20 parts of talcum powder, 10 parts of chrysanthemum essence, 4 parts of polyacrylamide and 10 parts of adsorbent;
the adsorbent is 120-mesh modified mica powder, 100-mesh straw charcoal powder and 600-mesh montmorillonite, wherein the weight ratio of the modified mica powder to the straw charcoal powder to the montmorillonite is 1: 2: 0.5;
in the preparation process of the modified mica powder, adding the mica powder into guar gum water solution with the mass fraction of 3wt% and uniformly mixing, swelling for 20h, cooling to-60 ℃, and carrying out freeze vacuum drying for 24h to obtain an intermediate material; adding the intermediate material into a borax water solution with the mass fraction of 6wt%, uniformly mixing, standing for 10min, washing, cooling to-60 ℃, carrying out freeze vacuum drying for 24h, and crushing to obtain modified mica powder, wherein the weight ratio of the mica powder to the guar gum is 4: 1, the volume ratio of the guar gum aqueous solution to the borax aqueous solution is 1.5: 1.
the preparation method of the incense with chrysanthemum fragrance comprises the following steps: cutting dried chrysanthemum stems into segments, crushing the cut dried chrysanthemum stems into 80 meshes, adding other residual raw materials, and uniformly mixing to obtain a mixture; adding water, and stirring for 55min to obtain dough-like material; then pressing and forming, drying in the shade to obtain the incense with chrysanthemum fragrance, wherein the weight ratio of the mixture to the water is 1: 1.1, drying in the shade at 28 ℃ for 2 days.
Example 6
The incense with chrysanthemum fragrance comprises the following raw materials in parts by weight: 60 parts of dried chrysanthemum overground part, 15 parts of talcum powder, 5 parts of chrysanthemum essence, 9 parts of adhesive and 15 parts of adsorbent;
wherein, the overground part of the chrysanthemum is a mixture of chrysanthemum stems, chrysanthemum leaves and chrysanthemum flowers;
the adhesive is starch, sticky powder and polyacrylamide;
the adsorbent is 80-mesh modified mica powder, 200-mesh straw charcoal powder and 400-mesh montmorillonite, wherein the weight ratio of the modified mica powder to the straw charcoal powder to the montmorillonite is 3: 1: 1;
in the preparation process of the modified mica powder, adding the mica powder into guar gum water solution with the mass fraction of 1 wt% and uniformly mixing, swelling for 24 hours, cooling to-40 ℃, and carrying out freeze vacuum drying for 36 hours to obtain an intermediate material; adding the intermediate material into a borax water solution with the mass fraction of 4 wt%, uniformly mixing, standing for 30min, washing, cooling to-40 ℃, carrying out freeze vacuum drying for 36h, and crushing to obtain modified mica powder, wherein the weight ratio of the mica powder to the guar gum is 7: 3, the volume ratio of the guar gum aqueous solution to the borax aqueous solution is 1: 1.
the preparation method of the incense with chrysanthemum fragrance comprises the following steps: cutting the overground part of the dried chrysanthemum into segments, crushing the segments into 120 meshes, adding other residual raw materials, and uniformly mixing to obtain a mixture; adding water, and stirring for 50min to obtain dough-like material; then pressing and forming, drying in the shade to obtain the incense with chrysanthemum fragrance, wherein the weight ratio of the mixture to the water is 1: 1.4, drying in the shade at 25 ℃ for 3 days.
Test example 1
The performance tests of example 5 and example 6 were carried out, and the results were as follows:
detecting items Breaking resistance g Water content% Smoke amount mg/g Fragrance
Example 5 461 4.5 2.5 Chrysanthemum fragrance
Example 6 463 4.0 2.6 Chrysanthemum fragrance
As can be seen from the above table, the invention has high breaking strength, less smoke and dust after combustion and chrysanthemum fragrance.
The above description is only for the preferred embodiment of the present invention, but the scope of the present invention is not limited thereto, and any person skilled in the art should be considered to be within the technical scope of the present invention, and the technical solutions and the inventive concepts thereof according to the present invention should be equivalent or changed within the scope of the present invention.

Claims (4)

1. The incense with chrysanthemum fragrance is characterized by being prepared from the following raw materials in parts by weight: 50-82 parts of chrysanthemum overground part, 0-20 parts of talcum powder, 0-20 parts of chrysanthemum essence, 4-10 parts of adhesive and adsorbent;
wherein the weight ratio of the overground part of the chrysanthemum to the adsorbent is 50-82: 10-15 parts of;
the adsorbent is modified mica powder, straw charcoal powder and montmorillonite, wherein the weight ratio of the modified mica powder to the straw charcoal powder to the montmorillonite is 1-3: 1-2: 0.5 to 1;
in the preparation process of the modified mica powder, adding the mica powder into a guar gum water solution with the mass fraction of 1-3wt%, uniformly mixing, swelling for 20-24h, cooling to-40 to-60 ℃, and carrying out freeze vacuum drying for 24-36h to obtain an intermediate material; adding the intermediate material into a borax water solution with the mass fraction of 4-6wt%, uniformly mixing, standing for 10-30min, washing with water, cooling to-40 to-60 ℃, freeze-vacuum drying for 24-36h, and crushing to obtain modified mica powder;
in the preparation process of the modified mica powder, the weight ratio of the mica powder to the guar gum is 7-8: 2-3, wherein the volume ratio of the guar gum aqueous solution to the borax aqueous solution is 1-1.5: 1;
the modified mica powder is 80-120 meshes, the straw charcoal powder is 100-200 meshes, and the montmorillonite is 400-600 meshes;
the adhesive is at least one of starch, guar gum, sticky powder and polyacrylamide.
2. Incense with chrysanthemum aroma according to claim 1, characterized in that the aerial part of the chrysanthemum is sun-dried.
3. Incense with chrysanthemum aroma according to claim 1 or 2, wherein the above-ground part of the chrysanthemum is one of the group consisting of a chrysanthemum stem, a mixture of chrysanthemum stems and chrysanthemum leaves, and a mixture of chrysanthemum stems, chrysanthemum leaves and chrysanthemum flowers.
4. A process for the preparation of a fragrance having a chrysanthemum fragrance as claimed in any one of claims 1 to 3, characterized by comprising the following steps: cutting the above-ground part of the chrysanthemum into segments, crushing the segments to 80-120 meshes, adding other residual raw materials, and uniformly mixing to obtain a mixture; adding water, and stirring for 45-60min to obtain dough-like material; then pressing and forming, drying in the shade to obtain the incense with chrysanthemum fragrance, wherein the weight ratio of the mixture to the water is 1: 1-1.5, drying in the shade at 20-30 deg.C for 2-3 days.
CN201810768986.5A 2018-07-13 2018-07-13 Incense with chrysanthemum fragrance and preparation method thereof Active CN108853168B (en)

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CN111135795A (en) * 2020-01-21 2020-05-12 温州子久堂生物科技有限公司 Preparation method and application of adsorption material for gardenia essential oil head fragrance extraction
CN113425880A (en) * 2021-04-29 2021-09-24 河北古城香业集团股份有限公司 Environment-friendly smokeless incense and preparation method thereof
CN114470288B (en) * 2022-03-14 2023-08-22 浙江宋朝臻选科技有限公司 Fragrance with relieving effect and preparation method thereof

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101020071A (en) * 2006-07-18 2007-08-22 马德学 Incense made of chrysanthemum powder and chrysanthemum charcoal powder
CN101946806A (en) * 2010-01-18 2011-01-19 中山榄菊日化实业有限公司 Combustion mosquito coil incense and preparation method thereof
CN103891783A (en) * 2014-02-26 2014-07-02 张燕 Mosquito-repellent incense and preparation method thereof
CN107810954A (en) * 2017-10-25 2018-03-20 成都彩虹电器(集团)股份有限公司 A kind of white mosquito-repellent incense and preparation method thereof

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101020071A (en) * 2006-07-18 2007-08-22 马德学 Incense made of chrysanthemum powder and chrysanthemum charcoal powder
CN101946806A (en) * 2010-01-18 2011-01-19 中山榄菊日化实业有限公司 Combustion mosquito coil incense and preparation method thereof
CN103891783A (en) * 2014-02-26 2014-07-02 张燕 Mosquito-repellent incense and preparation method thereof
CN107810954A (en) * 2017-10-25 2018-03-20 成都彩虹电器(集团)股份有限公司 A kind of white mosquito-repellent incense and preparation method thereof

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