CN100402094C - Liquid Tibetan incense and its prepn. method - Google Patents
Liquid Tibetan incense and its prepn. method Download PDFInfo
- Publication number
- CN100402094C CN100402094C CNB2006100215723A CN200610021572A CN100402094C CN 100402094 C CN100402094 C CN 100402094C CN B2006100215723 A CNB2006100215723 A CN B2006100215723A CN 200610021572 A CN200610021572 A CN 200610021572A CN 100402094 C CN100402094 C CN 100402094C
- Authority
- CN
- China
- Prior art keywords
- water
- ethanol
- volatile oil
- thick paste
- extractum
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
Images
Landscapes
- Medicines Containing Plant Substances (AREA)
- Fats And Perfumes (AREA)
- Cosmetics (AREA)
Abstract
A liquid-state Tibetan incense as a fumigant is prepared from 8 Chinese-medicinal materials including Himalaya common four-o'clock, sandal wood, cloves, borneol, etc through distilling the extract volatile oil and aromatic liquid, concentrating, depositing in alcohol, and mixing.
Description
(1) technical field:
A kind of liquid Tibetan incense and preparation method thereof belongs to the scent goods, particularly is the scent goods of raw material with the plant, and its preparation method.
(2) background technology:
The present scent goods that are used to purify air that use of people, the usually said perfume (or spice) of people just, as Lignum Santali Albi, India's perfume (or spice), the overwhelming majority exists with solid-state form, needs during use light with fire, discharges the scent material in incendiary mode and purifies air.The shortcoming that its exists is: 1, it wants contaminated air equally when burning, causes secondary pollution, and particularly easier contaminated air during concentrated combustion is unfavorable for environmental protection; 2, the existing way of this solid perfume (or spice) is to smear the scent raw material at an end of bamboo let, takes up room, and inconvenience is carried, and using method is single, is unsuitable for the traveller especially and uses; 3, this fragrant most single raw materials that adopt, fragrance is single, and its function of use also is restricted.
(3) summary of the invention:
The problem to be solved in the present invention provides a kind of easy to carry, clean environment firendly at above deficiency exactly, can not produce secondary pollution, and the various liquid Tibetan incense of using method.Its technical scheme is as follows:
It mainly is to be made by the raw material that comprises following weight parts:
Lignum Santali Albi 5-20, Lignum Aquilariae Resinatum 5-20, Flos Caryophylli 5-20, Radix Et Rhizoma Nardostachyos 5-20, Himalaya Mirabilis jalapa 5-20, Semen Myristicae 5-20, Radix Inulae 5-20, Borneolum Syntheticum 5-15
In order to reach better effect, medicine material of the present invention also comprises Fructus Tsaoko 5-20 or/and Cortex Cinnamomi 5-20.
In order to obtain optimum efficiency, medicine material of the present invention further comprises Fructus Chebulae 5-20 or/and Radix Angelicae Sinensis 5-20.
Preparation method of the present invention may further comprise the steps:
1) Lignum Santali Albi, Lignum Aquilariae Resinatum, Flos Caryophylli, Radix Et Rhizoma Nardostachyos, Himalaya Mirabilis jalapa, Semen Myristicae, Radix Inulae are added 6--8 times of water gaging, distilled 2.5-3.5 hour, it is standby to collect volatile oil and Aromatic water;
2) will collect medicinal residues behind volatile oil and the Aromatic water and medicinal liquid and add water to 8--12 and doubly measure, and boil and extract 2-3 time, extract 1.5-2.5 hour at every turn, filter, merging filtrate refilters, is to concentrate under the 0.04-0.06Mpa condition filtrate at 50--70 ℃, vacuum, receives cream;
3) with above-mentioned extractum with 80-85% ethanol precipitation 24-30 hour, reclaim ethanol, be to be concentrated into thick paste under the 0.04-0.06Mpa condition with extractum at 50-70 ℃, vacuum, thick paste is dissolved in the 90%-95% ethanol, make the thick paste alcoholic solution, standby;
4) Borneolum Syntheticum, volatile oil, Aromatic water are dissolved in the 90%--95% ethanol altogether, add in the above-mentioned thick paste alcoholic solution, mixing is adjusted relative density to 1.05-1.08, promptly.
If also with the Fructus Tsaoko combination, its preparation method is:
1) Lignum Santali Albi, Lignum Aquilariae Resinatum, Flos Caryophylli, Radix Et Rhizoma Nardostachyos, Fructus Tsaoko, Himalaya Mirabilis jalapa, Semen Myristicae, Radix Inulae are added 6--8 times of water gaging, distilled 2.5-3.5 hour, it is standby to collect volatile oil and Aromatic water;
2) will collect medicinal residues behind volatile oil and the Aromatic water and medicinal liquid and add water to 8--12 and doubly measure, and boil and extract 2-3 time, extract 1.5-2.5 hour at every turn, filter, merging filtrate refilters, is to concentrate under the 0.04-0.06Mpa condition filtrate at 50--70 ℃, vacuum, receives cream;
3) with above-mentioned extractum with 80-85% ethanol precipitation 24-30 hour, reclaim ethanol, be to be concentrated into thick paste under the 0.04-0.06Mpa condition with extractum at 50-70 ℃, vacuum, be dissolved in the 90%-95% ethanol thick paste standby;
4) Borneolum Syntheticum, volatile oil, Aromatic water are dissolved in the 90%--95% ethanol altogether, add in the above-mentioned thick paste alcoholic solution, mixing is adjusted relative density to 1.05-1.08, promptly.
If also with the Cortex Cinnamomi combination, its preparation method is:
1) Lignum Santali Albi, Lignum Aquilariae Resinatum, Flos Caryophylli, Radix Et Rhizoma Nardostachyos, Fructus Tsaoko, Cortex Cinnamomi, Himalaya Mirabilis jalapa, Semen Myristicae, Radix Inulae are added 6--8 times of water gaging, distilled 2.5-3.5 hour, it is standby to collect volatile oil and Aromatic water;
2) will collect medicinal residues behind volatile oil and the Aromatic water and medicinal liquid and add water to 8--12 and doubly measure, and boil and extract 2-3 time, extract 1.5-2.5 hour at every turn, filter, merging filtrate refilters, is to concentrate under the 0.04-0.06Mpa condition filtrate at 50--70 ℃, vacuum, receives cream;
3) with above-mentioned extractum with 80-85% ethanol precipitation 24-30 hour, reclaim ethanol, be to be concentrated into thick paste under the 0.04-0.06Mpa condition with extractum at 50-70 ℃, vacuum, be dissolved in the 90%-95% ethanol thick paste standby;
4) Borneolum Syntheticum, volatile oil, Aromatic water are dissolved in the 90%--95% ethanol altogether, add in the above-mentioned thick paste alcoholic solution, mixing is adjusted relative density to 1.05-1.08, promptly.
If also with Fructus Chebulae's combination, its preparation method is:
1) Lignum Santali Albi, Lignum Aquilariae Resinatum, Flos Caryophylli, Radix Et Rhizoma Nardostachyos, Fructus Tsaoko, Cortex Cinnamomi, Himalaya Mirabilis jalapa, Semen Myristicae, Fructus Chebulae, Radix Inulae are added 6--8 times of water gaging, distilled 2.5-3.5 hour, it is standby to collect volatile oil and Aromatic water;
2) will collect medicinal residues behind volatile oil and the Aromatic water and medicinal liquid and add water to 8--12 and doubly measure, and boil and extract 2-3 time, extract 1.5-2.5 hour at every turn, filter, merging filtrate refilters, is to concentrate under the 0.04-0.06Mpa condition filtrate at 50--70 ℃, vacuum, receives cream;
3) with above-mentioned extractum with 80-85% ethanol precipitation 24-30 hour, reclaim ethanol, be to be concentrated into thick paste under the 0.04-0.06Mpa condition with extractum at 50-70 ℃, vacuum, be dissolved in the 90%-95% ethanol thick paste standby;
4) Borneolum Syntheticum, volatile oil, Aromatic water are dissolved in the 90%--95% ethanol altogether, add in the above-mentioned thick paste alcoholic solution, mixing is adjusted relative density to 1.05-1.08, promptly.
If also with the Radix Angelicae Sinensis combination, its preparation method is:
1) Lignum Santali Albi, Lignum Aquilariae Resinatum, Flos Caryophylli, Radix Et Rhizoma Nardostachyos, Fructus Tsaoko, Cortex Cinnamomi, Himalaya Mirabilis jalapa, Semen Myristicae, Fructus Chebulae, Radix Inulae, Radix Angelicae Sinensis are added 6-8 times of water gaging, distilled 2.5-3.5 hour, it is standby to collect volatile oil and Aromatic water;
2) will collect medicinal residues behind volatile oil and the Aromatic water and medicinal liquid and add water to 8--12 and doubly measure, and boil and extract 2-3 time, extract 1.5-2.5 hour at every turn, filter, merging filtrate refilters, is to concentrate under the 0.04-0.06Mpa condition filtrate at 50--70 ℃, vacuum, receives cream;
3) with above-mentioned extractum with 80-85% ethanol precipitation 24-30 hour, reclaim ethanol, be to be concentrated into thick paste under the 0.04-0.06Mpa condition with extractum at 50-70 ℃, vacuum, be dissolved in the 90-95% ethanol thick paste standby;
4) Borneolum Syntheticum, volatile oil, Aromatic water are dissolved in the 90%--95% ethanol altogether, add in the above-mentioned thick paste alcoholic solution, mixing is adjusted relative density to 1.05-1.08, promptly.
Be used for crude drug Radix Inulae of the present invention and promptly be recording in the Radix Inulae of one one of Pharmacopoeia of the People's Republic of China version in 2005, be called as Radix Inulae in the Tibetan area; The Himalaya Mirabilis jalapa records in " Drug Standard of Ministry of Public Health of the Peoples Republic of China " Tibetan medicine fascicle nineteen ninety-five version.
It is special to be used for crude drug Lignum Santali Albi of the present invention, Lignum Aquilariae Resinatum, Flos Caryophylli, Radix Inulae fragrance, can promoting the circulation of QI to relieve pain, promoting the flow of QI for relieving the stagnancy; Radix Et Rhizoma Nardostachyos, Himalaya Mirabilis jalapa, Borneolum Syntheticum can have one's ideas straightened out refreshment, resolving depression pain relieving, stifling with it, remove airborne different, the stink effect is fine, makes human body sensory salubrious, comfortable; After increasing Fructus Tsaoko, Cortex Cinnamomi, Fructus Chebulae, Radix Angelicae Sinensis in the prescription, remove airborne different, stink better effects if, make the people feel more salubrious, comfortable.Each medicine assembly energy fresh air is removed airborne different, stink, makes human body sensory salubrious, comfortable, and harmless, and crude drug source is natural plants, has no side effect, and is safe in utilization, reliable, uses the back noresidue, clean environment firendly.
Advantage of the present invention is: 1, it need not burn, and can not produce secondary pollution, helps environmental protection; 2, easy to carry, be particularly suitable for the traveller and use; 3, its prescription is reasonable, and scent is effective, and fragrance is moderate; 4, it can make solution dosage, spray, quintessence oil dosage form and inuncts etc., and using method is various.
(4) drawing explanation:
Accompanying drawing is a process chart of the present invention.
(5) specific embodiment:
Embodiment one:
Take by weighing each medicine by following weight proportion:
Lignum Santali Albi 13, Lignum Aquilariae Resinatum 13, Flos Caryophylli 13, Radix Et Rhizoma Nardostachyos 13, Himalaya Mirabilis jalapa 13, Semen Myristicae 13, Radix Inulae 13, Borneolum Syntheticum 9
Its preparation method may further comprise the steps:
1) Lignum Santali Albi, Lignum Aquilariae Resinatum, Flos Caryophylli, Radix Et Rhizoma Nardostachyos, Himalaya Mirabilis jalapa, Semen Myristicae, Radix Inulae are added 6 times of water gagings, distilled 3 hours, it is standby to collect volatile oil and Aromatic water;
2) will collect medicinal residues behind volatile oil and the Aromatic water and medicinal liquid and add water boil and extract 2 times, add water to 10 times of amounts for the first time, and boil and extracted 2 hours, medicinal liquid is crossed 120 mesh sieves, collects filtrate I, adds water to 8 times of amounts for the second time, extracted 1.5 hours, medicinal liquid is crossed 120 mesh sieves, collects filtrate II, merging filtrate I, II, centrifugal filtration is at 60 ℃, under the vacuum 0.04MPa, be concentrated into relative density 1.25, receive cream;
3) with above-mentioned extractum with 80% ethanol precipitation 24 hours, get supernatant, reclaim ethanol, at 50 ℃, under the vacuum 0.06MPa extractum is concentrated into the thick paste of relative density 1.25, thick paste is dissolved in makes the thick paste alcoholic solution in 95% ethanol, standby;
4) Borneolum Syntheticum, volatile oil, Aromatic water are dissolved in 95% ethanol altogether, add in the thick paste alcoholic solution, mixing is adjusted relative density to 1.05, makes liquid Tibetan incense, check, packing, outer package, warehouse-in.During use liquid Tibetan incense spilt in indoor or human body and get final product, also can be in container with its splendid attire, to the container heating, fragrance can fill the air and come then.
Embodiment two:
Take by weighing each medicine by following weight proportion:
Lignum Santali Albi 5, Lignum Aquilariae Resinatum 5, Flos Caryophylli 5, Radix Et Rhizoma Nardostachyos 5, Fructus Tsaoko 5, Himalaya Mirabilis jalapa 5, Semen Myristicae 5, Radix Inulae 5, Borneolum Syntheticum 5
Its preparation method may further comprise the steps:
1) Lignum Santali Albi, Lignum Aquilariae Resinatum, Flos Caryophylli, Radix Et Rhizoma Nardostachyos, Fructus Tsaoko, Himalaya Mirabilis jalapa, Semen Myristicae, Radix Inulae are added 6 times of water gagings, distilled 2.5 hours, it is standby to collect volatile oil and Aromatic water;
2) will collect medicinal residues behind volatile oil and the Aromatic water and medicinal liquid and add water boil and extract 2 times, add water to 8 times of amounts for the first time, and boil and extracted 1.5 hours, medicinal liquid is crossed 120 mesh sieves, collects filtrate I, adds water to 8 times of amounts for the second time, extracted 1.5 hours, medicinal liquid is crossed 120 mesh sieves, collects filtrate II, merging filtrate I, II, centrifugal filtration is at 70 ℃, under the vacuum 0.06MPa, be concentrated into relative density 1.35, receive cream;
3) with above-mentioned extractum with 85% ethanol precipitation 24 hours, get supernatant, reclaim ethanol, at 60 ℃, under the vacuum 0.04MPa extractum is concentrated into the thick paste of relative density 1.35, thick paste is dissolved in 95% ethanol, standby;
4) Borneolum Syntheticum, volatile oil, Aromatic water are dissolved in 95% ethanol altogether, add in the thick paste alcoholic solution, mixing is adjusted relative density to 1.08, and check is sub-packed in the automiser spray, makes the liquid Tibetan incense of spray, outer package again, warehouse-in.Be sprayed on the spray liquid Tibetan incense indoor during use or human body gets final product.
Embodiment three:
Take by weighing each medicine by following weight proportion:
Lignum Santali Albi 20, Lignum Aquilariae Resinatum 20, Flos Caryophylli 20, Radix Et Rhizoma Nardostachyos 20, Fructus Tsaoko 20, Cortex Cinnamomi 20, Himalaya Mirabilis jalapa 20, Semen Myristicae 20, Radix Inulae 20, Borneolum Syntheticum 15
Its preparation method may further comprise the steps:
1) Lignum Santali Albi, Lignum Aquilariae Resinatum, Flos Caryophylli, Radix Et Rhizoma Nardostachyos, Fructus Tsaoko, Cortex Cinnamomi, Himalaya Mirabilis jalapa, Semen Myristicae, Radix Inulae are added 8 times of water gagings, distilled 3.5 hours, it is standby to collect volatile oil and Aromatic water;
2) will collect medicinal residues behind volatile oil and the Aromatic water and medicinal liquid and add water boil and extract 3 times, add water to 10 times of amounts for the first time, and boil and extracted 2 hours, medicinal liquid is crossed 120 mesh sieves, collects filtrate I, adds water to 8 times of amounts for the second time and for the third time respectively, extracted 1.5 hours, medicinal liquid is crossed 120 mesh sieves, collects filtrate II and filtrate II I, merging filtrate I, II, III, centrifugal filtration is at 65 ℃, under the vacuum 0.05MPa, be concentrated into relative density 1.3, receive cream;
3) with above-mentioned extractum with 85% ethanol precipitation 30 hours, get supernatant, reclaim ethanol, at 55 ℃, under the vacuum 0.05MPa extractum is concentrated into the thick paste of relative density 1.3, thick paste is dissolved in 95% ethanol, standby;
4) Borneolum Syntheticum, volatile oil, Aromatic water are dissolved in 95% ethanol altogether, add in the thick paste alcoholic solution, mixing is adjusted relative density to 1.06, makes liquid Tibetan incense, check, packing, outer package, warehouse-in.
Embodiment four:
Take by weighing each medicine by following weight proportion:
Lignum Santali Albi 8, Lignum Aquilariae Resinatum 8, Flos Caryophylli 8, Radix Et Rhizoma Nardostachyos 8, Fructus Tsaoko 8, Cortex Cinnamomi 8, Himalaya Mirabilis jalapa 8, Semen Myristicae 8, Fructus Chebulae 8, Radix Inulae 8, Borneolum Syntheticum 6
Its preparation method may further comprise the steps:
1) Lignum Santali Albi, Lignum Aquilariae Resinatum, Flos Caryophylli, Radix Et Rhizoma Nardostachyos, Fructus Tsaoko, Cortex Cinnamomi, Himalaya Mirabilis jalapa, Semen Myristicae, Fructus Chebulae, Radix Inulae are added 8 times of water gagings, distilled 2.5 hours, it is standby to collect volatile oil and Aromatic water;
2) will collect medicinal residues behind volatile oil and the Aromatic water and medicinal liquid and add water boil and extract 2 times, add water to 12 times of amounts for the first time, and boil and extracted 2 hours, medicinal liquid is crossed 120 mesh sieves, collects filtrate I, adds water to 8 times of amounts for the second time, extracted 1.5 hours, medicinal liquid is crossed 120 mesh sieves, collects filtrate II, merging filtrate I, II, centrifugal filtration is at 70 ℃, under the vacuum 0.06MPa, be concentrated into relative density 1.25, receive cream;
3) with above-mentioned extractum with 80% ethanol precipitation 24 hours, get supernatant, reclaim ethanol, at 60 ℃, under the vacuum 0.05MPa extractum is concentrated into the thick paste of relative density 1.35, thick paste is dissolved in 95% ethanol, standby;
4) Borneolum Syntheticum, volatile oil, Aromatic water are dissolved in 95% ethanol altogether, add in the thick paste alcoholic solution, mixing is adjusted relative density to 1.07, makes liquid Tibetan incense, check, packing, outer package, warehouse-in.
Embodiment five:
Take by weighing each medicine by following weight proportion:
Lignum Santali Albi 18, Lignum Aquilariae Resinatum 18, Flos Caryophylli 18, Radix Et Rhizoma Nardostachyos 18, Fructus Tsaoko 18, Cortex Cinnamomi 18, the purple Rong Li 18 of Himalaya, Semen Myristicae 18, Fructus Chebulae 18, Radix Inulae 18, Radix Angelicae Sinensis 18, Borneolum Syntheticum 13
Its preparation method is: Lignum Santali Albi, Lignum Aquilariae Resinatum, Flos Caryophylli, Radix Et Rhizoma Nardostachyos, Fructus Tsaoko, Cortex Cinnamomi, Himalaya Mirabilis jalapa, Semen Myristicae, Fructus Chebulae, Radix Inulae, Radix Angelicae Sinensis are added 8 times of water gagings, distilled 3.5 hours, collect volatile oil I and Aromatic water; Medicinal residues and medicinal liquid behind collection volatile oil I and the Aromatic water are added water to 8 times of amounts, distilled 3.5 hours, collect volatile oil II, volatile oil I and volatile oil II are merged, add Borneolum Syntheticum, make a quintessence oil type joss stick produced in Xizang, check, packing, outer package is put in storage.Be applied in indoor during use or human body gets final product.
Embodiment six:
Take by weighing each medicine by following weight proportion:
Lignum Santali Albi 18, Lignum Aquilariae Resinatum 18, Flos Caryophylli 18, Radix Et Rhizoma Nardostachyos 18, Fructus Tsaoko 18, Cortex Cinnamomi 18, Himalaya Mirabilis jalapa 18, Semen Myristicae 18, Fructus Chebulae 18, Radix Inulae 18, Radix Angelicae Sinensis 18, Borneolum Syntheticum 13
Its preparation method may further comprise the steps:
1) Lignum Santali Albi, Lignum Aquilariae Resinatum, Flos Caryophylli, Radix Et Rhizoma Nardostachyos, Fructus Tsaoko, Cortex Cinnamomi, the purple Rong Li of Himalaya, Semen Myristicae, Fructus Chebulae, Radix Inulae, Radix Angelicae Sinensis are added 8 times of water gagings, distilled 2.5 hours, it is standby to collect volatile oil and Aromatic water;
2) will collect medicinal residues behind volatile oil and the Aromatic water and medicinal liquid and add water boil and extract 2 times, add water to 12 times of amounts for the first time, and boil and extracted 2 hours, medicinal liquid is crossed 120 mesh sieves, collects filtrate I, adds water to 8 times of amounts for the second time, extracted 1.5 hours, medicinal liquid is crossed 120 mesh sieves, collects filtrate II, merging filtrate I, II, centrifugal filtration, at 70 ℃, be concentrated into relative density 1.25 under the vacuum 0.06MPa, receive cream;
3) with above-mentioned extractum with 80% ethanol precipitation 24 hours, get supernatant, reclaim ethanol, at 60 ℃, under the vacuum 0.05MPa extractum is concentrated into the thick paste of relative density 1.35, thick paste is dissolved in 95% ethanol, standby;
4) Borneolum Syntheticum, volatile oil, Aromatic water are dissolved in 95% ethanol altogether, add in the thick paste alcoholic solution, mixing is adjusted relative density to 1.07, makes the liquid Tibetan incense inuncts, check, packing, outer package, warehouse-in.
Claims (10)
1. a liquid Tibetan incense is characterized in that it mainly comprises the raw material of following weight portion: Lignum Santali Albi 5-20, Lignum Aquilariae Resinatum 5-20, Flos Caryophylli 5-20, Radix Et Rhizoma Nardostachyos 5-20, Himalaya Mirabilis jalapa 5-20, Semen Myristicae 5-20, Radix Inulae 5-20, Borneolum Syntheticum 5-15.
2. the preparation method of the described liquid Tibetan incense of claim 1 is characterized in that may further comprise the steps:
1) Lignum Santali Albi, Lignum Aquilariae Resinatum, Flos Caryophylli, Radix Et Rhizoma Nardostachyos, Himalaya Mirabilis jalapa, Semen Myristicae, Radix Inulae are added 6--8 times of water gaging, distilled 2.5-3.5 hour, it is standby to collect volatile oil and Aromatic water;
2) will collect medicinal residues behind volatile oil and the Aromatic water and medicinal liquid and add water to 8--12 and doubly measure, and boil and extract 2-3 time, extract 1.5-2.5 hour at every turn, and filter, merging filtrate refilters, and filtrate is concentrated receipts extractum;
3) above-mentioned extractum is used 80-85% ethanol precipitation 24-30 hour, reclaim ethanol, extractum is concentrated into thick paste, be dissolved in the 90%--95% ethanol thick paste standby;
4) Borneolum Syntheticum, volatile oil, Aromatic water are dissolved in the 90%--95% ethanol altogether, add in the above-mentioned thick paste alcoholic solution, mixing is adjusted relative density to 1.05-1.08, promptly.
3. liquid Tibetan incense according to claim 1 is characterized in that wherein raw material also has Fructus Tsaoko 5-20.
4. the preparation method of liquid Tibetan incense according to claim 3 is characterized in that may further comprise the steps:
1) Lignum Santali Albi, Lignum Aquilariae Resinatum, Flos Caryophylli, Radix Et Rhizoma Nardostachyos, Fructus Tsaoko, Himalaya Mirabilis jalapa, Semen Myristicae, Radix Inulae are added 6 times of water gagings, distilled 3 hours, it is standby to collect volatile oil and Aromatic water;
2) will collect medicinal residues behind volatile oil and the Aromatic water and medicinal liquid and add water boil and extract 2 times, add water to 10 times of amounts for the first time, and boil and extracted 2 hours, filter, for the second time add water to 8 times of amounts, extracted 1.5 hours, filter merging filtrate, refilter, filtrate is concentrated, receive extractum;
3) above-mentioned extractum is used 80-85% ethanol precipitation 24 hours, reclaim ethanol, extractum is concentrated into thick paste, be dissolved in 95% ethanol thick paste standby;
4) Borneolum Syntheticum, volatile oil, Aromatic water are dissolved in 95% ethanol altogether, add in the above-mentioned thick paste alcoholic solution, mixing is adjusted relative density to 1.05-1.08, promptly.
5. liquid Tibetan incense according to claim 3 is characterized in that wherein raw material also has Cortex Cinnamomi 5-20.
6. the preparation method of a kind of liquid Tibetan incense according to claim 5 is characterized in that may further comprise the steps:
1) Lignum Santali Albi, Lignum Aquilariae Resinatum, Flos Caryophylli, Radix Et Rhizoma Nardostachyos, Fructus Tsaoko, Cortex Cinnamomi, Himalaya Mirabilis jalapa, Semen Myristicae, Radix Inulae are added 6--8 times of water gaging, distilled 2.5-3.5 hour, it is standby to collect volatile oil and Aromatic water;
2) will collect medicinal residues behind volatile oil and the Aromatic water and medicinal liquid and add water to 8--12 and doubly measure, and boil and extract 2-3 time, extract 1.5-2.5 hour at every turn, and filter, merging filtrate refilters, and filtrate is concentrated receipts extractum;
3) above-mentioned extractum is used 80-85% ethanol precipitation 24-30 hour, reclaim ethanol, extractum is concentrated into thick paste, be dissolved in the 90%--95% ethanol thick paste standby;
4) Borneolum Syntheticum, volatile oil, Aromatic water are dissolved in the 90%--95% ethanol altogether, add in the above-mentioned thick paste alcoholic solution, mixing is adjusted relative density to 1.05-1.08, promptly.
7. liquid Tibetan incense according to claim 5 is characterized in that wherein raw material also has Fructus Chebulae 5-20.
8. the preparation method of liquid Tibetan incense according to claim 7 is characterized in that may further comprise the steps:
1) Lignum Santali Albi, Lignum Aquilariae Resinatum, Flos Caryophylli, Radix Et Rhizoma Nardostachyos, Fructus Tsaoko, Cortex Cinnamomi, Himalaya Mirabilis jalapa, Semen Myristicae, Fructus Chebulae, Radix Inulae are added 6 times of water gagings, distilled 3 hours, it is standby to collect volatile oil and Aromatic water;
2) will collect medicinal residues behind volatile oil and the Aromatic water and medicinal liquid and add water boil and extract 2 times, add water to 10 times of amounts for the first time, and boil and extracted 2 hours, filter, for the second time add water to 8 times of amounts, extracted 1.5 hours, filter merging filtrate, refilter, filtrate is concentrated, receive extractum;
3) above-mentioned extractum is used 80-85% ethanol precipitation 24 hours, reclaim ethanol, extractum is concentrated into thick paste, be dissolved in 95% ethanol thick paste standby;
4) Borneolum Syntheticum, volatile oil, Aromatic water are dissolved in 95% ethanol altogether, add in the above-mentioned thick paste alcoholic solution, mixing is adjusted relative density to 1.05-1.08, promptly.
9. liquid Tibetan incense according to claim 7 is characterized in that wherein raw material also has Radix Angelicae Sinensis 5-20.
10. the preparation method of liquid Tibetan incense according to claim 9 is characterized in that may further comprise the steps:
1) Lignum Santali Albi, Lignum Aquilariae Resinatum, Flos Caryophylli, Radix Et Rhizoma Nardostachyos, Fructus Tsaoko, Cortex Cinnamomi, Himalaya Mirabilis jalapa, Semen Myristicae, Fructus Chebulae, Radix Inulae, Radix Angelicae Sinensis are added 6 times of water gagings, distilled 3 hours, it is standby to collect volatile oil and Aromatic water;
2) will collect medicinal residues behind volatile oil and the Aromatic water and medicinal liquid and add water boil and extract 2 times, add water to 10 times of amounts for the first time, and boil and extracted 2 hours, filter, for the second time add water to 8 times of amounts, extracted 1.5 hours, filter merging filtrate, refilter, filtrate is concentrated, receive extractum;
3) above-mentioned extractum is used 80-85% ethanol precipitation 24 hours, reclaim ethanol, extractum is concentrated into thick paste, be dissolved in 95% ethanol thick paste standby;
4) Borneolum Syntheticum, volatile oil, Aromatic water are dissolved in 95% ethanol altogether, add in the above-mentioned thick paste alcoholic solution, mixing is adjusted relative density to 1.05-1.08, promptly.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CNB2006100215723A CN100402094C (en) | 2006-08-09 | 2006-08-09 | Liquid Tibetan incense and its prepn. method |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CNB2006100215723A CN100402094C (en) | 2006-08-09 | 2006-08-09 | Liquid Tibetan incense and its prepn. method |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN1903379A CN1903379A (en) | 2007-01-31 |
| CN100402094C true CN100402094C (en) | 2008-07-16 |
Family
ID=37672839
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CNB2006100215723A Active CN100402094C (en) | 2006-08-09 | 2006-08-09 | Liquid Tibetan incense and its prepn. method |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN100402094C (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110384813A (en) * | 2019-08-21 | 2019-10-29 | 西藏宇拓健康品有限公司 | A kind of liquid Tibetan incense and its preparation process |
Families Citing this family (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101129316B (en) * | 2007-08-30 | 2010-09-08 | 中国热带农业科学院热带生物技术研究所 | Ligaloes perfumes and method of producing the same |
| CN103113988A (en) * | 2013-02-22 | 2013-05-22 | 红云红河烟草(集团)有限责任公司 | Tobacco flavor for improving sensory comfort of cigarette and application thereof |
| CN103330662A (en) * | 2013-06-08 | 2013-10-02 | 吴江市利达上光制品有限公司 | Perfume containing herbal component |
| CN104667329A (en) * | 2015-02-06 | 2015-06-03 | 西藏圣火文化传媒有限公司 | Tibetan incense and preparation method thereof |
| CN106139208A (en) * | 2015-04-01 | 2016-11-23 | 当周 | A kind of air freshener and preparation method thereof |
| CN105105329A (en) * | 2015-08-18 | 2015-12-02 | 昆明理工大学 | Moisture-increasing fragrance-carrying plant particles, and preparation method and application thereof |
| CN109105393A (en) * | 2018-08-31 | 2019-01-01 | 阿坝州慈愿民族传统文化有限责任公司 | A kind of rhizoma nardostachyos taste joss stick produced in Xizang and preparation method thereof |
| CN114177128A (en) * | 2021-11-23 | 2022-03-15 | 上海海洋大学 | A Chinese medicinal perfume for preventing respiratory infectious diseases and enhancing immunity, and its preparation method |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1098317A (en) * | 1993-08-05 | 1995-02-08 | 铜陵市人民医院 | Health-care sachet and preparation method thereof |
| CN1161849A (en) * | 1997-01-31 | 1997-10-15 | 白玛加措 | Tibetan preparatory medicine and preparation method thereof |
| CN1781542A (en) * | 2004-11-29 | 2006-06-07 | 马根灿 | Medicine for human body to disperse fragrance and its preparing method |
-
2006
- 2006-08-09 CN CNB2006100215723A patent/CN100402094C/en active Active
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1098317A (en) * | 1993-08-05 | 1995-02-08 | 铜陵市人民医院 | Health-care sachet and preparation method thereof |
| CN1161849A (en) * | 1997-01-31 | 1997-10-15 | 白玛加措 | Tibetan preparatory medicine and preparation method thereof |
| CN1781542A (en) * | 2004-11-29 | 2006-06-07 | 马根灿 | Medicine for human body to disperse fragrance and its preparing method |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110384813A (en) * | 2019-08-21 | 2019-10-29 | 西藏宇拓健康品有限公司 | A kind of liquid Tibetan incense and its preparation process |
Also Published As
| Publication number | Publication date |
|---|---|
| CN1903379A (en) | 2007-01-31 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN100402094C (en) | Liquid Tibetan incense and its prepn. method | |
| CN101518507B (en) | Tibetan incense cosmetic daily chemical product and preparation method thereof | |
| CN103392748B (en) | Natural mosquito repellent incense and preparation method thereof | |
| CN105594766A (en) | Natural bamboo charcoal mosquito-repellent incense and manufacturing method thereof | |
| CN103262865A (en) | Preparation method of tea shell mosquito-repellent incense | |
| CN106265147A (en) | A kind of floral water containing natural plant essential oils and preparation method thereof | |
| CN105125438A (en) | Mosquito-repellent composition and mosquito-repellent liquid preparation method | |
| CN102211343A (en) | Shen Nung life-prolonged compound plate and manufacturing method thereof | |
| CN101664482B (en) | Externally-applied medicine for treating beriberi and skin pruritus and preparation method thereof | |
| CN111714674B (en) | Traditional Chinese medicine volatile oil and preparation method and application thereof | |
| CN112891504A (en) | Four-season skin-care epidemic-prevention ginger paste with ginger decoction dregs as base materials and preparation method | |
| KR20170130690A (en) | Natural detergent composition and preparation method thereof | |
| CN102266422A (en) | Chinese medicinal preparation for treating slight and severe chilblains and production method thereof | |
| CN112450702A (en) | Traditional Chinese medicine joss stick and preparation method thereof | |
| CN103263680B (en) | Preparation method of tea shell sandalwood | |
| CN102657375B (en) | Method for preparing extract from traditional Chinese medicines and application of extract as tobacco additive | |
| CN101721543A (en) | Pure traditional Chinese medicine lotion for treating gynecological diseases | |
| CN107998025B (en) | Pepper essential oil mosquito-repellent floral water and preparation method thereof | |
| CN103494749B (en) | Natural mosquito repellent | |
| CN106377604A (en) | Antibacterial inflammation diminishing and itching relieving traditional Chinese medicine ointment and preparation method thereof | |
| CN111514219A (en) | Traditional Chinese medicine formula capable of improving self-disease resistance | |
| CN113663049B (en) | Li nationality medicine postpartum medicated bath effervescent granules and preparation method thereof | |
| CN103341044A (en) | Itching-relieving compound preparation and preparation method thereof | |
| CN113509537B (en) | Jiangyao bath composition capable of expelling wind, clearing away cold, inducing sweat and relieving exterior syndrome as well as preparation method and application thereof | |
| JP2002249435A (en) | Composition and patch for facilitating blood circulation |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| CP03 | Change of name, title or address |
Address after: 618300 Chengdu Chengdu ABA industrial concentrated development zone, Sichuan, China Patentee after: Sichuan King month eco Tibetan Pharmaceutical Co.,Ltd. Address before: 618300 Chengdu Jintang ABA industrial concentrated development zone, Chengdu, Sichuan Patentee before: Sichuan Yuewang Biotechnology Co.,Ltd. Address after: 618300 Chengdu Jintang ABA industrial concentrated development zone, Chengdu, Sichuan Patentee after: SICHUAN YUEWANG BIOTECHNOLOGY Co.,Ltd. Address before: Science and Technology Industrial Park, No. 5 Chengdu high tech Zone Gaopeng east of Sichuan province 610041 City 2 Building 4 layer Patentee before: SICHUAN YANGJIN TIBETAN MEDICI |
|
| TR01 | Transfer of patent right | ||
| TR01 | Transfer of patent right |
Effective date of registration: 20191127 Address after: 850000 Lhasa economic and Technological Development Zone, Tibet City, Lhasa Road, No. 9 Patentee after: TIBET YUEWANG TIBETAN MEDICINE TECHNOLOGY CO.,LTD. Address before: 618300 Chengdu Chengdu ABA industrial concentrated development zone, Sichuan, China Patentee before: Sichuan King month eco Tibetan Pharmaceutical Co.,Ltd. |