CN108851213B - Cigarette filter rod containing large-particle solid aromatic beads and preparation method thereof - Google Patents
Cigarette filter rod containing large-particle solid aromatic beads and preparation method thereof Download PDFInfo
- Publication number
- CN108851213B CN108851213B CN201810886849.1A CN201810886849A CN108851213B CN 108851213 B CN108851213 B CN 108851213B CN 201810886849 A CN201810886849 A CN 201810886849A CN 108851213 B CN108851213 B CN 108851213B
- Authority
- CN
- China
- Prior art keywords
- beads
- bead
- filter rod
- particle solid
- cigarette
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
Images
Classifications
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24D—CIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
- A24D3/00—Tobacco smoke filters, e.g. filter-tips, filtering inserts; Filters specially adapted for simulated smoking devices; Mouthpieces for cigars or cigarettes
- A24D3/02—Manufacture of tobacco smoke filters
- A24D3/0204—Preliminary operations before the filter rod forming process, e.g. crimping, blooming
- A24D3/0212—Applying additives to filter materials
- A24D3/0216—Applying additives to filter materials the additive being in the form of capsules, beads or the like
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24D—CIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
- A24D3/00—Tobacco smoke filters, e.g. filter-tips, filtering inserts; Filters specially adapted for simulated smoking devices; Mouthpieces for cigars or cigarettes
- A24D3/06—Use of materials for tobacco smoke filters
- A24D3/061—Use of materials for tobacco smoke filters containing additives entrapped within capsules, sponge-like material or the like, for further release upon smoking
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Cigarettes, Filters, And Manufacturing Of Filters (AREA)
- Fats And Perfumes (AREA)
Abstract
A cigarette filter rod containing large-particle solid fragrant beads and a preparation method thereof belong to the field of tobacco essence and spice, wherein the middle section of a filter rod filament bundle is loaded with one large-particle solid fragrant bead, the fragrant bead is prepared by taking porous quartz powder as a main raw material through processes of pulping and forming, calcining and pore forming, attaching fragrance and the like, and the tobacco essence which is light and easy to volatilize is added. In the process of smoking, the essence is slowly and uniformly released along with the smoke, so that the problem of aroma deterioration caused by combustion is solved. The cigarette holder takes the single solid flavor beads in the cigarette holder, has simple structure, is non-toxic and harmless, and avoids the safety worry of smokers about small additives; the preparation process of the aromatic bead is simple, the overall control rate of the concentration of the aromatic bead is more stable, the qualification rate and the production stability are better, no additional solvent is needed when the aromatic bead is attached, and the aroma is elegant and transparent.
Description
Technical Field
The invention relates to the field of tobacco essence and flavor, in particular to a cigarette filter rod containing large-particle solid aromatic beads and a preparation method thereof.
Background
In the tobacco industry, the cigarette stereoscopic flavor blending technology is developed rapidly, and particularly, a new method and a new technology in a cigarette filter rod are developed, wherein the new technology comprises cigarette blasting beads, microcapsules, nano particles, powdery particles and the like. At present, through the inspection of consumer market, the overall acceptance of the cigarette bead blasting is better, and additives such as microcapsules, nano particles, powder particles and the like easily cause the smoking safety worry of consumers due to fine particles. However, the addition of the cigarette popping beads and dropping pills also has certain disadvantages, including low forming rate, high cost and the like, and the solvent olive oil, ODO and the like of the popping beads and the dropping pills have trace unpleasant odor, so that the popping beads are mainly used for wrapping essence and spice with strong fragrance such as ginseng, mint and the like. On the basis of the cigarette filter rod containing silica gel aroma beads disclosed by the prior art CN201710990115.3 and the preparation method of the silica gel aroma beads for cigarettes and the cigarette filter rod containing zeolite aroma beads disclosed by CN201710990114.9, the bead preparation and the subsequent processes of the invention ensure that the overall control rate of aroma bead concentration is more stable, and the worry of consumers about the safety of smoking of fine additives such as charcoal powder, silica gel powder, zeolite powder, cyclodextrin particles and the like is avoided.
The porous powder quartz belongs to volcanic sedimentary rock, is fine in natural particle size (about 5 mu m), uniform in particle distribution, large in specific surface area (8.3 m x 2/g), approximately spherical and non-angular in shape structure, and forms a paste under high-speed stirring, can absorb 35% of water of the weight of the porous powder quartz, and is lower than diatomite commonly used in cigarettes (the diatomite can absorb water 1.5-4 times of the weight of the diatomite). But its thixotropy is quite similar to that of diatomaceous earth. At present, the price of the porous powder quartz is only 20 to 25 percent of that of the diatomite.
On the basis of three-dimensional flavoring of cigarettes, aiming at the adding requirements of the essence for the cigarettes with light fragrance and easy volatilization, the large-particle solid aromatic bead cigarette filter rod which does not participate in combustion and has an essence slow release function is developed and obtained, and is prepared by adopting natural china clay raw materials such as porous powder quartz, water glass and the like, so that the cigarette filter rod is non-toxic, low in cost and high in forming rate; the cigarette filter tip is applied to a cigarette filter tip in a single solid aromatic bead form, so that the cigarette filter tip is visual and concise, and the production stability is better; the porous quartz has a natural porous structure, so that the solid aromatic bead is superior to an exploded bead in the aspect of essence slow release, pinching breakage is not needed, no solvent is leaked out, and the 1-20 mu m microporous slow release structure has obvious advantages in the use of the essence for light-aroma and volatile cigarettes; compared with the traditional cigarette filter rod, the cigarette filter rod with the large-particle aromatic beads with the porous structure has the advantages that the essence is slowly and uniformly released along with smoke, and the problem of aroma deterioration caused by combustion is solved.
Disclosure of Invention
Aiming at the technical problems, the invention provides a cigarette filter rod of large-particle solid flavor beads which does not participate in combustion, is non-toxic, is stable in forming, has more stable overall control rate of flavor bead concentration, has an essence slow-release function and is not easy to deteriorate in flavor, and a preparation method thereof.
In order to solve the problems, the technical scheme of the invention is as follows:
a preparation method of a cigarette filter tip containing large-particle solid fragrant beads comprises preparing large-particle dry beads with slow release function, adding fragrance according to a certain proportion, and adding the fragrant large-particle solid fragrant beads into cigarette filter tip filament bundles.
Further, the method specifically comprises the following steps:
1) pulping and forming: porous powder quartz, water glass, ethyl silicate, liquid paraffin and distilled water are mixed according to the weight ratio of 100-200: 10-50: 10-50: 1-2: uniformly mixing 500-1000 parts by mass, adding into a grinding machine, and mixing according to a ball material ratio of 1-15: 1, grinding for 2-4 h, filtering slurry by using a sieve, adopting a spherical mould with the diameter of 3.65mm for compression molding, drying for 24h at room temperature, and drying for 2-4 h at 45 ℃ to obtain a dried bead-shaped blank.
2) Calcining and pore-forming: calcining the bead-shaped blank at 1000-1300 ℃ for 2-6 h, washing with water, and drying to obtain large-particle dry beads with porous property;
3) adding fragrance: uniformly mixing the dry beads and the tobacco essence according to the mass ratio of 1:2, slowly stirring for 6-12 h to enable the tobacco essence to be uniformly adsorbed in porous channels of the dry beads, and air-drying for 2-4 h at 40-50 ℃ to obtain large-particle solid fragrant beads;
4) and (3) forming a filter tip: adding the large-particle solid aromatic bead into the middle section of the filter rod filament bundle of the cigarette, and molding to obtain the cigarette.
Further, in the step 1), the ratio of porous powder quartz, water glass, ethyl silicate, liquid paraffin and distilled water is 100-200: 20-50: 20-50: 1-2: the mass ratio of 500-700 is more excellent.
Further, the slurry in the step 1) is prepared by mixing the following raw materials in a ball-to-material ratio of 5-10: 1, grinding for 2 hours is more preferable; in the process of cultivation, the spherical mould is opened according to the diameter of 3.65mm in consideration of the micro deformation of the bead-shaped blank during calcination.
Further, the bead-shaped blank body in the step 2) is preferably calcined at 1200-1300 ℃ for 4-6 h.
Further, the porous quartz powder in the step 1) is white fine powder purified by water washing, and the content of silicon dioxide is more than 99.5%.
Further, the tobacco essence in the step 3) is one or more of dried orange peel extract, rose extract and raspberry extract.
Further, the fragrance adding rate of the large-particle solid fragrance beads in the step 3) is controlled to be 20-40%, wherein the fragrance adding rate is (weight after fragrance adding-weight before fragrance adding)/weight before fragrance adding.
Further, in the step 3), in the fragrance attaching process, air drying is carried out at 40-50 ℃ for 2-3 h optimally, and the fragrance attaching rate of the large-particle solid fragrance beads is controlled to be 30-40%.
Further, the large-particle solid fragrant beads in the step 4) are in a micro porous structure, and the average pore size of the micro porous fragrant beads is 1-20 mu m measured by a scanning tunneling microscope.
A cigarette filter rod containing large-particle solid aromatic beads is prepared by the preparation method, the circumference of the bottom surface of the cigarette filter rod is 24mm, the large-particle solid aromatic beads with the diameter of 3.65 +/-0.15 mm are loaded in the middle section of a tow, the aromatic beads are prepared by taking porous quartz powder as a main raw material, and essence for light-aroma and easily-volatilized cigarettes is adsorbed.
Furthermore, the volatile essence for cigarettes is mainly natural light-flavor essence such as cedar wood oil, cananga odorata oil and rose oil.
The application of the cigarette filter tip containing large-particle solid aromatic beads in cigarettes is realized by adopting the preparation method, and the cigarette filter tip is applied to the production of cigarettes with the circumference of 24mm and can play a role in slowly releasing the essence for the cigarettes with light fragrance and easy volatilization.
Compared with the prior art, the invention has the advantages and positive effects that:
1) the solid-state fragrant pearl of large granule in this mouth stick is porous structure, and average aperture is at 1~ 20 mu m, has good essence absorption and slow release performance, and the accessible changes the pore size of pore-forming agent addition control fragrant pearl granule. Especially under the process conditions of pulping, pore forming, aroma attaching and subsequent processes, the invention is characterized in that the aroma attaching rate of the aroma beads is integrally controlled to be 20-40%, the control rate is more stable than the existing integral control rate (the integral difference of the concentration of the existing aroma beads is large) and can be optimally controlled to be 30-40%, the adsorption performance of the aroma beads is in a saturated state, and the slow-release aroma can be played in the smoking process of cigarettes without influencing the original aroma of the cigarettes;
2) the cigarette filter stick is applied to a cigarette filter stick in a single solid fragrant bead form, is visual and simple, is non-toxic and harmless, and avoids the smoking safety worry of consumers on tiny additives such as charcoal powder, silica gel powder, zeolite powder, cyclodextrin particles and the like compared with the cigarette filter stick added with microcapsules and powdery particles;
3) the preparation process of the aromatic bead is simple, and compared with the cigarette filter stick added with the exploded bead and the dropping pill, the cigarette filter stick has better qualification rate and production stability, and the aromatic bead is added with fragrance without adding extra solvent, so that the fragrance is purer;
4) the circumference of the filter rod is 24mm, and the filter rod is between a thin cigarette and a common cigarette, and the application of the filter rod can become an innovative explosion point of the middle cigarette after the middle cigarette is marketed. The middle section of the filament bundle of the filter rod is loaded with a large-particle solid fragrant bead with the diameter of 3.65 +/-0.15 mm, the fragrant bead is prepared by taking porous powder quartz, water glass and ethyl silicate as main raw materials, and the adsorption effect prepared by the process is stronger than that of the prior art.
5) Compared with the traditional bead blasting and dropping pills for cigarettes, consumers do not need to pinch and break the aroma beads when smoking cigarettes and have no solvent exudation.
Drawings
FIG. 1 is a schematic view of a cigarette filter rod;
FIG. 2 is an SEM image of large solid beads of example 2 (before adsorption of perfume);
FIG. 3 is an SEM image of large solid beads of example 2 (after adsorbing perfume).
In the figure: 1-filter stick suction end, 2-large particle solid aromatic bead, 3-cigarette coil paper and 4-tobacco shred.
Detailed Description
The technical solutions in the embodiments of the present invention will be clearly and completely described below. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.
Example 1
A cigarette filter rod containing large-particle solid aromatic beads is characterized in that the circumference of the cigarette filter rod is 24mm, and the large-particle solid aromatic beads with the diameter of 3.65 +/-0.15 mm are loaded in the middle section of a tow. The preparation method of the cigarette filter rod containing the large-particle solid aromatic beads comprises the following steps:
the method comprises the following steps: pulping and forming. Mixing porous powder quartz, water glass, ethyl silicate, liquid paraffin and distilled water according to the weight ratio of 100: 20: 10: 2: uniformly mixing the materials in a mass ratio of 500, adding the materials into a grinding machine, and mixing the materials according to a ball material ratio of 5: 1, grinding for 2h, filtering slurry by using a sieve, adopting a spherical mould with the diameter of 3.65mm for compression moulding, drying for 24h at room temperature, and drying for 4h at 45 ℃ to obtain a dried bead-shaped blank.
The porous quartz powder is white fine powder purified by water washing, wherein the content of silicon dioxide is more than 99.5%.
Step two: and (6) calcining and forming pores. Calcining the bead-shaped blank at 1200 ℃ for 2h, washing with water, and drying to obtain the large-particle dry beads with porous property.
Step three: adding incense. Uniformly mixing the dry beads and the cedar wood oil according to the mass ratio of 1:2, slowly stirring for 12 hours to enable the tobacco essence to be uniformly adsorbed in porous channels of the dry beads, and air-drying for 4 hours at 40 ℃ to obtain large-particle solid fragrant beads, wherein the fragrance attaching rate is controlled to be 35-40%.
Step four: and (5) forming the filter tip. Adding the large-particle solid aromatic beads into the middle section of the cigarette filter rod tows with the circumference of 24mm for molding, and thus obtaining the cigarette filter rod.
Example 2
A cigarette filter rod containing large-particle solid aromatic beads is characterized in that the circumference of the cigarette filter rod is 24mm, and the large-particle solid aromatic beads with the diameter of 3.65 +/-0.15 mm are loaded in the middle section of a tow. The preparation method of the cigarette filter rod containing the large-particle solid aromatic beads comprises the following steps:
the method comprises the following steps: pulping and forming. Mixing porous powder quartz, water glass, ethyl silicate, liquid paraffin and distilled water according to the weight ratio of 100: 20: 10: 1: uniformly mixing the materials in a mass ratio of 500, adding the materials into a grinding machine, and mixing the materials according to a ball material ratio of 10: 1 grinding for 4h, filtering slurry by a sieve, adopting a spherical mould with the diameter of 3.65mm for compression moulding, drying for 24h at room temperature, and drying for 4h at 45 ℃ to obtain a dried bead-shaped blank.
The porous quartz powder is white fine powder purified by water washing, wherein the content of silicon dioxide is more than 99.5%.
Step two: and (6) calcining and forming pores. Calcining the bead-shaped green body at 1300 ℃ for 2h, washing with water and drying to obtain the large-particle dry beads with porous property.
Step three: adding incense. Uniformly mixing the dry beads and the cedar wood oil according to the mass ratio of 1:2, slowly stirring for 12 hours to enable the tobacco essence to be uniformly adsorbed in porous channels of the dry beads, and air-drying for 4 hours at 40 ℃ to obtain large-particle solid fragrant beads, wherein the fragrance adsorption rate is controlled to be 25-30%.
Step four: and (5) forming the filter tip. Adding the large-particle solid aromatic beads into the middle section of the cigarette filter rod tows with the circumference of 24mm for molding, and thus obtaining the cigarette filter rod.
Example 3
A cigarette filter rod containing large-particle solid aromatic beads is characterized in that the circumference of the cigarette filter rod is 24mm, and the large-particle solid aromatic beads with the diameter of 3.65 +/-0.15 mm are loaded in the middle section of a tow. The preparation method of the cigarette filter rod containing the large-particle solid aromatic beads comprises the following steps:
the method comprises the following steps: pulping and forming. Mixing porous powder quartz, water glass, ethyl silicate, liquid paraffin and distilled water according to the weight ratio of 180: 30: 20: 1: 700, and adding the mixture into a grinder according to a ball material ratio of 10: 1 grinding for 4h, filtering slurry by a sieve, adopting a spherical mould with the diameter of 3.65mm for compression moulding, drying for 24h at room temperature, and drying for 4h at 45 ℃ to obtain a dried bead-shaped blank.
The porous quartz powder is white fine powder purified by water washing, wherein the content of silicon dioxide is more than 99.5%.
Step two: and (6) calcining and forming pores. Calcining the bead-shaped blank at 1000 ℃ for 2h, washing with water, and drying to obtain the large-particle dry beads with porous property.
Step three: adding incense. Uniformly mixing the dry beads and the cedar wood oil according to the mass ratio of 1:2, slowly stirring for 12 hours to enable the tobacco essence to be uniformly adsorbed in porous channels of the dry beads, and air-drying for 4 hours at 40 ℃ to obtain large-particle solid fragrant beads, wherein the fragrance adsorption rate is controlled to be 25-30%.
Step four: and (5) forming the filter tip. Adding the large-particle solid aromatic beads into the middle section of the cigarette filter rod tows with the circumference of 24mm for molding, and thus obtaining the cigarette filter rod.
Example 4
A cigarette filter rod containing large-particle solid aromatic beads is characterized in that the circumference of the cigarette filter rod is 24mm, and the large-particle solid aromatic beads with the diameter of 3.65 +/-0.15 mm are loaded in the middle section of a tow. The preparation method of the cigarette filter rod containing the large-particle solid aromatic beads comprises the following steps:
the method comprises the following steps: pulping and forming. Mixing porous powder quartz, water glass, ethyl silicate, liquid paraffin and distilled water according to the weight ratio of 180: 30: 20: 1: 700, and adding the mixture into a grinder according to a ball material ratio of 10: 1 grinding for 4h, filtering slurry by a sieve, adopting a spherical mould with the diameter of 3.65mm for compression moulding, drying for 24h at room temperature, and drying for 4h at 45 ℃ to obtain a dried bead-shaped blank.
The porous quartz powder is white fine powder purified by water washing, wherein the content of silicon dioxide is more than 99.5%.
Step two: and (6) calcining and forming pores. Calcining the bead-shaped blank at 1200 ℃ for 2h, washing with water, and drying to obtain the large-particle dry beads with porous property.
Step three: adding incense. Uniformly mixing the dry beads and cananga odorata oil according to the mass ratio of 1:2, slowly stirring for 12 hours to enable the tobacco essence to be uniformly adsorbed in porous channels of the dry beads, and air-drying for 4 hours at 40 ℃ to obtain large-particle solid fragrant beads, wherein the fragrance adsorption rate is controlled to be 25-30%.
Step four: and (5) forming the filter tip. Adding the large-particle solid aromatic beads into the middle section of the cigarette filter rod tows with the circumference of 24mm for molding, and thus obtaining the cigarette filter rod.
Example 5
A cigarette filter rod containing large-particle solid aromatic beads is characterized in that the circumference of the cigarette filter rod is 24mm, and the large-particle solid aromatic beads with the diameter of 3.65 +/-0.15 mm are loaded in the middle section of a tow. The preparation method of the cigarette filter rod containing the large-particle solid aromatic beads comprises the following steps:
the method comprises the following steps: pulping and forming. Mixing porous powder quartz, water glass, ethyl silicate, liquid paraffin and distilled water according to the weight ratio of 150: 20: 20: 1: 600, and adding the mixture into a grinding machine according to a ball material ratio of 15: 1 grinding for 4h, filtering slurry by a sieve, adopting a spherical mould with the diameter of 3.65mm for compression moulding, drying for 24h at room temperature, and drying for 4h at 45 ℃ to obtain a dried bead-shaped blank.
The porous quartz powder is white fine powder purified by water washing, wherein the content of silicon dioxide is more than 99.5%.
Step two: and (6) calcining and forming pores. Calcining the bead-shaped blank at 1200 ℃ for 4h, washing with water, and drying to obtain the large-particle dry beads with porous property.
Step three: adding incense. Uniformly mixing the dry beads and cananga odorata oil according to the mass ratio of 1:2, slowly stirring for 12 hours to enable the tobacco essence to be uniformly adsorbed in porous channels of the dry beads, and air-drying for 4 hours at 40 ℃ to obtain large-particle solid fragrant beads, wherein the fragrance adsorption rate is controlled to be 30-35%.
Step four: and (5) forming the filter tip. Adding the large-particle solid aromatic beads into the middle section of the cigarette filter rod tows with the circumference of 24mm for molding, and thus obtaining the cigarette filter rod.
Example 6
A cigarette filter rod containing large-particle solid aromatic beads is characterized in that the circumference of the cigarette filter rod is 24mm, and the large-particle solid aromatic beads with the diameter of 3.65 +/-0.15 mm are loaded in the middle section of a tow. The preparation method of the cigarette filter rod containing the large-particle solid aromatic beads comprises the following steps:
the method comprises the following steps: pulping and forming. Mixing porous powder quartz, water glass, ethyl silicate, liquid paraffin and distilled water according to the weight ratio of 150: 20: 20: 1: 600, and adding the mixture into a grinding machine according to a ball material ratio of 10: 1 grinding for 4h, filtering slurry by a sieve, adopting a spherical mould with the diameter of 3.65mm for compression moulding, drying for 24h at room temperature, and drying for 4h at 45 ℃ to obtain a dried bead-shaped blank.
The porous quartz powder is white fine powder purified by water washing, wherein the content of silicon dioxide is more than 99.5%.
Step two: and (6) calcining and forming pores. Calcining the bead-shaped blank at 1200 ℃ for 3h, washing with water, and drying to obtain the large-particle dry beads with porous property.
Step three: adding incense. Uniformly mixing the dry beads and the rose oil according to the mass ratio of 1:2, slowly stirring for 12 hours to enable the tobacco essence to be uniformly adsorbed in porous channels of the dry beads, and air-drying for 4 hours at 40 ℃ to obtain large-particle solid fragrant beads, wherein the fragrance adsorption rate is controlled to be 30-35%.
Step four: and (5) forming the filter tip. Adding the large-particle solid aromatic beads into the middle section of the cigarette filter rod tows with the circumference of 24mm for molding, and thus obtaining the cigarette filter rod.
The test effect is as follows:
the cigarette filter rod containing the large-particle solid flavor beads prepared in the embodiments 1 to 6 is applied to cigarettes to prepare a filter rod, and common cigarettes which are not prepared by using the large-particle solid flavor bead filter rod are used as a comparison sample. An expert smoking group organized to qualify for national cigarette smoking according to the five ginseng standard GB5606.4-2005 cigarette part 4: sensory technical requirements and YC/T497-.
TABLE 1 cigarette sensory evaluation results
Compared with a control sample, a medium cigarette (the circumference of the filter rod is 24mm) product prepared by the cigarette filter rod containing the large-particle solid aromatic beads of the embodiment 1-6 has more obvious sweet taste style, the richness of the aroma is obviously increased, and the smoke permeability is improved. The cigarette prepared by the filter stick in example 2 has the highest score mainly because the fragrance of the dried orange peel is more coordinated with the smoking taste of the cigarette, and the slow release performance of the solid flavor beads is optimal, so that in the flavor bead preparation process, the pulp grinder is used for preparing the solid flavor beads according to the ball-to-material ratio of 3: 1. and the effect is better when the calcination is carried out for 4 hours at 800 ℃.
The invention also performs SEM scanning on the aromatic beads in example 2 with the best application effect to confirm the porous structure and the essence adsorption performance.
The above embodiments are merely preferred embodiments of the present invention, and any simple modifications and alternative changes made to the above embodiments according to the technical spirit of the present invention are within the technical scope of the present invention.
Claims (5)
1. A preparation method of a cigarette filter rod containing large-particle solid aromatic beads is characterized by comprising the following steps: adding perfume to the prepared large-particle dry beads with the slow release function according to a certain proportion, and adding the perfume-added large-particle solid perfume beads into a filter stick tow of a cigarette, wherein the preparation method specifically comprises the following steps:
step 1) pulping and forming: porous powder quartz, water glass, ethyl silicate, liquid paraffin and distilled water are mixed according to the weight ratio of 100-200: 10-50: 10-50: 1-2: uniformly mixing 500-1000 parts by mass, adding into a grinding machine, and mixing according to a ball material ratio of 1-15: 1, grinding for 2-4 h, filtering slurry by using a sieve, performing compression molding by using a spherical mold with the diameter of 3.65mm, drying for 24h at room temperature, and drying for 2-4 h at 45 ℃ to obtain a dried bead-shaped blank;
step 2) calcining and pore-forming: calcining the bead-shaped blank at 1000-1300 ℃ for 2-6 h, washing with water, and drying to obtain large-particle dry beads with porous property;
step 3), adding perfume: uniformly mixing the dry beads and the tobacco essence according to the mass ratio of 1:2, slowly stirring for 6-12 h to enable the tobacco essence to be uniformly adsorbed in porous channels of the dry beads, and air-drying for 2-4 h at 40-50 ℃ to obtain large-particle solid fragrant beads;
step 4), forming a filter tip: adding the large-particle solid aromatic beads into the middle section of a filter rod tow of a cigarette, and molding to obtain the cigarette;
and in the step 3), the fragrance adding rate of the large-particle solid fragrance bead is controlled to be 20-40%, wherein the fragrance adding rate is (weight after fragrance adding-weight before fragrance adding)/weight before fragrance adding.
2. The method of claim 1, wherein the filter tip comprises a plurality of solid flavor beads, wherein the solid flavor beads comprise: in the step 1), the porous quartz powder is white micro powder purified by water washing, and the content of silicon dioxide is more than 99.5%.
3. The method of claim 1, wherein the filter tip comprises a plurality of solid flavor beads, wherein the solid flavor beads comprise: the tobacco essence in the step 3) is one or more of dried orange peel extract, rose extract and raspberry extract.
4. A cigarette filter rod containing large-particle solid aromatic beads is characterized in that: the preparation method according to any one of claims 1 to 3, wherein the circumference of the bottom surface of the cigarette filter rod is 24mm, and a large-particle solid flavor bead with the diameter of 3.65 +/-0.15 mm is loaded in the middle section of the filament bundle, and the flavor bead is prepared by taking porous quartz powder as a main raw material and adsorbs essence for light-flavor and volatile-style cigarettes.
5. The application of the cigarette filter tip containing large-particle solid aromatic beads in cigarettes is characterized in that: the production method according to any one of claims 1 to 3, wherein the cigarette filter rod is used in the production of cigarettes with a circumference of 24 mm.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810886849.1A CN108851213B (en) | 2018-08-06 | 2018-08-06 | Cigarette filter rod containing large-particle solid aromatic beads and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810886849.1A CN108851213B (en) | 2018-08-06 | 2018-08-06 | Cigarette filter rod containing large-particle solid aromatic beads and preparation method thereof |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN108851213A CN108851213A (en) | 2018-11-23 |
| CN108851213B true CN108851213B (en) | 2020-12-29 |
Family
ID=64307759
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201810886849.1A Active CN108851213B (en) | 2018-08-06 | 2018-08-06 | Cigarette filter rod containing large-particle solid aromatic beads and preparation method thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN108851213B (en) |
Families Citing this family (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109907368B (en) * | 2019-03-01 | 2021-10-01 | 江西中烟工业有限责任公司 | Preparation method of active nano ceramic solid aromatic beads and application of active nano ceramic solid aromatic beads in cigarette filter stick |
| CN110292207A (en) * | 2019-03-21 | 2019-10-01 | 重庆中烟工业有限责任公司 | Aerosol cooling filter element and low temperature cigarette |
| CN112029587A (en) * | 2020-09-07 | 2020-12-04 | 广西中烟工业有限责任公司 | Preparation method of cedar oil binary composite flavoring filter stick |
Citations (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101397137A (en) * | 2007-09-27 | 2009-04-01 | 刘文红 | Globular inorganic oxide material, synthetic method, modification method and use thereof |
| CN102669816A (en) * | 2012-05-22 | 2012-09-19 | 南通烟滤嘴有限责任公司 | Filter tip and filter stick pre-filled with large-particle materials |
| CN102892316A (en) * | 2010-03-26 | 2013-01-23 | 菲利普莫里斯生产公司 | Plug space plug filter with flavor bead |
| CN102936015A (en) * | 2012-11-23 | 2013-02-20 | 苏州知益微球科技有限公司 | Preparation method of silica gel microspheres |
| CN104336776A (en) * | 2013-08-05 | 2015-02-11 | 贵州中烟工业有限责任公司 | Slow release aromatic base material, particles as well as preparation method and application thereof |
| CN104529506A (en) * | 2015-01-16 | 2015-04-22 | 临江北峰硅藻土有限公司 | Preparation method of compound natural porous mineral ceramic microbeads |
| JP2015521488A (en) * | 2012-08-01 | 2015-07-30 | セラニーズ アセテート，エルエルシー | Process for producing filter and filter rod with porous mass and related article |
| CN206303202U (en) * | 2016-08-31 | 2017-07-07 | 刘迎春 | A kind of spacetabs type flavouring composite filter |
-
2018
- 2018-08-06 CN CN201810886849.1A patent/CN108851213B/en active Active
Patent Citations (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101397137A (en) * | 2007-09-27 | 2009-04-01 | 刘文红 | Globular inorganic oxide material, synthetic method, modification method and use thereof |
| CN102892316A (en) * | 2010-03-26 | 2013-01-23 | 菲利普莫里斯生产公司 | Plug space plug filter with flavor bead |
| CN102669816A (en) * | 2012-05-22 | 2012-09-19 | 南通烟滤嘴有限责任公司 | Filter tip and filter stick pre-filled with large-particle materials |
| JP2015521488A (en) * | 2012-08-01 | 2015-07-30 | セラニーズ アセテート，エルエルシー | Process for producing filter and filter rod with porous mass and related article |
| CN102936015A (en) * | 2012-11-23 | 2013-02-20 | 苏州知益微球科技有限公司 | Preparation method of silica gel microspheres |
| CN104336776A (en) * | 2013-08-05 | 2015-02-11 | 贵州中烟工业有限责任公司 | Slow release aromatic base material, particles as well as preparation method and application thereof |
| CN104529506A (en) * | 2015-01-16 | 2015-04-22 | 临江北峰硅藻土有限公司 | Preparation method of compound natural porous mineral ceramic microbeads |
| CN206303202U (en) * | 2016-08-31 | 2017-07-07 | 刘迎春 | A kind of spacetabs type flavouring composite filter |
Also Published As
| Publication number | Publication date |
|---|---|
| CN108851213A (en) | 2018-11-23 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN109198721B (en) | Medium cigarette filter tip containing large-particle solid aromatic beads and preparation method thereof | |
| CN108851214B (en) | Fine cigarette holder rod containing single solid aromatic bead particles and preparation method thereof | |
| CN108851213B (en) | Cigarette filter rod containing large-particle solid aromatic beads and preparation method thereof | |
| CN109123775B (en) | Heating non-combustion cigarette containing herbal fragrance type solid aromatic beads and preparation method thereof | |
| TWI308484B (en) | Improvements relating to smoking articles and smokable filler materials therefor | |
| RU2572168C2 (en) | Smoking product filter | |
| RU2549064C2 (en) | Smoke filtration | |
| CN110250565A (en) | A kind of plant granule perfume (or spice) pearl and the preparation method and application thereof | |
| US12022860B2 (en) | Cellulose acetate particle aggregate, preparation method therefor and application thereof | |
| CN108851215B (en) | Cigarette filter rod containing double solid flavor bead particles and preparation method thereof | |
| EA013393B1 (en) | Smoking articles with activated carbon and sodium bicarbonate-treated fibers and method of treating mainstream smoke | |
| EP3797606A1 (en) | Cooling filter rod, application and cigarette | |
| CN112273718A (en) | Structure capable of enhancing aroma and reducing cigarette smoke temperature, preparation method and application | |
| CN110226774B (en) | Dry cigarette bead tip rod capable of improving sweet feeling of cigarettes | |
| CN109875114B (en) | Functional microsphere with core-shell sandwich structure for cigarettes and preparation method and application thereof | |
| CN114133983A (en) | Aroma-enhancing spice, slow-release aroma-carrying particle and preparation method and application thereof | |
| CN102178350B (en) | Fibroin composite filter tip and preparation method thereof | |
| CN113841922A (en) | Preparation method and application of compound-flavor essence spice for cigarettes | |
| JPH0230261B2 (en) | ||
| CN110403236B (en) | Cigarette dry bead filter rod with function of improving smoke permeation | |
| CN107476136B (en) | Milk-flavor cigarette paper with moisture retention and harm reduction functions and preparation process thereof | |
| CN110946325A (en) | Filter stick flavoring particle with natural substance as carrier and preparation method thereof | |
| CN210226894U (en) | Binary composite filter stick for reducing cigarette irritation | |
| JP6535810B2 (en) | Filter for smoking article, smoking article, and method of manufacturing filter for smoking article | |
| CN112772971B (en) | Fragrant bead for hollow large-particle filter stick and preparation method thereof |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| GR01 | Patent grant | ||
| GR01 | Patent grant |