CN108835591A - A kind of preparation method of halogen material - Google Patents

A kind of preparation method of halogen material Download PDF

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Publication number
CN108835591A
CN108835591A CN201810749360.XA CN201810749360A CN108835591A CN 108835591 A CN108835591 A CN 108835591A CN 201810749360 A CN201810749360 A CN 201810749360A CN 108835591 A CN108835591 A CN 108835591A
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parts
preparation
halogen material
heating
temperature
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朱建军
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Fuyang Fumeng Food Co Ltd
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Fuyang Fumeng Food Co Ltd
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    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23LFOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L27/00Spices; Flavouring agents or condiments; Artificial sweetening agents; Table salts; Dietetic salt substitutes; Preparation or treatment thereof
    • A23L27/10Natural spices, flavouring agents or condiments; Extracts thereof
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23LFOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L27/00Spices; Flavouring agents or condiments; Artificial sweetening agents; Table salts; Dietetic salt substitutes; Preparation or treatment thereof
    • A23L27/20Synthetic spices, flavouring agents or condiments
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23LFOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L27/00Spices; Flavouring agents or condiments; Artificial sweetening agents; Table salts; Dietetic salt substitutes; Preparation or treatment thereof
    • A23L27/20Synthetic spices, flavouring agents or condiments
    • A23L27/204Aromatic compounds
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23LFOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L27/00Spices; Flavouring agents or condiments; Artificial sweetening agents; Table salts; Dietetic salt substitutes; Preparation or treatment thereof
    • A23L27/20Synthetic spices, flavouring agents or condiments
    • A23L27/205Heterocyclic compounds
    • A23L27/2052Heterocyclic compounds having oxygen or sulfur as the only hetero atoms
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23LFOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L33/00Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
    • A23L33/10Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof using additives

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  • Life Sciences & Earth Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Nutrition Science (AREA)
  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Food Science & Technology (AREA)
  • Polymers & Plastics (AREA)
  • Mycology (AREA)
  • Medicines Containing Plant Substances (AREA)
  • Fats And Perfumes (AREA)

Abstract

The invention discloses a kind of preparation methods of halogen material, belong to halogen material preparation technical field, include the following steps:(1)The preparation of modified Lotus Plumule;(2)Pulverization process;(3)The preparation of fragrance;(4)The preparation of halogen material.The halogen material that the present invention is finally prepared, salty perfume is palatable, aromatic flavour, and smooth exquisiteness is in good taste, fragrant and oiliness, clearing heat and detoxicating, excessive internal heat rate is low, and shelf life is long, health-care efficacy with blood pressure lowering, wide suitable for range, safety coefficient is high, has good economic value and market popularization value.

Description

A kind of preparation method of halogen material
Technical field
The invention belongs to halogen material preparation technical fields, and in particular to a kind of preparation method of halogen material.
Background technique
Halogen material is the condiment for making pot-stewed meat or fowl, generally refers to the Chinese medicine fragrance of production brine.Halogen material has strong fragranced, can The smell of raw-food material is removed, and increases the function of the fragrance of food.Halogen material is placed in halogen pot plus water tanning is just made into Brine, different halogen material formulas can be made into the brine of different flavor.The fragrance with halogen material has several hundred kinds in the market, relatively common There are illiciumverum, cassia bark, Chinese prickly ash, rhizoma nardostachyos, fennel seeds, Bai Kou, meat bandit, fructus amomi, spiceleaf, flos caryophylli, Fructus Caryophylli, husky ginger, Nan Jiang, lemongrass Grass, Radix Glycyrrhizae, tsaoko etc..Ten multidigit such as fructus amomi, cardamom, tsaoko, dried orange peel, cortex cinnamomi, cloves, galanga, fennel for being put into stew in soy sauce Drug, it is not only delicious and tasty, it is also full of nutrition, have the function of stomach invigorating, it is pleasant, promote appetite.
The preparation of existing halogen material often only considers the shelf life of halogen material, and ignores mouthfeel and nutritive value, preparation Halogen meat excessive internal heat rate is very high, and mouthfeel is general, and nutritive value is low, is unable to satisfy the demand of people.
Summary of the invention
The purpose of the present invention is being directed to existing problem, a kind of preparation method of halogen material is provided.The present invention is finally prepared Halogen material, salty perfume is palatable, aromatic flavour, and smooth exquisiteness is in good taste, and fragrant and oiliness, clearing heat and detoxicating, excessive internal heat rate is low, and shelf life is long, Health-care efficacy with blood pressure lowering, wide suitable for range, safety coefficient is high, has good economic value and marketing valence Value.
The present invention is achieved by the following technical solutions:
A kind of preparation method of halogen material, includes the following steps:
(1)The preparation of modified Lotus Plumule:
A. by soybean lecithin and dodecyl-dimethyl amine second lactone according to weight ratio 1.4 ~ 2.0:1 is put into stirring jointly In tank, heating the temperature being kept stirring in tank is 48 ~ 52 DEG C, takes out to obtain modifier A after being stirred continuously 34 ~ 40min of mixed processing It is spare;
B. by resin acid and beta lactoglobulin according to weight ratio 2 ~ 2.8:1, jointly in reaction kettle, is then added its gross mass 3 ~ 4 Times glycerol, after being stirred continuously 24 ~ 28min of processing, then resin acid and beta lactoglobulin total weight parts are added into reaction kettle 0.4 ~ 0.5 times of carthamin yellow, while the heating of the temperature of reaction kettle is remained 70 ~ 80 DEG C, and by the pressure in reaction kettle Rise to 0.2 ~ 0.3MPa, be stirred continuously after 35 ~ 39min of processing take out modifying agent B is spare;
C. by Lotus Plumule equipped with purified water pot in, by pot temperature heating remain 55 ~ 65 DEG C, be stirred continuously processing 30 ~ It is filtered out after 40min spare;
D. the Lotus Plumule filtered out in c will be operated and be placed in modifier A and impregnated, filtered out after being stirred continuously 32 ~ 36min of processing It is spare;
E. will treated in operation d that Lotus Plumule is placed in modifying agent B impregnates, filtered after being stirred continuously 43 ~ 47min of processing It is spare out;
F. the Lotus Plumule operated in e is put in a drying box and is dried, dry temperature is 55 ~ 65 DEG C, and dry 2 ~ 3h is It can;
(2)Pulverization process:Weigh 5 ~ 6 parts of the modification Lotus Plumules of corresponding parts by weight, 6 ~ 7 parts of water chestnut, 2 ~ 3 parts of gingko, peppermint 2.4 ~ 2.8 parts are collectively disposed in water-cooled pulverizer and are crushed, and after crushing 40 ~ 50min, it is spare to cross 10 meshes;
(3)The preparation of fragrance:6 ~ 8 parts of 12 ~ 14 parts of sesame oil, galanga for weighing corresponding parts by weight is collectively disposed in pot, stir-fries it Afterwards, 5 ~ 7 parts of illiciumverum of corresponding parts by weight, 2 ~ 3 parts of purple cool, 2 ~ 4 parts of fructus amomi, 4 ~ 5 parts of nutmeg, 3 ~ 5 parts of cortex cinnamomi, cloves 1 ~ 2 are weighed Part, 0.9 ~ 1.1 part of Chinese prickly ash, 0.8 ~ 1.2 part of fennel, 0.6 ~ 0.8 part of radix aucklandiae, 1 ~ 2 part of the root of Dahurain angelica, 18 ~ 24 parts of edible salt, purified water 120 ~ 160 parts are collectively disposed in pot, continue high fire heating until boiling, after 13 ~ 17min of constantly boiling, carry out small fire heating, small Fragrance is obtained after 3 ~ 4h of fire heating;
(4)The preparation of halogen material:Weigh 0.4 ~ 0.5 part of ascorbyl palmitate, the resveratrol 0.2 ~ 0.3 of corresponding parts by weight Part and step(2)Powder after middle sieving is collectively disposed at step(3)It in prepared fragrance, is heated, heating keeps temperature Degree is 88 ~ 98 DEG C, heats 1 ~ 2h.
Further, the step(1)It operates in d, the temperature of heating holding modifier A is during the immersion treatment 45~51℃。
Further, the step(1)It operates in e, the temperature of heating holding modifier A is during the immersion treatment 53~57℃。
Further, the step(2)The revolving speed of middle pulverizer is 380 ~ 420rpm.
The present invention has the following advantages that compared with prior art:
The present invention has done very big improvement on the basis of existing halogen preparation method for material, and modified Lotus Plumule is added in halogen material, Lotus Plumule is the dark green plumule in lotus seeds center, and bitter has the effect of heat-clearing, controlling nocturnal emission with astringent drugs, tranquilizing the mind, heart tonifying, by Lotus Plumule boiled water It is drunk after immersion, the diseases such as dysphoria caused by high fever, clouded in mind and emission can be treated and be also used for treatment hypertension, the heart Throb with fear and has a sleepless night;Because having certain bitter taste, lotus containing Pronuciferine, lotusin, methyl-corypalline in Lotus Plumule The sub- heart is also hardship, is added in food, and the quality and sale of the influence food of serious bitter taste greatly limit Lotus Plumule Application, therefore, the present invention is modified Lotus Plumule, places it in modifier A first, the soybean lecithin in modifier A Rouge and dodecyl-dimethyl amine second lactone are all surfactants, and the interface state of Lotus Plumule is made to change, and enhance lotus seeds The surface-active of the heart lays the foundation for subsequent further modification, and then Lotus Plumule is placed in modifying agent B, in modifying agent B Resin acid and beta lactoglobulin by competitiveness in conjunction with the g protein coupled receptor site of bitter substance, to inhibit bitter The carthamin yellow monascus ruber of the generation of matter, addition can be reduced oral cavity surface layer and be generated a kind of constringent touching with activating microcirculation and removing stasis medicinal Sense, can further refine the mouthfeel of Lotus Plumule, reduce the presence of bitter taste;In the preparation process of halogen material also added with water chestnut, Gingko, peppermint, they act synergistically with Lotus Plumule, have the effect of clearing heat and detoxicating, blood pressure lowering, in addition peppermint can increase The faint scent sense of halogen material, improves the quality of halogen material to a certain extent;The fragrance of suitable concentration proportion is added when preparing in halogen material, Optimize the preparation process of fragrance, raw material is subjected to high fire heating until boiling first, the effective component in fragrance is released, so Several minutes of constantly boiling afterwards are accelerated the release of effective component, then are heated by small fire, and the phase between each material effective component is promoted Interaction enhances the color of fragrance, improves the quality of halogen material;Ascorbyl palmitate, white is finally added in halogen material Veratryl alcohol, all having anti-oxidant, corrosion-resistant effect, especially resveratrol is the substance with health role to human body, is had The effect of stronger anti-oxidation and antisepsis, and resveratrol is able to suppress the formation of fat, therefore has the function of preventing obesity. The halogen material that the present invention is finally prepared, salty perfume is palatable, aromatic flavour, and smooth exquisiteness is in good taste, fragrant and oiliness, clearing heat and detoxicating, gets angry Rate is low, and shelf life is long, the health-care efficacy with blood pressure lowering, wide suitable for range, and safety coefficient is high, has good economic value And market popularization value.
Specific embodiment
Embodiment 1
A kind of preparation method of halogen material, includes the following steps:
(1)The preparation of modified Lotus Plumule:
A. by soybean lecithin and dodecyl-dimethyl amine second lactone according to weight ratio 1.4:1 is put into agitator tank jointly, Heating the temperature that is kept stirring in tank is 48 DEG C, be stirred continuously after mixed processing 34min take out modifier A is spare;
B. by resin acid and beta lactoglobulin according to weight ratio 2:1, jointly in reaction kettle, is then added the sweet of 3 times of its gross mass Oil is stirred continuously after handling 24min, then 0.4 times of safflower of resin acid and beta lactoglobulin total weight parts is added into reaction kettle Uranidin, while the heating of the temperature of reaction kettle is remained 70 DEG C, and the pressure in reaction kettle is risen into 0.2MPa, it is stirred continuously Processing 35min after take out modifying agent B is spare;
C. the temperature heating in pot is remained 55 DEG C, is stirred continuously processing 30min by Lotus Plumule equipped in the pot of purified water After filter out it is spare;
D. the Lotus Plumule that filters out in c will be operated and be placed in modifier A and impregnated, be stirred continuously after processing 32min filter out it is standby With;
E. will treated in operation d that Lotus Plumule is placed in modifying agent B impregnates, be stirred continuously after processing 43min filter out it is standby With;
F. the Lotus Plumule operated in e is put in a drying box and is dried, dry temperature is 55 DEG C, dry 2h;
(2)Pulverization process:Weigh 5 parts of the modification Lotus Plumules of corresponding parts by weight, 6 parts of water chestnut, 2 parts of gingko, 2.4 parts of peppermint set jointly It is crushed in water-cooled pulverizer, after crushing 40min, it is spare to cross 10 meshes;
(3)The preparation of fragrance:6 parts of 12 parts of sesame oil, galanga for weighing corresponding parts by weight is collectively disposed in pot, after stir-frying, is claimed Take 5 parts of illiciumverum of corresponding parts by weight, 2 parts of purple cool, 2 parts of fructus amomi, 4 parts of nutmeg, 3 parts of cortex cinnamomi, 1 part of cloves, 0.9 part of Chinese prickly ash, fennel 0.8 part, 0.6 part of radix aucklandiae, 1 part of the root of Dahurain angelica, 18 parts of edible salt, 120 parts of purified water be collectively disposed in pot, continue high fire heating until boiling It rises, after constantly boiling 13min, carries out small fire heating, small fire obtains fragrance after heating 3h;
(4)The preparation of halogen material:Weigh 0.2 part of 0.4 part of ascorbyl palmitate, the resveratrol of corresponding parts by weight, Yi Jibu Suddenly(2)Powder after middle sieving is collectively disposed at step(3)In prepared fragrance, to be heated, it is 88 DEG C that heating, which keeps temperature, Heat 1h.
Further, the step(1)It operates in d, the temperature of heating holding modifier A is during the immersion treatment 45℃。
Further, the step(1)It operates in e, the temperature of heating holding modifier A is during the immersion treatment 53℃。
Further, the step(2)The revolving speed of middle pulverizer is 380rpm.
Embodiment 2
A kind of preparation method of halogen material, includes the following steps:
(1)The preparation of modified Lotus Plumule:
A. by soybean lecithin and dodecyl-dimethyl amine second lactone according to weight ratio 1.7:1 is put into agitator tank jointly, Heating the temperature that is kept stirring in tank is 50 DEG C, be stirred continuously after mixed processing 37min take out modifier A is spare;
B. by resin acid and beta lactoglobulin according to weight ratio 2.4:1, jointly in reaction kettle, is then added 3.5 times of its gross mass Glycerol, after being stirred continuously processing 26min, then be added into reaction kettle 0.45 times of resin acid and beta lactoglobulin total weight parts Carthamin yellow, while the heating of the temperature of reaction kettle is remained 75 DEG C, and the pressure in reaction kettle is risen into 0.25MPa, Be stirred continuously processing 37min after take out modifying agent B is spare;
C. the temperature heating in pot is remained 60 DEG C, is stirred continuously processing 35min by Lotus Plumule equipped in the pot of purified water After filter out it is spare;
D. the Lotus Plumule that filters out in c will be operated and be placed in modifier A and impregnated, be stirred continuously after processing 34min filter out it is standby With;
E. will treated in operation d that Lotus Plumule is placed in modifying agent B impregnates, be stirred continuously after processing 45min filter out it is standby With;
F. the Lotus Plumule operated in e is put in a drying box and is dried, dry temperature is 60 DEG C, dry 2.5h;
(2)Pulverization process:Weigh 5.5 parts of modification Lotus Plumule, 6.5 parts of the water chestnut, 2.5 parts of gingko, 2.6 parts of peppermint of corresponding parts by weight It is collectively disposed in water-cooled pulverizer and is crushed, after crushing 45min, it is spare to cross 10 meshes;
(3)The preparation of fragrance:7 parts of 13 parts of sesame oil, galanga for weighing corresponding parts by weight is collectively disposed in pot, after stir-frying, is claimed Take 6 parts of illiciumverum of corresponding parts by weight, 2.5 parts of purple cool, 3 parts of fructus amomi, 4.5 parts of nutmeg, 4 parts of cortex cinnamomi, 1.5 parts of cloves, 1 part of Chinese prickly ash, 1 part of fennel, 0.7 part of radix aucklandiae, 1.5 parts of the root of Dahurain angelica, 21 parts of edible salt, 140 parts of purified water be collectively disposed in pot, it is straight to continue high fire heating To boiling, after constantly boiling 15min, small fire heating is carried out, small fire heats after 3 ~ 4h to obtain fragrance;
(4)The preparation of halogen material:0.25 part of 0.45 part of ascorbyl palmitate, the resveratrol of corresponding parts by weight are weighed, and Step(2)Powder after middle sieving is collectively disposed at step(3)It in prepared fragrance, is heated, it is 93 that heating, which keeps temperature, DEG C, heat 1.5h.
Further, the step(1)It operates in d, the temperature of heating holding modifier A is during the immersion treatment 48℃。
Further, the step(1)It operates in e, the temperature of heating holding modifier A is during the immersion treatment 55℃。
Further, the step(2)The revolving speed of middle pulverizer is 400rpm.
Embodiment 3
A kind of preparation method of halogen material, includes the following steps:
(1)The preparation of modified Lotus Plumule:
A. by soybean lecithin and dodecyl-dimethyl amine second lactone according to weight ratio 2.0:1 is put into agitator tank jointly, Heating the temperature that is kept stirring in tank is 52 DEG C, be stirred continuously after mixed processing 40min take out modifier A is spare;
B. by resin acid and beta lactoglobulin according to weight ratio 2.8:1, jointly in reaction kettle, is then added 4 times of its gross mass After being stirred continuously processing 28min, then 0.5 times of resin acid and beta lactoglobulin total weight parts red is added into reaction kettle in glycerol Anthoxanthin, while the heating of the temperature of reaction kettle is remained 80 DEG C, and the pressure in reaction kettle is risen into 0.3MPa, constantly stir Mix processing 39min after take out modifying agent B is spare;
C. the temperature heating in pot is remained 65 DEG C, is stirred continuously processing 40min by Lotus Plumule equipped in the pot of purified water After filter out it is spare;
D. the Lotus Plumule that filters out in c will be operated and be placed in modifier A and impregnated, be stirred continuously after processing 36min filter out it is standby With;
E. will treated in operation d that Lotus Plumule is placed in modifying agent B impregnates, be stirred continuously after processing 47min filter out it is standby With;
F. the Lotus Plumule operated in e is put in a drying box and is dried, dry temperature is 65 DEG C, dry 3h;
(2)Pulverization process:Weigh 6 parts of the modification Lotus Plumules of corresponding parts by weight, 7 parts of water chestnut, 3 parts of gingko, 2.8 parts of peppermint set jointly It is crushed in water-cooled pulverizer, after crushing 50min, it is spare to cross 10 meshes;
(3)The preparation of fragrance:8 parts of 14 parts of sesame oil, galanga for weighing corresponding parts by weight is collectively disposed in pot, after stir-frying, is claimed Take 7 parts of illiciumverum of corresponding parts by weight, 3 parts of purple cool, 4 parts of fructus amomi, 5 parts of nutmeg, 5 parts of cortex cinnamomi, 2 parts of cloves, 1.1 parts of Chinese prickly ash, fennel 1.2 parts, 0.8 part of radix aucklandiae, 2 parts of the root of Dahurain angelica, 24 parts of edible salt, 160 parts of purified water be collectively disposed in pot, continue high fire heating until boiling It rises, after constantly boiling 17min, carries out small fire heating, small fire obtains fragrance after heating 4h;
(4)The preparation of halogen material:Weigh 0.3 part of 0.5 part of ascorbyl palmitate, the resveratrol of corresponding parts by weight, Yi Jibu Suddenly(2)Powder after middle sieving is collectively disposed at step(3)In prepared fragrance, to be heated, it is 98 DEG C that heating, which keeps temperature, Heat 2h.
Further, the step(1)It operates in d, the temperature of heating holding modifier A is during the immersion treatment 51℃。
Further, the step(1)It operates in e, the temperature of heating holding modifier A is during the immersion treatment 57℃。
Further, the step(2)The revolving speed of middle pulverizer is 420rpm.
Comparative example 1
This comparative example 1 compared with Example 2, by step(2)Modification Lotus Plumule in pulverization process the quality such as changes into not The Lotus Plumule of modified processing, and save step(1)The preparation of modified Lotus Plumule, method and step in addition to this are all the same.
Comparative example 2
This comparative example 2 compared with Example 2, saves step(2)Modification Lotus Plumule in pulverization process, and modified lotus seeds The preparation of the heart, method and step in addition to this are all the same.
Comparative example 3
This comparative example 3 compared with Example 2, saves step(2)Water chestnut, gingko, peppermint in pulverization process, in addition to this Method and step is all the same.
Comparative example 4
This comparative example 4 compared with Example 2, saves step(2)Pulverization process, method and step in addition to this are all the same.
Comparative example 5
This comparative example 5 compared with Example 2, saves step(4)Ascorbyl palmitate, white Chenopodiaceae in the preparation of halogen material Reed alcohol, method and step in addition to this are all the same.
Control group
Existing commercially available conventional halogen material.
In order to compare effect of the present invention, same series-produced fresh pork 7kg is bought, by their strippings and slicings, then by meat piece 7 groups, every group of 1kg are randomly divided into, it is real with embodiment 2, comparative example 1, comparative example 2, comparative example 3, comparison respectively The halogen material for applying example 4, the halogen material of the method for comparative example 5 preparation and control group, with conventional mode respectively to every group of pork into Row stew in soy sauce after curing, carries out subjective appreciation through 20 for Black-pepper beef of the professional to each group;The halogen meat of each group is without packet Dress, is placed in 25 DEG C and is placed, and detects shelf life;Subject 700 of health are randomly choosed, are randomly divided into 7 groups, every group 100, every group of subject eats the halogen meat 60g of the group daily, and other diet are all the same, and the tested time is 30 days, observation and note Record the excessive internal heat personnel in subject.
Specific experiment correlation data is as shown in table 1 below:
Table 1
The halogen material that the present invention is finally prepared it can be seen from upper table 1, salty perfume is palatable, aromatic flavour, and smooth exquisiteness is in good taste, fragrant And it is oiliness, clearing heat and detoxicating, excessive internal heat rate is low, and shelf life is long, has good economic value and market popularization value.
In order to further compare effect of the present invention, stomach-filling experiment is carried out to original hypertensive rat, specially:
The essential hypertension male rat of 50 10 week old is taken, while taking the rat of 10 normotensive 10 week old as empty White control group, adapts to after feeding 7 days, and 50 original hypertensive rats are randomly divided into 5 groups, and every group 10, every group of rat serum Voltage levels are no different, and then use embodiment 2 respectively, prepared by comparative example 2, comparative example 3, the method for comparative example 4 The halogen material of halogen material and control group carries out stomach-filling experiment after continuous gavage 36 days to 5 groups of rats respectively and successively puts all rats In the incubator for entering BP-6 animal non-invasive blood pressure tester, 36 DEG C of preheating 10 min are normal to rat occur on computer monitor After pulse waveform figure, pressurization is deflated after protecting 10 s of gas, systolic pressure in wave recording figure(SBP)Numerical value.Repeatedly for several times, Immediate 5 pressure values are chosen, it is for statistical analysis.Period all rat normally feeds drinking-water, during experiment daily The hair color and mental status of each group rat are observed,
Specific experiment correlation data is as shown in table 2 below:
Table 2
Note:The mean blood pressure of each group original hypertensive rat is 192 ± 0.12mmHg before stomach-filling.
The final halogen material obtained of the present invention is not only in good taste it can be seen from upper table 2, also with the health care function of blood pressure lowering Effect, wide suitable for range, safety coefficient is high, has good market value.

Claims (4)

1. a kind of preparation method of halogen material, which is characterized in that include the following steps:
(1)The preparation of modified Lotus Plumule:
A. by soybean lecithin and dodecyl-dimethyl amine second lactone according to weight ratio 1.4 ~ 2.0:1 is put into stirring jointly In tank, heating the temperature being kept stirring in tank is 48 ~ 52 DEG C, takes out to obtain modifier A after being stirred continuously 34 ~ 40min of mixed processing It is spare;
B. by resin acid and beta lactoglobulin according to weight ratio 2 ~ 2.8:1, jointly in reaction kettle, is then added its gross mass 3 ~ 4 Times glycerol, after being stirred continuously 24 ~ 28min of processing, then resin acid and beta lactoglobulin total weight parts are added into reaction kettle 0.4 ~ 0.5 times of carthamin yellow, while the heating of the temperature of reaction kettle is remained 70 ~ 80 DEG C, and by the pressure in reaction kettle Rise to 0.2 ~ 0.3MPa, be stirred continuously after 35 ~ 39min of processing take out modifying agent B is spare;
C. by Lotus Plumule equipped with purified water pot in, by pot temperature heating remain 55 ~ 65 DEG C, be stirred continuously processing 30 ~ It is filtered out after 40min spare;
D. the Lotus Plumule filtered out in c will be operated and be placed in modifier A and impregnated, filtered out after being stirred continuously 32 ~ 36min of processing It is spare;
E. will treated in operation d that Lotus Plumule is placed in modifying agent B impregnates, filtered after being stirred continuously 43 ~ 47min of processing It is spare out;
F. the Lotus Plumule operated in e is put in a drying box and is dried, dry temperature is 55 ~ 65 DEG C, and dry 2 ~ 3h is It can;
(2)Pulverization process:Weigh 5 ~ 6 parts of the modification Lotus Plumules of corresponding parts by weight, 6 ~ 7 parts of water chestnut, 2 ~ 3 parts of gingko, peppermint 2.4 ~ 2.8 parts are collectively disposed in water-cooled pulverizer and are crushed, and after crushing 40 ~ 50min, it is spare to cross 10 meshes;
(3)The preparation of fragrance:6 ~ 8 parts of 12 ~ 14 parts of sesame oil, galanga for weighing corresponding parts by weight is collectively disposed in pot, stir-fries it Afterwards, 5 ~ 7 parts of illiciumverum of corresponding parts by weight, 2 ~ 3 parts of purple cool, 2 ~ 4 parts of fructus amomi, 4 ~ 5 parts of nutmeg, 3 ~ 5 parts of cortex cinnamomi, cloves 1 ~ 2 are weighed Part, 0.9 ~ 1.1 part of Chinese prickly ash, 0.8 ~ 1.2 part of fennel, 0.6 ~ 0.8 part of radix aucklandiae, 1 ~ 2 part of the root of Dahurain angelica, 18 ~ 24 parts of edible salt, purified water 120 ~ 160 parts are collectively disposed in pot, continue high fire heating until boiling, after 13 ~ 17min of constantly boiling, carry out small fire heating, small Fragrance is obtained after 3 ~ 4h of fire heating;
(4)The preparation of halogen material:Weigh 0.4 ~ 0.5 part of ascorbyl palmitate, the resveratrol 0.2 ~ 0.3 of corresponding parts by weight Part and step(2)Powder after middle sieving is collectively disposed at step(3)It in prepared fragrance, is heated, heating keeps temperature Degree is 88 ~ 98 DEG C, heats 1 ~ 2h.
2. a kind of preparation method of halogen material according to claim 1, which is characterized in that the step(1)It operates in d, it is described Immersion treatment during heating keep modifier A temperature be 45 ~ 51 DEG C.
3. a kind of preparation method of halogen material according to claim 1, which is characterized in that the step(1)It operates in e, it is described Immersion treatment during heating keep modifier A temperature be 53 ~ 57 DEG C.
4. a kind of preparation method of halogen material according to claim 1, which is characterized in that the step(2)Middle pulverizer turns Speed is 380 ~ 420rpm.
CN201810749360.XA 2018-07-10 2018-07-10 A kind of preparation method of halogen material Withdrawn CN108835591A (en)

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110292154A (en) * 2019-08-02 2019-10-01 潮州市庵埠食品工业卫生检验所 A kind of preparation method of flavor Salt roasted chicken wing

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110292154A (en) * 2019-08-02 2019-10-01 潮州市庵埠食品工业卫生检验所 A kind of preparation method of flavor Salt roasted chicken wing
CN110292154B (en) * 2019-08-02 2023-08-15 潮州市庵埠食品工业卫生检验所 Preparation method of flavored salt roasted chicken wings

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