CN108719693A - A kind of water shield health drink and preparation method thereof - Google Patents
A kind of water shield health drink and preparation method thereof Download PDFInfo
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- CN108719693A CN108719693A CN201710273623.XA CN201710273623A CN108719693A CN 108719693 A CN108719693 A CN 108719693A CN 201710273623 A CN201710273623 A CN 201710273623A CN 108719693 A CN108719693 A CN 108719693A
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- water
- water shield
- jujube
- arillus longan
- aqueous extracts
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- 244000267222 Brasenia schreberi Species 0.000 title claims abstract description 148
- 235000006506 Brasenia schreberi Nutrition 0.000 title claims abstract description 148
- 230000036541 health Effects 0.000 title claims abstract description 37
- 238000002360 preparation method Methods 0.000 title claims abstract description 22
- 240000001008 Dimocarpus longan Species 0.000 claims abstract description 81
- 235000000235 Euphoria longan Nutrition 0.000 claims abstract description 81
- 241001247821 Ziziphus Species 0.000 claims abstract description 78
- BUGBHKTXTAQXES-UHFFFAOYSA-N Selenium Chemical compound [Se] BUGBHKTXTAQXES-UHFFFAOYSA-N 0.000 claims abstract description 17
- 239000011669 selenium Substances 0.000 claims abstract description 17
- 229910052711 selenium Inorganic materials 0.000 claims abstract description 17
- 239000006286 aqueous extract Substances 0.000 claims description 67
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 67
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- 230000000259 anti-tumor effect Effects 0.000 description 4
- HEBKCHPVOIAQTA-UHFFFAOYSA-N meso ribitol Natural products OCC(O)C(O)C(O)CO HEBKCHPVOIAQTA-UHFFFAOYSA-N 0.000 description 4
- 229960001881 sodium selenate Drugs 0.000 description 4
- 235000018716 sodium selenate Nutrition 0.000 description 4
- 239000011655 sodium selenate Substances 0.000 description 4
- 235000010447 xylitol Nutrition 0.000 description 4
- 239000000811 xylitol Substances 0.000 description 4
- HEBKCHPVOIAQTA-SCDXWVJYSA-N xylitol Chemical compound OC[C@H](O)[C@@H](O)[C@H](O)CO HEBKCHPVOIAQTA-SCDXWVJYSA-N 0.000 description 4
- 229960002675 xylitol Drugs 0.000 description 4
- 241001092040 Crataegus Species 0.000 description 3
- 235000009917 Crataegus X brevipes Nutrition 0.000 description 3
- 235000013204 Crataegus X haemacarpa Nutrition 0.000 description 3
- 235000009685 Crataegus X maligna Nutrition 0.000 description 3
- 235000009444 Crataegus X rubrocarnea Nutrition 0.000 description 3
- 235000009486 Crataegus bullatus Nutrition 0.000 description 3
- 235000017181 Crataegus chrysocarpa Nutrition 0.000 description 3
- 235000009682 Crataegus limnophila Nutrition 0.000 description 3
- 235000004423 Crataegus monogyna Nutrition 0.000 description 3
- 235000002313 Crataegus paludosa Nutrition 0.000 description 3
- 235000009840 Crataegus x incaedua Nutrition 0.000 description 3
- 241000196324 Embryophyta Species 0.000 description 3
- WQZGKKKJIJFFOK-GASJEMHNSA-N Glucose Natural products OC[C@H]1OC(O)[C@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-GASJEMHNSA-N 0.000 description 3
- 206010028980 Neoplasm Diseases 0.000 description 3
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- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 2
- 206010017553 Furuncle Diseases 0.000 description 2
- 239000009636 Huang Qi Substances 0.000 description 2
- 208000025865 Ulcer Diseases 0.000 description 2
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- 239000000470 constituent Substances 0.000 description 2
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- -1 (Wang Qian Substances 0.000 description 1
- CHHHXKFHOYLYRE-UHFFFAOYSA-M 2,4-Hexadienoic acid, potassium salt (1:1), (2E,4E)- Chemical compound [K+].CC=CC=CC([O-])=O CHHHXKFHOYLYRE-UHFFFAOYSA-M 0.000 description 1
- 206010000087 Abdominal pain upper Diseases 0.000 description 1
- 241001061264 Astragalus Species 0.000 description 1
- 235000010110 Astragalus glycyphyllos Nutrition 0.000 description 1
- 241000209433 Brasenia Species 0.000 description 1
- JGEVJQBAHWCNEN-UHFFFAOYSA-N C1(=CC=CC=C1)O.S(=O)(=O)(O)O.C1=CC=CC=C1 Chemical compound C1(=CC=CC=C1)O.S(=O)(=O)(O)O.C1=CC=CC=C1 JGEVJQBAHWCNEN-UHFFFAOYSA-N 0.000 description 1
- 241000218208 Caltha Species 0.000 description 1
- 235000008749 Caltha palustris Nutrition 0.000 description 1
- 206010007247 Carbuncle Diseases 0.000 description 1
- XDVZNDLANFJOQR-UHFFFAOYSA-N Coptisine Natural products O=Cc1c2OCOc2ccc1C=C3/NCCc4cc5OCOc5cc34 XDVZNDLANFJOQR-UHFFFAOYSA-N 0.000 description 1
- ZGTMUACCHSMWAC-UHFFFAOYSA-L EDTA disodium salt (anhydrous) Chemical compound [Na+].[Na+].OC(=O)CN(CC([O-])=O)CCN(CC(O)=O)CC([O-])=O ZGTMUACCHSMWAC-UHFFFAOYSA-L 0.000 description 1
- 208000012895 Gastric disease Diseases 0.000 description 1
- 206010020772 Hypertension Diseases 0.000 description 1
- 241000801118 Lepidium Species 0.000 description 1
- 206010028813 Nausea Diseases 0.000 description 1
- 241000209477 Nymphaeaceae Species 0.000 description 1
- 206010033546 Pallor Diseases 0.000 description 1
- 231100000215 acute (single dose) toxicity testing Toxicity 0.000 description 1
- 238000003556 assay Methods 0.000 description 1
- 235000006533 astragalus Nutrition 0.000 description 1
- 238000009924 canning Methods 0.000 description 1
- 230000008859 change Effects 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- XYHOBCMEDLZUMP-UHFFFAOYSA-N coptisine Chemical compound C1=C2C=C(C3=C(C=C4OCOC4=C3)CC3)[N+]3=CC2=C2OCOC2=C1 XYHOBCMEDLZUMP-UHFFFAOYSA-N 0.000 description 1
- 238000005520 cutting process Methods 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 238000011049 filling Methods 0.000 description 1
- 208000003512 furunculosis Diseases 0.000 description 1
- 241000411851 herbal medicine Species 0.000 description 1
- 230000002218 hypoglycaemic effect Effects 0.000 description 1
- 239000012535 impurity Substances 0.000 description 1
- 238000000338 in vitro Methods 0.000 description 1
- 238000001727 in vivo Methods 0.000 description 1
- 150000002632 lipids Chemical class 0.000 description 1
- 230000003211 malignant effect Effects 0.000 description 1
- 238000005360 mashing Methods 0.000 description 1
- 150000002772 monosaccharides Chemical class 0.000 description 1
- 230000008693 nausea Effects 0.000 description 1
- 239000002245 particle Substances 0.000 description 1
- 230000000144 pharmacologic effect Effects 0.000 description 1
- 239000004302 potassium sorbate Substances 0.000 description 1
- 229940069338 potassium sorbate Drugs 0.000 description 1
- 235000010241 potassium sorbate Nutrition 0.000 description 1
- 230000008569 process Effects 0.000 description 1
- 230000009467 reduction Effects 0.000 description 1
- 239000011435 rock Substances 0.000 description 1
- PRKRTJSKTGAVMH-UHFFFAOYSA-N selenic acid;sodium Chemical compound [Na].O[Se](O)(=O)=O PRKRTJSKTGAVMH-UHFFFAOYSA-N 0.000 description 1
- GCLGEJMYGQKIIW-UHFFFAOYSA-H sodium hexametaphosphate Chemical compound [Na]OP1(=O)OP(=O)(O[Na])OP(=O)(O[Na])OP(=O)(O[Na])OP(=O)(O[Na])OP(=O)(O[Na])O1 GCLGEJMYGQKIIW-UHFFFAOYSA-H 0.000 description 1
- 230000007480 spreading Effects 0.000 description 1
- 238000003892 spreading Methods 0.000 description 1
- 238000007920 subcutaneous administration Methods 0.000 description 1
- 125000000185 sucrose group Chemical group 0.000 description 1
- 230000002195 synergetic effect Effects 0.000 description 1
- 235000018553 tannin Nutrition 0.000 description 1
- 229920001864 tannin Polymers 0.000 description 1
- 239000001648 tannin Substances 0.000 description 1
- 238000012360 testing method Methods 0.000 description 1
- 239000003440 toxic substance Substances 0.000 description 1
- 230000004614 tumor growth Effects 0.000 description 1
- 238000010792 warming Methods 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L2/00—Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
- A23L2/02—Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation containing fruit or vegetable juices
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L2/00—Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
- A23L2/52—Adding ingredients
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L2/00—Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
- A23L2/52—Adding ingredients
- A23L2/60—Sweeteners
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs
Landscapes
- Health & Medical Sciences (AREA)
- Nutrition Science (AREA)
- Life Sciences & Earth Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Food Science & Technology (AREA)
- Polymers & Plastics (AREA)
- Non-Alcoholic Beverages (AREA)
- Coloring Foods And Improving Nutritive Qualities (AREA)
Abstract
The invention belongs to food processing technology fields, and in particular to a kind of water shield health drink and preparation method thereof.The water shield health drink, after being extracted using water extraction, match with arillus longan and jujube three, with arillus longan, the temperate-dryness of jujube inhibits the cold and cool of water shield, the water shield health drink that can not only make is not warm not cool to tend to levelling, whole body is nourished with levelling effect, substantially increase safety, it overcomes and is applied alone water shield cold in nature, the defect that should not be eaten more and eat long, it is suitable as health product long-term use, and the water shield of Return liver the spleen channel is clearing heat and detoxicating, the arillus longan nourishing blood and tranquilization of thoughts of returning home the spleen channel, the jujube tonifying middle-Jiao and Qi of returns spleen stomach the heart channel of Hang-Shaoyin, three acts synergistically, health-care effect is good；Meanwhile selenium can further increase immune and anticancer function, enhance the immune and health-care efficacy of composition, nutritive value is complete, is suitable as health food long-term consumption.
Description
Technical field
The invention belongs to food processing technology fields, and in particular to a kind of water shield health drink and preparation method thereof.
Background technology
Water shield (Brasenia schreber J.F.Gmel), original perianth subclass Nymphaeceae (Nymphaeaceae) Lepidium
Perennial fresh water aquatic herbaceous plant also known as membranaceous marshmarigold herb, lake dish, water certain herbaceous plants with big flowers, dew certain herbaceous plants with big flowers, are grown in pond, lake and marsh, property
It is cold, have the function of clearing heat and detoxicating, preventing or arresting vomiting etc., swell for hypertension, rush down dysentery, stomachache, vomiting, gastric disorder causing nausea, ulcer malignant boil, furuncle etc. (《Entirely
State's Chinese herbal medicine compilation》).Modern pharmacy research has shown that the principle active component of water shield is Polysaccharide of Brasenia Schreberi, have antitumor, hypoglycemic,
(Gong Jiang, Ni Shifeng, take charge of pleasure of spreading out, Luo Rongfang, Wu Yifei, Tong Ying, Chen Qianliang to the multiple pharmacological effects such as reducing blood lipid, and water shield pharmacy is ground
Study carefully general introduction, Agriculture of Anhui science, 2009,37 (10)：4489—4490)." but long food should not be eaten more, probably feel cold gas, is stranded taste,
Also can hurt sb.'s feelings " (《Collected statements on the herbal foundation》, bright Ni Zhumo, 1624), the daily highest amount of Chinese medicine referrer is no more than 30g, it is difficult to have
Effect plays its health-care effect.
Currently, the utilization of water shield mainly " is eaten raw ", for exporting after canning is fresh-keeping, added value is low.Water shield not yet carries out
The development technique of deep development, report is mainly two classes, and the first kind is by the simple preliminary working of water shield as after shredding, being directly added into food
Product additive prepares water shield food, and such technology not only cannot overcome water shield cold in nature, the defect that should not be eaten more and eat long, and unit
Active ingredient polyoses content is low in volume, health-care effect unobvious, as 106135980 A of patent document CN disclose one kind directly
Connect using the water shield Normal juice for cutting into single-size as raw material, with purified water, monocrystal rock sugar, calgon, potassium sorbate/
The food additives such as EDTA-2Na are mixed with beverage of water shield, cold in nature, should not drink excessive, and polyoses content is not in unit volume
It is high；After second class is extraction Polysaccharide of Brasenia Schreberi active ingredient, then extract and food additives are prepared into water shield food, but water shield is more
The extractive technique of sugar is still immature, be easy to cause Polysaccharide of Brasenia Schreberi extraction is not complete or decomposed metamorphic, reduce health-care effect, and such
The defect that technology still cannot overcome water shield cold in nature completely.
Up to the present, not yet find can high efficiency extraction Polysaccharide of Brasenia Schreberi, and overcome water shield cold in nature, be suitble to long-term or a large amount of
Edible health product is set to report.
Invention content
It is an object of the present invention to provide a kind of water shield health drink, the defect that water shield can not only be overcome cold in nature, and
Polyoses content is high, and nutritive value is complete, is suitable as health food long-term consumption.
It is a further object to provide the preparation methods of water shield health drink.
For achieving the above object, the present invention provides following technical scheme：
A kind of water shield health drink, often the Aqueous extracts comprising the preparation of 80-100g water shields, 0.1-10g are imperial in 1000mL beverages
Aqueous extracts, 0-0.001g selenium prepared by eye meat and 0.1-10g jujubes, surplus is water.
Water shield health drink according to the present invention, also include food additives, the food additives be selected from sweetener,
It is one or more in preservative, flavorant；Preferably, the food additives are sweetener, sweetener choosing
From sucrose, white sugar, Sucralose and honey element.
Water shield health drink according to the present invention, Aqueous extracts prepared by the water shield are by the fresh water shield use etc. of formula ratio
The water of weight keeps the temperature 1-60 minutes at 50-100 DEG C, filters the extracting solution of acquisition；Preferably, the Aqueous extracts that prepared by the water shield
To clean the fresh water shield of formula ratio, with etc. the water of weight keep the temperature 10-30 minutes at 60-90 DEG C, filter the extraction of acquisition
Liquid；It is further preferred that Aqueous extracts prepared by the water shield are to clean the fresh water shield of formula ratio, with etc. weight water 80
10-20 minutes are kept the temperature at DEG C, filters the extracting solution of acquisition.
Aqueous extracts prepared by water shield health drink according to the present invention, the arillus longan and jujube are by the longan of formula ratio
Meat and jujube are added at arillus longan and 80-100 DEG C of the water of 3-5 times of jujube total weight and keep the temperature 1-60 minutes, filter the extraction of acquisition
Liquid；Preferably, the Aqueous extracts that prepared by the arillus longan and jujube are that arillus longan and big is added in the arillus longan of formula ratio and jujube
10-30 minutes are kept the temperature at 90-100 DEG C of the water of 3-5 times of jujube total weight, filters the extracting solution of acquisition；It is further preferred that the dragon
Aqueous extracts prepared by eye meat and jujube are the water that the arillus longan of formula ratio and jujube are added to 4-5 times of arillus longan and jujube total weight
20-30 minutes are kept the temperature at 90-100 DEG C, filters the extracting solution of acquisition.
Water shield health drink according to the present invention, the water are purified water.
In some preferred embodiments, the water shield health drink includes often 80-100g water shields in 1000mL beverages
Aqueous extracts, 0-0.001g selenium prepared by Aqueous extracts, 0.1-10g arillus longans and 0.1-10g jujubes prepared by dish, food additives
0.1-20g, surplus are purified water, Aqueous extracts prepared by the water shield be by 80-100g water shields with etc. weight water at 60-90 DEG C
Lower heat preservation 10-30 minutes, filters the extracting solution of acquisition；Aqueous extracts prepared by the arillus longan and jujube are by 0.1-10g longans
After meat and the mixing of 0.1-10g jujubes, 10-30 minutes are kept the temperature at 90-100 DEG C of arillus longan and the water of 3-5 times of jujube total weight, mistake
Filter the extracting solution obtained.
In some preferred embodiments, the water shield health drink includes often 80-90g water shields in 1000mL beverages
Aqueous extracts, 0.00001-0.0001g selenium prepared by Aqueous extracts, 0.1-1g arillus longans and 0.1-1g jujubes prepared by dish, 0.1-10g
Sweetener, surplus are purified water, Aqueous extracts prepared by the water shield be by 80-90g water shields with etc. weight purified water at 80 DEG C
Lower heat preservation 10-20 minutes, filters the extracting solution of acquisition；Aqueous extracts prepared by the arillus longan and jujube are by 0.1-10g longans
After meat and the mixing of 0.1-10g jujubes, divide with 20-30 is kept the temperature at 90-100 DEG C of the purified water of 4-5 times of arillus longan and jujube total weight
Clock, filters the extracting solution of acquisition, and the sweetener is selected from sucrose, white sugar, Sucralose and honey element.
The inventors discovered that in the preparation of water shield Aqueous extracts, Extracting temperature and extraction time are to polyoses content in Aqueous extracts
Be affected, temperature is too low, and polysaccharide extract rate is not high, and temperature is excessively high, polysaccharide easily decompose lose bioactivity, in Aqueous extracts
In preparation process, preferably at 50 DEG C or more, best extracting method is to keep the temperature 10-20 minutes at 80 DEG C to temperature, extracts acquisition
Polyoses content highest, bioactivity are best.
Water shield is cold in nature, sweet in flavor, Return liver, the spleen channel, tool heat-clearing, Li Shui, detumescence, removing toxic substances and other effects, for treating hot dysentery, Huang
Subcutaneous ulcer, carbuncle swells, furunculosis；Arillus longan (longan) is warm-natured, sweet in flavor, the thoughts of returning home, the spleen channel, tool tonifying heart and spleen, nourishing blood and tranquilization and other effects；Jujube
Temperature, sweet in flavor, returns spleen, stomach, the heart channel of Hang-Shaoyin have tonifying middle-Jiao and Qi, nourishing blood and tranquilization and other effects.Water shield health drink provided by the invention, will
Water shield, arillus longan and jujube three match, and inhibit the cold and cool of water shield with the temperate-dryness of arillus longan, jujube, on the one hand can make
Water shield health drink it is not warm it is not cool tend to levelling, with levelling effect nourish whole body, overcome and be applied alone water shield cold in nature, should not eat more
The defect eaten long is suitable as health product long-term use, and on the other hand, the water shield of Return liver the spleen channel is clearing heat and detoxicating, thoughts of returning home spleen
Through arillus longan nourishing blood and tranquilization, the jujube tonifying middle-Jiao and Qi of returns spleen stomach the heart channel of Hang-Shaoyin, three's synergistic effect, health-care effect is good.Meanwhile selenium can
To further increase immune and anticancer function, enhance the immune and health-care efficacy of composition.
Second aspect, the present invention provide the preparation method of water shield health drink, include the following steps：
(1) under room temperature, the Aqueous extracts mixing of Aqueous extracts and arillus longan, jujube preparation prepared by water shield；
(2) selenium of formula ratio is added into step (1) gains, mixing adds water to formula volume, mixing, sterilizing, packaging
To obtain the final product.
In a specific embodiment, water shield health drink of the invention is prepared by following methods：
(1) it presses per Aqueous extracts, 0.1-10g arillus longans and the 0.1-10g prepared comprising 80-100g water shields in 1000mL beverages
Aqueous extracts, the 0-0.001g selenium of jujube, 0.1-20g food additives are prepared, surplus is the formula of purified water, weighs formula ratio
Water shield is cleaned, and the water of the weight such as addition keeps the temperature 1-60 minutes at 50-100 DEG C, filters, and obtains Aqueous extracts prepared by water shield；
(2) arillus longan and the jujube mixing for weighing formula ratio, are added the water 80-100 of 3-5 times of arillus longan and jujube total weight
1-60 minutes are kept the temperature at DEG C, is filtered, obtains arillus longan, Aqueous extracts prepared by jujube；
(3) water prepared by arillus longan, the jujube that the Aqueous extracts and step (2) that prepared by the water shield for obtaining step (1) obtain
Extract is uniformly mixed, and the selenium and food additives of formula ratio is added, mixing adds water to formula volume, again mixing, sterilizing, packet
It fills to obtain the final product.
In another specific embodiment, water shield health drink of the invention, is prepared by following methods：
(1) it presses per Aqueous extracts, 0.1-1g arillus longans and the 0.1-1g systems prepared comprising 80-90g water shields in 1000mL beverages
Aqueous extracts, the 0.00001-0.0001g selenium of standby jujube, 0.1-10g food additives, surplus are the formula of purified water, weigh and match
The water shield just measured is cleaned, and the water of the weight such as addition keeps the temperature 10-20 minutes at 80 DEG C, filters, and obtains water prepared by water shield and carries
Liquid；
(2) arillus longan and the jujube mixing for weighing formula ratio, are added the water 90-100 of 3-5 times of arillus longan and jujube total weight
20-30 minutes are kept the temperature at DEG C, is filtered, obtains arillus longan, Aqueous extracts prepared by jujube；
(3) water prepared by arillus longan, the jujube that the Aqueous extracts and step (2) that prepared by the water shield for obtaining step (1) obtain
Extract is uniformly mixed, and the selenium and food additives of formula ratio is added, mixing adds water to formula volume, again mixing, sterilizing, packet
It fills to obtain the final product.
Specific implementation mode
The influence that 1 different temperatures of embodiment extracts Polysaccharide of Brasenia Schreberi
The fresh water shields of 900g are cleaned, are divided into 9 parts, every part of 100g adds 100mL water (1:1), respectively 20 DEG C, 30 DEG C, 40
DEG C, 50 DEG C, 60 DEG C, 70 DEG C, 80 DEG C, 90 DEG C, heat preservation extraction 10 minutes at 100 DEG C, each population of samples accumulates constant volume to 200mL.
With glucose be control, using improvement phend-sulphuric acid measure polyoses content in solution (Wang Qian, the extraction of Polysaccharide of Brasenia Schreberi and its
The research of functional characteristic, Southern Yangtze University's master thesis, 2008), it the results are shown in Table 1.
Polysaccharide of Brasenia Schreberi extraction result (extraction 10 minutes) under table 1, different temperatures
| Temperature (DEG C) | 20 | 30 | 40 | 50 | 60 | 70 | 80 | 90 | 100 |
| Polyoses content (mg/mL) | 0.20 | 0.25 | 0.40 | 1.5 | 2.0 | 2.3 | 2.4 | 2.4 | 2.4 |
It can be seen that, with the increase of Extracting temperature, polyoses content increases in solution from table, to after 50 DEG C, solution
Middle polyoses content increases sharply, and to after 80 DEG C, the polyoses content in solution is not further added by, due to polysaccharide high temperature in aqueous solution
Under be easily decomposed to monosaccharide, lose its bioactivity, should not for a long time extract at high temperature, therefore, the extraction temperature of Polysaccharide of Brasenia Schreberi
Degree is 50 DEG C or more, and optimum temperature range is 80 DEG C.
The influence that the different extraction times of embodiment 2 extract Polysaccharide of Brasenia Schreberi
The fresh water shields of 800g are cleaned, are divided into 8 parts, every part of 100g adds 100mL water (1:1), at 80 DEG C heat preservation extraction 0,
1,10,20,30,40,50,60 minutes, each population of samples accumulated constant volume to 200mL.It is control with glucose, using improvement benzene
Phenol-sulfuric acid method measures polyoses content in solution, and (Wang Qian, the extraction of Polysaccharide of Brasenia Schreberi and its research of functional characteristic, Southern Yangtze University are large
Bachelorship paper, 2008), the results are shown in Table 2.
Table 2, Polysaccharide of Brasenia Schreberi extraction result (80 DEG C) under different extraction times
| Time (min) | 0 | 1 | 10 | 20 | 30 | 40 | 50 | 60 |
| Polyoses content (mg/mL) | 0.45 | 1.8 | 2.4 | 2.4 | 2.4 | 2.4 | 2.4 | 2.4 |
It can be seen that, as extraction time increases, polyoses content increases in solution from table, to after 20 minutes, solution
Middle polyoses content is not further added by.Due to unstable under polysaccharide in aqueous solution high temperature, it is easy to lose its bioactivity, therefore, water shield
The extraction time of dish polysaccharide is 10 minutes or more, preferably 10-20 minutes.
3 water shield health drink optimum proportioning of embodiment is studied
The fresh water shields of 10000g are cleaned, according to 1:1 weight ratio adds water, and 80 DEG C keep the temperature 20 minutes, and filtering obtains water shield
Extracting solution 200000mL (0.05g water shields/mL)；Arillus longan and each 200g of jujube add 1000mL water, 80 DEG C of 60 points of heat preservation extractions
Clock, filtering, obtains arillus longan, jujube Aqueous extracts 500mL (0.2g/mL)；Sodium selenate is formulated as the solution for standby of 1mg/mL.By water shield
Dish Aqueous extracts, longan aqueous extract, jujube Aqueous extracts are uniformly mixed according to the ratio of table 3, prepare different product；Concentration 100
Times, as zoopery raw material, the acute toxicity in relation to sample is detected according to National Standard Method (GB T 21826-2008), is as a result seen
Table 3.
Table 3, the variation of different ratio Product Safety
| Product identification | 1 | 2 | 3 | 4 | 5 | 6 | 7 | 8 | 9 |
| Water shield extracting solution (mL) | 20000 | 20000 | 20000 | 20000 | 20000 | 20000 | 20000 | 20000 | 20000 |
| Longan extracting solution (mL) | 0 | 5 | 50 | 500 | 0 | 0 | 0 | 50 | 50 |
| Hawthorn extract (mL) | 0 | 0 | 0 | 0 | 5 | 50 | 500 | 50 | 50 |
| Sodium selenate (mL) | 0 | 0 | 0 | 0 | 0 | 0 | 0 | 10 | 100 |
| LD50 (mL concentrates/Kg) | 50 | 250 | 890 | 910 | 230 | 850 | 890 | 920 | 920 |
It can see from table, the LD of water shield extracting solution50Smaller, after adding longan and hawthorn, safety improves rapidly,
When additive amount is more than after 1%, increased amplitude is smaller, and therefore, optimum addition is best with 1-10%.It is also seen that simultaneously
The effect of mixing addition is individually added better than longan and hawthorn.In addition, in the case where the additive amount of selenium is less than 0.01%, not shadow
Ring its safety.
4 water shield health drink healthcare function of embodiment is studied
The fresh water shields of 1000g are cleaned, according to 1:1 weight ratio adds water, and 80 DEG C keep the temperature 20 minutes, and filtering obtains water shield
Extracting solution 20000mL (0.05g/mL)；Arillus longan and each 100g of jujube add 500mL water, 80 DEG C of heat preservations to extract 60 minutes, filtering,
Obtain arillus longan, jujube Aqueous extracts 500mL (0.2g/mL)；Sodium selenate is formulated as the solution for standby of 1mg/mL.Water shield water is carried
Liquid, longan aqueous extract, jujube Aqueous extracts, selenic acid sodium solution are uniformly mixed according to different proportion, prepare different product；Concentration
100 times, as zoopery raw material, each Antitumor Activity of Drugs research of reference literature technique study, dosage concentrates for 5ml
Liquid/Kg weight, 30 days (Tao Huang, etc.Coptisine from Rhizoma Coptidis of successive administration
Suppresses HCT-116Cells-related Tumor Growth in vitro and in vivo.Scientific
Reports, 2017,7:38524|DOI:10.1038), it the results are shown in Table 4.
Table 4, different ratio product antitumor activity
| Product identification | 1 | 2 | 3 | 4 | 5 | 6 | 7 | 8 |
| Water shield extracting solution (mL) | 0 | 2000 | 2000 | 2000 | 2000 | 2000 | 2000 | 2000 |
| Longan extracting solution (mL) | 0 | 0 | 0.5 | 5 | 50 | 50 | 50 | 50 |
| Hawthorn extract (mL) | 0 | 0 | 0.5 | 5 | 50 | 50 | 50 | 50 |
| Sodium selenate (mL) | 0 | 0 | 0 | 0 | 0 | 0.1 | 1 | 10 |
| Gross tumor volume (mm3) | 1200 | 980 | 870 | 790 | 720 | 680 | 560 | 540 |
It can be seen that, water shield extracting solution also has the effect of certain pre- preventing tumor, after adding longan and hawthorn, resist from table
Tumor effect enhances, when additive amount is more than increasing degree reduction after 1%, optimum addition 1-10%；Add selenium element
Afterwards, antitumor activity further increases, and when selenium element additive amount is more than after 0.001%, increasing degree is little；Optimum addition
Preferably 0.001%.
The preparation of 5 water shield health drink of embodiment
Water shield 80g, arillus longan 0.1g, jujube 10g, Sucralose 0.1g.Preparation method is：Water shield is cleaned, according to 1:1
Weight ratio add water, 50 DEG C keep the temperature 60 minutes, and filtering obtains water shield Aqueous extracts；Arillus longan and jujube mixing, be added arillus longan and
The water that 3 times of jujube total weight, 80 DEG C keep the temperature 60 minutes, and filtering obtains arillus longan, jujube Aqueous extracts；By water shield Aqueous extracts and dragon
Eye meat, jujube Aqueous extracts are uniformly mixed, and Sucralose is added, and are uniformly mixed, and are added water to total volume to 1000mL, are sterilized, packaging
To obtain the final product.
The preparation of 6 water shield health drink of embodiment
Water shield 100g, longan 0.1g, jujube 0.1g, 100 μ g of selenium, honey element 0.5g.Preparation method is：Water shield clean,
According to 1:1 weight ratio adds water, and 1 minute is kept the temperature at 100 DEG C, and filtering obtains water shield Aqueous extracts；Arillus longan and jujube mixing, add
Enter the water of 5 times of arillus longan and jujube total weight, 100 DEG C keep the temperature 1 minute, and filtering obtains arillus longan, jujube Aqueous extracts；By water shield
Aqueous extracts and arillus longan, jujube Aqueous extracts are uniformly mixed, and selenium and honey element is added, is uniformly mixed, adds water to total volume extremely
1000mL, sterilizing, is packed to obtain the final product.
The preparation of 7 water shield health drink of embodiment
Water shield 90g, longan 10g, jujube 0.1g, white sugar 10g.Preparation method is：Water shield is cleaned, according to 1:1 weight
Than adding water, 80 DEG C keep the temperature 20 minutes, and filtering obtains water shield Aqueous extracts；Arillus longan and jujube mixing, are added arillus longan and jujube are total
The water that 4 times of weight, 90 DEG C keep the temperature 30 minutes, and filtering obtains arillus longan, jujube Aqueous extracts；By water shield Aqueous extracts and arillus longan, big
Jujube Aqueous extracts are uniformly mixed, and white sugar is added, and are uniformly mixed, and add water to total volume to 1000mL, sterilizing is packed to obtain the final product.
The preparation of 8 water shield health drink of embodiment
Water shield 90g, longan 5g, jujube 5g, xylitol 5g.Preparation method is：Water shield is cleaned, according to 1:1 weight ratio
Add water, 80 DEG C keep the temperature 20 minutes, and filtering obtains water shield Aqueous extracts；Arillus longan and jujube mixing, are added arillus longan and jujube gross weight
The water of 4 times of amount, 100 DEG C keep the temperature 30 minutes, and filtering obtains arillus longan, jujube Aqueous extracts；By water shield Aqueous extracts and arillus longan, big
Jujube Aqueous extracts are uniformly mixed, and xylitol is added, and are uniformly mixed, and add water to total volume to 1000mL, sterilizing is packed to obtain the final product.
The preparation of 9 water shield health drink of embodiment
Water shield 90g, longan 5g, jujube 5g, xylitol 5g.Preparation method is：Water shield is cleaned, according to 1:1 weight ratio
Add water, 80 DEG C keep the temperature 10 minutes, and filtering obtains water shield Aqueous extracts；Arillus longan and jujube mixing, are added arillus longan and jujube gross weight
The water of 4 times of amount, 90 DEG C keep the temperature 20 minutes, and filtering obtains arillus longan, jujube Aqueous extracts；By water shield Aqueous extracts and arillus longan, jujube
Aqueous extracts are uniformly mixed, and xylitol is added, and are uniformly mixed, and add water to total volume to 1000mL, sterilizing is packed to obtain the final product.
Comparative example 1 (201610456835.7 technology of patent document)
Fresh water shield 90g, is rinsed with clear water, and sorting cuts into uniform particle, 100 DEG C of -110 DEG C of high-temperature short-time sterilizations,
Sterilizing juice keeps the temperature 5-10 minutes at 75-85 DEG C, obtains water shield Normal juice 90mL.Add water to adjust total volume to 1000mL, sterilize,
It packs to obtain the final product.
Comparative example 2 (201510338836.7 technology of patent document)
Water shield 90g adds 1000mL water, is warming up to 100 DEG C of heat preservations and extracts 10 minutes, filtering obtains extracting solution；Extracting solution is used
0.5% activated carbon decolorizing removes the impurity such as tannin；After filtering, destainer is obtained, adds water to adjust total volume to 1000mL, sterilizes, packet
It fills to obtain the final product.
Comparative example 3 (201110138443.3 technology of patent document)
Water shield 90g finishes in 90~100 DEG C of blanchings, then smashs the water shield after water-removing to pieces mashing, water shield is obtained after filtering
Juice；Radix Astragali is made it is powdered, and by Milkvetch Root and water according to 1:It boils and filters after 25 mass ratio mixing, after filtering
To Sucus Astragali；By water shield juice and Sucus Astragali according to 1:1 mass ratio mixing adds water to adjust total volume to 1000mL, disappears through sterilization
It is filling after poison that beverage of water shield is made.
10 active constituent content of embodiment compares
It is control with glucose, using improvement phend-sulphuric acid, (Wang Qian, Polysaccharide of Brasenia Schreberi carry Polysaccharide of Brasenia Schreberi assay
It takes and its research of functional characteristic, Southern Yangtze University's master thesis, 2008).It the results are shown in Table 5.
Table 5, active constituent content
| Polyoses content (mg/mL) | |
| Comparative example 1 | 0.45 |
| Comparative example 2 | 0.32 |
Compared with comparative example 2, the polyoses content of comparative example 2 also significantly reduces comparative example 1, and mainly decoloration leads to polysaccharide
Loss is serious.
11 safety evaluatio of embodiment compares
Each 1000mL of products such as Example 9, comparative example 1, comparative example 2 and comparative example 3, is concentrated to 10mL, as experiment
Drug, every milliliter of concentrate contain 9 grams of water shields, and acute toxicity testing method is carried out according to National Standard Method (GB T 21826-2008),
LD50It is indicated with " g water shields/Kg weight ", the results are shown in Table 6.
The acute toxicity of table 6, article
| LD50(g/Kg) | |
| Embodiment 9 | 4500 |
| Comparative example 1 | 250 |
| Comparative example 2 | 3800 |
| Comparative example 3 | 230 |
As can be seen from Table 6, comparative example 1 (water shield directly processes obtained product), LD50 is smaller, there is higher poison
Property, LD50Similar with the result of document report (Gong Jiang etc., water shield study of pharmacy are summarized, Agriculture of Anhui science, and 2009,37
(10)：4489—4490).Water shield product (comparative example 2) after decoloration, safety increases substantially；Add Radix Astragali group
At compound, safety does not change, and is declined slightly (comparative example 3)；The LD of this product (embodiment 9)50It is very big, show it
Safety increases substantially, and is very safe product.
Claims (7)
1. a kind of water shield health drink includes often Aqueous extracts, 0.1-10g longans prepared by 80-100g water shields in 1000mL beverages
Aqueous extracts, 0-0.001g selenium prepared by meat and 0.1-10g jujubes, surplus is water.
2. water shield health drink according to claim 1, it is characterised in that：Also include food additives.
3. water shield health drink according to claim 2, it is characterised in that：The food additives be selected from sweetener,
It is one or more in preservative, flavorant；Preferably, the food additives are sweetener, sweetener choosing
From sucrose, white sugar, Sucralose and honey element.
4. water shield health drink according to claim 1, it is characterised in that：Aqueous extracts prepared by the water shield are will to be formulated
The water of the weight such as the fresh water shield use of amount keeps the temperature 1-60 minutes at 50-100 DEG C, filters the extracting solution of acquisition；Preferably, described
Water shield prepare Aqueous extracts be to clean the fresh water shield of formula ratio, with etc. weight water keep the temperature at 60-90 DEG C 10-30 divide
Clock filters the extracting solution of acquisition；It is further preferred that Aqueous extracts prepared by the water shield are to wash the fresh water shield of formula ratio
Only, with etc. the water of weight keep the temperature 10-20 minutes at 80 DEG C, filter the extracting solution of acquisition.
5. water shield health drink according to claim 1, it is characterised in that：Aqueous extracts prepared by the arillus longan and jujube
It is that 1-60 points of heat preservation at arillus longan and 80-100 DEG C of the water of 3-5 times of jujube total weight is added in the arillus longan of formula ratio and jujube
Clock filters the extracting solution of acquisition；Preferably, the Aqueous extracts that prepared by the arillus longan and jujube are by the arillus longan of formula ratio and big
Jujube is added at arillus longan and 90-100 DEG C of the water of 3-5 times of jujube total weight and keeps the temperature 10-30 minutes, filters the extracting solution of acquisition；Into
Preferably, Aqueous extracts prepared by the arillus longan and jujube are that arillus longan and big is added in the arillus longan of formula ratio and jujube to one step
20-30 minutes are kept the temperature at 90-100 DEG C of the water of 4-5 times of jujube total weight, filters the extracting solution of acquisition.
6. water shield health drink according to claim 1, it is characterised in that：The water is purified water.
7. the preparation method of claim 1-6 any one of them water shield health drinks, includes following steps：
(1) under room temperature, the Aqueous extracts mixing of Aqueous extracts and arillus longan, jujube preparation prepared by water shield；
(2) selenium of formula ratio is added into step (1) gains, mixing adds water to formula volume, and mixing, sterilizing, packaging are
?.
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| CN110892956A (en) * | 2019-10-17 | 2020-03-20 | 贵州理工学院 | Water shield health-care beverage and preparation method thereof |
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