CN108691032A - The preparation method of vinasse and shell charing powder composite fibre - Google Patents

The preparation method of vinasse and shell charing powder composite fibre Download PDF

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Publication number
CN108691032A
CN108691032A CN201710219523.9A CN201710219523A CN108691032A CN 108691032 A CN108691032 A CN 108691032A CN 201710219523 A CN201710219523 A CN 201710219523A CN 108691032 A CN108691032 A CN 108691032A
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China
Prior art keywords
raw material
charing
vinasse
shell
composite fibre
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CN201710219523.9A
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Chinese (zh)
Inventor
柯汉哲
柯宥成
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Individual
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Individual
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Priority to CN201710219523.9A priority Critical patent/CN108691032A/en
Publication of CN108691032A publication Critical patent/CN108691032A/en
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    • DTEXTILES; PAPER
    • D01NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
    • D01FCHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
    • D01F8/00Conjugated, i.e. bi- or multicomponent, artificial filaments or the like; Manufacture thereof
    • D01F8/04Conjugated, i.e. bi- or multicomponent, artificial filaments or the like; Manufacture thereof from synthetic polymers
    • D01F8/14Conjugated, i.e. bi- or multicomponent, artificial filaments or the like; Manufacture thereof from synthetic polymers with at least one polyester as constituent
    • DTEXTILES; PAPER
    • D01NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
    • D01FCHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
    • D01F8/00Conjugated, i.e. bi- or multicomponent, artificial filaments or the like; Manufacture thereof
    • D01F8/18Conjugated, i.e. bi- or multicomponent, artificial filaments or the like; Manufacture thereof from other substances
    • DTEXTILES; PAPER
    • D01NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
    • D01FCHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
    • D01F9/00Artificial filaments or the like of other substances; Manufacture thereof; Apparatus specially adapted for the manufacture of carbon filaments
    • D01F9/08Artificial filaments or the like of other substances; Manufacture thereof; Apparatus specially adapted for the manufacture of carbon filaments of inorganic material

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  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Textile Engineering (AREA)
  • Health & Medical Sciences (AREA)
  • Toxicology (AREA)
  • Reinforced Plastic Materials (AREA)

Abstract

A kind of preparation method of vinasse and shell charing powder composite fibre, comprises the steps of:Prepare charing vinasse raw material and charing shell raw material:One vinasse raw material is carbonized at a temperature of 800 DEG C to 1000 DEG C and a charing vinasse raw material is made, is carbonized at a temperature of 1000 DEG C to 1400 DEG C after a shell raw material is cleaned and a charing shell raw material is made;Prepare master batch:By the charing vinasse raw material and the charing shell raw material with 60~70:40~30 weight ratio is mixed into a mixed raw material, and after which is ground and polyester grain is with 10~16:Melt granulation becomes a master batch after 90~84 weight ratio mixing;Prepare mangcorn:By the master batch and polyester grain with 5~20:Melt granulation becomes a mangcorn after 95~80 weight ratio mixing;It reels off raw silk from cocoons:Mangcorn melting is reeled off raw silk from cocoons as a composite fibre.

Description

The preparation method of vinasse and shell charing powder composite fibre
Technical field
The present invention relates to a kind of preparation method of composite fibre, the system of especially a kind of vinasse and shell charing powder composite fibre Method.
Background technology
Polyester fiber is one of three big fibers, and intensity is good, retractility is big, Yi Gan, the advantages that being not easy to wrinkle are allowed to extensive Various fabrics are used in, it is also often blended with other plastic optical fibres, various function fabrics are made, purposes is very wide.
However, its moisture absorption still have with warming effect it is to be strengthened, and the shortcomings that easy to produce electrostatic and non-refractory, this Outside, polyester fiber is staple fibre, and the problem of having more not environmentally, therefore, still there are many improve when polyester fiber is on fabric Space.
Invention content
The object of the present invention is to provide the preparation method that a kind of vinasse and shell carbonize powder composite fibre, made compound fibres Dimension has many advantages, such as environmentally friendly, anti-oxidant, warming, antistatic.
To achieve the above object, the present invention takes following technical scheme:
The present invention provides a kind of preparation method of vinasse and shell charing powder composite fibre, comprises the steps of:
Prepare charing vinasse raw material and charing shell raw material:By a vinasse raw material at a temperature of 800 DEG C to 1000 DEG C into Row carbonizes and a charing vinasse raw material is made, and will be carbonized at a temperature of 1000 DEG C to 1400 DEG C after shell raw material cleaning And a charing shell raw material is made.
Prepare master batch:By the charing vinasse raw material and the charing shell raw material with 60~70:40~30 weight ratio mixing As a mixed raw material, after which is ground and polyester grain is with 10~16:It is melted after 90~84 weight ratio mixing Melt and is granulated into a master batch.
Prepare mangcorn:By the master batch and polyester grain with 5~20:Melt granulation becomes one after 95~80 weight ratio mixing Mangcorn.
It reels off raw silk from cocoons:Mangcorn melting is reeled off raw silk from cocoons as a composite fibre.
The present invention also provides a kind of preparation method of vinasse and shell charing powder composite fibre, comprises the steps of:
Prepare charing vinasse raw material and charing shell raw material:By a vinasse raw material at a temperature of 800 DEG C to 1000 DEG C into Row carbonizes and a charing vinasse raw material is made, and will be carbonized at a temperature of 1000 DEG C to 1400 DEG C after shell raw material cleaning And a charing shell raw material is made.
Prepare master batch:By the charing vinasse raw material and the charing shell raw material with 60~70:40~30 weight ratio mixing As a mixed raw material, after which is ground and polyester grain is with 10~16:It is melted after 90~84 weight ratio mixing Melt and is granulated into a master batch.
Mixed melting reels off raw silk from cocoons:By the master batch and polyester grain with 5~20:95~80 weight ratio is mixed and is reeled off raw silk from cocoons into after melting For a composite fibre.
In the step for preparing master batch, the mixed raw material is with the polyester grain with 16:84 weight ratio mixing.
The weight percent of mixed raw material described in the composite fibre is 0.8% to 2%.
The shell raw material includes the calcium carbonate of 90% or more weight percent.
The beneficial effects of the invention are as follows:Thereby, using the preparation method of the present invention, soft and tough, moisture absorption, antioxygen can be manufactured Change, warming and environmentally friendly composite fibre, can be suitably used for multiple use.
Description of the drawings
Fig. 1 and Fig. 2 is the flow chart of the present invention.
Drawing reference numeral:10:Vinasse raw material;10':Carbonize vinasse raw material;20:Shell raw material;20':Carbonize shell raw material; 30:Mixed raw material;40:Polyester grain;50:Master batch;60:Polyester grain;70:Mangcorn;80:Composite fibre.
Specific implementation mode
The possible state sample implementation of the present invention is only illustrated with embodiment below, so not to be protected to limit the present invention Scope, conjunction are first chatted bright.
Referring to FIG. 1, the present invention provides a kind of preparation method of vinasse and shell charing powder composite fibre, including following step Suddenly:
Prepare charing vinasse raw material and charing shell raw material:By a vinasse raw material 10 at a temperature of 800 DEG C to 1000 DEG C It is carbonized and a charing vinasse raw material 10 ' is made, after a shell raw material 20 is cleaned at a temperature of 1000 DEG C to 1400 DEG C Carbonized and a charing shell raw material 20 ' be made, wherein preferably, the shell raw material 20 include weight percent 90% with On calcium carbonate, oyster shell, CONCHA MERETRICID SEU CYCLINAE etc. can be selected.
Prepare master batch:By the charing vinasse raw material 10 ' and the charing shell raw material 20 ' with 60~70:40~30 weight Than being mixed into a mixed raw material 30, after which is ground and polyester grain 40 is with 10~16:90~84 weight Amount becomes a master batch 50 than melt granulation after mixing, preferably, the mixed raw material 30 is with polyester grain 40 with 16:84 weight ratio is mixed It closes.
Prepare mangcorn:By the master batch 50 and polyester grain 60 with 5~20:95~80 weight ratio mixing after melt granulation at For a mangcorn 70, preferably, the weight percent of the mixed raw material 30 is 0.8% to 2% in the mangcorn 70.
It reels off raw silk from cocoons:The mangcorn 70 melting is reeled off raw silk from cocoons as a composite fibre 80.
Referring to FIG. 2, the present invention also provides the preparation method of another vinasse and shell charing powder composite fibre, including following Step:
Prepare charing vinasse raw material and charing shell raw material:By a vinasse raw material 10 at a temperature of 800 DEG C to 1000 DEG C It is carbonized and a charing vinasse raw material 10 ' is made, after a shell raw material 20 is cleaned at a temperature of 1000 DEG C to 1400 DEG C Carbonized and a charing shell raw material 20 ' be made, wherein preferably, the shell raw material 20 include weight percent 90% with On calcium carbonate.
Prepare master batch:By the charing vinasse raw material 10 ' and the charing shell raw material 20 ' with 60~70:40~30 weight Than being mixed into a mixed raw material 30, after which is ground and polyester grain 40 is with 10~16:90~84 weight Amount becomes a master batch 50 than melt granulation after mixing, preferably, the mixed raw material 30 and polyester grain 40 are with 16:84 weight ratio is mixed It closes.
Mixed melting reels off raw silk from cocoons:By the master batch 50 and polyester grain 60 with 5~20:95~80 weight ratio is mixed and is taken out after melting Silk becomes a composite fibre 80, preferably, the weight percent of the mixed raw material 30 is 0.8% to 2% in the composite fibre 80.
That is, the master batch and polyester grain can first melt granulation stored as mangcorn, remelted pumping when needing Silk becomes composite fibre, also can directly reel off raw silk from cocoons after melting as composite fibre without mangcorn is made.
By above-mentioned preparation method, the present invention can produce performance better than simple using discarded vinasse and shell as raw material The composite fibre of polyester fiber, has many advantages, such as smelly eliminating, antibacterial, moisture absorption, anti-oxidant, warming, but with good intensity with Degree of drawing, is applicable to multiple use, it is great progressive the benefits of.

Claims (8)

1. the preparation method of a kind of vinasse and shell charing powder composite fibre, which is characterized in that it includes the following steps:
Prepare charing vinasse raw material and charing shell raw material:One vinasse raw material is subjected to charcoal at a temperature of 800 DEG C to 1000 DEG C Change and a charing vinasse raw material is made, carbonized at a temperature of 1000 DEG C to 1400 DEG C after a shell raw material is cleaned and is made Obtain a charing shell raw material;
Prepare master batch:By the charing vinasse raw material and the charing shell raw material with 60~70:40~30 weight ratio is mixed into One mixed raw material, after which is ground and polyester grain is with 10~16:System is melted after 90~84 weight ratio mixing Grain becomes a master batch;
Prepare mangcorn:By the master batch and polyester grain with 5~20:Melt granulation becomes a mixing after 95~80 weight ratio mixing Grain;
It reels off raw silk from cocoons:Mangcorn melting is reeled off raw silk from cocoons as a composite fibre.
2. the preparation method of vinasse as described in claim 1 and shell charing powder composite fibre, which is characterized in that preparing master batch Step when, the mixed raw material and the polyester grain are with 16:84 weight ratio mixing.
3. the preparation method of vinasse as described in claim 1 and shell charing powder composite fibre, which is characterized in that the mangcorn Described in mixed raw material weight percent be 0.8% to 2%.
4. the preparation method of vinasse as described in claim 1 and shell charing powder composite fibre, which is characterized in that the shell is former Material includes the calcium carbonate of 90% or more weight percent.
5. the preparation method of a kind of vinasse and shell charing powder composite fibre, which is characterized in that it includes the following steps:
Prepare charing vinasse raw material and charing shell raw material:One vinasse raw material is subjected to charcoal at a temperature of 800 DEG C to 1000 DEG C Change and a charing vinasse raw material is made, carbonized at a temperature of 1000 DEG C to 1400 DEG C after a shell raw material is cleaned and is made Obtain a charing shell raw material;
Prepare master batch:By the charing vinasse raw material and the charing shell raw material with 60~70:40~30 weight ratio is mixed into One mixed raw material, after which is ground and polyester grain is with 10~16:System is melted after 90~84 weight ratio mixing Grain becomes a master batch;
Mixed melting reels off raw silk from cocoons:By the master batch and polyester grain with 5~20:95~80 weight ratio is mixed and is reeled off raw silk from cocoons as one after melting Composite fibre.
6. the preparation method of vinasse as claimed in claim 5 and shell charing powder composite fibre, which is characterized in that preparing master batch Step when, the mixed raw material and the polyester grain are with 16:84 weight ratio mixing.
7. the preparation method of vinasse as claimed in claim 5 and shell charing powder composite fibre, which is characterized in that the compound fibre The weight percent of mixed raw material described in dimension is 0.8% to 2%.
8. the preparation method of vinasse as claimed in claim 5 and shell charing powder composite fibre, which is characterized in that the shell is former Material includes the calcium carbonate of 90% or more weight percent.
CN201710219523.9A 2017-04-06 2017-04-06 The preparation method of vinasse and shell charing powder composite fibre Pending CN108691032A (en)

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CN201710219523.9A CN108691032A (en) 2017-04-06 2017-04-06 The preparation method of vinasse and shell charing powder composite fibre

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Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102534848A (en) * 2010-12-21 2012-07-04 上海德福伦化纤有限公司 Production method of coffee polyester multifunctional fiber
CN104988597A (en) * 2015-07-17 2015-10-21 安徽月娇家具有限公司 Health mattress fabric capable of alleviating fatigue and improving sleep quality, and making method thereof
CN105970337A (en) * 2016-05-16 2016-09-28 长兴华海纺织有限公司 Preparation method of environment-friendly antibacterial polyester fiber
CN105986335A (en) * 2015-03-05 2016-10-05 王叶训 Seawool
TWI561692B (en) * 2016-02-18 2016-12-11 Han-Che Ke Method To Manufacture Composite Fibers Of Rice Husk And Charcoal
CN106350895A (en) * 2016-08-31 2017-01-25 浙江全美实业有限公司 Preparation method of multifunctional polyester fiber

Patent Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102534848A (en) * 2010-12-21 2012-07-04 上海德福伦化纤有限公司 Production method of coffee polyester multifunctional fiber
CN105986335A (en) * 2015-03-05 2016-10-05 王叶训 Seawool
CN104988597A (en) * 2015-07-17 2015-10-21 安徽月娇家具有限公司 Health mattress fabric capable of alleviating fatigue and improving sleep quality, and making method thereof
TWI561692B (en) * 2016-02-18 2016-12-11 Han-Che Ke Method To Manufacture Composite Fibers Of Rice Husk And Charcoal
CN105970337A (en) * 2016-05-16 2016-09-28 长兴华海纺织有限公司 Preparation method of environment-friendly antibacterial polyester fiber
CN106350895A (en) * 2016-08-31 2017-01-25 浙江全美实业有限公司 Preparation method of multifunctional polyester fiber

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* Cited by examiner, † Cited by third party
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邹礼根等: "《农产品加工副产物综合利用技术》", 31 March 2013, 浙江大学出版社 *

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Application publication date: 20181023