A kind of moisturizing, whitening, light spot composition of plant extracts
Technical field
The present invention relates to daily chemicals field, more specifically a kind of moisturizing, whitening, light spot composition of plant extracts.
Background technology
With the development of society, people more focus on U.S.A, many people promote U.S. of appearance by various beauty products
Sense, in addition, containing there are many dust, impurity in air, if not paying attention to nursing, if things go on like this, people will appear on the face pore it is coarse,
The problems such as colour of skin obscure, dry, long spot.
Hyaluronic acid, also referred to as sodium hyaluronate are a kind of acid mucopolysaccharides, have humectant, viscoplasticity and biocompatibility
Etc. characteristics.Hyaluronic acid is mainly present in the form of gluey in the dermal tissue of human skin, is responsible for storage moisture, is increased skin
Volume allows skin to seem full, plentiful, flexible.Young infant skin comparable to Hard boiled eggs, sodium hyaluronate content with regard to high, with
The growth at people's age, sodium hyaluronate, which is lost in, to be accelerated, and 30 years old when is only left the brephic 65%, and 60 years old when is only left 25%.It is adjoint
The loss of hyaluronic acid, a series of skin problem can be caused.
Therefore, many people achieve the effect that replenishing water and preserving moisture by using the product containing hyaluronic acid, however, for people
Face, although what hyaluronic acid can be quickly is absorbed by skin corium, at cuticula be easy to be lost in, listed about
The product effect of hyaluronic acid is not very good.In addition, periocualr skin compared to the skin in other regions for, only 1/5 thickness,
Therefore periocualr skin also becomes the position of most sensitive most easy aging, has the periocualr skin meeting pigment accumulation of many women, is formed
Spot may cause eye hair week angling, there are no commercialized products at this stage due to improper use or the wrong skin care item of choosing
Eye hair week angling and eye spot can be solved the problems, such as simultaneously, therefore there is an urgent need for a kind of novel product is developed, not only
Can moisturizing, whitening, it is anti-oxidant, additionally it is possible to effective desalination eye circumference spot, eye hair week angling of releiving.
Invention content
To solve the above-mentioned problems, the first aspect of the present invention provides a kind of moisturizing, whitening, light spot plant extracts group
Object is closed, including following components:Oil phase part, aqueous portion, emulsifier and preservative.
As a kind of perferred technical scheme, the oil phase part, in parts by weight, including 5-10 parts of saualane, anti-
5-10 parts of oxidized extract, 2-3 parts of Ascorbyl Tetraisopalmitate;The aqueous portion, in parts by weight, including glycerine
5-8 parts, 2.5-5 parts of grape seed extract, 2.5-5 parts of lactobacillus fermentation product, 2-3 parts of black truffle extract, licorice
10-50 parts of 2-4 parts of extract, 5-10 parts of hyaluronic acid, 1-2 parts of dried tremella extract and deionized water.
As a kind of perferred technical scheme, the oil phase part also includes in parts by weight dimethicone 2-4
Part, 1-3 parts of camellia oil, 1-2 parts of butter berry extract, 1-2 parts of carbomer and 1-2 parts of Sweet Almond Oil;The aqueous portion, according to
Parts by weight meter also includes 2-4 parts of aloe vera extract, 1-2 parts of mulberry bark extract, 2-3 parts of Radix Paeoniae Alba medicament extract, race
1-2 parts of extract, 1-2 parts of Fructus Cucumidis sativi extract, 1-2 parts of Folium Artemisiae Argyi extract, 2-3 parts of wolfberry fruit extract, Leonurus extract 1-2
Part, 2-3 parts of Flos Rosae Rugosae extract, 2-3 parts of peony root extractive, 2-4 parts of green-tea extract, 2-4 parts of extract of Trichosanthes, lactic acid
- 1.5 parts of 1-2 parts of sodium and Cer EOS.
As a kind of perferred technical scheme, the antioxidant extract, lactobacillus fermentation product and grape pip extraction
The weight proportion of object is 2:1:1.
As a kind of perferred technical scheme, the weight proportion of the hyaluronic acid and saualane is 1:1, licorice extraction
The weight proportion of object and black truffle extract is 1:2.5.
As a kind of perferred technical scheme, the antioxidant extract is raspberry leaf, granatum and gallic mixed
Close extract.
To solve the above-mentioned problems, the second aspect of the invention provides a kind of extraction process of antioxidant extract.
As a kind of perferred technical scheme, the preparation method of the antioxidant extract is as follows:
S1:Raspberry leaf, granatum and Chinese gall are weighed, air-dries, pulverizes, it is spare to cross 60 mesh sieve;
S2:Mixture is weighed in round-bottomed flask, the diluted ethyl alcohol of use deionized water that a concentration of 15-25wt% is added is molten
Liquid, the weight proportion for controlling mixture and ethanol solution is 1:12-15 starts after having extracting solution to generate 10min with per second 1
Control, extraction time 60-80min, extraction temperature is hydrolyzed in the dilute hydrochloric acid that 3-3.5wt% is added dropwise into extracting solution for the speed of drop
Degree is 85-95 DEG C;
S3:To the end of reflux course, stop that dilute hydrochloric acid is added dropwise, filter extracting solution while hot, residue is cleaned twice with ethyl alcohol, closed
And filtrate and cleaning solution;
S4:Decompression filters, and is preserved at shady and cool ventilation.
To solve the above-mentioned problems, the third aspect of the present invention provides a kind of moisturizing, whitening, light spot plant extracts group
Close the preparation method of object.
As a kind of perferred technical scheme, preparation method is as follows:
A1:The preparation of oil phase part
By the dimethicone of formula ratio, saualane, antioxidant extract, camellia oil, butter berry extract, carbomer,
Oil cauldron is added after weighing in Sweet Almond Oil, continues to be heated to 60-70 DEG C, and constant temperature disinfection under the stirring of 10-20 revs/min of rotating speed
Ascorbyl Tetraisopalmitate is added before emulsifying in 20-30min, stirs evenly, for use;
A2:The preparation of aqueous portion
By the glycerine of formula ratio, grape seed extract, aloe vera extract, mulberry bark extract, RADIX PAEONIAE ALBA extraction
Object, ginger-root extract, Fructus Cucumidis sativi extract, Folium Artemisiae Argyi extract, wolfberry fruit extract, licorice root extract, Leonurus extract, rose
Flower extract, peony root extractive, green-tea extract, extract of Trichosanthes, lactobacillus fermentation product, black truffle extraction
Newborn pot is added in object, sodium lactate, hyaluronic acid, ceramide, dried tremella extract after weighing, be added thereto formula ratio go from
Sub- water continues to be heated to 60-70 DEG C, and constant temperature 20-30min under the rotating speed of 10-20 revs/min of rotating speed;
A3:Newborn pot oil phase part being slowly added into where aqueous portion, and scrape wall stirring, rotating speed increase to 30-35 turn/
Point, 5-10min is stirred, until oil phase is uniformly mixed with water phase, reduction of speed is dropped to 20-30 revs/min in keeping rotation process later
Temperature waits for that temperature drops to 35 DEG C, and the emulsifier and preservative of formula ratio are added thereto, under the speed for being kept for 10-20 revs/min
Continue to stir 20-30min, you can discharging.
As a kind of perferred technical scheme, the emulsifier, in parts by weight, including stearine and/or
0.3-0.5 parts of polyethylene glycol stearate.
As a kind of perferred technical scheme, the preservative is in parts by weight salicylic acid preservative 0.1-
0.2 part.
As a kind of perferred technical scheme, a kind of moisturizing, whitening, light spot composition of plant extracts are applied to
In eye hair week angling of releiving and the cosmetics for desalinating eye circumference spot.
The beneficial effects of the invention are as follows:
1) the present invention provides a kind of moisturizing, whitening, light spot composition of plant extracts, moisturizing, whitening, light can be reached
Spot, the effect for desalinating acne print;
2) present invention is using antioxidant extract, lactobacillus fermentation product, licorice root extract, grape seed extract group
It closes, realizes the effect of high-efficiency antioxidant, Whitening, spot, can effectively desalinate the spot of periocualr skin, eye of effectively releiving
The all angling of hair, new acne of effectively releiving;
3) present invention employs saualane, hyaluronic acid and black truffle extract, can achieve the effect that high moisturizing,
Also the moisturizing of 8 hours can be kept in subzero 15 DEG C of environment;
4) present invention can achieve the effect that antiallergic using licorice root extract, saualane and black truffle extract, i.e.,
Make to be small pox flesh skin, can also use.
5) for the present invention by being combined antioxidant extract with grape seed extract, physicochemical property is good.
Specific implementation mode
To solve the above-mentioned problems, the first aspect of the present invention provides a kind of moisturizing, whitening, light spot plant extracts group
Object is closed, including following components:Oil phase part, aqueous portion, emulsifier and preservative composition.
In some specific embodiments, the oil phase part, in parts by weight, including 5-10 parts of saualane, anti-
2-3 parts of 5-10 parts of oxidized extract and Ascorbyl Tetraisopalmitate;The aqueous portion, in parts by weight, including sweet
5-8 parts oily, 2.5-5 parts of grape seed extract, 2.5-5 parts of lactobacillus fermentation product, 2-3 parts of black truffle extract, Radix Glycyrrhizae
10-50 parts of 2-4 parts of root extract, 5-10 parts of hyaluronic acid, 1-2 parts of dried tremella extract and deionized water.
Preferably, the oil phase part, in parts by weight, including 6-9 parts of saualane, 6-9 parts of antioxidant extract and
2.2-2.8 parts of Ascorbyl Tetraisopalmitate;The aqueous portion, in parts by weight, including 6-7 parts of glycerine, grape pip
3-4.5 parts of extract, 3-4.5 parts of lactobacillus fermentation product, 2.3-2.7 parts of black truffle extract, licorice root extract
30-45 parts of 2.2-3.8 parts, 6-9 parts of hyaluronic acid, 1.3-1.7 parts of dried tremella extract and deionized water.
It is further preferred that the oil phase part, in parts by weight, including 6.5-8.5 parts of saualane, anti-oxidant extraction
2.4-2.6 parts of 6-8 parts of object and Ascorbyl Tetraisopalmitate;The aqueous portion, in parts by weight, including glycerine 6.2-
6.8 parts, 3.2-3.8 parts of grape seed extract, 3.2-4.2 parts of lactobacillus fermentation product, black truffle extract 2.4-2.6
Part, 2.5-3.5 parts of licorice root extract, 6.5-8.5 parts of hyaluronic acid, 1.4-1.6 parts of dried tremella extract and deionized water 35-45
Part.
Still more preferably, the oil phase part, in parts by weight, including 7.5 parts of saualane, antioxidant extract
7 parts and 2.5 parts of Ascorbyl Tetraisopalmitate;The aqueous portion, in parts by weight, including 6.4 parts of glycerine, grape pip
3.5 parts of extract, 3.5 parts of lactobacillus fermentation product, 2.5 parts of black truffle extract, 3 parts of licorice root extract, hyalomitome
40 parts of 7.5 parts of acid, 1.5 parts of dried tremella extract and deionized water.
In some specific embodiments, the oil phase part also includes in parts by weight dimethicone 2-4
Part, 1-3 parts of camellia oil, 1-2 parts of butter berry extract, 1-2 parts of carbomer and 1-2 parts of Sweet Almond Oil;The aqueous portion, according to
Parts by weight meter also includes 2-4 parts of aloe vera extract, 1-2 parts of mulberry bark extract, 2-3 parts of Radix Paeoniae Alba medicament extract, race
1-2 parts of extract, 1-2 parts of Fructus Cucumidis sativi extract, 1-2 parts of Folium Artemisiae Argyi extract, 2-3 parts of wolfberry fruit extract, Leonurus extract 1-2
Part, 2-3 parts of Flos Rosae Rugosae extract, 2-3 parts of peony root extractive, 2-4 parts of green-tea extract, 2-4 parts of extract of Trichosanthes, lactic acid
- 1.5 parts of 1-2 parts of sodium and Cer EOS.
Preferably, the oil phase part also includes in parts by weight 2.2-3.8 parts of dimethicone, camellia oil 1.5-
1.3-1.7 parts of 2.5 parts, 1.2-1.8 parts of butter berry extract, 1.2-1.8 parts of carbomer and Sweet Almond Oil;The aqueous portion,
In parts by weight, also include 2.2-3.8 parts of aloe vera extract, 1.2-1.8 parts of mulberry bark extract, RADIX PAEONIAE ALBA extraction
2.2-2.8 parts of object, 1.3-1.7 parts of ginger-root extract, 1.2-1.8 parts of Fructus Cucumidis sativi extract, 1.3-1.7 parts of Folium Artemisiae Argyi extract, matrimony vine
2.2-2.8 parts of extract, 1.3-1.7 parts of Leonurus extract, 2.3-2.7 parts of Flos Rosae Rugosae extract, peony root extractive 2.2-
2.8 parts, 2.3-2.7 parts of green-tea extract, 2.3-2.7 parts of extract of Trichosanthes, 1.3-1.7 parts of sodium lactate and Cer EOS .1-
1.4 part.
It is further preferred that the oil phase part also includes in parts by weight 2.8-3.2 parts of dimethicone, camellia
1.4-1.6 parts of 1.8-2.2 parts oily, 1.4-1.6 parts of butter berry extract, 1.4-1.6 parts of carbomer and Sweet Almond Oil;The water phase
Part also includes in parts by weight 2.8-3.2 parts of aloe vera extract, 1.4-1.6 parts of mulberry bark extract, Radix Paeoniae Alba
2.2-2.8 parts of medicament extract, 1.3-1.7 parts of ginger-root extract, 1.2-1.8 parts of Fructus Cucumidis sativi extract, Folium Artemisiae Argyi extract 1.3-1.7
Part, the extraction of 2.2-2.6 parts of wolfberry fruit extract, 1.5-1.7 parts of Leonurus extract, 2.5-2.7 parts of Flos Rosae Rugosae extract, tree peony root
2.6-2.8 parts of object, 2.5-2.7 parts of green-tea extract, 2.4-2.6 parts of extract of Trichosanthes, 1.5-1.7 parts of sodium lactate and neural acyl
1.1-1.3 parts of amine.
Still more preferably, the oil phase part also includes in parts by weight 3 parts of dimethicone, camellia oil 2
Part, 1.5 parts of butter berry extract, 1.5 parts of carbomer and 1.5 parts of Sweet Almond Oil;The aqueous portion, in parts by weight, also
Including 3 parts of aloe vera extract, 1.5 parts of mulberry bark extract, 2.5 parts of Radix Paeoniae Alba medicament extract, 1.5 parts of ginger-root extract,
1.4 parts of Fructus Cucumidis sativi extract, 1.5 parts of Folium Artemisiae Argyi extract, 2.4 parts of wolfberry fruit extract, 1.6 parts of Leonurus extract, rose extraction
2.6 parts of object, 2.7 parts of peony root extractive, 2.6 parts of green-tea extract, 2.5 parts of extract of Trichosanthes, 1.6 parts of sodium lactate and nerve
1.2 parts of amide.
In some specific embodiments, the antioxidant extract, lactobacillus fermentation product and grape pip extraction
The weight proportion of object is 2:1:1.
In some specific embodiments, the weight proportion of the hyaluronic acid and saualane is 1:1, licorice extraction
The weight proportion of object and black truffle extract is 1:2.5.
In some specific embodiments, the antioxidant extract is raspberry leaf, granatum and gallic mixed
Close extract.In some preferred embodiments, raspberry leaf, granatum and gallic weight are 2:1:1.
The present invention contains a large amount of component, and each component is described below:
Saualane:Saualane is the hydrogenated obtained a kind of hydrocarbon haveing excellent performance of squalene extracted from hydrogenated hydro carbons grease
Quasi-grease, it is also known as eepwater shark liver oils.No. CAS:111-01-3.
Antioxidant extract:Heretofore described antioxidant extract is raspberry leaf, granatum and gallic mixed
Close extract.Raspberry (Rubus idaeus L);Pomegranate (Punica granatum L);Chinese gall:This product is planted for Anacardiaceae
Object Chinese sumac Rhus chinensis Mill., potanin sumac Rhus potaninii Maxim. or redpunjab sumac root Rhus pun-
Insect gall on jabensis Stew.var.sinica (Diels) Rehd.et Wils. leaves, mainly by melaphis chinensis Baker Melaphis
Chinensis (Bell) Baker is parasitic and is formed.Matrimony vine:This product is in class spindle or ellipse, long 6~20mm, and diameter 3~
10mm.Surface is red or kermesinus, top have the stylar scar of small convex, base portion to have the carpopodium trace of white.Pericarp is flexible, wrinkle
Contracting;Pulp meat, it is soft and moist.20~50, seed, class kidney shape is flat and stick up, long 1.5~1.9mm, wide 1~1.7mm, and surface is pale yellow
Color or brown color.Gas is micro-, sweet.
Ascorbyl Tetraisopalmitate:Ascorbyl palmitate is the natural components ester such as palmitic acid and L-AA
Change, molecular formula C22H38O7, it is a kind of efficient oxygen scavenger and synergist is that China uniquely can be used for infant's food
The antioxidant of product, this product can play anti-oxidant, food color protection, fortification and other effects for food.No. CAS:183476-
82-6。
Glycerine:It is typically used for moisturizing.No. CAS:56-81-5.
Grape seed extract:Grape seed extract is that a kind of polyphenols being separated to is extracted from grape pip, is resisted
Oxidation effectiveness is 30~50 times of vitamin C and vitamin E, and procyanidine has extremely strong activity, can inhibit the cause in cigarette
Cancer object is 2~7 times of general antioxidant to the capturing ability of free radical in water phase, such as higher by two than the activity of alpha-tocopherol
Times or more.No. CAS:84929-27-1.
Lactobacillus fermentation product:Lactobacillus fermentation product is metabolized through Bifidobacterium culture, inactivation and decomposition
Product, cytoplasmic fragment, cell-wall components and polysaccharide composite body.No. CAS:96507-89-0.
Black truffle extract:Protein and carbohydrate are very high, are a kind of substances of very moisturizing, contain mine simultaneously
Substance and trace element have the effect of good antiallergy and adjust sebum secretion.No. CAS:85085-76-3.
Licorice root extract:Licorice root extract has the effect of preferable skin whitening.No. CAS:97676-23-8.
Hyaluronic acid:D-Glucose aldehydic acid and N-acetyl-glucosamine composition dissacharide units sodium hyaluronate, also known as uronic acid, thoroughly
Bright matter acid, the large-scale polysaccharide that basic structure is made of two dissacharide units D-Glucose aldehydic acid and N-acetyl-glucosamine.CAS
Number:9004-61-9.
Dimethicone:With good skin-protecting function, belong to the Synthetic Oil in cosmetic material.This product is nontoxic, right
Skin and mucous membrane are nonirritant.No. CAS:8050-81-5.
Camellia oil:After tested:Unsaturated fatty acid is up to 90% or more in tea oil, and oleic acid reaches 80-83%, and linoleic acid reaches
To 7-13%, and it is rich in protein and vitamin A, B, D, E etc..No. CAS:68916-73-4.
Butter berry extract:The skin-friendly of butter berry extract and human skin is good, is easily absorbed.It buys from Xi'an Tianrui
Bio tech ltd.
Carbomer:Carbomer is the acrylic acid crosslinked resin being crosslinked with acrylic acid with pentaerythrite etc., is a kind of non-
Often important rheology control agent, the carbomer after neutralization are outstanding gel-type vehicles, there is the important uses such as thickening, suspension, technique
Simply, stability is good, is widely used in lotion, cream, gel.No. CAS:9007-17-4.
Sweet Almond Oil:There is good skin-friendly, even most delicate baby can also use.And contain the spy of high nutrition element
Matter is good moist and miscella.It is suitble to baby, dryness, wrinkle, acne and sensibility skin to use.No. CAS:8007-
69-0。
Aloe vera extract:Aloe polysaccharide and vitamin have good nutrition to the skin of human body, moisten, brighten work
With.And blandness, it is comfortable after, there is certain curative effect to pachylosis, facial wrinkles, scar, freckle, acne etc..CAS
Number:85507-69-3.
Mulberry bark extract:Mulberry bark extract cures mainly removing heat from lung and relieving asthma, inducing diuresis for removing edema.For dyspnea and cough due to lung-heat, oedema turgor
Oliguria, appearance skin edema.It buys from Hubei ferry-boat Chemical Co., Ltd..
Radix Paeoniae Alba medicament extract:With anti-inflammatory, analgesia, immunoregulation effect.No. CAS:23180-57-6.
Ginger-root extract:Race has antibacterial, antiinflammation, also has very strong oxidation resistance.No. CAS:
84696-15-1。
Fructus Cucumidis sativi extract:Fructus Cucumidis sativi extract, which has, releives, calm effect, moisturizing and Bearberry Extract.No. CAS:89998-
01-6。
Folium Artemisiae Argyi extract:Eliminating cold to stop pain, warming channel for arresting bleeding.Control pruitus outside.No. CAS:94-24-6.
Wolfberry fruit extract:Polysaccharides in matrimony vine is its important effective ingredient, and polysaccharides (LBP) is containing trace element
And amino acid, it is made of six kinds of monosaccharide.Immune, antitumor, reducing blood lipid, antithrombotic, anti-aging and other effects with enhancing.CAS
Number:107-43-7.
Leonurus extract:Motherwort contains various trace elements.Selenium has enhancing immunocyte vigor, mitigates artery congee
The generation of sample hardening and the effect for improving human body defence function of diseases system;Manganese can be anti-oxidant, anti-aging, antifatigue and be inhibited
The hyperplasia of cancer cell.No. CAS:4136-37-2.
Flos Rosae Rugosae extract:Property is mild, can chill out, balances endocrine, replenishing blood and vital energy, U.S. face skin care, to liver and stomach
Play the role of conditioning and can dispelling fatigue, improve constitution, moisten beauty treatment, improve looks, liver and stomach nourishing the liver are protected in promoting blood circulation,
Dispelling fatigue, the function of promoting blood circulation.No. CAS:8007-01-0.
Peony root extractive:The root skin of tree peony, the referred to as root bark of tree peony, the medicinal ingredient containing there are many, and contain volatility and plant steroid
Alcohol etc..It buys from the Wuhan bio tech ltd Hong Heshan.
Green-tea extract:Green-tea extract is the active constituent extracted from green tea blade, includes mainly tea polyphenols, coffee
Alkali, aromatic oil, moisture, minerals, pigment, carbohydrate, protein, amino acid, vitamin etc..No. CAS:154-23-4.
Extract of Trichosanthes:Extract of Trichosanthes has the function of clearing heat and detoxicating.It buys from Shaanxi Si Nuote biotechnologies
Co., Ltd.
Sodium lactate:Lactic acid and lactate are the natural constituents of human skin and hair, have unique pH adjustings and moisturizing
Function is widely used in a variety of daily chemical products, as bath product, skin nursing products, hair care product and oral cavity are protected
Manage product etc..No. CAS:72-17-3.
Ceramide:Ceramide forms sphingoin matter one kind by sphingosine long chain base and aliphatic acid.
40%~50% sebum is made of ceramide in cuticula, and ceramide is the major part of intercellular matrix, is being kept
It plays an important role in the balance of cuticula moisture.No. CAS:100403-19-8.
Deionized water:No. CAS:2189-80-2.
To solve the above-mentioned problems, the second aspect of the invention provides a kind of extraction process of antioxidant extract.
In a particular embodiment, the extraction process of the antioxidant extract is as follows:
S1:Raspberry leaf, granatum and Chinese gall are weighed, air-dries, pulverizes, it is spare to cross 60 mesh sieve;
S2:Mixture is weighed in round-bottomed flask, the diluted ethyl alcohol of use deionized water that a concentration of 15-25wt% is added is molten
Liquid, the weight proportion for controlling mixture and ethanol solution is 1:12-15, when have extracting solution generate 10min after, start slowly with
The dilute hydrochloric acid that 3-3.5wt% is added dropwise into extracting solution for the speed of 1 drop per second is hydrolyzed, and control extraction time is 60-80min,
Extracting temperature is 85-95 DEG C;
S3:To the end of reflux course, stop that dilute hydrochloric acid is added dropwise, filter extracting solution while hot, residue is cleaned twice with ethyl alcohol, closed
And filtrate and cleaning solution;
S4:Decompression filters, and is preserved at shady and cool ventilation.
Preferably, the extraction process of the antioxidant extract is as follows:
S1:Raspberry leaf, granatum and Chinese gall are weighed, air-dries, pulverizes, it is spare to cross 60 mesh sieve;
S2:Mixture is weighed in round-bottomed flask, the diluted ethyl alcohol of use deionized water that a concentration of 18-22wt% is added is molten
Liquid, the weight proportion for controlling mixture and ethanol solution is 1:12-14, when have extracting solution generate 10min after, start slowly with
The dilute hydrochloric acid that 3.1-3.4wt% is added dropwise into extracting solution for the speed of 1 drop per second is hydrolyzed, and control extraction time is 65-
75min, Extracting temperature are 87-92 DEG C;
S3:To the end of reflux course, stop that dilute hydrochloric acid is added dropwise, filter extracting solution while hot, residue is cleaned twice with ethyl alcohol, closed
And filtrate and cleaning solution;
S4:Decompression filters, and is preserved at shady and cool ventilation.
It is further preferred that the extraction process of the antioxidant extract is as follows:
S1:Raspberry leaf, granatum and Chinese gall are weighed, air-dries, pulverizes, it is spare to cross 60 mesh sieve;
S2:Mixture is weighed in round-bottomed flask, the diluted ethyl alcohol of use deionized water that a concentration of 19-21wt% is added is molten
Liquid, the weight proportion for controlling mixture and ethanol solution is 1:12-13, when have extracting solution generate 10min after, start slowly with
The dilute hydrochloric acid that 3.1-3.3wt% is added dropwise into extracting solution for the speed of 1 drop per second is hydrolyzed, and control extraction time is 68-
72min, Extracting temperature are 88-91 DEG C;
S3:To the end of reflux course, stop that dilute hydrochloric acid is added dropwise, filter extracting solution while hot, residue is cleaned twice with ethyl alcohol, closed
And filtrate and cleaning solution;
S4:Decompression filters, and is preserved at shady and cool ventilation.
Still more preferably, the extraction process of the antioxidant extract is as follows:
S1:Raspberry leaf, granatum and Chinese gall are weighed, air-dries, pulverizes, it is spare to cross 60 mesh sieve;
S2:Mixture is weighed in round-bottomed flask, the diluted ethanol solution of use deionized water of a concentration of 20wt% is added,
The weight proportion for controlling mixture and ethanol solution is 1:12.5, after thering is extracting solution to generate 10min, start slowly with per second
The dilute hydrochloric acid that 3.2wt% is added dropwise into extracting solution for the speed of 1 drop is hydrolyzed, and control extraction time is 70min, and Extracting temperature is
90℃;
S3:To the end of reflux course, stop that dilute hydrochloric acid is added dropwise, filter extracting solution while hot, residue is cleaned twice with ethyl alcohol, closed
And filtrate and cleaning solution;
S4:Decompression filters, and is preserved at shady and cool ventilation.
To solve the above-mentioned problems, the third aspect of the present invention provides a kind of moisturizing, whitening, light spot plant extracts group
Close the preparation method of object.
Preferably, the moisturizing, whitening, the preparation method of light spot composition of plant extracts are as follows:
A1:The preparation of oil phase part
By the dimethicone of formula ratio, saualane, antioxidant extract, camellia oil, butter berry extract, carbomer,
Oil cauldron is added after weighing in Sweet Almond Oil, continues to be heated to 60-70 DEG C, and constant temperature disinfection under the stirring of 10-20 revs/min of rotating speed
Ascorbyl Tetraisopalmitate is added before emulsifying in 20-30min, stirs evenly, for use;
A2:The preparation of aqueous portion
By the glycerine of formula ratio, grape seed extract, aloe vera extract, mulberry bark extract, RADIX PAEONIAE ALBA extraction
Object, ginger-root extract, Fructus Cucumidis sativi extract, Folium Artemisiae Argyi extract, wolfberry fruit extract, licorice root extract, Leonurus extract, rose
Flower extract, peony root extractive, green-tea extract, extract of Trichosanthes, lactobacillus fermentation product, black truffle extraction
Newborn pot is added in object, sodium lactate, hyaluronic acid, ceramide, dried tremella extract after weighing, be added thereto formula ratio go from
Sub- water continues to be heated to 60-70 DEG C, and constant temperature 20-30min under the rotating speed of 10-20 revs/min of rotating speed;
A3:Newborn pot oil phase part being slowly added into where aqueous portion, and scrape wall stirring, rotating speed increase to 30-35 turn/
Point, 5-10min is stirred, until oil phase is uniformly mixed with water phase, reduction of speed is dropped to 20-30 revs/min in keeping rotation process later
Temperature waits for that temperature drops to 35 DEG C, and the emulsifier and preservative of formula ratio are added thereto, under the speed for being kept for 10-20 revs/min
Continue to stir 20-30min, you can discharging.
It is further preferred that the moisturizing, whitening, the preparation method of light spot composition of plant extracts are as follows:
A1:The preparation of oil phase part
By the dimethicone of formula ratio, saualane, antioxidant extract, camellia oil, butter berry extract, carbomer,
Oil cauldron is added after weighing in Sweet Almond Oil, continues to be heated to 62-68 DEG C, and constant temperature disinfection under the stirring of 12-18 revs/min of rotating speed
Ascorbyl Tetraisopalmitate is added before emulsifying in 22-28min, stirs evenly, for use;
A2:The preparation of aqueous portion
By the glycerine of formula ratio, grape seed extract, aloe vera extract, mulberry bark extract, RADIX PAEONIAE ALBA extraction
Object, ginger-root extract, Fructus Cucumidis sativi extract, Folium Artemisiae Argyi extract, wolfberry fruit extract, licorice root extract, Leonurus extract, rose
Flower extract, peony root extractive, green-tea extract, extract of Trichosanthes, lactobacillus fermentation product, black truffle extraction
Newborn pot is added in object, sodium lactate, hyaluronic acid, ceramide, dried tremella extract after weighing, be added thereto formula ratio go from
Sub- water continues to be heated to 62-68 DEG C, and constant temperature 22-28min under the rotating speed of 12-18 revs/min of rotating speed;
A3:Newborn pot oil phase part being slowly added into where aqueous portion, and scrape wall stirring, rotating speed increase to 31-34 turn/
Point, 6-9min is stirred, until oil phase is uniformly mixed with water phase, reduction of speed is dropped to 22-28 revs/min in keeping rotation process later
Temperature waits for that temperature drops to 35 DEG C, and the emulsifier and preservative of formula ratio are added thereto, under the speed for being kept for 12-18 revs/min
Continue to stir 22-28min, you can discharging.
Still more preferably, the moisturizing, whitening, the preparation method of light spot composition of plant extracts are as follows:
A1:The preparation of oil phase part
By the dimethicone of formula ratio, saualane, antioxidant extract, camellia oil, butter berry extract, carbomer,
Oil cauldron is added after weighing in Sweet Almond Oil, continues to be heated to 65 DEG C, and constant temperature disinfection 25min under the stirring of 15 revs/min of rotating speed,
Ascorbyl Tetraisopalmitate is added before emulsifying, stirs evenly, for use;
A2:The preparation of aqueous portion
By the glycerine of formula ratio, grape seed extract, aloe vera extract, mulberry bark extract, RADIX PAEONIAE ALBA extraction
Object, ginger-root extract, Fructus Cucumidis sativi extract, Folium Artemisiae Argyi extract, wolfberry fruit extract, licorice root extract, Leonurus extract, rose
Flower extract, peony root extractive, green-tea extract, extract of Trichosanthes, lactobacillus fermentation product, black truffle extraction
Newborn pot is added in object, sodium lactate, hyaluronic acid, ceramide, dried tremella extract after weighing, be added thereto formula ratio go from
Sub- water continues to be heated to 65 DEG C, and constant temperature 25min under the rotating speed of 15 revs/min of rotating speed;
A3:Newborn pot oil phase part being slowly added into where aqueous portion, and wall stirring is scraped, rotating speed increases to 33 revs/min,
8min is stirred, until oil phase is uniformly mixed with water phase, reduction of speed cools down in keeping rotation process to 25 revs/min, waits for temperature later
Drop to 35 DEG C, the emulsifier and preservative of formula ratio are added thereto, continues to stir under the speed for being kept for 15 revs/min
25min, you can discharging.
In some specific embodiments, in parts by weight, the emulsifier includes stearine and/or gathers
0.3-0.5 parts of ethylene glycol stearate;Preferably, in parts by weight, the emulsifier is stearine and poly- second two
0.3-0.5 parts of alcohol stearate;It is further preferred that in parts by weight, the emulsifier is stearine and poly- second
0.4 part of the mixture of glycol stearate.
In some specific embodiments, in parts by weight, the preservative is salicylic acid preservative 0.1-
0.2 part;Preferably, in parts by weight, the preservative is 0.15 part of salicylic acid preservative.
In some embodiments, a kind of moisturizing, whitening, light spot composition of plant extracts are applied to relax
In the cosmetics of slow eye hair week angling and desalination eye circumference spot.
Embodiment
The first aspect of embodiment 1-27 provides a kind of moisturizing, whitening, light spot composition of plant extracts, according to weight
Part meter, component see the table below 1
If saualane is component A, antioxidant extract is component B, and Ascorbyl Tetraisopalmitate is component C, glycerine
For component D, grape seed extract is component E, and lactobacillus fermentation product is component F, and black truffle extract is component G, sweet
Grass roots extract is component H, and hyaluronic acid is component I, and dried tremella extract is component J, and deionized water is component K, dimethyl-silicon
Oil is component L, and camellia oil is component M, and butter berry extract is component N, and carbomer is component O, and Sweet Almond Oil is component P, library
Drag-line aloe extract is component R, and mulberry bark extract is component S, and Radix Paeoniae Alba medicament extract is component T, and ginger-root extract is group
It is component V to divide U, Fructus Cucumidis sativi extract, and Folium Artemisiae Argyi extract is component W, and wolfberry fruit extract is component X, and Leonurus extract is component
Y, Flos Rosae Rugosae extract are component Z, and peony root extractive is component a, and green-tea extract is component b, and extract of Trichosanthes is group
It is component d to divide c, sodium lactate, and ceramide is component e, and emulsifier is component f, and preservative is component g.
Embodiment 1
The first aspect of embodiment 1 provides a kind of moisturizing, whitening, light spot composition of plant extracts, according to parts by weight
Meter, including following component:
Oil phase part:7.5 parts of A, 7.5 parts of B, 2.5 parts of C, 3 parts of L, 2 parts of M, 1.5 parts of N, 1.5 parts of O and P 1.5
Part;Aqueous portion:6.4 parts of D, 3.5 parts of E, 3.5 parts of F, 2.5 parts of G, 3 parts of H, 7.5 parts of I, 1.5 parts of J, 3 parts of R, S 1.5
Part, 2.5 parts of T, 1.5 parts of U, 1.4 parts of V, 1.5 parts of W, 2.4 parts of X, 1.6 parts of Y, 2.6 parts of Z, 2.7 parts of a, 2.6 parts of b, c
40 parts of 2.5 parts, 1.6 parts of d, 1.2 parts of e and K;0.4 part of e;0.15 part of f.
The second aspect of embodiment 1 provides a kind of preparation method of antioxidant extract, and specific preparation method is as follows:
S1:Raspberry leaf, granatum and Chinese gall are weighed, air-dries, pulverizes, it is spare to cross 60 mesh sieve;
S2:Mixture is weighed in round-bottomed flask, the diluted ethanol solution of use deionized water of a concentration of 20wt% is added,
The weight proportion for controlling mixture and ethanol solution is 1:12.5, after thering is extracting solution to generate 10min, start slowly with per second
The dilute hydrochloric acid that 3.2wt% is added dropwise into extracting solution for the speed of 1 drop is hydrolyzed, and control extraction time is 70min, and Extracting temperature is
90℃;
S3:To the end of reflux course, stop that dilute hydrochloric acid is added dropwise, filter extracting solution while hot, residue is cleaned twice with ethyl alcohol, closed
And filtrate and cleaning solution;
S4:Decompression filters, and is preserved at shady and cool ventilation.
The third aspect of embodiment 1 provide a kind of moisturizing, whitening, light spot composition of plant extracts preparation method,
Specific preparation method is as follows:
A1:The preparation of oil phase part
By L, A, B, M, N, O, P of formula ratio, oil cauldron is added after weighing, continues to heat under the stirring of 15 revs/min of rotating speed
To 65 DEG C, and constant temperature disinfection 25min, C is added before emulsifying, stirs evenly, for use;
A2:The preparation of aqueous portion
Newborn pot is added by D, E, R, S, T, U, V, W, X, H, Y, Z, a, b, c, F, G, d, I, e, J of formula ratio, after weighing, to
The deionized water that formula ratio is wherein added continues to be heated to 65 DEG C, and constant temperature 25min under the rotating speed of 15 revs/min of rotating speed;
A3:Newborn pot oil phase part being slowly added into where aqueous portion, and wall stirring is scraped, rotating speed increases to 33 revs/min,
8min is stirred, until oil phase is uniformly mixed with water phase, reduction of speed cools down in keeping rotation process to 25 revs/min, waits for temperature later
Drop to 35 DEG C, the f and g of formula ratio are added thereto, continues to stir 25min under the speed for being kept for 15 revs/min, you can go out
Material.
Embodiment 2
The first aspect of embodiment 2 provides a kind of moisturizing, whitening, light spot composition of plant extracts, according to parts by weight
Meter, including following component:
Oil phase part:1 part of 5 parts of A, 5 parts of B, 2 parts of C, 2 parts of L, 1 part of M, 1 part of N, 1 part of O and P;Aqueous portion:D
5 parts, 2.5 parts of E, 2.5 parts of F, 2 parts of G, 2 parts of H, 5 parts of I, 1 part of J, 2 parts of R, 1 part of S, 2 parts of T, 1 part of U, 1 part of V, W 1
Part, 2 parts of X, 1 part of Y, 2 parts of Z, 2 parts of a, 2 parts of b, 2 parts of c, 1 part of d, 1 part of e and 10 parts of K;0.4 part of e;0.15 part of f.
The second aspect of embodiment 2 provides a kind of preparation method of antioxidant extract, specific preparation method and implementation
Example 1 is identical.
The third aspect of embodiment 2 provide a kind of moisturizing, whitening, light spot composition of plant extracts preparation method,
Specific preparation method is same as Example 1.
Embodiment 3
The first aspect of embodiment 3 provides a kind of moisturizing, whitening, light spot composition of plant extracts, according to parts by weight
Meter, including following component:
Oil phase part:10 parts of A, 10 parts of B, 3 parts of C, L4 parts, 3 parts of M, 2 parts of N, 2 parts and P2 parts of O;Aqueous portion:D
8 parts, 5 parts of E, 5 parts of F, 3 parts of G, 4 parts of H, 10 parts of I, 2 parts of J, 1 part of R, 2 parts of S, 3 parts of T, 2 parts of U, 2 parts of V, 2 parts of W,
50 parts of 3 parts of X, 2 parts of Y, 3 parts of Z, 3 parts of a, 4 parts of b, 4 parts of c, 2 parts of d, 1.5 parts of e and K;0.4 part of e;0.15 part of f.
The second aspect of embodiment 3 provides a kind of preparation method of antioxidant extract, specific preparation method and implementation
Example 1 is identical.
The third aspect of embodiment 3 provide a kind of moisturizing, whitening, light spot composition of plant extracts preparation method,
Specific preparation method is same as Example 1.
Embodiment 4
The first aspect of embodiment 4 provides a kind of moisturizing, whitening, light spot composition of plant extracts, according to parts by weight
Meter, including following component:
Oil phase part:2.5 parts of 7.5 parts of A, 7.5 parts of B and C;Aqueous portion:6.4 parts of D, 3.5 parts of E, F3.5 parts, G
40 parts of 2.5 parts, 3 parts of H, 7.5 parts of I, 1.5 parts of J and K;0.4 part of f;0.15 part of g.
The second aspect of embodiment 4 provides a kind of preparation method of antioxidant extract, specific preparation method and implementation
Example 1 is identical.
The third aspect of embodiment 4 provide a kind of moisturizing, whitening, light spot composition of plant extracts preparation method,
Specific preparation method is as follows:
A1:The preparation of oil phase part
By the A and B of formula ratio, oil cauldron is added after weighing, continues to be heated to 65 DEG C under the stirring of 15 revs/min of rotating speed, and
Ascorbyl Tetraisopalmitate is added before emulsifying in constant temperature disinfection 25min, stirs evenly, for use;
A2:The preparation of aqueous portion
Newborn pot is added by D, E, F, G, H, I and J of formula ratio, after weighing, the K of formula ratio is added thereto, in rotating speed 15
Rev/min rotating speed under, continue to be heated to 65 DEG C, and constant temperature 25min;
A3:Newborn pot oil phase part being slowly added into where aqueous portion, and wall stirring is scraped, rotating speed increases to 33 revs/min,
8min is stirred, until oil phase is uniformly mixed with water phase, reduction of speed cools down in keeping rotation process to 25 revs/min, waits for temperature later
Drop to 35 DEG C, the emulsifier and preservative of formula ratio are added thereto, continues to stir under the speed for being kept for 15 revs/min
25min, you can discharging.
Embodiment 5
The first aspect of embodiment 5 provides a kind of moisturizing, whitening, light spot composition of plant extracts, according to parts by weight
Meter, including following component:
Oil phase part:2 parts of 5 parts of A, 5 parts of B and C;Aqueous portion:5 parts of D, 3.5 parts of E, 2.5 parts of F, 2 parts of G, H 2
Part, 5 parts of I, 1 part of J and 40 parts of K;0.4 part of f;0.15 part of g.
The second aspect of embodiment 5 provides a kind of preparation method of antioxidant extract, specific preparation method and implementation
Example 1 is identical.
The third aspect of embodiment 5 provide a kind of moisturizing, whitening, light spot composition of plant extracts preparation method,
Specific preparation method is same as Example 4.
Embodiment 6
The first aspect of embodiment 6 provides a kind of moisturizing, whitening, light spot composition of plant extracts, according to parts by weight
Meter, including following component:
Oil phase part:3 parts of 10 parts of A, 10 parts of B and C;Aqueous portion:8 parts of D, 5 parts of E, 5 parts of F, 3 parts of G, 4 parts of H,
40 parts of 10 parts of I, 2 parts of J and K;0.4 part of f;0.15 part of g.
The second aspect of embodiment 6 provides a kind of preparation method of antioxidant extract, specific preparation method and implementation
Example 1 is identical.
The third aspect of embodiment 6 provide a kind of moisturizing, whitening, light spot composition of plant extracts preparation method,
Specific preparation method is same as Example 4.
Embodiment 7
The first aspect of embodiment 7 provides a kind of moisturizing, whitening, light spot composition of plant extracts, according to parts by weight
Meter, it is similar to Example 1, the difference is that 8 parts of 4 parts of H, I.
The second aspect of embodiment 7 provides a kind of preparation method of antioxidant extract, specific preparation method and implementation
Example 1 is identical.
The third aspect of embodiment 7 provide a kind of moisturizing, whitening, light spot composition of plant extracts preparation method,
Specific preparation method is same as Example 1.
Embodiment 8
The first aspect of embodiment 8 provides a kind of moisturizing, whitening, light spot composition of plant extracts, according to parts by weight
Meter, it is similar to Example 1, the difference is that 9 parts of I.
The second aspect of embodiment 8 provides a kind of preparation method of antioxidant extract, specific preparation method and implementation
Example 1 is identical.
The third aspect of embodiment 8 provide a kind of moisturizing, whitening, light spot composition of plant extracts preparation method,
Specific preparation method is same as Example 1.
Embodiment 9
The first aspect of embodiment 9 provides a kind of moisturizing, whitening, light spot composition of plant extracts, according to parts by weight
Meter, it is similar to Example 1, the difference is that 2 parts of H.
The second aspect of embodiment 9 provides a kind of preparation method of antioxidant extract, specific preparation method and implementation
Example 1 is identical.
The third aspect of embodiment 9 provide a kind of moisturizing, whitening, light spot composition of plant extracts preparation method,
Specific preparation method is same as Example 1.
Embodiment 10
The first aspect of embodiment 10 provides a kind of moisturizing, whitening, light spot composition of plant extracts, according to parts by weight
Meter, it is similar to Example 1, the difference is that without B component.
The second aspect of embodiment 10 provide a kind of moisturizing, whitening, light spot composition of plant extracts preparation method,
Specific preparation method is similar to Example 1, the difference is that without B component.
Embodiment 11
The first aspect of embodiment 11 provides a kind of moisturizing, whitening, light spot composition of plant extracts, according to parts by weight
Meter, it is similar to Example 1, the difference is that there is no F components.
The second aspect of embodiment 11 provides a kind of preparation method of antioxidant extract, specific preparation method and implementation
Example 1 is identical.
The third aspect of embodiment 11 provide a kind of moisturizing, whitening, light spot composition of plant extracts preparation method,
Specific preparation method is similar to Example 1, the difference is that not having F components.
Embodiment 12
The first aspect of embodiment 12 provides a kind of moisturizing, whitening, light spot composition of plant extracts, according to parts by weight
Meter, it is similar to Example 1, the difference is that there is no H components.
The second aspect of embodiment 12 provides a kind of preparation method of antioxidant extract, specific preparation method and implementation
Example 1 is identical.
The third aspect of embodiment 12 provide a kind of moisturizing, whitening, light spot composition of plant extracts preparation method,
Specific preparation method is similar to Example 1, the difference is that not having H components.
Embodiment 13
The first aspect of embodiment 13 provides a kind of moisturizing, whitening, light spot composition of plant extracts, according to parts by weight
Meter, it is similar to Example 1, the difference is that without component E.
The second aspect of embodiment 13 provides a kind of preparation method of antioxidant extract, specific preparation method and implementation
Example 1 is identical.
The third aspect of embodiment 13 provide a kind of moisturizing, whitening, light spot composition of plant extracts preparation method,
Specific preparation method is similar to Example 1, the difference is that without component E.
Embodiment 14
The first aspect of embodiment 14 provides a kind of moisturizing, whitening, light spot composition of plant extracts, according to parts by weight
Meter, it is similar to Example 1, the difference is that without B and component E.
The second aspect of embodiment 14 provide a kind of moisturizing, whitening, light spot composition of plant extracts preparation method,
Specific preparation method is similar to Example 1, the difference is that without B and component E.
Embodiment 15
The first aspect of embodiment 15 provides a kind of moisturizing, whitening, light spot composition of plant extracts, according to parts by weight
Meter, it is similar to Example 1, the difference is that without B and H components.
The second aspect of embodiment 15 provide a kind of moisturizing, whitening, light spot composition of plant extracts preparation method,
Specific preparation method is similar to Example 1, the difference is that without B and H components.
Embodiment 16
The first aspect of embodiment 16 provides a kind of moisturizing, whitening, light spot composition of plant extracts, according to parts by weight
Meter, it is similar to Example 1, the difference is that without E and F components.
The second aspect of embodiment 16 provides a kind of preparation method of antioxidant extract, specific preparation method and implementation
Example 1 is identical.
The third aspect of embodiment 16 provide a kind of moisturizing, whitening, light spot composition of plant extracts preparation method,
Specific preparation method is similar to Example 1, the difference is that without E and F components.
Embodiment 17
The first aspect of embodiment 17 provides a kind of moisturizing, whitening, light spot composition of plant extracts, according to parts by weight
Meter, it is similar to Example 1, the difference is that without B, E, F and H component.
The second aspect of embodiment 17 provide a kind of moisturizing, whitening, light spot composition of plant extracts preparation method,
Specific preparation method is similar to Example 1, the difference is that without B, E, F and H component.
Embodiment 18
The first aspect of embodiment 18 provides a kind of moisturizing, whitening, light spot composition of plant extracts, according to parts by weight
Meter, it is similar to Example 1, the difference is that there is no I components.
The second aspect of embodiment 18 provides a kind of preparation method of antioxidant extract, specific preparation method and implementation
Example 1 is identical.
The third aspect of embodiment 18 provide a kind of moisturizing, whitening, light spot composition of plant extracts preparation method,
Specific preparation method is similar to Example 1, the difference is that not having I components.
Embodiment 19
The first aspect of embodiment 19 provides a kind of moisturizing, whitening, light spot composition of plant extracts, according to parts by weight
Meter, it is similar to Example 1, the difference is that without component A.
The second aspect of embodiment 19 provides a kind of preparation method of antioxidant extract, specific preparation method and implementation
Example 1 is identical.
The third aspect of embodiment 19 provide a kind of moisturizing, whitening, light spot composition of plant extracts preparation method,
Specific preparation method is similar to Example 1, the difference is that without component A.
Embodiment 20
The first aspect of embodiment 20 provides a kind of moisturizing, whitening, light spot composition of plant extracts, according to parts by weight
Meter, it is similar to Example 1, the difference is that there is no G components.
The second aspect of embodiment 20 provides a kind of preparation method of antioxidant extract, specific preparation method and implementation
Example 1 is identical.
The third aspect of embodiment 20 provide a kind of moisturizing, whitening, light spot composition of plant extracts preparation method,
Specific preparation method is similar to Example 1, the difference is that not having G components.
Embodiment 21
The first aspect of embodiment 21 provides a kind of moisturizing, whitening, light spot composition of plant extracts, according to parts by weight
Meter, it is similar to Example 1, the difference is that without A and I components.
The second aspect of embodiment 21 provides a kind of preparation method of antioxidant extract, specific preparation method and implementation
Example 1 is identical.
The third aspect of embodiment 21 provide a kind of moisturizing, whitening, light spot composition of plant extracts preparation method,
Specific preparation method is similar to Example 1, the difference is that without A and I components.
Embodiment 22
The first aspect of embodiment 22 provides a kind of moisturizing, whitening, light spot composition of plant extracts, according to parts by weight
Meter, it is similar to Example 1, the difference is that without G and I components.
The second aspect of embodiment 22 provides a kind of preparation method of antioxidant extract, specific preparation method and implementation
Example 1 is identical.
The third aspect of embodiment 22 provide a kind of moisturizing, whitening, light spot composition of plant extracts preparation method,
Specific preparation method is similar to Example 1, the difference is that without G and I components.
Embodiment 23
The first aspect of embodiment 23 provides a kind of moisturizing, whitening, light spot composition of plant extracts, according to parts by weight
Meter, it is similar to Example 1, the difference is that without A, G and I component.
The second aspect of embodiment 23 provides a kind of preparation method of antioxidant extract, specific preparation method and implementation
Example 1 is identical.
The third aspect of embodiment 23 provide a kind of moisturizing, whitening, light spot composition of plant extracts preparation method,
Specific preparation method is similar to Example 1, the difference is that without A, G and I component.
Embodiment 24
The first aspect of embodiment 24 provides a kind of moisturizing, whitening, light spot composition of plant extracts, according to parts by weight
Meter, it is similar to Example 1, the difference is that without H and I components.
The second aspect of embodiment 24 provides a kind of preparation method of antioxidant extract, specific preparation method and implementation
Example 1 is identical.
The third aspect of embodiment 24 provide a kind of moisturizing, whitening, light spot composition of plant extracts preparation method,
Specific preparation method is similar to Example 1, the difference is that without H and I components.
Embodiment 25
The first aspect of embodiment 25 provides a kind of moisturizing, whitening, light spot composition of plant extracts, concrete component with
Embodiment 1 is identical.
The second aspect of embodiment 25 provides a kind of preparation method of antioxidant extract, specific preparation method and implementation
Example 1 is identical.
The third aspect of embodiment 25 provide a kind of moisturizing, whitening, light spot composition of plant extracts preparation method,
Specific preparation method is as follows:
A1:The preparation of oil phase part
By L, A, B, M, N, O, P of formula ratio, oil cauldron is added after weighing, continues to heat under the stirring of 50 revs/min of rotating speed
To 50 DEG C, and constant temperature disinfection 15min, C is added before emulsifying, stirs evenly, for use;
A2:The preparation of aqueous portion
Newborn pot is added by D, E, R, S, T, U, V, W, X, H, Y, Z, a, b, c, F, G, d, I, e, J of formula ratio, after weighing, to
The deionized water that formula ratio is wherein added continues to be heated to 50 DEG C, and constant temperature 30min under the rotating speed of 50 revs/min of rotating speed;
A3:Newborn pot oil phase part being slowly added into where aqueous portion, and wall stirring is scraped, rotating speed increases to 33 revs/min,
8min is stirred, until oil phase is uniformly mixed with water phase, reduction of speed cools down in keeping rotation process to 30 revs/min, waits for temperature later
Drop to 35 DEG C, the f and g of formula ratio are added thereto, continues to stir 25min under the speed for being kept for 30 revs/min, you can go out
Material.
Embodiment 26
The first aspect of embodiment 26 provides a kind of moisturizing, whitening, light spot composition of plant extracts, concrete component with
Embodiment 1 is identical.
The second aspect of embodiment 26 provide a kind of moisturizing, whitening, light spot composition of plant extracts preparation method,
Specific preparation method is as follows:
S1:Raspberry leaf, granatum and Chinese gall are weighed, air-dries, pulverizes, it is spare to cross 60 mesh sieve;
S2:Mixture is weighed in round-bottomed flask, thereto with it is per second 2 drop speed be added dropwise 3.2wt% dilute hydrochloric acid into
Row hydrolysis, controls 90 DEG C of time for adding 20min of temperature, the diluted ethanol solution of use deionized water of a concentration of 20wt% is added,
The weight proportion for controlling mixture and ethanol solution is 1:12.5, it flows back;
S3:To the end of reflux course, stop that dilute hydrochloric acid is added dropwise, filter extracting solution while hot, residue is cleaned twice with ethyl alcohol, closed
And filtrate and cleaning solution;
S4:Decompression filters, and is preserved at shady and cool ventilation.
The third aspect of embodiment 26 provides a kind of preparation method of antioxidant extract, specific preparation method and implementation
Example 1 is identical.
Embodiment 27
The first aspect of embodiment 27 provide a kind of moisturizing, whitening, light spot composition of plant extracts formula, with reality
It applies example 1 to compare, without A, B, E, F, G, H and I component.
The second aspect of embodiment 27 provide a kind of moisturizing, whitening, light spot composition of plant extracts preparation method,
Specific preparation method is as follows:
A1:The preparation of oil phase part
By L, M, N, O, P of formula ratio, oil cauldron is added after weighing in proportion, continue under the stirring of 15 revs/min of rotating speed plus
Heat is to 65 DEG C, and constant temperature disinfection 25min, and Ascorbyl Tetraisopalmitate is added before emulsifying, stirs evenly, for use;
A2:The preparation of aqueous portion
Newborn pot is added by D, R, S, T, U, V, W, X, Y, Z, a, b, c, d, e, J of formula ratio, after weighing, is added matches thereto
The deionized water just measured continues to be heated to 65 DEG C, and constant temperature 25min under the rotating speed of 15 revs/min of rotating speed;
A3:Newborn pot oil phase part being slowly added into where aqueous portion, and wall stirring is scraped, rotating speed increases to 33 revs/min,
8min is stirred, until oil phase is uniformly mixed with water phase, reduction of speed cools down in keeping rotation process to 25 revs/min, waits for temperature later
Drop to 35 DEG C, the emulsifier and preservative of formula ratio are added thereto, continues to stir under the speed for being kept for 15 revs/min
25min, you can discharging.
Performance evaluation
One, physical and chemical index is tested
Sensory testing:The character for visually observing product, sees if there is exception;
Resistance to Thermal test:Sample is put into the electro-heating standing-temperature cultivator of (40 ± 1) DEG C for 24 hours, is seen whether after restoring room temperature
There is phenomena such as thinning, discoloration, layering and firmness change, with the heat resistance of judgement sample;
Low temperature resistant test:Sample is put into the refrigerator of (- 5~-10) DEG C ± 1 DEG C for 24 hours, has been seen whether after restoring room temperature
Phenomena such as thinning, discoloration, layering and firmness change, with the cold tolerance of judgement sample;
Centrifugal test:Sample is placed in a centrifuge, with the speed test 30min of (2000~4000) r/min, observes sample
The separation of product, layering situation.Test result is shown in Table 1
1 physicochemical property of table is tested
Two, security test
1) the skin irritation test of multiple dosing
Using zoopery, experimental animal (is purchased from the big biotechnology of Qingdao health using the Japanese big-ear white rabbit of health
Co., Ltd), take rabbit 10, half male and half female to be randomly divided into 2 groups by gender and weight:Intact skin group and damaged skin group,
Every group 5.Preceding 24 hours of administration goes the gross area to be about with 8% (mass percent) vulcanized sodium by the depilation of family's rabbit back both sides
100cm2.When experiment, lower regions on the left of skin, each stroke of right side intermediate region are sterilized in damaged skin hair removal section with knife blade
One " well " word cut, the vertical and horizontal each about 2cm of cut, is degree with oozing of blood.Two groups of animals uniformly smear this in left side depilation upper and lower region
Inventive embodiments 1-27 composition 0.1g, right side are smeared 1ml physiological saline and are compared, and the daily upper and lower noon, respectively painting was primary, and continuous 7
It.Animal divides cage to be fed with full nutrient fodder during coating.After medication 7 days, warm water washes away remaining embodiment in a rabbit skin
1-27 products, with 1 after drug withdrawal, detect by an unaided eye within 2,3,4,5,6,7 days and carry out histopathologic examination and record coating position
Whether there is or not erythema and oedema situation for skin, carry out skin irritation reaction scoring and intensity evaluation.
Skin irritation reaction standards of grading are as shown in table 2, and skin irritation intensity evaluation standard is as shown in table 3, to family
The results are shown in Table 4 for rabbit skin irritative response.
Table 2
Erythema |
Score value |
Oedema |
Score value |
Without erythema |
0 |
Without oedema |
0 |
It is visible reluctantly |
1 |
It is visible reluctantly |
1 |
It is clearly visible |
2 |
It can be seen that (edge is higher by skin) |
2 |
Poisoning or Severe erythema |
3 |
Cutaneous protuberance about 1mm, is clearly outlined |
|
Aubergine erythema simultaneously has eschar to be formed |
4 |
Oedema protuberance >=1mm or more and range expansion |
4 |
Table 3
React average value |
Evaluation |
0-0.49 |
It is nonirritant |
0.5-2.99 |
Slight stimulation |
3.0-5.99 |
Moderate irritation |
6.0-8.0 |
Strong and stimulating |
React average value=(erythema forms total score+oedema and forms total score)/total number of animals
4 rabbit skin irritation reaction result of table
Three, skin quality evaluation test
This test is specific as follows mainly for five kinds of skin problems:
1) skin is obscure or dark yellow;
2) eye hair week angling;
3) eye circumference spot;
4) it has dry skin;
5) acne print or new acne.
Two evaluation indexes:
1) slight to improve.Slight improve refers to that the colour of skin highlights, the desalination of eye circumference spot, hair week angling shoal, skin is no longer dry
Dry, acne print shoals or new acne anti-inflammatory.
2) it is obviously improved.It refers to that the colour of skin obviously bleaches to be obviously improved, and spot disappears, and hair week angling recovery from illness, skin water profit has
Elasticity, acne print disappears or new acne disappears.
Selected experimenter is the personnel perplexed for a long time by these problems, and every group of embodiment tester is 50 people.Year
Age interval is 25-45 Sui.Specific test result is shown in Table 5.
5 skin quality test result of table
Four, the test of moisturizing degree
The test of moisturizing degree picks out 25 experiment people to carry out test using KSN skin detections instrument from Harbin City
Member, in subzero 15 DEG C or so of wintry weather, humidity is 10 ± 5%, is tested, in addition 25 people are random, wet at 20 ± 5 DEG C
It is tested at 55 ± 5 DEG C of degree, test result such as table 6:
6 moisturizing Tachistoscope of table