CN108634318A - A kind of Dendrobidium huoshanness baste and preparation method thereof for health care - Google Patents
A kind of Dendrobidium huoshanness baste and preparation method thereof for health care Download PDFInfo
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- CN108634318A CN108634318A CN201810934128.3A CN201810934128A CN108634318A CN 108634318 A CN108634318 A CN 108634318A CN 201810934128 A CN201810934128 A CN 201810934128A CN 108634318 A CN108634318 A CN 108634318A
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- dendrobidium huoshanness
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- 238000002360 preparation method Methods 0.000 title claims abstract description 16
- 244000178870 Lavandula angustifolia Species 0.000 claims abstract description 34
- 235000010663 Lavandula angustifolia Nutrition 0.000 claims abstract description 34
- 239000001102 lavandula vera Substances 0.000 claims abstract description 34
- 235000018219 lavender Nutrition 0.000 claims abstract description 34
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- 238000000227 grinding Methods 0.000 claims abstract description 16
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- QNAYBMKLOCPYGJ-REOHCLBHSA-N L-alanine Chemical compound C[C@H](N)C(O)=O QNAYBMKLOCPYGJ-REOHCLBHSA-N 0.000 claims abstract description 14
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- QSNCUGULHPBRGR-UHFFFAOYSA-N Dendramine Natural products CC12C3(O)CCC2CN(C)C1C1C(C(C)C)C3C(=O)O1 QSNCUGULHPBRGR-UHFFFAOYSA-N 0.000 description 1
- IAIIJNHQMKXPHL-JMMPBUAGSA-N Dendrine Natural products O=C(OC)C[C@@H]1N(C)[C@H]2[C@@]3(C)[C@@H]1CC[C@H]3[C@H]1[C@H](C(C)C)[C@H]2OC1=O IAIIJNHQMKXPHL-JMMPBUAGSA-N 0.000 description 1
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- CCEAFOJVRQZWQC-KFYGABLUSA-N Dendroxine Natural products O=C1O[C@@H]2[C@@H](C(C)C)[C@@H]1[C@H]1[C@]3(C)[C@@H](CN4[C@]23OCC4)CC1 CCEAFOJVRQZWQC-KFYGABLUSA-N 0.000 description 1
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- 241000607479 Yersinia pestis Species 0.000 description 1
- HCHKCACWOHOZIP-UHFFFAOYSA-N Zinc Chemical compound [Zn] HCHKCACWOHOZIP-UHFFFAOYSA-N 0.000 description 1
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- RYAHJFGVOCZDEI-CZKZLRAZSA-N dendrobine Natural products O=C1O[C@@H]2[C@H](C(C)C)[C@H]1[C@H]1[C@@]3(C)[C@@H]2N(C)C[C@H]3CC1 RYAHJFGVOCZDEI-CZKZLRAZSA-N 0.000 description 1
- 230000018109 developmental process Effects 0.000 description 1
- 206010012601 diabetes mellitus Diseases 0.000 description 1
- PXEDJBXQKAGXNJ-QTNFYWBSSA-L disodium L-glutamate Chemical compound [Na+].[Na+].[O-]C(=O)[C@@H](N)CCC([O-])=O PXEDJBXQKAGXNJ-QTNFYWBSSA-L 0.000 description 1
- 238000001035 drying Methods 0.000 description 1
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Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L33/00—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
- A23L33/10—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof using additives
- A23L33/105—Plant extracts, their artificial duplicates or their derivatives
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L33/00—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
- A23L33/10—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof using additives
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/48—Fabaceae or Leguminosae (Pea or Legume family); Caesalpiniaceae; Mimosaceae; Papilionaceae
- A61K36/484—Glycyrrhiza (licorice)
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/53—Lamiaceae or Labiatae (Mint family), e.g. thyme, rosemary or lavender
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/53—Lamiaceae or Labiatae (Mint family), e.g. thyme, rosemary or lavender
- A61K36/537—Salvia (sage)
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/82—Theaceae (Tea family), e.g. camellia
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/88—Liliopsida (monocotyledons)
- A61K36/898—Orchidaceae (Orchid family)
- A61K36/8984—Dendrobium
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs
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- Health & Medical Sciences (AREA)
- Natural Medicines & Medicinal Plants (AREA)
- Life Sciences & Earth Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
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- Botany (AREA)
- Microbiology (AREA)
- Animal Behavior & Ethology (AREA)
- Medicinal Chemistry (AREA)
- Biotechnology (AREA)
- Alternative & Traditional Medicine (AREA)
- Pharmacology & Pharmacy (AREA)
- Epidemiology (AREA)
- Medical Informatics (AREA)
- General Health & Medical Sciences (AREA)
- Public Health (AREA)
- Veterinary Medicine (AREA)
- Nutrition Science (AREA)
- Food Science & Technology (AREA)
- Polymers & Plastics (AREA)
- Medicines Containing Plant Substances (AREA)
- Cosmetics (AREA)
Abstract
The Dendrobidium huoshanness baste and preparation method thereof that the invention discloses a kind of for health care, it is related to medicinal plant manufacture field, based on Dendrobidium huoshanness product prepare complicated, utilization rate is low, the problem more than nutrient loss and propose, Dendrobidium huoshanness baste of the invention is made of the raw material of following weight fraction：30 40 parts of Dendrobidium huoshanness, 15 parts of Salvia japonica, 5 10 parts of thyme, 5 10 parts of lavender, 15 20 parts of tealeaves, 20 25 parts of Radix Glycyrrhizae, 15 parts of edible gelatin, 1 10 parts of L alanine.The beneficial effects of the present invention are：Dendrobidium huoshanness carries out ultramicro grinding under freezing conditions, and nutrient loss is few, and the active ingredient in Dendrobidium huoshanness can fully discharge.
Description
Technical field
The present invention relates to medicinal plant manufacture fields, and in particular to a kind of Dendrobidium huoshanness baste and its system for health care
Preparation Method.
Background technology
Dendrobidium huoshanness is orchid, scientific name Dendrobium huoshanense C.Z.Tang et S.J.
(Cheng), it is《Anhui Province's prepared slices of Chinese crude drugs concocted specification》Kind is included, medicinal effects are fresh or drying stem, mainly contain stone
The bioactive substances such as dry measure used in former times polysaccharide, dendrobine, dendramine, nobilonine, dendroxine, dendrine, 6-hydroxydendroxine.Suddenly
Mountain stem of noble dendrobium maple bucket can be for tea or as Baoshang material, as high-class healthy product, to chronic fatigue syndrome, tuberculosis, coronary heart disease, kidney
The diseases such as disease, chronic liver disease, hypertension, hyperlipidemia, diabetes, chronic gastropathy, dry syndrome, cancer have definite curative effect and
Improve rehabilitative action, and immunity of organisms, anti-oxidant, anti-aging can be enhanced, to excessive drinking and smoking, overwork, night life excessively,
There is special efficacy with rehabilitations such as eye is overstrain one's nerves, hoarseness, mouth parched and tongue scorched, the weak power of old age decline, the deficiency of Yin.
With social development, operating pressure increases, and aging of population aggravates, and demand of the people to health is all the more apparent, with
Dendrobidium huoshanness is that the high-class healthy product that raw material produces and Chinese patent drug are also more and more.
The preparation of Dendrobidium huoshanness product is complicated, utilization rate is low, nutrient loss is more, to the comprehensive utilization value of Dendrobidium huoshanness
Exploitation also urgently needs further to enrich its product category, to expand its occupation rate of market.
Invention content
Present invention solves the technical problem that being prepared in Dendrobidium huoshanness product, complicated, utilization rate is low, nutrient loss is more.
The present invention adopts the following technical solutions solves above-mentioned technical problem：
A kind of Dendrobidium huoshanness baste for health care is made of the raw material of following weight fraction：Dendrobidium huoshanness 30-40
Part, 1-5 parts of Salvia japonica, 5-10 parts of thyme, 5-10 parts of lavender, 15-20 parts of tealeaves, 20-25 parts of Radix Glycyrrhizae, edible gelatin 1-5
Part, 1-10 parts of l-Alanine.
Preferably, the Dendrobidium huoshanness baste for health care, including following preparation process：
(1) Salvia japonica of above-mentioned parts by weight, thyme, Radix Glycyrrhizae, tealeaves are crushed to 50-70 mesh, it is spare；
(2) toward Salvia japonica, thyme, Radix Glycyrrhizae crushed material in suitable quantity of water is added, make solid-liquid ratio be 1:(9-11), is surpassed
Sound extracts, and extracting solution is made, spare；
(3) after Dendrobidium huoshanness and lavender being carried out steam sterilizing at a temperature of 110-120 DEG C, in (- 30)-(- 25) DEG C
In the environment of, ultramicro grinding is carried out, Dendrobidium huoshanness juice and lavender Ultramicro-powder are respectively obtained；
(4) appropriate 70% ethyl alcohol is added in the tealeaves after crushing, it is 1 to make solid-liquid ratio:(10-15) carries out ultrasonic extraction,
Extracting temperature is 70-90 DEG C, and tea extract is made, spare；
(5) extracting solution obtained in step (4) is centrifuged, the supernatant of acquisition crosses polyamide chromatography column, using steaming
Distilled water be eluted to it is colourless, then with 70% ethanol elution of pH8.5, until eluent meets FeCl3Until solution is non-discolouring, eluted
Liquid；
(6) after mixing by Dendrobidium huoshanness juice obtained in extracting solution obtained in step (2) and step (3), centrifugation
Take filtrate；
(7) by the eluent in the edible gelatin of above-mentioned parts by weight, l-Alanine and step (5), the filter in step (6)
Liquid mixes, and carries out negative pressure concentration；
(8) the lavender Ultramicro-powder obtained in step (3) is added in the concentrate of step (7), is Huoshan after cooling
Stem of noble dendrobium baste.
Preferably, the extraction time in the step (2), (4) is 2-4 times.
Preferably, the lavender ultramicro grinding in the step (3) is to 400-600 mesh.
Preferably, the condition of negative pressure in the step (8) is：Negative pressure -0.08Mpa, temperature are 60 DEG C, and negative pressure is concentrated into close
Degree is 0.98-1.35g/mL.
The present invention also provides a kind of preparation methods of the Dendrobidium huoshanness baste for health care, including following preparation process：
(1) 1-5 parts of Salvia japonicas, 5-10 parts of thymes, 20-25 portions of Radix Glycyrrhizaes, 15-20 portions of tealeaves are crushed to 50-70
Mesh, it is spare；
(2) toward Salvia japonica, thyme, Radix Glycyrrhizae crushed material in suitable quantity of water is added, make solid-liquid ratio be 1:(9-11), is surpassed
Sound extracts, and extracting solution is made, spare；
(3) after 30-40 parts of Dendrobidium huoshanness and 5-10 portions of lavenders being carried out steam sterilizing at a temperature of 110-120 DEG C, in
In the environment of (- 30)-(- 25) DEG C, ultramicro grinding is carried out, Dendrobidium huoshanness juice and lavender Ultramicro-powder are respectively obtained；
(4) ethanol in proper amount is added in the tealeaves after crushing, it is 1 to make solid-liquid ratio:(10-15) carries out ultrasonic extraction, extraction
Temperature is 70-90 DEG C, and tea extract is made, spare；
(5) extracting solution obtained in step (4) is centrifuged, the supernatant of acquisition crosses polyamide chromatography column, using steaming
Distilled water be eluted to it is colourless, then with ethanol elution, until eluent meets FeCl3Until solution is non-discolouring, eluent is obtained；
(6) after mixing by Dendrobidium huoshanness juice obtained in extracting solution obtained in step (2) and step (3), centrifugation
Take filtrate；
(7) by 1-5 parts of edible gelatins, 1-10 parts of l-Alanine and the eluent in step (5), the filtrate in step (6)
Mixing carries out negative pressure concentration；
(8) the lavender Ultramicro-powder obtained in step (3) is added in the concentrate of step (7), is Huoshan after cooling
Stem of noble dendrobium baste.
Preferably, the extraction time in the step (2), (4) is 2-4 times.
Preferably, the lavender ultramicro grinding in the step (3) is to 400-600 mesh.
Preferably, 70% ethyl alcohol is used in the step (4), and 70% ethyl alcohol of pH8.5 is used in step (5).
Preferably, the condition of negative pressure in the step (8) is：Negative pressure -0.08Mpa, temperature are 60 DEG C, and negative pressure is concentrated into close
Degree is 0.98-1.35g/mL.
The beneficial effects of the present invention are：
(1) Dendrobidium huoshanness carries out ultramicro grinding under freezing conditions, and nutrient loss is few, and having in Dendrobidium huoshanness
Effect ingredient can fully discharge；
(2) tealeaves crosses polyamide chromatography column, can effectively extract the active constituent such as tea in tealeaves after the extraction of ultrasonic water
Polyphenol；
(3) by mixing Dendrobidium huoshanness and other above-mentioned various medicinal materials, all medicines complement each other with using；Both it made a distinction between the important and the lesser one,
Cooperation is tight, and curative effect can be improved, and is not easy to cause other lesions, and Small side effects can reach significant health-care effect.
Specific implementation mode
The effect of to make to structure feature of the invention and being reached, has a better understanding and awareness, to preferable
The present invention will be described in detail for embodiment.
In the present invention, involved component and raw material are conventional commercial product, or can pass through the ordinary skill in the art
Means obtain.
Embodiment 1
A kind of Dendrobidium huoshanness baste for health care, including following preparation process：
(1) 1 part of Salvia japonica, 6 parts of thymes, 24 portions of Radix Glycyrrhizaes are crushed to 60 mesh, 18 portions of tealeaves are crushed to 50 mesh, spare；
(2) toward Salvia japonica, thyme, Radix Glycyrrhizae crushed material in suitable quantity of water is added, make solid-liquid ratio be 1:10, it carries out ultrasound and carries
It takes, extraction time is 2 times, and extracting solution is made, spare；
(3) after 36 parts of Dendrobidium huoshanness and 9 portions of lavenders being carried out steam sterilizing at a temperature of 115 DEG C, in -27 DEG C of environment
Under, ultramicro grinding is carried out, Dendrobidium huoshanness juice and lavender Ultramicro-powder are respectively obtained, wherein lavender powder is broken to 500 mesh；
(4) appropriate 70% ethyl alcohol is added in the tealeaves after crushing, it is 1 to make solid-liquid ratio:12, carry out ultrasonic extraction, extraction
Temperature is 80 DEG C, and extraction time is 2 times, and tea extract is made, spare；
(5) tea extract obtained in step (4) is centrifuged, the supernatant of acquisition crosses polyamide chromatography column, adopts
Be eluted to distilled water it is colourless, then with 70% ethanol elution of pH8.5, until eluent meets FeCl3Until solution is non-discolouring, obtain
Eluent, wherein centrifugation step use tube centrifuge, are centrifuged with 12000r/min, when tube centrifuge works, lower end
Charging, lower end discharging, discharges immediately, and centrifugation time is determined according to inlet amount, and tea extract is obtained as long as can meet；
(6) after mixing by Dendrobidium huoshanness juice obtained in extracting solution obtained in step (2) and step (3), centrifugation
Filtrate is taken, wherein centrifugation step is used tube centrifuge, is centrifuged with 12000r/min, when tube centrifuge works, lower end
Charging, lower end discharging, discharges immediately, and centrifugation time is determined according to inlet amount, as long as can meet thick in removal Dendrobidium huoshanness juice
Fiber；
(7) 2 parts of edible gelatins, 6 parts of l-Alanine are mixed with the eluent in step (5), the filtrate in step (6),
It carries out negative pressure and is concentrated into density to be 1.05g/mL, condition of negative pressure is：Negative pressure -0.08Mpa, temperature are 60 DEG C；
(8) before waiting for the concentrate cooling in step (7), the lavender Ultramicro-powder obtained in step (3) is added, after cooling i.e.
For Dendrobidium huoshanness baste.
What needs to be explained here is that：Ultramicro grinding is the prior art, and edible gelatin, l-Alanine are food grade materials.
Dendrobidium huoshanness：Hawk relieving sore-throat, nourishing Yin and moistening lung, nourishing the stomach to improve the production of body fluid, brain nourishing and eyesight improving, liver protection calming heart, heat-clearing and fire-reducing, tonifying five zang organs
Consumptive disease, macrobiosis of making light of one's life by commiting suicide；
Salvia japonica：Blade has effects that the antitoxin removing toxic substances of sterilization sterilizing, drives pest except epidemic disease, cold and dressed with sauce can eat；Cauline leaf and flower can steep
Tea-drinking use, can peace and quiet internal grease, help to recycle, skin maintenance；
Thyme：Removable fishy smell, carbohydrate, protein, vitamin C and selenium, iron, calcium, zinc in thyme
Content be intended to it is higher than common vegetable；
Radix Glycyrrhizae：It can clearing heat and detoxicating, expelling phlegm and arresting coughing；
Lavender：Lavender has the effects that tranquilizing soporific, spasmolysis use, antibacterial, neuroprotection, lipid-loweringing, is inhibited with reaching
Bacterium, Bergamot Mint Extract, the effect of consoling skin；
L-Alanine：Nutritive value of food can be improved, increase freshness, and more traditional sodium glutamate reduces salinity.
Embodiment 2
(1) 1 part of Salvia japonica, 5 parts of thymes, 26 portions of Radix Glycyrrhizaes are crushed to 60 mesh, 18 portions of tealeaves are crushed to 50 mesh, spare；
(2) toward Salvia japonica, thyme, Radix Glycyrrhizae crushed material in suitable quantity of water is added, make solid-liquid ratio be 1:10, it carries out ultrasound and carries
It takes, extraction time is 3 times, and extracting solution is made, spare；
(3) after 34 parts of Dendrobidium huoshanness and 9 portions of lavenders being carried out steam sterilizing at a temperature of 115 DEG C, in -27 DEG C of environment
Under, ultramicro grinding is carried out, Dendrobidium huoshanness juice and lavender Ultramicro-powder are respectively obtained, wherein lavender powder is broken to 500 mesh；
(4) appropriate 70% ethyl alcohol is added in the tealeaves after crushing, it is 1 to make solid-liquid ratio:12, carry out ultrasonic extraction, extraction
Temperature is 80 DEG C, and extraction time is 3 times, and tea extract is made, spare；
(5) tea extract obtained in step (4) is centrifuged, the supernatant of acquisition crosses polyamide chromatography column, adopts
Be eluted to distilled water it is colourless, then with 70% ethanol elution of pH8.5, until eluent meets FeCl3Until solution is non-discolouring, obtain
Eluent, wherein centrifugation step use tube centrifuge, are centrifuged with 12000r/min, when tube centrifuge works, lower end
Charging, lower end discharging, discharges immediately, and centrifugation time is determined according to inlet amount, and tea extract is obtained as long as can meet；
(6) after mixing by Dendrobidium huoshanness juice obtained in extracting solution obtained in step (2) and step (3), centrifugation
Filtrate is taken, wherein centrifugation step is used tube centrifuge, is centrifuged with 12000r/min, when tube centrifuge works, lower end
Charging, lower end discharging, discharges immediately, and centrifugation time is determined according to inlet amount, as long as can meet thick in removal Dendrobidium huoshanness juice
Fiber；
(7) 2 parts of edible gelatins, 4 parts of l-Alanine are mixed with the eluent in step (5), the filtrate in step (6),
It carries out negative pressure and is concentrated into density to be 1.05g/mL, condition of negative pressure is：Negative pressure -0.08Mpa, temperature are 60 DEG C；
(8) before waiting for the concentrate cooling in step (7), the lavender Ultramicro-powder obtained in step (3) is added, after cooling i.e.
For Dendrobidium huoshanness baste.
Embodiment 3
(1) 1 part of Salvia japonica, 5 parts of thymes, 23 portions of Radix Glycyrrhizaes, 18 portions of tealeaves are crushed to 70 mesh, it is spare；
(2) toward Salvia japonica, thyme, Radix Glycyrrhizae crushed material in suitable quantity of water is added, make solid-liquid ratio be 1:11, it carries out ultrasound and carries
It takes, extraction time is 3 times, and extracting solution is made, spare；
(3) after 37 parts of Dendrobidium huoshanness and 9 portions of lavenders being carried out steam sterilizing at a temperature of 115 DEG C, in -27 DEG C of environment
Under, ultramicro grinding is carried out, Dendrobidium huoshanness juice and lavender Ultramicro-powder are respectively obtained, wherein lavender powder is broken to 500 mesh；
(4) appropriate 70% ethyl alcohol is added in the tealeaves after crushing, it is 1 to make solid-liquid ratio:15, carry out ultrasonic extraction, extraction
Temperature is 80 DEG C, and extraction time is 3 times, and tea extract is made, spare；
(5) tea extract obtained in step (4) is centrifuged, the supernatant of acquisition crosses polyamide chromatography column, adopts
Be eluted to distilled water it is colourless, then with 70% ethanol elution of pH8.5, until eluent meets FeCl3Until solution is non-discolouring, obtain
Eluent, wherein centrifugation step use tube centrifuge, are centrifuged with 12000r/min, when tube centrifuge works, lower end
Charging, lower end discharging, discharges immediately, and centrifugation time is determined according to inlet amount, and tea extract is obtained as long as can meet；
(6) after mixing by Dendrobidium huoshanness juice obtained in extracting solution obtained in step (2) and step (3), centrifugation
Filtrate is taken, wherein centrifugation step is used tube centrifuge, is centrifuged with 12000r/min, when tube centrifuge works, lower end
Charging, lower end discharging, discharges immediately, and centrifugation time is determined according to inlet amount, as long as can meet thick in removal Dendrobidium huoshanness juice
Fiber；
(7) 1 part of edible gelatin, 5 parts of l-Alanine are mixed with the eluent in step (5), the filtrate in step (6),
It carries out negative pressure and is concentrated into density to be 1.25g/mL, condition of negative pressure is：Negative pressure -0.08Mpa, temperature are 60 DEG C；
(8) before waiting for the concentrate cooling in step (7), the lavender Ultramicro-powder obtained in step (3) is added, after cooling i.e.
For Dendrobidium huoshanness baste.
Embodiment 4
(1) 3 parts of Salvia japonicas, 8 parts of thymes, 22 portions of Radix Glycyrrhizaes, 18 portions of tealeaves are crushed to 60 mesh, it is spare；
(2) toward Salvia japonica, thyme, Radix Glycyrrhizae crushed material in suitable quantity of water is added, make solid-liquid ratio be 1:10, it carries out ultrasound and carries
It takes, extraction time is 3 times, and extracting solution is made, spare；
(3) after 37 parts of Dendrobidium huoshanness and 7 portions of lavenders being carried out steam sterilizing at a temperature of 115 DEG C, in -27 DEG C of environment
Under, ultramicro grinding is carried out, Dendrobidium huoshanness juice and lavender Ultramicro-powder are respectively obtained, wherein lavender powder is broken to 500 mesh；
(4) appropriate 70% ethyl alcohol is added in the tealeaves after crushing, it is 1 to make solid-liquid ratio:12, carry out ultrasonic extraction, extraction
Temperature is 80 DEG C, and extraction time is 3 times, and tea extract is made, spare；
(5) tea extract obtained in step (4) is centrifuged, the supernatant of acquisition crosses polyamide chromatography column, adopts
Be eluted to distilled water it is colourless, then with 70% ethanol elution of pH8.5, until eluent meets FeCl3Until solution is non-discolouring, obtain
Eluent, wherein centrifugation step use tube centrifuge, are centrifuged with 12000r/min, when tube centrifuge works, lower end
Charging, lower end discharging, discharges immediately, and centrifugation time is determined according to inlet amount, and tea extract is obtained as long as can meet；
(6) after mixing by Dendrobidium huoshanness juice obtained in extracting solution obtained in step (2) and step (3), centrifugation
Filtrate is taken, wherein centrifugation step is used tube centrifuge, is centrifuged with 12000r/min, when tube centrifuge works, lower end
Charging, lower end discharging, discharges immediately, and centrifugation time is determined according to inlet amount, as long as can meet thick in removal Dendrobidium huoshanness juice
Fiber；
(7) 3 parts of edible gelatins, 6 parts of l-Alanine are mixed with the eluent in step (5), the filtrate in step (6),
It carries out negative pressure and is concentrated into density to be 1.16g/mL, condition of negative pressure is：Negative pressure -0.08Mpa, temperature are 60 DEG C；
(8) before waiting for the concentrate cooling in step (7), the lavender Ultramicro-powder obtained in step (3) is added, after cooling i.e.
For Dendrobidium huoshanness baste.
Embodiment 5
(1) 5 parts of Salvia japonicas, 10 parts of thymes, 25 portions of Radix Glycyrrhizaes, 20 portions of tealeaves are crushed to 60 mesh, it is spare；
(2) toward Salvia japonica, thyme, Radix Glycyrrhizae crushed material in suitable quantity of water is added, make solid-liquid ratio be 1:11, it carries out ultrasound and carries
It takes, extraction time is 4 times, and extracting solution is made, spare；
(3) after 40 parts of Dendrobidium huoshanness and 10 portions of lavenders being carried out steam sterilizing at a temperature of 120 DEG C, in -25 DEG C of ring
Under border, ultramicro grinding is carried out, Dendrobidium huoshanness juice and lavender Ultramicro-powder are respectively obtained, wherein lavender powder is broken to 600 mesh；
(4) appropriate 70% ethyl alcohol is added in the tealeaves after crushing, it is 1 to make solid-liquid ratio:15, carry out ultrasonic extraction, extraction
Temperature is 90 DEG C, and extraction time is 4 times, and tea extract is made, spare；
(5) tea extract obtained in step (4) is centrifuged, the supernatant of acquisition crosses polyamide chromatography column, adopts
Be eluted to distilled water it is colourless, then with 70% ethanol elution of pH8.5, until eluent meets FeCl3Until solution is non-discolouring, obtain
Eluent, wherein centrifugation step use tube centrifuge, are centrifuged with 12000r/min, when tube centrifuge works, lower end
Charging, lower end discharging, discharges immediately, and centrifugation time is determined according to inlet amount, and tea extract is obtained as long as can meet；
(6) after mixing by Dendrobidium huoshanness juice obtained in extracting solution obtained in step (2) and step (3), centrifugation
Removal crude fibre takes filtrate centrifuging and taking filtrate, wherein centrifugation step to use tube centrifuge, centrifuged with 12000r/min, managed
When formula centrifuge works, lower endfeed, lower end discharging discharges, centrifugation time is determined according to inlet amount, is gone as long as can meet immediately
Except the crude fibre in Dendrobidium huoshanness juice；
(7) 5 parts of edible gelatins, 10 parts of l-Alanine are mixed with the eluent in step (5), the filtrate in step (6),
It carries out negative pressure and is concentrated into density to be 1.35g/mL, condition of negative pressure is：Negative pressure -0.08Mpa, temperature are 60 DEG C；
(8) before waiting for the concentrate cooling in step (7), the lavender Ultramicro-powder obtained in step (3) is added, after cooling i.e.
For Dendrobidium huoshanness baste.
The above is only the preferred embodiment of the present invention, protection scope of the present invention is not limited in above-described embodiment, with
The various process programs of present inventive concept indifference are within the scope of the invention.
Claims (10)
1. a kind of Dendrobidium huoshanness baste for health care, it is characterised in that：It is made of the raw material of following weight fraction：Huoshan stone
30-40 parts of dry measure used in former times, 1-5 parts of Salvia japonica, 5-10 parts of thyme, 5-10 parts of lavender, 15-20 parts of tealeaves, 20-25 parts of Radix Glycyrrhizae eat
1-5 parts of gelatin, 1-10 parts of l-Alanine.
2. the Dendrobidium huoshanness baste according to claim 1 for health care, it is characterised in that：It is described to be used for health care suddenly
Mountain stem of noble dendrobium baste, including following preparation process：
(1) Salvia japonica of above-mentioned parts by weight, thyme, Radix Glycyrrhizae, tealeaves are crushed to 50-70 mesh, it is spare；
(2) toward Salvia japonica, thyme, Radix Glycyrrhizae crushed material in suitable quantity of water is added, make solid-liquid ratio be 1:(9-11) carries out ultrasound and carries
It takes, extracting solution is made, it is spare；
(3) after Dendrobidium huoshanness and lavender being carried out steam sterilizing at a temperature of 110-120 DEG C, the ring in (- 30)-(- 25) DEG C
Under border, ultramicro grinding is carried out, Dendrobidium huoshanness juice and lavender Ultramicro-powder are respectively obtained；
(4) appropriate 70% ethyl alcohol is added in the tealeaves after crushing, it is 1 to make solid-liquid ratio:(10-15) carries out ultrasonic extraction, extraction
Temperature is 70-90 DEG C, and tea extract is made, spare；
(5) extracting solution obtained in step (4) is centrifuged, the supernatant of acquisition crosses polyamide chromatography column, using distilled water
Be eluted to it is colourless, then with 70% ethanol elution of pH8.5, until eluent meets FeCl3Until solution is non-discolouring, eluent is obtained；
(6) after mixing by Dendrobidium huoshanness juice obtained in extracting solution obtained in step (2) and step (3), centrifuging and taking filter
Liquid；
(7) eluent in the edible gelatin of above-mentioned parts by weight, l-Alanine and step (5), the filtrate in step (6) is mixed
It closes, carries out negative pressure concentration；
(8) the lavender Ultramicro-powder obtained in step (3) is added in the concentrate of step (7), is Dendrobidium huoshanness after cooling
Baste.
3. the Dendrobidium huoshanness baste according to claim 2 for health care, it is characterised in that：The step (2), (4)
In extraction time be 2-4 times.
4. the Dendrobidium huoshanness baste according to claim 2 for health care, it is characterised in that：In the step (3)
Lavender ultramicro grinding is to 400-600 mesh.
5. the Dendrobidium huoshanness baste according to claim 2 for health care, it is characterised in that：In the step (8)
Condition of negative pressure is：Negative pressure -0.08Mpa, temperature are 60 DEG C, and it is 0.98-1.35g/mL that negative pressure, which is concentrated into density,.
6. a kind of preparation method of Dendrobidium huoshanness baste for health care, it is characterised in that：Including following preparation process：
(1) 1-5 parts of Salvia japonicas, 5-10 parts of thymes, 20-25 portions of Radix Glycyrrhizaes, 15-20 portions of tealeaves are crushed to 50-70 mesh, it is standby
With；
(2) toward Salvia japonica, thyme, Radix Glycyrrhizae crushed material in suitable quantity of water is added, make solid-liquid ratio be 1:(9-11) carries out ultrasound and carries
It takes, extracting solution is made, it is spare；
(3) after 30-40 parts of Dendrobidium huoshanness and 5-10 portions of lavenders being carried out steam sterilizing at a temperature of 110-120 DEG C, in (-
30) in the environment of-(- 25) DEG C, ultramicro grinding is carried out, Dendrobidium huoshanness juice and lavender Ultramicro-powder are respectively obtained；
(4) ethanol in proper amount is added in the tealeaves after crushing, it is 1 to make solid-liquid ratio:(10-15) carries out ultrasonic extraction, Extracting temperature
It is 70-90 DEG C, tea extract is made, it is spare；
(5) extracting solution obtained in step (4) is centrifuged, the supernatant of acquisition crosses polyamide chromatography column, using distilled water
Be eluted to it is colourless, then with ethanol elution, until eluent meets FeCl3Until solution is non-discolouring, eluent is obtained；
(6) after mixing by Dendrobidium huoshanness juice obtained in extracting solution obtained in step (2) and step (3), centrifuging and taking filter
Liquid；
(7) 1-5 parts of edible gelatins, 1-10 parts of l-Alanine are mixed with the eluent in step (5), the filtrate in step (6),
Carry out negative pressure concentration；
(8) the lavender Ultramicro-powder obtained in step (3) is added in the concentrate of step (7), is Dendrobidium huoshanness after cooling
Baste.
7. the preparation method of the Dendrobidium huoshanness baste according to claim 6 for health care, it is characterised in that：The step
Suddenly the extraction time in (2), (4) is 2-4 times.
8. the preparation method of the Dendrobidium huoshanness baste according to claim 6 for health care, it is characterised in that：The step
Suddenly the lavender ultramicro grinding in (3) is to 400-600 mesh.
9. the preparation method of the Dendrobidium huoshanness baste according to claim 6 for health care, it is characterised in that：The step
Suddenly 70% ethyl alcohol is used in (4), and 70% ethyl alcohol of pH8.5 is used in step (5).
10. the preparation method of the Dendrobidium huoshanness baste according to claim 6 for health care, it is characterised in that：It is described
Condition of negative pressure in step (8) is：Negative pressure -0.08Mpa, temperature are 60 DEG C, and it is 0.98-1.35g/mL that negative pressure, which is concentrated into density,.
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| CN110432414A (en) * | 2019-08-26 | 2019-11-12 | 九仙尊霍山石斛股份有限公司 | A kind of Dendrobidium huoshanness combined beverage and preparation method thereof adjusting function of human body |
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