CN108587818B - Peony seed oil antibacterial skin care soap and preparation method thereof - Google Patents
Peony seed oil antibacterial skin care soap and preparation method thereof Download PDFInfo
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/02—Compositions of detergents based essentially on soap on alkali or ammonium soaps
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- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/48—Medical, disinfecting agents, disinfecting, antibacterial, germicidal or antimicrobial compositions
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/04—Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
- C11D9/22—Organic compounds, e.g. vitamins
- C11D9/30—Organic compounds, e.g. vitamins containing nitrogen
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/04—Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
- C11D9/22—Organic compounds, e.g. vitamins
- C11D9/34—Organic compounds, e.g. vitamins containing phosphorus
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/04—Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
- C11D9/22—Organic compounds, e.g. vitamins
- C11D9/38—Products in which the composition is not well defined
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Abstract
The invention discloses a peony seed oil bacteriostatic skin-care soap and a preparation method thereof, wherein the peony seed oil bacteriostatic skin-care soap is prepared from the following raw materials in parts by weight: 45-65 parts of peony seed oil, 3-8 parts of camellia oil, 1-5 parts of sweet almond oil, 6-10 parts of sodium hydroxide, 20-30 parts of water, 2-5 parts of honey, 3-8 parts of moutan bark extract, 0.01-0.05 part of chelating agent and 0.2-0.8 part of preservative. The peony seed oil antibacterial skin-care perfumed soap obtained by the preparation method of the peony seed oil antibacterial skin-care perfumed soap is rich in natural plant components, is mild in skin care, strong in cleaning power and good in antibacterial effect, is suitable for most people, is a safe and effective washing product, and is beneficial to environmental protection.
Description
Technical Field
The invention relates to the technical field of washing and caring products, and particularly relates to a peony seed oil antibacterial skin-care soap and a preparation method thereof.
Background
The soap is one of the most common and widely used washing products, belongs to the daily-life washing products, and the antibacterial soap is widely applied to daily life of people in recent years. The soap is prepared mainly by the steps of carrying out saponification reaction on animal and vegetable oil and alkaline substances such as sodium hydroxide under certain conditions, adding a certain amount of perfume and the like, and cooling. With the development of society, the improvement of living standard of people and the enhancement of health care consciousness of skin, the requirements of people on the soap are also increased year by year, and the soap is not a special product for young women at present and has no consumers for old people and babies.
The peony seed oil is rich in VA, VE, nicotinic acid, carotene and unsaturated fatty acid, has excellent nutrition nursing effect on skin, can obviously improve the circulation function of skin epidermal cells, delays skin aging, has the functions of resisting wrinkles, preserving moisture and whitening, has smooth and relaxed skin after use, and has certain treatment effects on chloasma, skin aging wrinkles, skin cutin hardening and peeling, skin chapping and skin dryness, and the contained α -linolenic acid has the inhibition effect on anaphylactic reaction and inflammation.
In the prior art, the peony seed oil is less developed for daily chemicals, particularly for toilet soap. The peony seed oil is used for the perfumed soap, is rich in natural components, is mild in skin care, has no residue, and cannot pollute the environment.
Disclosure of Invention
Aiming at the defects in the prior art, the invention aims to solve the technical problem of providing the peony seed oil antibacterial skin-care perfumed soap and the preparation method thereof.
The purpose of the invention is realized by the following technical scheme:
the peony seed oil bacteriostatic skin-care perfumed soap is prepared from the following raw materials in parts by weight: 45-65 parts of peony seed oil, 3-8 parts of camellia oil, 1-5 parts of sweet almond oil, 6-10 parts of sodium hydroxide, 20-30 parts of water, 2-5 parts of honey, 3-8 parts of moutan bark extract, 0.01-0.05 part of chelating agent and 0.2-0.8 part of preservative.
The chelating agent is sodium phytate and/or tetrasodium iminodisuccinate.
Preferably, the chelating agent is a mixture of 25 to 35 wt% sodium phytate and 65 to 75 wt% tetrasodium iminodisuccinate.
The preservative is mulberry leaf extract and/or gentiana macrophylla extract.
Preferably, the preservative is a mixture of 50-70 wt% of mulberry leaf extract and 30-50 wt% of gentiana macrophylla extract.
The moutan bark extract is prepared by the following method: crushing tree peony bark, sieving with a 40-mesh sieve to obtain tree peony bark powder, mixing 80-120g of tree peony bark powder with 1000-1500mL of water, standing at 20-30 ℃ for 20-40 minutes, carrying out ultrasonic treatment for 35-55 minutes, and filtering with 300-mesh filter cloth to obtain filtrate and filter residue; mixing the filter residue with 800-: the ultrasonic temperature is 60-70 ℃, the ultrasonic power is 100-.
Preferably, the moutan bark extract is prepared by the following method: crushing tree peony bark, sieving with a 40-mesh sieve to obtain tree peony bark powder, mixing 80-120g of tree peony bark powder with 1000-1500mL of water, standing at 20-30 ℃ for 20-40 minutes, carrying out ultrasonic treatment for 20-30 minutes, carrying out ultrasonic treatment for 10-20 minutes after 1-3 minutes, carrying out ultrasonic treatment for 5-10 minutes after 1-3 minutes again, and filtering with 300-mesh filter cloth to obtain filtrate and filter residue; mixing the filter residue with 800-: the ultrasonic temperature is 60-70 ℃, the ultrasonic power is 100-.
The mulberry leaf extract is prepared by the following method: crushing mulberry leaves, sieving by a 40-mesh sieve to obtain mulberry leaf powder, mixing the mulberry leaf powder 60-100g with 800-plus-1200 mL of water, carrying out water extraction at 80-90 ℃ for 60-90 minutes, filtering by 300-mesh filter cloth to obtain filtrate and filter residue, adding 1000mL of 600-plus-600 mL of water into the filter residue, carrying out water extraction at 80-90 ℃ for 40-60 minutes, filtering by 300-mesh filter cloth to obtain filtrate, combining the two filtrates, and concentrating under reduced pressure until the density at 65 ℃ is 1.10-1.15g/mL to obtain the mulberry leaf extract.
The gentiana macrophylla extract is prepared by the following method: crushing the gentiana macrophylla, sieving by a 40-mesh sieve to obtain gentiana macrophylla powder, mixing 60-100g of gentiana macrophylla powder with 1200mL of 800-plus-one water, adding 0.2-0.6g of complex enzyme, stirring at 40-50 ℃ for 2-4 hours at 300 revolutions per minute, continuing stirring at 90-98 ℃ for 40-60 minutes, filtering by 300-mesh filter cloth to obtain filtrate and filter residue, adding 1000mL of ethanol water solution with volume fraction of 70-80% into the filter residue, reflux-extracting at 60-70 ℃ for 1-2 hours, filtering by 300-mesh filter cloth to obtain filtrate, combining the two filtrates, concentrating under reduced pressure to 65 ℃ with density of 1.10-1.15g/mL to obtain the gentiana macrophylla extract.
Preferably, the gentiana macrophylla extract is prepared by the following method: crushing the gentiana macrophylla, sieving by a 40-mesh sieve to obtain gentiana macrophylla powder, mixing 60-100g of gentiana macrophylla powder with 1200mL of 800-plus water, adding 0.2-0.6g of complex enzyme and 1-3g of citric acid, stirring at 40-50 ℃ for 2-4 hours at 300 turns/min, continuing stirring at 90-98 ℃ for 40-60 minutes, filtering by 300-mesh filter cloth to obtain filtrate and filter residue, adding 1000mL of ethanol aqueous solution with volume fraction of 70-80% into the filter residue, extracting at 60-70 ℃ for 1-2 hours under reflux by the filter cloth, filtering by 300-mesh filter cloth to obtain filtrate, combining the two filtrates, and concentrating under reduced pressure to 65 ℃ with density of 1.10-1.15g/mL to obtain the gentiana macrophylla extract.
The compound enzyme is a mixture of 60-70 wt% of cellulase and 30-40 wt% of pectinase.
The preparation method of the peony seed oil bacteriostatic skin-care perfumed soap comprises the following steps:
(1) mixing sodium hydroxide and water, and stirring at 40-50 ℃ at 300 revolutions per minute of 100-;
(2) adding peony seed oil, camellia oil and sweet almond oil into a reaction kettle, stirring and heating to 40-50 ℃ to obtain an oil phase, pouring alkali liquor into the oil phase while stirring at 200-400 rpm, and continuously stirring for 30-40 minutes to obtain a saponification solution;
(3) adding Mel, cortex moutan extract, chelating agent, and antiseptic into the saponification solution, stirring at 40-50 deg.C at 200 rpm and 100-;
(4) pouring the mixed soap liquid into a mould, sealing, standing for 24-48 hours at 30-40 ℃, demoulding, and drying for 4-8 hours at 40-50 ℃ to obtain the peony seed oil antibacterial skin-care soap.
The peony seed oil antibacterial skin-care perfumed soap obtained by the preparation method of the peony seed oil antibacterial skin-care perfumed soap is rich in natural plant components, is mild in skin care, strong in cleaning power and good in antibacterial effect, is suitable for most people, is a safe and effective washing product, and is beneficial to environmental protection.
Detailed Description
In the present invention, all the equipment and materials are commercially available or commonly used in the art, and the methods in the following examples are conventional in the art unless otherwise specified.
Tetrasodium iminodisuccinate, CAS No.: 144538-83-0. The method adopts Shandong far-reaching energy chemical industry limited company to provide iminodisuccinic acid with the model number: IDS Na 4.
Sodium phytate, CAS number: 14306-25-3, provided by Henan Shihe chemical Co., Ltd, and the product number: SP881003
Pectinase, provided by Wuhan Baixing Biotechnology Co., Ltd, and the enzyme activity is 3 ten thousand U/g.
The cellulase is provided by Wuhan Baixing biological science and technology limited company, and the enzyme activity is 3 ten thousand U/g.
Peony seed oil, available from Lizhong Zijiyuan Biotech Co., Ltd.
Camellia oil, available from Lizhong Zi Jianyuan Biotech Co., Ltd.
Sweet almond oil, available from Nethereto Lijianyuan biotechnology limited.
Sodium hydroxide, available from Beijing Tianyukang chemical engineering science and technology Ltd.
The Mel is acacia Mel provided by Shanxi Shengkang bee industry Co.
Cortex moutan is dried root bark of Paeonia suffruticosa Andr. Cissant Biotech, Inc., Mr. of milli-State.
Folium Mori is dry leaf of Morus alba L. Cissant Biotech, Inc., Mr. of milli-State.
The Gentiana macrophylla is dried root of Gentiana macrophylla pall.of Gentiana macrophylla of Gentianaceae, Gentiana straminea Maxim.of Gentiana straminea, Gentiana macrophylla Gentiana crassilis Duthie ex Burk. or Gentiana macrophylla Dahurica Fisch. Xiyao county Xiangguang medicinal materials, Inc.
Citric acid, available from Shanghai Michelin Biochemical technology, Inc., product number: C805019.
and (3) testing the antibacterial effect: 5g of peony seed oil bacteriostatic skin-care soap is mixed with 40g of water, and the mixture is stirred at the temperature of 45 ℃ at 200 revolutions per minute until the soap is completely dissolved, and the weight ratio of the mixture to the water is 1 g: 8mL of the sample solution was tested for its bacteriostatic effect against E.coli (ATCC 25922) and Candida albicans (ATCC10231) by the method of the bacteriostatic test in example 6 of application No. 201511016139.6.
And (3) testing foaming force: dissolving 1g of the peony seed oil bacteriostatic skin-care perfumed soap in 99g of water to prepare a 1% solution, and testing the foaming power of the peony seed oil bacteriostatic skin-care perfumed soap in 5.5 parts of QB/T2486-2008 laundry soap at 25 ℃.
And (3) washing effect test: the peony seed oil bacteriostatic skin-care perfumed soap is prepared into a 1000ppm solution, and the solution is prepared according to application research of anti-redeposition agents in laundry detergent, such as the admitted sister, the Xijiu and the Xijiu, daily chemical science 2011, 34 (10): the method in 21 was tested to test the whiteness of the white cotton knitted fabric and calculate the whiteness maintenance value.
Example 1
The peony seed oil bacteriostatic skin-care perfumed soap comprises the following raw materials in parts by weight: 55 parts of peony seed oil, 4 parts of camellia oil, 3 parts of sweet almond oil, 9 parts of sodium hydroxide, 25 parts of water, 3 parts of honey, 6 parts of tree peony bark extract, 0.03 part of chelating agent and 0.5 part of preservative.
The chelating agent is sodium phytate.
The preservative is mulberry leaf extract.
The moutan bark extract is prepared by the following method: crushing tree peony bark, sieving with a 40-mesh sieve to obtain tree peony bark powder, mixing 100g of tree peony bark powder with 1200mL of water, standing at 25 ℃ for 30 minutes, performing ultrasonic treatment for 48 minutes, and filtering with 300-mesh filter cloth to obtain filtrate and filter residue; mixing the filter residue with 1000mL of ethanol water solution with volume fraction of 75%, reflux-extracting at 65 ℃ for 3 hours, filtering with 300-mesh filter cloth to obtain filtrate, combining the two filtrates, and concentrating under reduced pressure at 0.02MPa and 65 ℃ to a density of 1.08g/mL at 65 ℃ to obtain the moutan bark extract, wherein the ultrasonic treatment conditions are as follows: the ultrasonic temperature is 65 ℃, the ultrasonic power is 150W, and the ultrasonic frequency is 20 kHz.
The mulberry leaf extract is prepared by the following method: crushing mulberry leaves, sieving with a 40-mesh sieve to obtain mulberry leaf powder, mixing 80g of the mulberry leaf powder with 1000mL of water, carrying out water extraction at 85 ℃ for 80 minutes, filtering with 300-mesh filter cloth to obtain filtrate and filter residue, adding 800mL of water into the filter residue, carrying out water extraction at 85 ℃ for 50 minutes, filtering with 300-mesh filter cloth to obtain filtrate, combining the two filtrates, and carrying out reduced pressure concentration at the pressure of 0.02MPa and the temperature of 65 ℃ until the density of 65 ℃ is 1.12g/mL to obtain the mulberry leaf extract.
The preparation method of the peony seed oil bacteriostatic skin-care perfumed soap comprises the following steps:
(1) mixing sodium hydroxide and water, and stirring at 45 ℃ at 200 revolutions per minute until the sodium hydroxide is completely dissolved to obtain an alkali liquor;
(2) adding peony seed oil, camellia oil and sweet almond oil into a reaction kettle, stirring at 300 revolutions per minute, heating to 45 ℃ to obtain an oil phase, pouring alkali liquor into the oil phase while stirring at 300 revolutions per minute, and continuously stirring at 300 revolutions per minute for 35 minutes to obtain a saponified solution;
(3) adding Mel, cortex moutan extract, chelating agent, and antiseptic into the saponified solution, stirring at 45 deg.C at 150 rpm for 15 min, and standing for 6 min to obtain mixed soap solution;
(4) pouring the mixed soap liquid into a mould, sealing, standing for 36 hours at 35 ℃, demoulding, and drying for 6 hours at 45 ℃ to obtain the peony seed oil antibacterial skin-care soap.
Comparative example 1
The peony seed oil bacteriostatic skin-care perfumed soap comprises the following raw materials in parts by weight: 55 parts of peony seed oil, 4 parts of camellia oil, 3 parts of sweet almond oil, 9 parts of sodium hydroxide, 25 parts of water, 3 parts of honey, 0.03 part of chelating agent and 0.5 part of preservative.
The chelating agent is sodium phytate.
The preservative is mulberry leaf extract.
The mulberry leaf extract is prepared by the following method: crushing mulberry leaves, sieving with a 40-mesh sieve to obtain mulberry leaf powder, mixing 80g of the mulberry leaf powder with 1000mL of water, carrying out water extraction at 85 ℃ for 80 minutes, filtering with 300-mesh filter cloth to obtain filtrate and filter residue, adding 800mL of water into the filter residue, carrying out water extraction at 85 ℃ for 50 minutes, filtering with 300-mesh filter cloth to obtain filtrate, combining the two filtrates, and carrying out reduced pressure concentration at the pressure of 0.02MPa and the temperature of 65 ℃ until the density of 65 ℃ is 1.12g/mL to obtain the mulberry leaf extract.
The preparation method of the peony seed oil bacteriostatic skin-care perfumed soap comprises the following steps:
(1) mixing sodium hydroxide and water, and stirring at 45 ℃ at 200 revolutions per minute until the sodium hydroxide is completely dissolved to obtain an alkali liquor;
(2) adding peony seed oil, camellia oil and sweet almond oil into a reaction kettle, stirring at 300 revolutions per minute, heating to 45 ℃ to obtain an oil phase, pouring alkali liquor into the oil phase while stirring at 300 revolutions per minute, and continuously stirring at 300 revolutions per minute for 35 minutes to obtain a saponified solution;
(3) adding Mel, chelating agent, and antiseptic into the saponified solution, stirring at 45 deg.C at 150 rpm for 15 min, and standing for 6 min to obtain mixed soap solution;
(4) pouring the mixed soap liquid into a mould, sealing, standing for 36 hours at 35 ℃, demoulding, and drying for 6 hours at 45 ℃ to obtain the peony seed oil antibacterial skin-care soap.
Example 2
The peony seed oil bacteriostatic skin-care perfumed soap comprises the following raw materials in parts by weight: 55 parts of peony seed oil, 4 parts of camellia oil, 3 parts of sweet almond oil, 9 parts of sodium hydroxide, 25 parts of water, 3 parts of honey, 6 parts of tree peony bark extract, 0.03 part of chelating agent and 0.5 part of preservative.
The chelating agent is sodium phytate.
The preservative is mulberry leaf extract.
The moutan bark extract is prepared by the following method: crushing tree peony bark, sieving with a 40-mesh sieve to obtain tree peony bark powder, mixing 100g of tree peony bark powder with 1200mL of water, standing at 25 ℃ for 30 minutes, carrying out ultrasonic treatment for 25 minutes, carrying out ultrasonic treatment for 15 minutes after 2 minutes, carrying out ultrasonic treatment for 8 minutes after 2 minutes, and filtering with 300-mesh filter cloth to obtain filtrate and filter residue; mixing the filter residue with 1000mL of ethanol water solution with volume fraction of 75%, reflux-extracting at 65 ℃ for 3 hours, filtering with 300-mesh filter cloth to obtain filtrate, combining the two filtrates, and concentrating under reduced pressure at 0.02MPa and 65 ℃ to a density of 1.08g/mL at 65 ℃ to obtain the moutan bark extract, wherein the ultrasonic treatment conditions are as follows: the ultrasonic temperature is 65 ℃, the ultrasonic power is 150W, and the ultrasonic frequency is 20 kHz.
The mulberry leaf extract is prepared by the following method: crushing mulberry leaves, sieving with a 40-mesh sieve to obtain mulberry leaf powder, mixing 80g of the mulberry leaf powder with 1000mL of water, carrying out water extraction at 85 ℃ for 80 minutes, filtering with 300-mesh filter cloth to obtain filtrate and filter residue, adding 800mL of water into the filter residue, carrying out water extraction at 85 ℃ for 50 minutes, filtering with 300-mesh filter cloth to obtain filtrate, combining the two filtrates, and carrying out reduced pressure concentration at the pressure of 0.02MPa and the temperature of 65 ℃ until the density of 65 ℃ is 1.12g/mL to obtain the mulberry leaf extract.
The preparation method of the peony seed oil bacteriostatic skin-care perfumed soap comprises the following steps:
(1) mixing sodium hydroxide and water, and stirring at 45 ℃ at 200 revolutions per minute until the sodium hydroxide is completely dissolved to obtain an alkali liquor;
(2) adding peony seed oil, camellia oil and sweet almond oil into a reaction kettle, stirring at 300 revolutions per minute, heating to 45 ℃ to obtain an oil phase, pouring alkali liquor into the oil phase while stirring at 300 revolutions per minute, and continuously stirring at 300 revolutions per minute for 35 minutes to obtain a saponified solution;
(3) adding Mel, cortex moutan extract, chelating agent, and antiseptic into the saponified solution, stirring at 45 deg.C at 150 rpm for 15 min, and standing for 6 min to obtain mixed soap solution;
(4) pouring the mixed soap liquid into a mould, sealing, standing for 36 hours at 35 ℃, demoulding, and drying for 6 hours at 45 ℃ to obtain the peony seed oil antibacterial skin-care soap.
Example 3
The peony seed oil bacteriostatic skin-care perfumed soap comprises the following raw materials in parts by weight: 55 parts of peony seed oil, 4 parts of camellia oil, 3 parts of sweet almond oil, 9 parts of sodium hydroxide, 25 parts of water, 3 parts of honey, 6 parts of tree peony bark extract, 0.03 part of chelating agent and 0.5 part of preservative.
The chelating agent is tetrasodium iminodisuccinate.
The preservative is mulberry leaf extract.
The moutan bark extract is prepared by the following method: crushing tree peony bark, sieving with a 40-mesh sieve to obtain tree peony bark powder, mixing 100g of tree peony bark powder with 1200mL of water, standing at 25 ℃ for 30 minutes, carrying out ultrasonic treatment for 25 minutes, carrying out ultrasonic treatment for 15 minutes after 2 minutes, carrying out ultrasonic treatment for 8 minutes after 2 minutes, and filtering with 300-mesh filter cloth to obtain filtrate and filter residue; mixing the filter residue with 1000mL of ethanol water solution with volume fraction of 75%, reflux-extracting at 65 ℃ for 3 hours, filtering with 300-mesh filter cloth to obtain filtrate, combining the two filtrates, and concentrating under reduced pressure at 0.02MPa and 65 ℃ to a density of 1.08g/mL at 65 ℃ to obtain the moutan bark extract, wherein the ultrasonic treatment conditions are as follows: the ultrasonic temperature is 65 ℃, the ultrasonic power is 150W, and the ultrasonic frequency is 20 kHz.
The mulberry leaf extract is prepared by the following method: crushing mulberry leaves, sieving with a 40-mesh sieve to obtain mulberry leaf powder, mixing 80g of the mulberry leaf powder with 1000mL of water, carrying out water extraction at 85 ℃ for 80 minutes, filtering with 300-mesh filter cloth to obtain filtrate and filter residue, adding 800mL of water into the filter residue, carrying out water extraction at 85 ℃ for 50 minutes, filtering with 300-mesh filter cloth to obtain filtrate, combining the two filtrates, and carrying out reduced pressure concentration at the pressure of 0.02MPa and the temperature of 65 ℃ until the density of 65 ℃ is 1.12g/mL to obtain the mulberry leaf extract.
The preparation method of the peony seed oil bacteriostatic skin-care perfumed soap comprises the following steps:
(1) mixing sodium hydroxide and water, and stirring at 45 ℃ at 200 revolutions per minute until the sodium hydroxide is completely dissolved to obtain an alkali liquor;
(2) adding peony seed oil, camellia oil and sweet almond oil into a reaction kettle, stirring at 300 revolutions per minute, heating to 45 ℃ to obtain an oil phase, pouring alkali liquor into the oil phase while stirring at 300 revolutions per minute, and continuously stirring at 300 revolutions per minute for 35 minutes to obtain a saponified solution;
(3) adding Mel, cortex moutan extract, chelating agent, and antiseptic into the saponified solution, stirring at 45 deg.C at 150 rpm for 15 min, and standing for 6 min to obtain mixed soap solution;
(4) pouring the mixed soap liquid into a mould, sealing, standing for 36 hours at 35 ℃, demoulding, and drying for 6 hours at 45 ℃ to obtain the peony seed oil antibacterial skin-care soap.
Example 4
The peony seed oil bacteriostatic skin-care perfumed soap comprises the following raw materials in parts by weight: 55 parts of peony seed oil, 4 parts of camellia oil, 3 parts of sweet almond oil, 9 parts of sodium hydroxide, 25 parts of water, 3 parts of honey, 6 parts of tree peony bark extract, 0.03 part of chelating agent and 0.5 part of preservative.
The chelating agent is a mixture of 30 wt% of sodium phytate and 70 wt% of imino disuccinic acid tetrasodium.
The preservative is mulberry leaf extract.
The moutan bark extract is prepared by the following method: crushing tree peony bark, sieving with a 40-mesh sieve to obtain tree peony bark powder, mixing 100g of tree peony bark powder with 1200mL of water, standing at 25 ℃ for 30 minutes, carrying out ultrasonic treatment for 25 minutes, carrying out ultrasonic treatment for 15 minutes after 2 minutes, carrying out ultrasonic treatment for 8 minutes after 2 minutes, and filtering with 300-mesh filter cloth to obtain filtrate and filter residue; mixing the filter residue with 1000mL of ethanol water solution with volume fraction of 75%, reflux-extracting at 65 ℃ for 3 hours, filtering with 300-mesh filter cloth to obtain filtrate, combining the two filtrates, and concentrating under reduced pressure at 0.02MPa and 65 ℃ to a density of 1.08g/mL at 65 ℃ to obtain the moutan bark extract, wherein the ultrasonic treatment conditions are as follows: the ultrasonic temperature is 65 ℃, the ultrasonic power is 150W, and the ultrasonic frequency is 20 kHz.
The mulberry leaf extract is prepared by the following method: crushing mulberry leaves, sieving with a 40-mesh sieve to obtain mulberry leaf powder, mixing 80g of the mulberry leaf powder with 1000mL of water, carrying out water extraction at 85 ℃ for 80 minutes, filtering with 300-mesh filter cloth to obtain filtrate and filter residue, adding 800mL of water into the filter residue, carrying out water extraction at 85 ℃ for 50 minutes, filtering with 300-mesh filter cloth to obtain filtrate, combining the two filtrates, and carrying out reduced pressure concentration at the pressure of 0.02MPa and the temperature of 65 ℃ until the density of 65 ℃ is 1.12g/mL to obtain the mulberry leaf extract.
The preparation method of the peony seed oil bacteriostatic skin-care perfumed soap comprises the following steps:
(1) mixing sodium hydroxide and water, and stirring at 45 ℃ at 200 revolutions per minute until the sodium hydroxide is completely dissolved to obtain an alkali liquor;
(2) adding peony seed oil, camellia oil and sweet almond oil into a reaction kettle, stirring at 300 revolutions per minute, heating to 45 ℃ to obtain an oil phase, pouring alkali liquor into the oil phase while stirring at 300 revolutions per minute, and continuously stirring at 300 revolutions per minute for 35 minutes to obtain a saponified solution;
(3) adding Mel, cortex moutan extract, chelating agent, and antiseptic into the saponified solution, stirring at 45 deg.C at 150 rpm for 15 min, and standing for 6 min to obtain mixed soap solution;
(4) pouring the mixed soap liquid into a mould, sealing, standing for 36 hours at 35 ℃, demoulding, and drying for 6 hours at 45 ℃ to obtain the peony seed oil antibacterial skin-care soap.
Example 5
The peony seed oil bacteriostatic skin-care perfumed soap comprises the following raw materials in parts by weight: 55 parts of peony seed oil, 4 parts of camellia oil, 3 parts of sweet almond oil, 9 parts of sodium hydroxide, 25 parts of water, 3 parts of honey, 6 parts of tree peony bark extract, 0.03 part of chelating agent and 0.5 part of preservative.
The chelating agent is a mixture of 30 wt% of sodium phytate and 70 wt% of imino disuccinic acid tetrasodium.
The antiseptic is radix Gentianae Marcrophyllae extract.
The moutan bark extract is prepared by the following method: crushing tree peony bark, sieving with a 40-mesh sieve to obtain tree peony bark powder, mixing 100g of tree peony bark powder with 1200mL of water, standing at 25 ℃ for 30 minutes, carrying out ultrasonic treatment for 25 minutes, carrying out ultrasonic treatment for 15 minutes after 2 minutes, carrying out ultrasonic treatment for 8 minutes after 2 minutes, and filtering with 300-mesh filter cloth to obtain filtrate and filter residue; mixing the filter residue with 1000mL of ethanol water solution with volume fraction of 75%, reflux-extracting at 65 ℃ for 3 hours, filtering with 300-mesh filter cloth to obtain filtrate, combining the two filtrates, and concentrating under reduced pressure at 0.02MPa and 65 ℃ to a density of 1.08g/mL at 65 ℃ to obtain the moutan bark extract, wherein the ultrasonic treatment conditions are as follows: the ultrasonic temperature is 65 ℃, the ultrasonic power is 150W, and the ultrasonic frequency is 20 kHz.
The gentiana macrophylla extract is prepared by the following method: crushing the gentiana macrophylla, sieving by a 40-mesh sieve to obtain gentiana macrophylla powder, mixing 80g of gentiana macrophylla powder with 1000mL of water, adding 0.4g of complex enzyme, stirring at 45 ℃ for 3 hours at 200 rpm, continuing stirring at 96 ℃ for 50 minutes, filtering by a 300-mesh filter cloth to obtain filtrate and filter residue, adding 800mL of 75 volume percent ethanol aqueous solution into the filter residue, carrying out reflux extraction at 65 ℃ for 1.5 hours, filtering by a 300-mesh filter cloth to obtain filtrate, combining the two filtrates, and concentrating under reduced pressure at 0.02MPa and 65 ℃ until the density of 65 ℃ is 1.12g/mL to obtain the gentiana macrophylla extract.
The compound enzyme is a mixture of 65 wt% of cellulase and 35 wt% of pectinase.
The preparation method of the peony seed oil bacteriostatic skin-care perfumed soap comprises the following steps:
(1) mixing sodium hydroxide and water, and stirring at 45 ℃ at 200 revolutions per minute until the sodium hydroxide is completely dissolved to obtain an alkali liquor;
(2) adding peony seed oil, camellia oil and sweet almond oil into a reaction kettle, stirring at 300 revolutions per minute, heating to 45 ℃ to obtain an oil phase, pouring alkali liquor into the oil phase while stirring at 300 revolutions per minute, and continuously stirring at 300 revolutions per minute for 35 minutes to obtain a saponified solution;
(3) adding Mel, cortex moutan extract, chelating agent, and antiseptic into the saponified solution, stirring at 45 deg.C at 150 rpm for 15 min, and standing for 6 min to obtain mixed soap solution;
(4) pouring the mixed soap liquid into a mould, sealing, standing for 36 hours at 35 ℃, demoulding, and drying for 6 hours at 45 ℃ to obtain the peony seed oil antibacterial skin-care soap.
Example 6
The peony seed oil bacteriostatic skin-care perfumed soap comprises the following raw materials in parts by weight: 55 parts of peony seed oil, 4 parts of camellia oil, 3 parts of sweet almond oil, 9 parts of sodium hydroxide, 25 parts of water, 3 parts of honey, 6 parts of tree peony bark extract, 0.03 part of chelating agent and 0.5 part of preservative.
The chelating agent is a mixture of 30 wt% of sodium phytate and 70 wt% of imino disuccinic acid tetrasodium.
The antiseptic is radix Gentianae Marcrophyllae extract.
The moutan bark extract is prepared by the following method: crushing tree peony bark, sieving with a 40-mesh sieve to obtain tree peony bark powder, mixing 100g of tree peony bark powder with 1200mL of water, standing at 25 ℃ for 30 minutes, carrying out ultrasonic treatment for 25 minutes, carrying out ultrasonic treatment for 15 minutes after 2 minutes, carrying out ultrasonic treatment for 8 minutes after 2 minutes, and filtering with 300-mesh filter cloth to obtain filtrate and filter residue; mixing the filter residue with 1000mL of ethanol water solution with volume fraction of 75%, reflux-extracting at 65 ℃ for 3 hours, filtering with 300-mesh filter cloth to obtain filtrate, combining the two filtrates, and concentrating under reduced pressure at 0.02MPa and 65 ℃ to a density of 1.08g/mL at 65 ℃ to obtain the moutan bark extract, wherein the ultrasonic treatment conditions are as follows: the ultrasonic temperature is 65 ℃, the ultrasonic power is 150W, and the ultrasonic frequency is 20 kHz.
The gentiana macrophylla extract is prepared by the following method: crushing gentiana macrophylla, sieving by a 40-mesh sieve to obtain gentiana macrophylla powder, mixing 80g of gentiana macrophylla powder with 1000mL of water, adding 0.4g of complex enzyme and 2g of citric acid, stirring at 45 ℃ at 200 rpm for 3 hours, continuing stirring at 96 ℃ for 50 minutes, filtering by a 300-mesh filter cloth to obtain filtrate and filter residue, adding 800mL of 75 volume percent ethanol aqueous solution into the filter residue, reflux-extracting at 65 ℃ for 1.5 hours, filtering by a 300-mesh filter cloth to obtain filtrate, combining the two filtrates, and concentrating under reduced pressure at 0.02MPa and 65 ℃ until the density of 65 ℃ is 1.12g/mL to obtain the gentiana macrophylla extract.
The compound enzyme is a mixture of 65 wt% of cellulase and 35 wt% of pectinase.
The preparation method of the peony seed oil bacteriostatic skin-care perfumed soap comprises the following steps:
(1) mixing sodium hydroxide and water, and stirring at 45 ℃ at 200 revolutions per minute until the sodium hydroxide is completely dissolved to obtain an alkali liquor;
(2) adding peony seed oil, camellia oil and sweet almond oil into a reaction kettle, stirring at 300 revolutions per minute, heating to 45 ℃ to obtain an oil phase, pouring alkali liquor into the oil phase while stirring at 300 revolutions per minute, and continuously stirring at 300 revolutions per minute for 35 minutes to obtain a saponified solution;
(3) adding Mel, cortex moutan extract, chelating agent, and antiseptic into the saponified solution, stirring at 45 deg.C at 150 rpm for 15 min, and standing for 6 min to obtain mixed soap solution;
(4) pouring the mixed soap liquid into a mould, sealing, standing for 36 hours at 35 ℃, demoulding, and drying for 6 hours at 45 ℃ to obtain the peony seed oil antibacterial skin-care soap.
Example 7
The peony seed oil bacteriostatic skin-care perfumed soap comprises the following raw materials in parts by weight: 55 parts of peony seed oil, 4 parts of camellia oil, 3 parts of sweet almond oil, 9 parts of sodium hydroxide, 25 parts of water, 3 parts of honey, 6 parts of tree peony bark extract, 0.03 part of chelating agent and 0.5 part of preservative.
The chelating agent is a mixture of 30 wt% of sodium phytate and 70 wt% of imino disuccinic acid tetrasodium.
The preservative is a mixture of 60 wt% of mulberry leaf extract and 40 wt% of gentiana macrophylla extract.
The moutan bark extract is prepared by the following method: crushing tree peony bark, sieving with a 40-mesh sieve to obtain tree peony bark powder, mixing 100g of tree peony bark powder with 1200mL of water, standing at 25 ℃ for 30 minutes, carrying out ultrasonic treatment for 25 minutes, carrying out ultrasonic treatment for 15 minutes after 2 minutes, carrying out ultrasonic treatment for 8 minutes after 2 minutes, and filtering with 300-mesh filter cloth to obtain filtrate and filter residue; mixing the filter residue with 1000mL of ethanol water solution with volume fraction of 75%, reflux-extracting at 65 ℃ for 3 hours, filtering with 300-mesh filter cloth to obtain filtrate, combining the two filtrates, and concentrating under reduced pressure at 0.02MPa and 65 ℃ to a density of 1.08g/mL at 65 ℃ to obtain the moutan bark extract, wherein the ultrasonic treatment conditions are as follows: the ultrasonic temperature is 65 ℃, the ultrasonic power is 150W, and the ultrasonic frequency is 20 kHz.
The mulberry leaf extract is prepared by the following method: crushing mulberry leaves, sieving with a 40-mesh sieve to obtain mulberry leaf powder, mixing 80g of the mulberry leaf powder with 1000mL of water, carrying out water extraction at 85 ℃ for 80 minutes, filtering with 300-mesh filter cloth to obtain filtrate and filter residue, adding 800mL of water into the filter residue, carrying out water extraction at 85 ℃ for 50 minutes, filtering with 300-mesh filter cloth to obtain filtrate, combining the two filtrates, and carrying out reduced pressure concentration at the pressure of 0.02MPa and the temperature of 65 ℃ until the density of 65 ℃ is 1.12g/mL to obtain the mulberry leaf extract.
The gentiana macrophylla extract is prepared by the following method: crushing gentiana macrophylla, sieving by a 40-mesh sieve to obtain gentiana macrophylla powder, mixing 80g of gentiana macrophylla powder with 1000mL of water, adding 0.4g of complex enzyme and 2g of citric acid, stirring at 45 ℃ at 200 rpm for 3 hours, continuing stirring at 96 ℃ for 50 minutes, filtering by a 300-mesh filter cloth to obtain filtrate and filter residue, adding 800mL of 75 volume percent ethanol aqueous solution into the filter residue, reflux-extracting at 65 ℃ for 1.5 hours, filtering by a 300-mesh filter cloth to obtain filtrate, combining the two filtrates, and concentrating under reduced pressure at 0.02MPa and 65 ℃ until the density of 65 ℃ is 1.12g/mL to obtain the gentiana macrophylla extract.
The compound enzyme is a mixture of 65 wt% of cellulase and 35 wt% of pectinase.
The preparation method of the peony seed oil bacteriostatic skin-care perfumed soap comprises the following steps:
(1) mixing sodium hydroxide and water, and stirring at 45 ℃ at 200 revolutions per minute until the sodium hydroxide is completely dissolved to obtain an alkali liquor;
(2) adding peony seed oil, camellia oil and sweet almond oil into a reaction kettle, stirring at 300 revolutions per minute, heating to 45 ℃ to obtain an oil phase, pouring alkali liquor into the oil phase while stirring at 300 revolutions per minute, and continuously stirring at 300 revolutions per minute for 35 minutes to obtain a saponified solution;
(3) adding Mel, cortex moutan extract, chelating agent, and antiseptic into the saponified solution, stirring at 45 deg.C at 150 rpm for 15 min, and standing for 6 min to obtain mixed soap solution;
(4) pouring the mixed soap liquid into a mould, sealing, standing for 36 hours at 35 ℃, demoulding, and drying for 6 hours at 45 ℃ to obtain the peony seed oil antibacterial skin-care soap.
The result of the bacteriostatic effect test is as follows: the diameter of an escherichia coli inhibition zone is 18.5mm, and the diameter of a candida albicans inhibition zone is 14.7 mm; foaming force test results: 5min foaming power 425 mL; washing effect test results: the whiteness retention value was 99.7%.
Test example 1
The bacteriostatic effect of the peony seed oil bacteriostatic skin-care soap prepared in the examples 1-6 and the comparative example 1 is tested, and the specific test result is shown in table 1.
Table 1 table of results of testing bacteriostatic effect of peony seed oil bacteriostatic skin-care toilet soap
Test example 2
The foaming power of the peony seed oil bacteriostatic skin-care toilet soap prepared in the examples 1-6 and the comparative example 1 is tested, and the specific test results are shown in table 2.
TABLE 2 foaming force test results table
| Foaming power, (5min)/mL | |
| Example 1 | 320 |
| Comparative example 1 | 310 |
| Example 2 | 342 |
| Example 3 | 350 |
| Example 4 | 385 |
| Example 5 | 372 |
| Example 6 | 390 |
Test example 3
The washing effects of the peony seed oil bacteriostatic skin-care toilet soap prepared in the examples 1-6 and the comparative example 1 are tested, and the specific test results are shown in table 3.
Table 3 table of washing effect test results
| Whiteness retention value,% | |
| Example 1 | 91.6 |
| Comparative example 1 | 90.7 |
| Example 2 | 92.4 |
| Example 3 | 93.2 |
| Example 4 | 95.6 |
| Example 5 | 95.1 |
| Example 6 | 95.8 |
In the embodiment 1, the peony bark extract is added, and the bacteriostatic effect, foaming power and washing effect of the peony seed oil bacteriostatic skin-care soap are superior to those of the comparative example 1. In the example 2, the peony seed oil bacteriostatic skin-care soap is extracted intermittently by ultrasonic, and the bacteriostatic effect, foaming power and washing effect of the peony seed oil bacteriostatic skin-care soap are superior to those of the example 1. Examples 2 to 4, which screen the types of the chelating agents, found that the embodiment 4 adopts the compound chelating agent with the optimal effect, because the compound chelating agent can significantly soften water quality, improve washing effect, and enhance the bacteriostatic effect of the soap. In the embodiment 6, citric acid with a certain mass is added in the extraction process of the gentiana macrophylla, and the effect is superior to that in the embodiment 5, because the citric acid is added, the compound enzyme can be in an acidic environment, the enzymolysis efficiency is improved, and meanwhile, the citric acid can chelate metal ions, so that the inhibition effect of the metal ions on the compound enzyme is reduced.
Claims (7)
1. The peony seed oil bacteriostatic skin-care perfumed soap is characterized by being prepared from the following raw materials in parts by weight: 45-65 parts of peony seed oil, 3-8 parts of camellia oil, 1-5 parts of sweet almond oil, 6-10 parts of sodium hydroxide, 20-30 parts of water, 2-5 parts of honey, 3-8 parts of moutan bark extract, 0.01-0.05 part of chelating agent and 0.2-0.8 part of preservative;
the chelating agent is a mixture of 25-35 wt% of sodium phytate and 65-75 wt% of tetrasodium iminodisuccinate;
the moutan bark extract is prepared by the following method: crushing tree peony bark, sieving with a 40-mesh sieve to obtain tree peony bark powder, mixing 80-120g of tree peony bark powder with 1000-1500mL of water, standing at 20-30 ℃ for 20-40 minutes, carrying out ultrasonic treatment for 20-30 minutes, carrying out ultrasonic treatment for 10-20 minutes after 1-3 minutes, carrying out ultrasonic treatment for 5-10 minutes after 1-3 minutes again, and filtering with 300-mesh filter cloth to obtain filtrate and filter residue; mixing the filter residue with 800-: the ultrasonic temperature is 60-70 ℃, the ultrasonic power is 100-.
2. The peony seed oil bacteriostatic skin-care perfumed soap as claimed in claim 1, wherein the preservative is mulberry leaf extract and/or gentiana macrophylla extract.
3. The peony seed oil bacteriostatic skin-care perfumed soap as claimed in claim 2, wherein the preservative is a mixture of 50-70 wt% of mulberry leaf extract and 30-50 wt% of gentiana macrophylla extract.
4. The peony seed oil bacteriostatic skin-care perfumed soap as claimed in claim 2, wherein the gentiana macrophylla extract is prepared by the following method: crushing the gentiana macrophylla, sieving by a 40-mesh sieve to obtain gentiana macrophylla powder, mixing 60-100g of gentiana macrophylla powder with 1200mL of 800-plus-one water, adding 0.2-0.6g of complex enzyme, stirring at 40-50 ℃ for 2-4 hours at 300 revolutions per minute, continuing stirring at 90-98 ℃ for 40-60 minutes, filtering by 300-mesh filter cloth to obtain filtrate and filter residue, adding 1000mL of ethanol water solution with volume fraction of 70-80% into the filter residue, reflux-extracting at 60-70 ℃ for 1-2 hours, filtering by 300-mesh filter cloth to obtain filtrate, combining the two filtrates, concentrating under reduced pressure to 65 ℃ with density of 1.10-1.15g/mL to obtain the gentiana macrophylla extract.
5. The peony seed oil bacteriostatic skin-care perfumed soap as claimed in claim 2, wherein the gentiana macrophylla extract is prepared by the following method: crushing the gentiana macrophylla, sieving by a 40-mesh sieve to obtain gentiana macrophylla powder, mixing 60-100g of gentiana macrophylla powder with 1200mL of 800-plus water, adding 0.2-0.6g of complex enzyme and 1-3g of citric acid, stirring at 40-50 ℃ for 2-4 hours at 300 turns/min, continuing stirring at 90-98 ℃ for 40-60 minutes, filtering by 300-mesh filter cloth to obtain filtrate and filter residue, adding 1000mL of ethanol aqueous solution with volume fraction of 70-80% into the filter residue, extracting at 60-70 ℃ for 1-2 hours under reflux by the filter cloth, filtering by 300-mesh filter cloth to obtain filtrate, combining the two filtrates, and concentrating under reduced pressure to 65 ℃ with density of 1.10-1.15g/mL to obtain the gentiana macrophylla extract.
6. The peony seed oil bacteriostatic skin-care soap as claimed in claim 4 or 5, wherein the complex enzyme is a mixture of 60-70 wt% of cellulase and 30-40 wt% of pectinase.
7. The preparation method of the peony seed oil bacteriostatic skin-care soap as claimed in any one of claims 1 to 6, comprising the following steps:
(1) mixing sodium hydroxide and water, and stirring at 40-50 ℃ at 300 revolutions per minute of 100-;
(2) adding peony seed oil, camellia oil and sweet almond oil into a reaction kettle, stirring and heating to 40-50 ℃ to obtain an oil phase, pouring alkali liquor into the oil phase while stirring at 200-400 rpm, and continuously stirring for 30-40 minutes to obtain a saponification solution;
(3) adding Mel, cortex moutan extract, chelating agent, and antiseptic into the saponification solution, stirring at 40-50 deg.C at 200 rpm and 100-;
(4) pouring the mixed soap liquid into a mould, sealing, standing for 24-48 hours at 30-40 ℃, demoulding, and drying for 4-8 hours at 40-50 ℃ to obtain the peony seed oil antibacterial skin-care soap.
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Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB1292352A (en) * | 1969-01-17 | 1972-10-11 | Unilever Ltd | Liquid detergent compositions |
| CN103119145A (en) * | 2010-07-23 | 2013-05-22 | 美国消毒者公司 | A biodegradable concentrated neutral detergent composition |
| WO2015134011A1 (en) * | 2014-03-05 | 2015-09-11 | Motsenbocker Gregg A | Low-voc water-based cleaner for pen, ink, markers, paint |
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| CN1670166A (en) * | 2005-04-16 | 2005-09-21 | 王浩贵 | Moutan bark cleaning products |
| CN102776087B (en) * | 2012-07-10 | 2015-08-12 | 广东名臣有限公司 | Multifunctional fancy soap |
| CN102911815A (en) * | 2012-10-31 | 2013-02-06 | 刘文锋 | Peony seed oil soap and manufacturing method thereof |
| CN103333752A (en) * | 2013-07-10 | 2013-10-02 | 福建农林大学 | Preparation method of camellia oil skin care soap |
| CN103589537B (en) * | 2013-11-19 | 2015-04-22 | 淮阴工学院 | Beautifying and antibacterial toilet soap |
| CN104152303A (en) * | 2014-08-25 | 2014-11-19 | 吴江市德佐日用化学品有限公司 | Anti-microbial toilet soap and preparation method thereof |
| CN106635531A (en) * | 2016-12-20 | 2017-05-10 | 铜陵凤丹种植科技开发有限责任公司 | Handmade peony seed oil soap and manufacturing method thereof |
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB1292352A (en) * | 1969-01-17 | 1972-10-11 | Unilever Ltd | Liquid detergent compositions |
| CN103119145A (en) * | 2010-07-23 | 2013-05-22 | 美国消毒者公司 | A biodegradable concentrated neutral detergent composition |
| WO2015134011A1 (en) * | 2014-03-05 | 2015-09-11 | Motsenbocker Gregg A | Low-voc water-based cleaner for pen, ink, markers, paint |
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