Invention content
The purpose of the present invention is to provide a kind of pure plants to wash shield agent and preparation method, it promotes by zymolysis technique
The release and conversion of active ingredient obtain the natural botanical extraction liquid rich in saponin and nutritional trace element, have relatively strong
Cleaning clean effect and nourish healthcare function, it is applied widely, have higher economic value.
The present invention to achieve the above object, is achieved through the following technical solutions:
A kind of pure plant washes shield agent, and raw material is counted in parts by weight includes:4~8 parts of soapberry, 1~3 part of gleditsia sinensis,
1~3 part of tea seed cake.
As a kind of optimal selection, the raw material that a kind of pure plant washes shield agent is counted and includes in parts by weight:Without trouble
6 parts of son, 2 parts of gleditsia sinensis, 2 parts of tea seed cake.
It is obtained by the following method that a kind of pure plant, which washes shield agent,:
(1) soapberry, gleditsia sinensis, tea seed cake are dried into powder processed, crosses 5~30 mesh sieve, mixing obtains raw material powder;
(2) the raw material powder is heated to 40~70 DEG C by weight the water that 5~10 times of amounts are added, adds acidity
Conditioning agent makes the pH value of feed liquid control between 4~6;
(3) cellulase is added in press the raw material powder weight 0.1%~0.3%, accomplished continuously or intermittently stirs 2~4 hours,
Filtering, gained filtrate are an extracting solution, and gained filter residue is a filter residue;
(4) filter residue is added to the water of 5~10 times of amounts according to weight ratio, is heated to 40~70 DEG C, addition
Acidity regulator makes the pH value of feed liquid control between 4~6;It is added by the 0.1%~0.3% of a filter residue weight compound
Enzyme is extracted, is accomplished continuously or intermittently stirred 2~4 hours, filtering, gained filtrate is secondary raffinate, and gained filter residue is secondary filter residue;
(5) the secondary filter residue is added to the water of 5~10 times of amounts according to weight ratio, is heated to 60~80 DEG C, continuously
Or intermittent stirring 2~4 hours, filtering, gained filtrate are extracting solution three times, gained filter residue is filter residue three times;
(6) by an extracting solution, secondary raffinate, three times extracting solution mixing, carry out clarifying treatment take clear liquid to get.
As a kind of optimum choice, it is obtained by the following method that a kind of pure plant, which washes shield agent,:
(1) soapberry, gleditsia sinensis, tea seed cake are dried by drying machine, is crushed, cross 15~20 mesh sieve, mixing obtains raw material powder;
(2) the raw material powder is heated to 48~50 DEG C, addition by weight the deionized water that 7~8 times of amounts are added
Acidity regulator make feed liquid pH value control between 4.8~5.0, the acidity regulator include lactic acid, citric acid, acetic acid,
One or more of oxalic acid;
(3) it presses the 0.1%~0.3% of the raw material powder weight and cellulase is added, it is continuous with the speed of 60~100rpm
Or intermittent stirring 2.5 hours, filtering, gained filtrate are an extracting solution, gained filter residue is a filter residue;
(4) filter residue is added to the deionized water of 7~8 times of amounts according to weight ratio, is heated to 48~50 DEG C,
Addition acidity regulator makes the pH value of feed liquid control between 4.8~5.0;By the 0.1%~0.3% of a filter residue weight
It is added and compound is carried by what cellulase, hemicellulase, 1,4 beta-glucanase, pectase, protease, lipase and amylase formed
Enzyme is taken, is accomplished continuously or intermittently stirred 2.5 hours with the speed of 60~100rpm, is filtered, gained filtrate is secondary raffinate, gained filter
Slag is secondary filter residue;
(5) the secondary filter residue is added to the deionized water of 7~8 times of amounts according to weight ratio, is heated to 70 DEG C, continuously
Or intermittent stirring 3 hours, filtering, gained filtrate are extracting solution three times, gained filter residue is filter residue three times;
(6) by an extracting solution, secondary raffinate, three times extracting solution mixing, by mixed extract be added ZTC fining agents into
Row clarification, stands overnight, and 600~1000r/min centrifuges 3~8min, takes clear liquid to obtain the final product.
A kind of pure plant washes the preparation method of shield agent, includes the following steps:
(1) soapberry, gleditsia sinensis, tea seed cake are dried into powder processed, crosses 5~30 mesh sieve, mixing obtains raw material powder;
(2) the raw material powder is heated to 40~70 DEG C by weight the water that 5~10 times of amounts are added, adds acidity
Conditioning agent makes the pH value of feed liquid control between 4~6;
(3) cellulase is added in press the raw material powder weight 0.1%~0.3%, accomplished continuously or intermittently stirs 2~4 hours,
Filtering, gained filtrate are an extracting solution, and gained filter residue is a filter residue;
(4) filter residue is added to the water of 5~10 times of amounts according to weight ratio, is heated to 40~70 DEG C, addition
Acidity regulator makes the pH value of feed liquid control between 4~6;It is added by the 0.1%~0.3% of a filter residue weight compound
Enzyme is extracted, is accomplished continuously or intermittently stirred 2~4 hours, filtering, gained filtrate is secondary raffinate, and gained filter residue is secondary filter residue;
(5) the secondary filter residue is added to the water of 5~10 times of amounts according to weight ratio, is heated to 60~80 DEG C, continuously
Or intermittent stirring 2~4 hours, filtering, gained filtrate are extracting solution three times, gained filter residue is filter residue three times;
(6) by an extracting solution, secondary raffinate, three times extracting solution mixing, carry out clarifying treatment take clear liquid to get.
Preferably, in the step (1), the method that soapberry, gleditsia sinensis, tea seed cake are dried can be solarization method, booth
Dry in the air method, dry any one of a heatable brick bed method, drying chamber and drying machine oven drying method, far infrared heating drying method, micro-wave drying method method.
Preferably, the acidity regulator that the step (2) uses include one kind in lactic acid, citric acid, acetic acid, oxalic acid or
It is several.
Preferably, the compound collecting enzyme that the step (4) uses is by cellulase, hemicellulase, 1,4 beta-glucanase, fruit
Glue enzyme, protease, lipase and amylase composition.
As a kind of prioritization scheme, the preparation method that a kind of pure plant washes shield agent includes the following steps:
(1) soapberry, gleditsia sinensis, tea seed cake are dried into powder processed, crosses 15~20 mesh sieve, mixing obtains raw material powder;
(2) the raw material powder is heated to 48~50 DEG C by weight the water that 7~8 times of amounts are added, adds acidity tune
Section agent makes the pH value of feed liquid control between 4.8~5.0;
(3) it presses the 0.1%~0.3% of the raw material powder weight and cellulase is added, it is continuous with the speed of 60~100rpm
Or intermittent stirring 2.5 hours, filtering, gained filtrate are an extracting solution, gained filter residue is a filter residue;
(4) filter residue is added to the water of 7~8 times of amounts according to weight ratio, is heated to 48~50 DEG C, addition acid
Degree conditioning agent makes the pH value of feed liquid control between 4.8~5.0;It is added by the 0.1%~0.3% of a filter residue weight multiple
Extraction enzyme is closed, is accomplished continuously or intermittently stirred 2.5 hours with the speed of 60~100rpm, is filtered, gained filtrate is secondary raffinate, institute
It is secondary filter residue to obtain filter residue;
(5) the secondary filter residue is added to the water of 7~8 times of amounts according to weight ratio, is heated to 70 DEG C, accomplished continuously or intermittently
Stirring 3 hours, filtering, gained filtrate are that extracting solution, gained filter residue are filter residue three times three times;
(6) by an extracting solution, secondary raffinate, three times extracting solution mixing, mixed extract is clear by natural subsidence
It is clear or fining agent is added is clarified, separation of solid and liquid take clear liquid to get;The fining agent refers to chitosan, ZTC fining agents, sulphur
Sour aluminium, alum or alum.
Preferably, the water used in reaction is deionized water.
The prior art is compared, the beneficial effects of the present invention are:
1, it is a kind of in the dark brown transparency liquid of nature that a kind of pure plant, which washes shield agent, rich in saponin and a variety of
It is micro- necessary to human body, can not only have natural decontamination directly as shield product are washed, for having one's hair wash, taking a shower, face cleaning
Cleaning action, but also there are the health cares such as good nourishing, moisturizing, whitening, antibacterial, anti-dandruff and itching-relieving to the hair of human body, skin
Effect.Obtained plant extraction liquid can also be used as raw material components, can be matched with other chemical surfactants, preparation contains
The chemical synthesis detergent of plant component can substantially improve chemical detergent because containing saponin and other nutrients
Irritation, keep its washing force milder, and there are the guarantors such as nourishing, moisturizing, whitening, antibacterial, anti-dandruff and itching-relieving to hair, skin
Strong effect;Also can be matched with other Chinese medicine preparations, be prepared into hair washing, hair care dual function washing product, have both hair washing,
Brighten the hair, black hair, nutrition hair quality, submissive hair quality and other effects.
2, a kind of pure plant washes the preparation method of shield agent and is utilized zymolysis technique, assists plant extraction and nutrition
Conversion is determined each experimental procedure and critical technical parameter in optimized scope, to significantly improve by proving and testing repeatedly
The extraction efficiency of active ingredient.Extraction process is not necessarily to the intervention of petrochemical industry inorganic reagent, avoids the residual of undesired impurities, Yi Jishi
Harmful effect caused by change product is possible to human skin.Due to the intervention of enzyme preparation, make entirely to react substantially in cryogenic conditions
Lower completion, therefore the preferable nutraceutical active ingredients remained in plant, such as ferulic acid, tea polyphenols, flavones, squalene, tannin
(tannin) etc. is preserved completely, the shortcomings that overcoming high temperature decocting method, and maintenance effect of obtained plant extraction liquid is more
Add brilliance.And preparation process, without putting into expensive equipment, production cost is relatively low, concise production process, temperature, time, PH etc.
Technical indicator is easily controllable, is advantageously implemented large-scale production.
3, the acidity regulator includes one or more of lactic acid, citric acid, acetic acid, oxalic acid.It is preferable to use natural
Organic acid avoids inorganic ions from remaining the injury to skin, hair etc. instead of inorganic reagent.
4, the compound collecting enzyme makes its active ingredient more fully discharge on the one hand further to plant enzymolysis;It is another
Aspect converts cellulose, fat, pectin, protein, the starch etc. in plant to the monosaccharide being easily absorbed by the human body, glucose
Etc. nutritional ingredients, to obtain a kind of plant extraction liquid rich in saponin and trophism trace element.