CN105434234B - A kind of pure plant washes shield agent and preparation method - Google Patents
A kind of pure plant washes shield agent and preparation method Download PDFInfo
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q17/00—Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
- A61Q17/005—Antimicrobial preparations
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/02—Preparations for care of the skin for chemically bleaching or whitening the skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/10—Washing or bathing preparations
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- A—HUMAN NECESSITIES
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- A61Q5/00—Preparations for care of the hair
- A61Q5/006—Antidandruff preparations
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/02—Preparations for cleaning the hair
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/12—Preparations containing hair conditioners
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
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Abstract
The invention discloses a kind of pure plants to wash shield agent and preparation method, relates generally to daily lotion field.Its raw material is counted in parts by weight：4~8 parts of soapberry, 1~3 part of gleditsia sinensis, 1~3 part of tea seed cake.Mainly by drying, crushing, repeatedly enzymolysis and extraction, water carry, clarify the step of prepared.The present invention promotes the release and conversion of active ingredient by zymolysis technique, obtains the natural botanical extraction liquid rich in saponin and nutritional trace element, has stronger cleaning clean effect and nourishes healthcare function, applied widely, has higher economic value.
Description
Technical field
The present invention relates to daily lotion field, specifically a kind of pure plant washes shield agent and preparation method.
Background technology
It is used in everyday to wash shield product, including mildy wash, leaves shampoo, shower cream, hand cleanser, liquid detergent etc., all it is using change
Surfactant is learned as main lotion, and chemical surfactant is all petrochemicals and spin-off.This kind of chemistry
Detergent also generates many toxic side effects while bringing convenience to people's lives --- various skin diseases, allergy, no
Pregnant sterility, leukaemia etc. make the harm there is a growing awareness that chemical detergent in hundred times, thousand times of growth.
There is some in nature natural, with cleaning function plant, wherein it is most representative have soapberry,
Gleditsia sinensis, tea seed cake etc..They are exactly all to contain a large amount of " saponin " there are one common feature, and this kind of saponin is a kind of day
Right, good nonionic surfactant, detergency is suitable with chemical surfactant, thus has fairly good washing
Cleaning function.
In addition, soapberry other than saponin, also contains fat, protein, pectin, tannin and much micro
Element, such as：Ferulic acid, carotenoid, group vitamins and lysine, tyrosine, phenylalanine, glutamic acid, glycine etc. more than ten
Kind amino acid.Wherein ferulic acid is known as the whitening factor of plant kingdom, has natural whitening and anti-oxidation efficacy.Gleditsia sinensis in addition to
Outside containing saponin, also contain the substances such as flavones, tannin, phenolic acid and amino acid.Wherein flavones is a kind of very strong antioxygen
Agent can remove internal oxygen radical, can prevent degeneration, the aging of cell, while also having magical antibacterial activity.
Tea seed cake is that camellia fruit squeezes byproduct after camellia oil, wherein containing a kind of (the natural non-ionic surface of Tea Saponin 12~18%
Activating agent), camellia oil 2% is remained, protein 12~16%, starch and carbohydrate 30~50%, fiber 10~12% and tea are more
The trace elements such as phenol, squalene, flavones.Camellia oil, tea polyphenols, squalene and flavones therein are all fabulous anti-oxidant, anti-
The nutritional ingredient of aging.Therefore, soapberry, gleditsia sinensis and tea seed cake not only have cleaning washing function, but also to hair, skin
Health-care effect with natural nourishing conditioning, is the natural washing product of auxotype of superior performance, has research significance and quotient
The value of industry exploitation.
The prior art still has a prodigious development space to the research of soapberry, gleditsia sinensis and tea seed cake, related ends and product
Cleaning effect is not good enough, and care action is undesirable, and it is still necessary to rely on the cooperation of petrochemical industry reagent, it is difficult to give full play to the work(of its cleaning-nursing
Effect.To find out its cause, being on the one hand because the formula of detergent is it is still necessary to optimize, to optimal by the allotment performance of each natural constituents
Cleaning and maintenance effect；On the other hand it is to prevent active ingredient from preferable because the extracting method of plant component is not perfect
It remains into product or remnants has other impurity, affect cleaning and the performance of maintenance effect.
The extracting method that the prior art extracts saponin from soapberry, gleditsia sinensis or tea seed cake is mainly water extraction and organic molten
Agent method.However it is well known that the active ingredient of plant is substantially all the inside for being present in plant, by fine and close, tough and tensile fiber
And cell wall is wrapped up, and water or organic solvent are merely relied on, it is difficult to break fine and close, tough and tensile fibrous layer and cell wall resistance
Every very low to the recovery rate of active ingredient.Part research water extraction, organic solvent method substantially, using ultrasonic wave, micro-
The householder methods such as wave improve extraction efficiency, but there is equipment investments big, complex process and are difficult to large-scale production
Defect, and its reaction is from inside to outside, speed is fast, temperature is high, on active influence, it is still necessary to further inquire into.
In conclusion how to inquire into out more rational formula, and significantly more efficient extracting method is developed, made full use of
Natural constituent in soapberry, gleditsia sinensis and tea seed cake is made cleaning, conserves the outstanding washing product of effect, is this field skill
The research direction of art personnel.
Invention content
The purpose of the present invention is to provide a kind of pure plants to wash shield agent and preparation method, it promotes by zymolysis technique
The release and conversion of active ingredient obtain the natural botanical extraction liquid rich in saponin and nutritional trace element, have relatively strong
Cleaning clean effect and nourish healthcare function, it is applied widely, have higher economic value.
The present invention to achieve the above object, is achieved through the following technical solutions：
A kind of pure plant washes shield agent, and raw material is counted in parts by weight includes：4~8 parts of soapberry, 1~3 part of gleditsia sinensis,
1~3 part of tea seed cake.
As a kind of optimal selection, the raw material that a kind of pure plant washes shield agent is counted and includes in parts by weight：Without trouble
6 parts of son, 2 parts of gleditsia sinensis, 2 parts of tea seed cake.
It is obtained by the following method that a kind of pure plant, which washes shield agent,：
(1) soapberry, gleditsia sinensis, tea seed cake are dried into powder processed, crosses 5~30 mesh sieve, mixing obtains raw material powder；
(2) the raw material powder is heated to 40~70 DEG C by weight the water that 5~10 times of amounts are added, adds acidity
Conditioning agent makes the pH value of feed liquid control between 4~6；
(3) cellulase is added in press the raw material powder weight 0.1%~0.3%, accomplished continuously or intermittently stirs 2~4 hours,
Filtering, gained filtrate are an extracting solution, and gained filter residue is a filter residue；
(4) filter residue is added to the water of 5~10 times of amounts according to weight ratio, is heated to 40~70 DEG C, addition
Acidity regulator makes the pH value of feed liquid control between 4~6；It is added by the 0.1%~0.3% of a filter residue weight compound
Enzyme is extracted, is accomplished continuously or intermittently stirred 2~4 hours, filtering, gained filtrate is secondary raffinate, and gained filter residue is secondary filter residue；
(5) the secondary filter residue is added to the water of 5~10 times of amounts according to weight ratio, is heated to 60~80 DEG C, continuously
Or intermittent stirring 2~4 hours, filtering, gained filtrate are extracting solution three times, gained filter residue is filter residue three times；
(6) by an extracting solution, secondary raffinate, three times extracting solution mixing, carry out clarifying treatment take clear liquid to get.
As a kind of optimum choice, it is obtained by the following method that a kind of pure plant, which washes shield agent,：
(1) soapberry, gleditsia sinensis, tea seed cake are dried by drying machine, is crushed, cross 15~20 mesh sieve, mixing obtains raw material powder；
(2) the raw material powder is heated to 48~50 DEG C, addition by weight the deionized water that 7~8 times of amounts are added
Acidity regulator make feed liquid pH value control between 4.8~5.0, the acidity regulator include lactic acid, citric acid, acetic acid,
One or more of oxalic acid；
(3) it presses the 0.1%~0.3% of the raw material powder weight and cellulase is added, it is continuous with the speed of 60~100rpm
Or intermittent stirring 2.5 hours, filtering, gained filtrate are an extracting solution, gained filter residue is a filter residue；
(4) filter residue is added to the deionized water of 7~8 times of amounts according to weight ratio, is heated to 48~50 DEG C,
Addition acidity regulator makes the pH value of feed liquid control between 4.8~5.0；By the 0.1%~0.3% of a filter residue weight
It is added and compound is carried by what cellulase, hemicellulase, 1,4 beta-glucanase, pectase, protease, lipase and amylase formed
Enzyme is taken, is accomplished continuously or intermittently stirred 2.5 hours with the speed of 60~100rpm, is filtered, gained filtrate is secondary raffinate, gained filter
Slag is secondary filter residue；
(5) the secondary filter residue is added to the deionized water of 7~8 times of amounts according to weight ratio, is heated to 70 DEG C, continuously
Or intermittent stirring 3 hours, filtering, gained filtrate are extracting solution three times, gained filter residue is filter residue three times；
(6) by an extracting solution, secondary raffinate, three times extracting solution mixing, by mixed extract be added ZTC fining agents into
Row clarification, stands overnight, and 600~1000r/min centrifuges 3~8min, takes clear liquid to obtain the final product.
A kind of pure plant washes the preparation method of shield agent, includes the following steps：
(1) soapberry, gleditsia sinensis, tea seed cake are dried into powder processed, crosses 5~30 mesh sieve, mixing obtains raw material powder；
(2) the raw material powder is heated to 40~70 DEG C by weight the water that 5~10 times of amounts are added, adds acidity
Conditioning agent makes the pH value of feed liquid control between 4~6；
(3) cellulase is added in press the raw material powder weight 0.1%~0.3%, accomplished continuously or intermittently stirs 2~4 hours,
Filtering, gained filtrate are an extracting solution, and gained filter residue is a filter residue；
(4) filter residue is added to the water of 5~10 times of amounts according to weight ratio, is heated to 40~70 DEG C, addition
Acidity regulator makes the pH value of feed liquid control between 4~6；It is added by the 0.1%~0.3% of a filter residue weight compound
Enzyme is extracted, is accomplished continuously or intermittently stirred 2~4 hours, filtering, gained filtrate is secondary raffinate, and gained filter residue is secondary filter residue；
(5) the secondary filter residue is added to the water of 5~10 times of amounts according to weight ratio, is heated to 60~80 DEG C, continuously
Or intermittent stirring 2~4 hours, filtering, gained filtrate are extracting solution three times, gained filter residue is filter residue three times；
(6) by an extracting solution, secondary raffinate, three times extracting solution mixing, carry out clarifying treatment take clear liquid to get.
Preferably, in the step (1), the method that soapberry, gleditsia sinensis, tea seed cake are dried can be solarization method, booth
Dry in the air method, dry any one of a heatable brick bed method, drying chamber and drying machine oven drying method, far infrared heating drying method, micro-wave drying method method.
Preferably, the acidity regulator that the step (2) uses include one kind in lactic acid, citric acid, acetic acid, oxalic acid or
It is several.
Preferably, the compound collecting enzyme that the step (4) uses is by cellulase, hemicellulase, 1,4 beta-glucanase, fruit
Glue enzyme, protease, lipase and amylase composition.
As a kind of prioritization scheme, the preparation method that a kind of pure plant washes shield agent includes the following steps：
(1) soapberry, gleditsia sinensis, tea seed cake are dried into powder processed, crosses 15~20 mesh sieve, mixing obtains raw material powder；
(2) the raw material powder is heated to 48~50 DEG C by weight the water that 7~8 times of amounts are added, adds acidity tune
Section agent makes the pH value of feed liquid control between 4.8~5.0；
(3) it presses the 0.1%~0.3% of the raw material powder weight and cellulase is added, it is continuous with the speed of 60~100rpm
Or intermittent stirring 2.5 hours, filtering, gained filtrate are an extracting solution, gained filter residue is a filter residue；
(4) filter residue is added to the water of 7~8 times of amounts according to weight ratio, is heated to 48~50 DEG C, addition acid
Degree conditioning agent makes the pH value of feed liquid control between 4.8~5.0；It is added by the 0.1%~0.3% of a filter residue weight multiple
Extraction enzyme is closed, is accomplished continuously or intermittently stirred 2.5 hours with the speed of 60~100rpm, is filtered, gained filtrate is secondary raffinate, institute
It is secondary filter residue to obtain filter residue；
(5) the secondary filter residue is added to the water of 7~8 times of amounts according to weight ratio, is heated to 70 DEG C, accomplished continuously or intermittently
Stirring 3 hours, filtering, gained filtrate are that extracting solution, gained filter residue are filter residue three times three times；
(6) by an extracting solution, secondary raffinate, three times extracting solution mixing, mixed extract is clear by natural subsidence
It is clear or fining agent is added is clarified, separation of solid and liquid take clear liquid to get；The fining agent refers to chitosan, ZTC fining agents, sulphur
Sour aluminium, alum or alum.
Preferably, the water used in reaction is deionized water.
The prior art is compared, the beneficial effects of the present invention are：
1, it is a kind of in the dark brown transparency liquid of nature that a kind of pure plant, which washes shield agent, rich in saponin and a variety of
It is micro- necessary to human body, can not only have natural decontamination directly as shield product are washed, for having one's hair wash, taking a shower, face cleaning
Cleaning action, but also there are the health cares such as good nourishing, moisturizing, whitening, antibacterial, anti-dandruff and itching-relieving to the hair of human body, skin
Effect.Obtained plant extraction liquid can also be used as raw material components, can be matched with other chemical surfactants, preparation contains
The chemical synthesis detergent of plant component can substantially improve chemical detergent because containing saponin and other nutrients
Irritation, keep its washing force milder, and there are the guarantors such as nourishing, moisturizing, whitening, antibacterial, anti-dandruff and itching-relieving to hair, skin
Strong effect；Also can be matched with other Chinese medicine preparations, be prepared into hair washing, hair care dual function washing product, have both hair washing,
Brighten the hair, black hair, nutrition hair quality, submissive hair quality and other effects.
2, a kind of pure plant washes the preparation method of shield agent and is utilized zymolysis technique, assists plant extraction and nutrition
Conversion is determined each experimental procedure and critical technical parameter in optimized scope, to significantly improve by proving and testing repeatedly
The extraction efficiency of active ingredient.Extraction process is not necessarily to the intervention of petrochemical industry inorganic reagent, avoids the residual of undesired impurities, Yi Jishi
Harmful effect caused by change product is possible to human skin.Due to the intervention of enzyme preparation, make entirely to react substantially in cryogenic conditions
Lower completion, therefore the preferable nutraceutical active ingredients remained in plant, such as ferulic acid, tea polyphenols, flavones, squalene, tannin
(tannin) etc. is preserved completely, the shortcomings that overcoming high temperature decocting method, and maintenance effect of obtained plant extraction liquid is more
Add brilliance.And preparation process, without putting into expensive equipment, production cost is relatively low, concise production process, temperature, time, PH etc.
Technical indicator is easily controllable, is advantageously implemented large-scale production.
3, the acidity regulator includes one or more of lactic acid, citric acid, acetic acid, oxalic acid.It is preferable to use natural
Organic acid avoids inorganic ions from remaining the injury to skin, hair etc. instead of inorganic reagent.
4, the compound collecting enzyme makes its active ingredient more fully discharge on the one hand further to plant enzymolysis；It is another
Aspect converts cellulose, fat, pectin, protein, the starch etc. in plant to the monosaccharide being easily absorbed by the human body, glucose
Etc. nutritional ingredients, to obtain a kind of plant extraction liquid rich in saponin and trophism trace element.
Specific implementation mode
Present invention will be further explained below with reference to specific examples.It should be understood that these embodiments are merely to illustrate the present invention
Rather than it limits the scope of the invention.In addition, it should also be understood that, after reading the content taught by the present invention, people in the art
Member can make various changes or modifications the present invention, and such equivalent forms equally fall within the application the appended claims and limited
Range.
Involved instrument, reagent, material etc., are existing in the prior art unless otherwise noted in following embodiments
Conventional instrument, reagent, material etc., can be obtained by regular commercial sources.Involved experimental method in following embodiments, inspection
Survey method etc. is unless otherwise noted existing routine experiment method in the prior art, detection method etc..
Embodiment 1：A kind of pure plant washes shield agent
Its raw material is counted in parts by weight：6 parts of soapberry, 2 parts of gleditsia sinensis, 2 parts of tea seed cake.By following steps system
It is standby：
600 grams of soapberry, 200 grams of gleditsia sinensis, 200 grams of tea seed cake are weighed, drying machine is dried, after pulverizer crushed 18 mesh sieve,
It is put into heating and thermal insulation bucket, 8000g deionized waters is added, addition lactic acid solution makes pH value be 4.8, and heat temperature raising waits for feed liquid temperature
Degree reaches 50 DEG C, adds cellulase 1g, is continuously stirred with the speed of 80rpm, keeps constant temperature 2.5 hours, solid using filter screen
Liquid detaches, and obtains first-time filtrate and a filter residue；
Filter residue is put into heating and thermal insulation bucket, 8000g deionized waters are added, addition lactic acid solution makes pH value be 4.8,
Heat temperature raising waits for that feed temperature reaches 50 DEG C, adds by cellulase, hemicellulase, 1,4 beta-glucanase, pectase, albumen
The compound collecting enzyme 1g of enzyme, lipase and amylase composition, is continuously stirred with the speed of 80rpm, keeps constant temperature 2.5 hours, is made
It is separated by solid-liquid separation with filter screen, obtains secondary filtrate and secondary filter residue；
Secondary filter residue is put into heating and thermal insulation bucket, 8000g deionized waters are added, are heated to 70 DEG C, 60rpm is continuous
Stirring, keeps constant temperature 3 hours, is separated by solid-liquid separation using filter screen, obtains filtrate three times and three times filter residue；
By first-time filtrate, secondary filtrate, filtrate is uniformly mixed three times, stands the clarification of natural sedimentation in 24 hours, takes supernatant
To obtain the final product.
Embodiment 2：A kind of pure plant washes shield agent
Its raw material is counted in parts by weight：7 parts of soapberry, 1 part of gleditsia sinensis, 2 parts of tea seed cake.By following steps system
It is standby：
700 grams of soapberry, 100 grams of gleditsia sinensis, 200 grams of tea seed cake are weighed, micro-wave oven is dried, after pulverizer crushed 15 mesh sieve,
It is put into constant temperature water bath pot, 7000g deionized waters is added, addition citric acid makes pH value be 5.0, and heat temperature raising waits for feed temperature
Reach 55 DEG C, add cellulase 2g, continuously stirred with the speed of 90rpm, keep constant temperature 3 hours, filter first-time filtrate and
Filter residue；
Filter residue is put into constant temperature water bath pot, 7000g deionized waters are added, addition citric acid makes pH value be 5.0, adds
Heat heating waits for that feed temperature reaches 55 DEG C, and addition is made of cellulase, hemicellulase, protease, lipase and amylase
Compound collecting enzyme 2g, continuously stirred with the speed of 90rpm, keep constant temperature 3.5 hours, filter to obtain secondary filtrate and secondary filter
Slag；
Secondary filter residue is put into constant temperature water bath pot, 6000g deionized waters are added, are heated to 80 DEG C, intermittent stirring,
It keeps constant temperature 3.5 hours, filters to obtain filtrate and three times filter residue three times；
By first-time filtrate, secondary filtrate, filtrate is uniformly mixed three times, and 200g chitosans are added, and it is small that 2 are stood after stirring evenly
When, 800r/min centrifuges 5min, takes clear liquid to obtain the final product.
Embodiment 3：A kind of pure plant washes shield agent
Its raw material is counted in parts by weight：4 parts of soapberry, 3 parts of gleditsia sinensis, 3 parts of tea seed cake.By following steps system
It is standby：
400 grams of soapberry, 300 grams of gleditsia sinensis, 300 grams of tea seed cake are weighed, 6000g is added after crushed 25 mesh sieve in dryness in the sun
Deionized water, addition oxalic acid solution make pH value be 5.5, and heat temperature raising waits for that feed temperature reaches 60 DEG C, adds cellulase 3g,
It is continuously stirred with the speed of 60rpm, keeps constant temperature 2 hours, filter to obtain first-time filtrate and a filter residue；
6000g deionized waters are added in filter residue, addition oxalic acid solution makes pH value be 5.0, and heat temperature raising waits for feed liquid temperature
Degree reaches 60 DEG C, adds the compound collecting being made of cellulase, hemicellulase, 1,4 beta-glucanase, protease and lipase
Enzyme 2.5g is continuously stirred with the speed of 60rpm, keeps constant temperature 2 hours, filters to obtain secondary filtrate and secondary filter residue；
6000g deionized waters are added in secondary filter residue, are heated to 65 DEG C, 60rpm is continuously stirred, and keeps constant temperature 3 small
When, filter to obtain filtrate and three times filter residue three times；
By first-time filtrate, secondary filtrate, filtrate is uniformly mixed three times, stands the clarification of natural sedimentation in 12 hours, takes supernatant
To obtain the final product.
Embodiment 4：Shield agent is washed as the experiment on probation of hair shampoo article using a kind of pure plant prepared by embodiment 1
It selects 15 volunteers at random in 15~35 years old healthy population, uses the common leaves shampoo of market purchasing respectively
Daily hair washing is carried out to nurse 20 days；Daily hair washing is carried out using brand leaves shampoo to nurse 20 days；And prepared using embodiment 1
Plant washes shield agent and carries out daily hair washing nursing 20 days, and corresponding point is provided according to sensory testing's evaluation criterion (2~table of table 7) is objective
Value is as a result as follows：
Table 1：Compare sensory test result
Evaluation conclusion：
Shield product are washed for having one's hair wash using the pure plant, human opinion is tested by organoleptic properties, are better than and purchased in market are commonly washed
Hair-cream is suitable with brand leaves shampoo performance.
Subordinate list：
Table 2：Wet hair comb rationality evaluation table
Table 3：Wet hair hand valuation table
Table 4：Hair drying comb rationality evaluation table
Table 5：Dry hair hand valuation table
Table 6：Dandruff index assessment table
Table 7：Itching of the scalp index assessment table
Claims (8)
1. a kind of pure plant washes shield agent, it is characterised in that：It includes 4~8 parts of soapberry, gleditsia sinensis that its raw material is counted in parts by weight
1~3 part, 1~3 part of tea seed cake is obtained by the following method：
(1) soapberry, gleditsia sinensis, tea seed cake are dried into powder processed, crosses 5~30 mesh sieve, mixing obtains raw material powder；
(2) the raw material powder is heated to 40~70 DEG C by weight the water that 5~10 times of amounts are added, adds acidity adjustment
Agent makes the pH value of feed liquid control between 4~6；
(3) cellulase is added in press the raw material powder weight 0.1%~0.3%, accomplished continuously or intermittently stirs 2~4 hours, mistake
Filter, gained filtrate are an extracting solution, and gained filter residue is a filter residue；
(4) filter residue is added to the water of 5~10 times of amounts according to weight ratio, is heated to 40~70 DEG C, adds acidity
Conditioning agent makes the pH value of feed liquid control between 4~6；Compound collecting is added by the 0.1%~0.3% of a filter residue weight
Enzyme, the compound collecting enzyme are by cellulase, hemicellulase, 1,4 beta-glucanase, pectase, protease, lipase and shallow lake
Powder enzyme, or by cellulase, hemicellulase, protease, lipase and amylase, or by cellulase, hemicellulase, β-
What dextranase, protease and lipase formed, it accomplished continuously or intermittently stirs 2~4 hours, filtering, gained filtrate is second extraction
Liquid, gained filter residue are secondary filter residue；
(5) the secondary filter residue is added to the water of 5~10 times of amounts according to weight ratio, is heated to 60~80 DEG C, it is continuous or
It has a rest stirring 2~4 hours, filtering, gained filtrate is extracting solution three times, and gained filter residue is filter residue three times；
(6) by an extracting solution, secondary raffinate, three times extracting solution mixing, carry out clarifying treatment take clear liquid to get.
2. a kind of pure plant washes shield agent according to claim 1, it is characterised in that：Its raw material is counted in parts by weight
4~8 parts of soapberry, 1~3 part of gleditsia sinensis, 1~3 part of tea seed cake are obtained by the following method：
(1) soapberry, gleditsia sinensis, tea seed cake are dried by drying machine, is crushed, cross 15~20 mesh sieve, mixing obtains raw material powder；
(2) the raw material powder is heated to 48~50 DEG C by weight the deionized water that 7~8 times of amounts are added, adds acidity
Conditioning agent makes the pH value of feed liquid control between 4.8~5.0, and the acidity regulator is selected from lactic acid, citric acid, acetic acid, oxalic acid
One or more of；
(3) cellulase is added in press the raw material powder weight 0.1%~0.3%, with the speed of 60~100rpm it is continuous or
It has a rest and stirs 2.5 hours, filtering, gained filtrate is an extracting solution, and gained filter residue is a filter residue；
(4) filter residue is added to the deionized water of 7~8 times of amounts according to weight ratio, is heated to 48~50 DEG C, addition
Acidity regulator makes the pH value of feed liquid control between 4.8~5.0；It is added by the 0.1%~0.3% of a filter residue weight
The compound collecting being made of cellulase, hemicellulase, 1,4 beta-glucanase, pectase, protease, lipase and amylase
Enzyme is accomplished continuously or intermittently stirred 2.5 hours with the speed of 60~100rpm, filtering, and gained filtrate is secondary raffinate, gained filter residue
For secondary filter residue；
(5) the secondary filter residue is added to the deionized waters of 7~8 times of amounts according to weight ratio, is heated to 70 DEG C, it is continuous or
It has a rest and stirs 3 hours, filtering, gained filtrate is that extracting solution, gained filter residue are filter residue three times three times；
(6) by an extracting solution, secondary raffinate, three times extracting solution mixing, it is clear that the progress of ZTC fining agents is added in mixed extract
Clearly, it stands overnight, 600~1000r/min centrifuges 3~8min, takes clear liquid to obtain the final product.
3. a kind of pure plant washes the preparation method of shield agent according to claim 1, it is characterised in that：Including following step
Suddenly：
(1) soapberry, gleditsia sinensis, tea seed cake are dried into powder processed, crosses 5~30 mesh sieve, mixing obtains raw material powder；
(2) the raw material powder is heated to 40~70 DEG C by weight the water that 5~10 times of amounts are added, adds acidity adjustment
Agent makes the pH value of feed liquid control between 4~6；
(3) cellulase is added in press the raw material powder weight 0.1%~0.3%, accomplished continuously or intermittently stirs 2~4 hours, mistake
Filter, gained filtrate are an extracting solution, and gained filter residue is a filter residue；
(4) filter residue is added to the water of 5~10 times of amounts according to weight ratio, is heated to 40~70 DEG C, adds acidity
Conditioning agent makes the pH value of feed liquid control between 4~6；Compound collecting is added by the 0.1%~0.3% of a filter residue weight
Enzyme, the compound collecting enzyme are by cellulase, hemicellulase, 1,4 beta-glucanase, pectase, protease, lipase and shallow lake
Powder enzyme, or by cellulase, hemicellulase, protease, lipase and amylase, or by cellulase, hemicellulase, β-
What dextranase, protease and lipase formed, it accomplished continuously or intermittently stirs 2~4 hours, filtering, gained filtrate is second extraction
Liquid, gained filter residue are secondary filter residue；
(5) the secondary filter residue is added to the water of 5~10 times of amounts according to weight ratio, is heated to 60~80 DEG C, it is continuous or
It has a rest stirring 2~4 hours, filtering, gained filtrate is extracting solution three times, and gained filter residue is filter residue three times；
(6) by an extracting solution, secondary raffinate, three times extracting solution mixing, carry out clarifying treatment take clear liquid to get.
4. a kind of pure plant washes the preparation method of shield agent according to claim 3, it is characterised in that：Including following step
Suddenly：
(1) soapberry, gleditsia sinensis, tea seed cake are dried into powder processed, crosses 15~20 mesh sieve, mixing obtains raw material powder；
(2) the raw material powder is heated to 48~50 DEG C by weight the water that 7~8 times of amounts are added, adds acidity regulator
The pH value of feed liquid is set to control between 4.8~5.0；
(3) cellulase is added in press the raw material powder weight 0.1%~0.3%, with the speed of 60~100rpm it is continuous or
It has a rest and stirs 2.5 hours, filtering, gained filtrate is an extracting solution, and gained filter residue is a filter residue；
(4) filter residue is added to the water of 7~8 times of amounts according to weight ratio, is heated to 48~50 DEG C, adds acidity tune
Section agent makes the pH value of feed liquid control between 4.8~5.0；Compound carry is added by the 0.1%~0.3% of a filter residue weight
Take enzyme, the compound collecting enzyme be by cellulase, hemicellulase, 1,4 beta-glucanase, pectase, protease, lipase and
Amylase, or by cellulase, hemicellulase, protease, lipase and amylase, or by cellulase, hemicellulase,
What 1,4 beta-glucanase, protease and lipase formed, it is accomplished continuously or intermittently stirred 2.5 hours, is filtered with the speed of 60~100rpm,
Gained filtrate is secondary raffinate, and gained filter residue is secondary filter residue；
(5) the secondary filter residue is added to the water of 7~8 times of amounts according to weight ratio, 70 DEG C is heated to, accomplished continuously or intermittently stirs
3 hours, filtering, gained filtrate was that extracting solution, gained filter residue are filter residue three times three times；
(6) by an extracting solution, secondary raffinate, three times extracting solution mixing, mixed extract is clarified by natural subsidence or
Be added fining agent clarified, separation of solid and liquid take clear liquid to get；The fining agent refer to chitosan, ZTC fining agents, aluminum sulfate,
Alum or alum.
5. a kind of pure plant washes the preparation method of shield agent according to claim 3, it is characterised in that：The step (1)
In, the method that soapberry, gleditsia sinensis, tea seed cake are dried, which is solarization method, airing method, dries a heatable brick bed method, drying chamber and drying machine dries
Any one of method, far infrared heating drying method, micro-wave drying method method.
6. a kind of pure plant washes the preparation method of shield agent according to claim 3, it is characterised in that：The step (2)
The acidity regulator used is selected from one or more of lactic acid, citric acid, acetic acid, oxalic acid.
7. a kind of pure plant washes the preparation method of shield agent according to claim 3, it is characterised in that：The step (4)
The compound collecting enzyme used is by cellulase, hemicellulase, 1,4 beta-glucanase, pectase, protease, lipase and amylase
Composition.
8. a kind of pure plant washes the preparation method of shield agent according to claim 3, it is characterised in that：Used in reaction
Water be deionized water.
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