CN108578314A - A kind of composition containing plant extracts and its application in except mite nursing product - Google Patents
A kind of composition containing plant extracts and its application in except mite nursing product Download PDFInfo
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- CN108578314A CN108578314A CN201810523689.4A CN201810523689A CN108578314A CN 108578314 A CN108578314 A CN 108578314A CN 201810523689 A CN201810523689 A CN 201810523689A CN 108578314 A CN108578314 A CN 108578314A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9794—Liliopsida [monocotyledons]
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9789—Magnoliopsida [dicotyledons]
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61P—SPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
- A61P33/00—Antiparasitic agents
- A61P33/14—Ectoparasiticides, e.g. scabicides
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/008—Preparations for oily skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/02—Preparations for care of the skin for chemically bleaching or whitening the skin
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Abstract
The present invention provides a kind of composition containing plant extracts, and the composition includes component A and B component, wherein：The component A is made of liquid component and powdery components；The liquid component includes Gotu Kola P.E, soapberry extract, Semen Tritici aestivi extract, Fructus Rosae Laevigatae extract, Fructus Chebulae extract, distilled water；The powdery components include sodium bicarbonate powder, Semen Cuscutae extract；The ingredient of the B component includes：Radix Stemonae extract, phellodendron extract, shrubby sophora extract, mulberry bark extract, licorice, green-tea extract, mint extract.
Description
Technical field
The present invention relates to personal care articles fields, are more related to a kind of personal care articles containing plant extracts.
Background technology
Acarid is divided into many kinds, is hair follicle acarid and sebaceous glands acarid with the acarid that the mankind most get close to；Acarid is widely distributed
In the dark corner in room, carpet, mattress, pillow, sofa, air-conditioning, summer sleeping mat etc., wherein the distribution of dust mite is most wide, influences most
Greatly, the corpse of acarid, secretion and excreta are all anaphylactogens, can make one to occur allergic dermatitis, asthma, bronchitis,
The diseases such as ephritis, allergic rhinitis seriously endanger health.
Skin once infects acarid, then can block pore, keeps skin dark and gloomy unglazed, causes that pore is coarse, skin is coarse
Heavy wool, or even cause acne.Meanwhile the procreation of acarid is very competent, is food with the scurf of the mankind；The female acarid of after fertilization
Activity is more frequent.
How the more focus of the more except mite personal-care supplies used on the market kills on acarid if being placed on；Human body
Skin surface is more fragile, and except mite is generally required just to win initial success by 3 weeks time, and drug, which is used for a long time, to cause skin
Drug resistance such as is festered at the even more serious situation；The excreta of acarid is only real anaphylactogen simultaneously, and it is insufficient only to kill acarid
To meet the needs of liking to be beautiful.
For the above situation, a kind of composition containing plant extracts of the present invention is arranged imported agent, promotes the quick-fried of acarid
Body removes the excreta of acarid by the way of absorption.
Invention content
The first aspect of the present invention provides a kind of composition containing plant extracts, and the composition includes component A and B groups
Point, wherein：
The component A is made of liquid component and powdery components；
The liquid component includes Gotu Kola P.E, soapberry extract, Semen Tritici aestivi extract, Fructus Rosae Laevigatae extract, scolds
Seed extract and distilled water；
The powdery components include sodium bicarbonate powder and Semen Cuscutae extract；
The ingredient of the B component includes：It is Radix Stemonae extract, phellodendron extract, shrubby sophora extract, mulberry bark extract, sweet
Careless extract, green-tea extract and mint extract.
As one embodiment of the present invention, the unit quantity ratio of the component A and B component is (1-3)：(0.5-1).
As one embodiment of the present invention, the unit quantity ratio of the liquid component and powdery components is (1-3)：(1-
2)。
As one embodiment of the present invention, the liquid component of 1 unit quantity include 1-5 parts of Gotu Kola P.E,
1-5 parts of soapberry extract, 0.1-0.5 parts of Semen Tritici aestivi extract, 0.1-0.3 parts of Fructus Rosae Laevigatae extract, Fructus Chebulae extract 0.01-
0.05 part, 5-10 parts of distilled water.
As one embodiment of the present invention, the liquid component of 1 unit quantity includes 2 parts of Gotu Kola P.E, nothing
Suffer from 3 parts of seed extract, 0.3 part of Semen Tritici aestivi extract, 0.2 part of Fructus Rosae Laevigatae extract, 0.03 part of Fructus Chebulae extract, 8 parts of distilled water.
As one embodiment of the present invention, the ingredient of the B component of 1 unit quantity includes：Radix Stemonae extract 1-3
Part, 0.1-0.5 parts of phellodendron extract, 1-3 parts of shrubby sophora extract, 0.1-1 parts of mulberry bark extract, 5-10 parts of licorice,
3-15 parts of green-tea extract, 0.1-1 parts of mint extract.
As one embodiment of the present invention, the ingredient of the B component of 1 unit quantity includes：2 parts of Radix Stemonae extract,
0.3 part of phellodendron extract, 2 parts of shrubby sophora extract, 0.6 part of mulberry bark extract, 6 parts of licorice, 8 parts of green-tea extract,
0.4 part of mint extract.
As one embodiment of the present invention, the Radix Stemonae extract includes that Radix stemonae japonicae extract and radix stemonae tuberosae carry
Take object.
A kind of above-mentioned composition containing plant extracts is used to remove acarid, whitening is dispelled scar.
The second aspect of the present invention provides a kind of except mite personal care articles, and it includes the above-mentioned groups containing plant extracts
Close object.
Advantageous effect：
1, cleaning is respectively adopted in the composition provided by the invention containing plant extracts, two steps of sterilization carry out that shield
Skin processing；
2, the composition provided by the invention containing plant extracts accelerates the quick-fried body of acarid, excludes protein allergens；
3, the holding skin that the present invention can be permanently effective is clean, salubrious, avoids Oily.
4, the present invention is suitable for water content of stratum corneum less than or equal to 10%, and crowd's (i.e. oiliness skin that sebum secretion is vigorous
Skin).
Specific implementation mode
The detailed description for preferred implementation method of the invention below of participating in the election of and including embodiment this hair can be more easily understood
Bright content.Unless otherwise defined, all technologies used herein and scientific terminology have common with fields of the present invention
The normally understood identical meaning of technical staff.When there is a conflict, the definition in this specification shall prevail.
As used herein term " by ... prepare " it is synonymous with "comprising".Term "comprising" used herein, " comprising ",
" having ", " containing " or its any other deformation, it is intended that cover non-exclusionism includes.For example, the combination comprising listed elements
Object, step, method, product or device are not necessarily limited to those elements, but may include not expressly listed other elements or
Such composition, step, method, product or the intrinsic element of device.
Conjunction " Consists of " excludes any element that do not point out, step or component.If in claim, this
Phrase will make claim be closed, so that it is not included the material in addition to the material of those descriptions, but relative normal
Except rule impurity.When being rather than immediately following after theme in the clause that phrase " Consists of " appears in claim main body,
It is only limited to the element described in the clause；Other elements are not excluded except the claim as a whole.
Equivalent, concentration or other values or parameter are excellent with range, preferred scope or a series of upper limit preferred values and lower limit
When the Range Representation that choosing value limits, this, which should be understood as, specifically discloses by any range limit or preferred value and any range
Any pairing of lower limit or preferred value is formed by all ranges, regardless of whether the range separately discloses.For example, when open
When range " 1 to 5 ", described range should be interpreted as including range " 1 to 4 ", " 1 to 3 ", " 1 to 2 ", " 1 to 2 and 4 to
5 ", " 1 to 3 and 5 " etc..When numberical range is described herein, unless otherwise stated, otherwise range intention includes its end
Value and all integers and score in the range.
Singulative includes that plural number discusses object, unless the context clearly dictates otherwise." optional " or it is " arbitrary
It is a kind of " refer to that the item described thereafter or event may or may not occur, and the description include situation that event occurs and
The situation that event does not occur.
Approximate term in specification and claims is used for modifying quantity, and it is specific to indicate that the present invention is not limited to this
Quantity further includes the modified part of the acceptable change without lead to related basic function close to the quantity.Phase
It answers, modifies a numerical value with " about ", " about " etc., mean that the present invention is not limited to the exact numericals.In some examples, approximate
Term likely corresponds to the precision of the instrument of measured value.In present specification and claims, range limits can be with
Combination and/or exchange, these ranges include all subranges contained therebetween if not stated otherwise.
In addition, indefinite article "an" before element of the present invention or component and "one" quantitative requirement to element or component
(i.e. occurrence number) unrestriction.Therefore "one" or "an" should be read as including one or at least one, and odd number
The element or component of form also include plural form, unless the apparent purport of the quantity refers to singulative.
The present invention provides a kind of composition containing plant extracts, and the composition includes component A and B component, wherein：
The component A is made of liquid component and powdery components；
The liquid component includes Gotu Kola P.E, soapberry extract, Semen Tritici aestivi extract, Fructus Rosae Laevigatae extract, scolds
Seed extract, distilled water；
The powdery components include sodium bicarbonate powder, Semen Cuscutae extract；
The ingredient of the B component includes：It is Radix Stemonae extract, phellodendron extract, shrubby sophora extract, mulberry bark extract, sweet
Careless extract, green-tea extract, mint extract.
In the present invention, the liquid component of 1 unit quantity refers to：The liquid component of 1 unit quantity contains Gotu Kola P.E 1-5
Part, 1-5 parts of soapberry extract, 0.1-0.5 parts of Semen Tritici aestivi extract, 0.1-0.3 parts of Fructus Rosae Laevigatae extract, Fructus Chebulae extract
0.01-0.05 parts, 5-10 parts of distilled water；Powdery components are similarly.
Then component A is the mixture by liquid component and powdery components, and the unit quantity of liquid component and powdery components
Unit quantity sums to 1.
The B component of 1 unit quantity includes 1-3 parts of Radix Stemonae extract, 0.1-0.5 parts of phellodendron extract, shrubby sophora extract 1-3
Part, 0.1-1 parts of mulberry bark extract, 5-10 parts of licorice, 3-15 parts of green-tea extract, 0.1-1 parts of mint extract.
Component A
In the present invention, the component A is made of liquid combination and powdery components.
Gotu Kola P.E
Centella, alias：Collapse jorum, Gotu Kola, blood clam shell grass, copper coin grass, is centellaed asiatica at membranaceous marshmarigold herb.Its nature and flavor bitter, acrid, cold.
It can clearing heat and promoting diuresis, removing toxicity for detumescence.
The ingredient of centella contains：Triterpenoid saponin, it is main to have asiaticosid, madecassoside, asiatic acid, centella
The ingredients such as sugar, thankuniside alkali.
As one embodiment of the present invention, in of the invention, the preparation method of the Gotu Kola P.E is as follows：
1. take centella, impurity is removed, is cleaned, segment is dried, and according to weight ratio is 1 by the centella after drying and water：
0.3 ratio mixing, is then added the benzene of 6.5 times of amounts of centella, and after being impregnated 30 minutes under 0 degree Celsius, 6% winestone is added
Acid carries out liquid-liquid anti-phase extraction, takes acid liquid, and it is 6-7 to adjust pH-value with ammonium hydroxide, is extracted with chloroform, takes chloroform solution；
2. taking chloroform solution, stand, be dehydrated, evaporated under reduced pressure, the absolute ethyl alcohols for being evaporated 2 times of amounts of rear product, stirring is then added
Afterwards, chloroform recovery is added, then is dehydrated with anhydrous sodium sulfate, is evaporated；
3. then using alumina column chromatography, benzene-chloroform (1：2) it elutes, takes back segment, the extract that rear end obtains is dissolved in
In absolute ethyl alcohol, stand, you can.
Gotu Kola P.E in the present invention can not only promote skin collagen to regenerate, and enhance cell basal layer cell
Vigor keeps elasticity of skin and consolidation；It is anti-oxidant, inhibit free radical activity, adjusts skin immunity；Desalinate melanin pigmentation,
Update skin cell regeneration；Increase skin water conservation degree, activation update skin cell；Antiallergic protective action, protects skin from outer
Boundary injures.Meanwhile containing a large amount of alkalescent substance in the Gotu Kola P.E that is prepared of preparation method provided by the invention,
It can accelerate the quick-fried body of acarid, promote the generation of excreta, reduce the allergy effect to skin.
Soapberry extract
Soapberry, alias：Wood is suffered from sub (Compendium of Materia Medica), and oil trouble sub (Sichuan) is bitter to suffer from tree (Hainan), yellow mesh tree, mesh wave tree
(Taiwan), You Luoshu, fruit of washing one's hands, elsewhere name：Rub mesh, false longan, Devil Frown etc. with the hands.
Its pericarp contains saponin, can do boxboard and wooden comb etc. for soap, timber.Root, browse, seed：Bitter, micro-pungent,
It is cold.It is slightly poisonous.Heat-clearing eliminating the phlegm, disperse accumulation desinsection.For diphtheria, abscess of throat, acute tonsillitis, cough, pertussis, food stagnation malnutrition due to parasitic infestation；It is used for outside
Trichomonas vaginalis.Benevolence：It is pungent, it puts down.Disperse accumulation wards off evil.For infantile malnutrition due to digestive disturbances or intestinalparasites, roundworm disease, inflatable in abdomen, halitosis.
In the present invention, the soapberry extract is the extract of soapberry fresh peel, and preparation method is as follows：
1. taking fresh soapberry pericarp, leachate is released after adding acetone soak 24 hours, repeats seepage pressure effects 2 times, is merged
Acetone solution；
2. acetone is recovered under reduced pressure, a small amount of ethyl acetate is added in filter residue and is stirred, filters, abandon solution, take product, so
Ethyl acetate is recrystallized afterwards, you can soapberry extract is prepared.
After the soapberry extract being prepared in the present invention can coordinate the processing quick-fried body of acarid with Gotu Kola P.E
Excreta wraps up excreta, after be detached from human body with the help of other costs.
Semen Tritici aestivi extract
Wheat refers to the caryopsis after wheat maturation in the present invention, in the present invention, the extract method of the Semen Tritici aestivi extract
It is as follows：
1. taking 5 parts by weight wheats, it is ground to crushing, the ether that 10 parts by weight are added extracts, and after extracting 10 hours, steams
It is dry, obtain extract；
2. the hydrochloric acid of 0.5mol/L, solid-liquid ratio 1 is added in the extract that step 1 is prepared：6, then extract 30 points
Zhong Hou takes supernatant, and Semen Tritici aestivi extract is obtained after concentration.
The Semen Tritici aestivi extract that the present invention is prepared can increase the effect of soapberry extract package acarid excreta, increase
Active force between acarid excreta and soapberry extract；It can be deep into inside skin with the effect of B component simultaneously,
Really improve the environment inside skin, improves originally greasy and less water content of stratum corneum situation；Its reason is extracted in wheat
Contain polyhydroxy substance in object, physiological reaction can occur with deep skin, fundamentally improve skin environment；Meanwhile this
Inventor has found that the stability of Semen Tritici aestivi extract is poor in the present invention, after being mixed with Fructus Rosae Laevigatae extract, Fructus Chebulae extract,
Its stability can be increased.
Fructus Rosae Laevigatae extract
The fruit of Cherokee rose, Chinese medicine name.For the dry mature fruit of rosaceous plant fruit of Cherokee rose Rosa laevigata Michx.,
Its is sour, sweet, puckery, mild-natured；Return kidney, bladder, large intestine channel.Its fruit includes citric acid, malic acid, tannin, resin, vitamin C,
Containing saponin 17.12%；Separately containing abundant carbohydrate, wherein have reduced sugar 60% (fructose 33%), sucrose 1.9%, and a small amount of shallow lake
Powder.
In the present invention, the preparation method of the fruit of Cherokee rose is as follows：Fruit of Cherokee rose powder is taken, 40-50 DEG C of hot water of 4 times of amounts is added,
Warm water impregnates 24 hours；Take leachate, be cooled to 5-8 DEG C, take filtrate by storng-acid cation exchange resin after, take exchange
Liquid, be concentrated under reduced pressure, take filtrate, after concentration drying Fructus Rosae Laevigatae extract can be prepared.
Fructus Chebulae extract
Myrobalan, is the dry mature fruit of combretaceae plant myrobalan or villus myrobalan, fruit containing tannin 23.60~
37.36%, ingredient is chebulinic acid, Chebulagic acid, 1,3,6- trigalloylglucoses and 1,2,3,4,6- five nutgall acyls
Glucose, terchebin, glucogallin, benzoaric acid and gallic acid etc..Contain shikimic acid, dehydrogenation thick grass again
Acid, quininic acid, arabinose, fructose, glucose, sucrose, rhamnose and amino acid, also contain Sennoside A, terchebin, tannase,
Polyphenol oxidase, peroxidase, ascorbic acid oxidase etc..
In the present invention, the preparation method of the Fructus Chebulae extract is as follows：
1. taking 1 parts by weight myrobalan that the methanol of 5 parts by weight is added, cold soaking is carried out, methanol extract liquid is taken, then carries out depressurizing dense
Contracting, obtains medicinal extract；
2. the medicinal extract that step 1 is obtained is in methanol/water/ethyl acetate (2：3：3) in the mixed solvent is extracted, extraction
After take ethyl acetate portion, be then concentrated to give paste, you can Fructus Chebulae extract is prepared.
Semen Cuscutae extract
This product is the dry mature seed of Cuscuta chinensis Lam. Cuscuta chinensis Lam..Autumn fruit at
Plant is harvested when ripe, is dried, seed is laid, and removes impurity.Its property sweet, warm；Return liver, kidney, the spleen channel.
In the present invention, the preparation method of the Semen Cuscutae extract is as follows：
1. taking 1 portion of Semen Cuscutae, crushes, after drying, after benzene cold soaking, take powder；
2. the first temperature leaching at 50 DEG C with 1% acetic acid, is soaked with 50 DEG C of hot water temperature again after filtering by powder, filtering takes filtrate；
3. the filtrate that step 2 is obtained abandons efflux after the exchange of highly acidic cation exchange column；
4. the exchange column in pair step 3 is washed with water to neutrality, it is used in combination the ammonium hydroxide of 0.15mol/L to elute, takes ammonium hydroxide eluent,
After being concentrated under reduced pressure again, ethyl alcohol crystallization, recrystallization is added, you can Semen Cuscutae extract is prepared.
Radix Stemonae extract
In the present invention, the Radix Stemonae extract includes Radix stemonae japonicae extract and radix stemonae tuberosae extract.The ratio of the two
It is 1：1.
Radix stemonae japonicae extract：The preparation method of heretofore described Radix stemonae japonicae extract is as follows：
1. taking Radix stemonae japonicae, segment is dried, by the Radix stemonae japonicae after drying and water according to 1：0.8 ratio mixing, then
The benzene of 5.3 times of amounts of Radix stemonae japonicae is added, 6% tartaric acid, which is added, after cold soaking carries out liquid-liquid anti-phase extraction, takes acid liquid, uses ammonia
It is 6-7 that water, which adjusts pH-value, is extracted with chloroform, takes chloroform solution；
2. taking chloroform solution, stand, be dehydrated, evaporated under reduced pressure, the absolute ethyl alcohols for being evaporated 3 times of amounts of rear product, stirring is then added
Afterwards, chloroform recovery is added, then is dehydrated with anhydrous sodium sulfate, is evaporated；
3. then using alumina column chromatography, benzene-chloroform (1：2) it elutes, takes back segment, the extract that leading portion obtains is dissolved in
In absolute ethyl alcohol, stand, you can obtain Radix stemonae japonicae extract.
Radix stemonae tuberosae extract：The preparation method of heretofore described radix stemonae tuberosae extract is as follows：
1. taking 1 parts by weight radix stemonae tuberosae that the methanol of 5 parts by weight is added, cold soaking is carried out, methanol extract liquid is taken, is then subtracted
Pressure concentration, obtains medicinal extract；
2. the medicinal extract that step 1 is obtained is in methanol/water/ethyl acetate (2：3：2) in the mixed solvent is extracted, extraction
After take ethyl acetate portion, be then concentrated into 0.3 times of content, you can radix stemonae tuberosae extract is prepared.
Phellodendron extract
Cortex Phellodendri, alias cork tree, first cypress, bark of a cork tree wood, property is bitter, trembles with fear, returns kidney, bladder warp.In the present invention, the phellodendron extract
Purchase extracts source from the Nanjing bio tech ltd Dao Sifu：The dry bark of rutaceae wampee or cork tree,
Its specification is 50：1.
Shrubby sophora extract
Kuh-seng, Chinese medicine name.For the dry root of legume kuh-seng.Its property is bitter, trembles with fear, the thoughts of returning home, liver, stomach, large intestine, bladder warp.
Its root contains a variety of alkaloids：D-Matrine, d-Oxymatrine, sophoranl l-Anagyrine, l- methylcytisines, that l- wears leaf is counterfeit
Indigo alkali and sophocarpine.Also contain flavonoids：Xanthohumol, isoxanthohumol, 3,4 ', 5-, tri- hydroxyl -7- methoxy -8- isoamylene radical chromocors, 8-
Isopentene group Kaempferol etc..Stem, the leaf glycosides of -7- containing cyanidenon.
In the present invention, the shrubby sophora extract is bought from Hunan Lang Lin living resources limited liability company.
Mulberry bark extract
The root bark of white mulberry, chemical composition containing umbelliferone, Scopoletin and flavone component morusin, mulberrin, mulberrochromene,
Cyclomulberrin, cyclomulberrochromene etc..
In the present invention, Anchang high mountain bio tech ltd, extraction source are westerly for the mulberry bark extract purchase
The dry root skin of moraceae plants mulberry；Its Extraction solvent is the mixture of water and ethyl alcohol.
Licorice
Radix Glycyrrhizae, alias：State is old, Herba Hedyotis cantonensis, Glycyrrhiza Uralensis, sweet tea root.Pulse family, Glycyrrhiza perennial herb, root and root shape
Stem thickness is strong, is a kind of help Chinese herbal medicine.
Its root and root-like stock contain glycyrrhizin 6~14%, are the sweet ingredient of Radix Glycyrrhizae, are a kind of triterpenoid saponins.
The leaf of Radix Glycyrrhizae contain chromocor compound, narcissin, nicotiflorin, rutin, Isoquercitrin, astragalin, uralenol,
Xin Wuer alcohol, uralenin, 3,3 '-dimethyl ether of Quercetin-, Uralenol-3-methylether, uralene, Quercetin etc.；Also contain crow
La Er Neogrosides.
In the present invention, the preparation method of the licorice is as follows：
1. taking 1 portion of Radix Glycyrrhizae, shred, add 4 parts of water, after impregnating 30 minutes, boil to 1 part of water, takes out；
2. after repeating step 1 twice, the water after boiling three times is collected, extracting solution is obtained；
3. the extracting solution that step obtains to be continued to the one third for being concentrated into former extracting liquid volume, concentrate is obtained；
4. the concentrated sulfuric acid is added in concentrate under stiring, it is acidified to and precipitation is no longer precipitated, stands；
5. collecting precipitation, it is washed with water to neutrality, it is dry to get licorice.
Green-tea extract
In the present invention, the preparation method of the green-tea extract is as follows：
1) 1 part of fresh green tea is taken, 50 mesh are crushed to, 30 parts of distilled water and 1 part of vitamin C is added, is mixed
Close object；
2) said mixture is placed in Ultrasound Instrument, by the effect of ultrasonic wave, then takes filtrate, you can obtain green tea
Extract；
Frequency is 30000 hertz, and the time is 20 minutes.
Mint extract
Peppermint, popular name are labiate, the chemical composition of mint extract is volatile oil, main in oily " lunar caustic grass "
To be I- menthols, 1- menthones and peppermint esters etc..
In the present invention, from the Nanjing bio tech ltd Pu Yi, shape of product is palm fibre for the mint extract purchase
Yellow powder, main technique are medicinal material-extraction-concentration-drying-granulation-tabletting.
As one embodiment of the present invention, the unit quantity ratio of the component A and B component is (1-3)：(0.5-1).
As one embodiment of the present invention, the unit quantity ratio of the liquid component and powdery components is (1-3)：(1-
2)。
As one embodiment of the present invention, the liquid component of 1 unit quantity include 1-5 parts of Gotu Kola P.E,
1-5 parts of soapberry extract, 0.1-0.5 parts of Semen Tritici aestivi extract, 0.1-0.3 parts of Fructus Rosae Laevigatae extract, Fructus Chebulae extract 0.01-
0.05 part, 5-10 parts of distilled water.
As one embodiment of the present invention, the liquid component of 1 unit quantity includes 2 parts of Gotu Kola P.E, nothing
Suffer from 3 parts of seed extract, 0.3 part of Semen Tritici aestivi extract, 0.2 part of Fructus Rosae Laevigatae extract, 0.03 part of Fructus Chebulae extract, 8 parts of distilled water.
As one embodiment of the present invention, the ingredient of the B component of 1 unit quantity includes：Radix Stemonae extract 1-3
Part, 0.1-0.5 parts of phellodendron extract, 1-3 parts of shrubby sophora extract, 0.1-1 parts of mulberry bark extract, 5-10 parts of licorice,
3-15 parts of green-tea extract, 0.1-1 parts of mint extract.
As one embodiment of the present invention, the ingredient of the B component of 1 unit quantity includes：2 parts of Radix Stemonae extract,
0.3 part of phellodendron extract, 2 parts of shrubby sophora extract, 0.6 part of mulberry bark extract, 6 parts of licorice, 8 parts of green-tea extract,
0.4 part of mint extract.
The application method of the composition containing plant extracts provided in the present invention is as follows：
1. clearing skin proportionally mixes the liquid component of component A and powdery components, after stirring, after generating gas,
Coated in skin surface, after 15 minutes, clean；
2. B component is coated in skin surface, after 15 minutes, cleans, carry out follow-up skin care step.
Mechanism is explained：Under certain moisture, temperature condition, acarid mad can be bred, while acarid can only be drained in life
Once, after acarid death, internal excreta can be retained in human body；Conventional fungicide, being capable of temporary killing mite
Worm, but the acarid excreta of that cannot be handled；Meanwhile the excreta of acarid is to block pore, causes the main of skin problem
One of problem.Composition provided by the invention containing plant extracts can promote the quick-fried body of acarid to drain, understand excreta
While, it keeps skin clean, maintains water and oil balance, avoid the generation again of acarid problem.
The composition provided by the invention containing plant extracts is described in detail with reference to specific embodiment.
Embodiment 1：The present embodiment provides a kind of composition containing plant extracts, the composition includes component A and B groups
Point, wherein：
The component A is made of liquid component and powdery components；
The liquid component of 1 unit quantity includes 2 parts of Gotu Kola P.E, 3 parts of soapberry extract, Semen Tritici aestivi extract
0.3 part, 0.2 part of Fructus Rosae Laevigatae extract, 0.03 part of Fructus Chebulae extract, 8 parts of distilled water；
The powdery components of 1 unit quantity include 2 parts of sodium bicarbonate powders, 3 parts of Semen Cuscutae extracts；
The ingredient of the B component of 1 unit quantity includes：2 parts of Radix Stemonae extract, 0.3 part of phellodendron extract, shrubby sophora extract
2 parts, 0.6 part of mulberry bark extract, 6 parts of licorice, 8 parts of green-tea extract, 0.4 part of mint extract.
The unit quantity of the component A and B component ratio is 2：1；The unit quantity of the liquid component and powdery components ratio is 2：
1。
Gotu Kola P.E：The preparation method of the Gotu Kola P.E is as follows：
1. taking centella, impurity is removed, is cleaned, segment is dried, by the centella after drying and water according to 1：0.3 ratio
Then the benzene of 6.5 times of amounts of centella is added in example mixing, after being impregnated 30 minutes under 0 degree Celsius, 6% tartaric acid is added and carries out
Liquid-liquid anti-phase extracts, and takes acid liquid, and it is 6-7 to adjust pH-value with ammonium hydroxide, is extracted with chloroform, takes chloroform solution；
2. taking chloroform solution, stand, be dehydrated, evaporated under reduced pressure, the absolute ethyl alcohols for being evaporated 2 times of amounts of rear product, stirring is then added
Afterwards, chloroform recovery is added, then is dehydrated with anhydrous sodium sulfate, is evaporated；
3. then using alumina column chromatography, benzene-chloroform (1：2) it elutes, takes back segment, the extract that rear end obtains is dissolved in
In absolute ethyl alcohol, stand, you can.
Soapberry extract：The soapberry extract is the extract of soapberry fresh peel, and preparation method is as follows：
1. taking fresh soapberry pericarp, leachate is released after adding acetone soak 24 hours, repeats seepage pressure effects 2 times, is merged
Acetone solution；
2. acetone is recovered under reduced pressure, a small amount of ethyl acetate is added in filter residue and is stirred, filters, abandon solution, take product, so
Ethyl acetate is recrystallized afterwards, you can soapberry extract is prepared.
Semen Tritici aestivi extract：The extract method of the Semen Tritici aestivi extract is as follows：
1. taking 5 parts by weight wheats, it is ground to crushing, the ether that 10 parts by weight are added extracts, and after extracting 10 hours, steams
It is dry, obtain extract；
2. the hydrochloric acid of 0.5mol/L, solid-liquid ratio 1 is added in the extract that step 1 is prepared：6, then extract 30 points
Zhong Hou takes supernatant, and Semen Tritici aestivi extract is obtained after concentration.
Fructus Rosae Laevigatae extract：The preparation method of the fruit of Cherokee rose is as follows：Fruit of Cherokee rose powder is taken, 40-50 DEG C of heat of 4 times of amounts is added
Water, warm water impregnate 24 hours；Take leachate, be cooled to 5-8 DEG C, take filtrate by storng-acid cation exchange resin after, take friendship
Change liquid, be concentrated under reduced pressure, take filtrate, after concentration drying Fructus Rosae Laevigatae extract can be prepared.
Fructus Chebulae extract：The preparation method of the Fructus Chebulae extract is as follows：
1. taking 1 parts by weight myrobalan that the methanol of 5 parts by weight is added, cold soaking is carried out, methanol extract liquid is taken, then carries out depressurizing dense
Contracting, obtains medicinal extract；
2. the medicinal extract that step 1 is obtained is in methanol/water/ethyl acetate (2：3：3) in the mixed solvent is extracted, extraction
After take ethyl acetate portion, be then concentrated to give paste, you can Fructus Chebulae extract is prepared.
Semen Cuscutae extract：The preparation method of the Semen Cuscutae extract is as follows：
1. taking 1 portion of Semen Cuscutae, crushes, after drying, after benzene cold soaking, take powder；
2. the first temperature leaching at 50 DEG C with 1% acetic acid, is soaked with 50 DEG C of hot water temperature again after filtering by powder, filtering takes filtrate；
3. the filtrate that step 2 is obtained abandons efflux after the exchange of highly acidic cation exchange column；
4. the exchange column in pair step 3 is washed with water to neutrality, it is used in combination the ammonium hydroxide of 0.15mol/L to elute, takes ammonium hydroxide eluent,
After being concentrated under reduced pressure again, ethyl alcohol crystallization, recrystallization is added, you can Semen Cuscutae extract is prepared.
The Radix Stemonae extract includes Radix stemonae japonicae extract and radix stemonae tuberosae extract.
Radix stemonae japonicae extract：The preparation method of heretofore described Radix stemonae japonicae extract is as follows：
1. taking Radix stemonae japonicae, segment is dried, by the Radix stemonae japonicae after drying and water according to 1：0.8 ratio mixing, then
The benzene of 5.3 times of amounts of Radix stemonae japonicae is added, 6% tartaric acid, which is added, after cold soaking carries out liquid-liquid anti-phase extraction, takes acid liquid, uses ammonia
It is 6-7 that water, which adjusts pH-value, is extracted with chloroform, takes chloroform solution；
2. taking chloroform solution, stand, be dehydrated, evaporated under reduced pressure, the absolute ethyl alcohols for being evaporated 3 times of amounts of rear product, stirring is then added
Afterwards, chloroform recovery is added, then is dehydrated with anhydrous sodium sulfate, is evaporated；
3. then using alumina column chromatography, benzene-chloroform (1：2) it elutes, takes back segment, the extract that leading portion obtains is dissolved in
In absolute ethyl alcohol, stand, you can obtain Radix stemonae japonicae extract.
Radix stemonae tuberosae extract：The preparation method of heretofore described radix stemonae tuberosae extract is as follows：
1. taking 1 parts by weight radix stemonae tuberosae that the methanol of 5 parts by weight is added, cold soaking is carried out, methanol extract liquid is taken, is then subtracted
Pressure concentration, obtains medicinal extract；
2. the medicinal extract that step 1 is obtained is in methanol/water/ethyl acetate (2：3：2) in the mixed solvent is extracted, extraction
After take ethyl acetate portion, be then concentrated into 0.3 times of content, you can radix stemonae tuberosae extract is prepared.
Phellodendron extract：The phellodendron extract is bought from the Nanjing bio tech ltd Dao Sifu.
Shrubby sophora extract：The shrubby sophora extract is bought from Hunan Lang Lin living resources limited liability company.
Mulberry bark extract：The mulberry bark extract buys Anchang high mountain bio tech ltd westerly.
Licorice：The preparation method of the licorice is as follows：
1. taking 1 portion of Radix Glycyrrhizae, shred, add 4 parts of water, after impregnating 30 minutes, boil to 1 part of water, takes out；
2. after repeating step 1 twice, the water after boiling three times is collected, extracting solution is obtained；
3. the extracting solution that step obtains to be continued to the one third for being concentrated into former extracting liquid volume, concentrate is obtained；
4. the concentrated sulfuric acid is added in concentrate under stiring, it is acidified to and precipitation is no longer precipitated, stands；
5. collecting precipitation, it is washed with water to neutrality, it is dry to get licorice.
Green-tea extract：The preparation method of the green-tea extract is as follows：
1) 1 part of fresh green tea is taken, 50 mesh are crushed to, 30 parts of distilled water and 1 part of vitamin C is added, is mixed
Close object；
2) said mixture is placed in Ultrasound Instrument, by the effect of ultrasonic wave, then takes filtrate, you can obtain green tea
Extract；
Frequency is 30000 hertz, and the time is 20 minutes.
Mint extract：The mint extract is bought from the Nanjing bio tech ltd Pu Yi.
The application method of the composition containing plant extracts provided in the present invention is as follows：
1. clearing skin proportionally mixes the liquid component of component A and powdery components, after stirring, after generating gas,
Coated in skin surface, after 15 minutes, clean；
2. B component is coated in skin surface, after 15 minutes, cleans, carry out follow-up skin care step.
Embodiment 2：The present embodiment provides a kind of composition containing plant extracts, the composition includes component A and B groups
Point, wherein：
The component A is made of liquid component and powdery components；
The liquid component of 1 unit quantity includes 1 part of Gotu Kola P.E, 1 part of soapberry extract, Semen Tritici aestivi extract
0.1 part, 0.1 part of Fructus Rosae Laevigatae extract, 0.01 part of Fructus Chebulae extract, 5 parts of distilled water；
The powdery components of 1 unit quantity include 2 parts of sodium bicarbonate powders, 3 parts of Semen Cuscutae extracts；
The ingredient of the B component of 1 unit quantity includes：1 part of Radix Stemonae extract, 0.1 part of phellodendron extract, shrubby sophora extract
1 part, 0.1 part of mulberry bark extract, 5 parts of licorice, 3 parts of green-tea extract, 0.1 part of mint extract.
The unit quantity of the component A and B component ratio is 2：1；The unit quantity of the liquid component and powdery components ratio is 2：
1。
Remaining is same as Example 1.
Embodiment 3：The present embodiment provides a kind of composition containing plant extracts, the composition includes component A and B groups
Point, wherein：
The component A is made of liquid component and powdery components；
The liquid component of 1 unit quantity includes 5 parts of Gotu Kola P.E, 5 parts of soapberry extract, Semen Tritici aestivi extract
0.5 part, 0.3 part of Fructus Rosae Laevigatae extract, 0.05 part of Fructus Chebulae extract, 10 parts of distilled water；
The powdery components of 1 unit quantity include 2 parts of sodium bicarbonate powders, 3 parts of Semen Cuscutae extracts；
The ingredient of the B component of 1 unit quantity includes：3 parts of Radix Stemonae extract, 0.5 part of phellodendron extract, shrubby sophora extract
3 parts, 1 part of mulberry bark extract, 10 parts of licorice, 15 parts of green-tea extract, 1 part of mint extract.
The unit quantity of the component A and B component ratio is 2：1；The unit quantity of the liquid component and powdery components ratio is 2：
1。
Remaining is same as Example 1.
Embodiment 4：Difference lies in the component A does not have powdery components, only liquid component with embodiment 1.
Embodiment 5：Difference lies in described the present embodiment provides a kind of composition containing plant extracts with embodiment 1
Composition includes Gotu Kola P.E, soapberry extract, Semen Tritici aestivi extract, Fructus Rosae Laevigatae extract, Fructus Chebulae extract, distillation
Water, Radix Stemonae extract, phellodendron extract, shrubby sophora extract, mulberry bark extract, licorice, green-tea extract, peppermint carry
Take object, parts by weight same as Example 1；I.e. component A is mixed with B component in the present embodiment, and component A does not include powdery components.
Embodiment 6：Difference lies in the component A does not include Gotu Kola P.E with embodiment 1.
Embodiment 7：Difference lies in the component A does not include soapberry extract with embodiment 1.
Embodiment 8：Difference lies in the component A does not include Semen Tritici aestivi extract with embodiment 1.
Embodiment 9：Difference lies in the component A does not include Fructus Rosae Laevigatae extract, Fructus Chebulae extract with embodiment 1.
Embodiment 10：With embodiment 1 difference lies in, in the B component, Radix Stemonae extract be Radix stemonae japonicae extract,
Not comprising radix stemonae tuberosae extract.
Embodiment 11：Difference lies in the preparation method of the Gotu Kola P.E is as follows with embodiment 1：
1. taking centella, impurity is removed, is cleaned, segment is dried, by the centella after drying and water according to 1：0.3 ratio
Then the benzene of 6.5 times of amounts of centella is added in example mixing, after being impregnated 30 minutes under 0 degree Celsius, 6% tartaric acid is added and carries out
Liquid-liquid anti-phase extracts, and takes acid liquid, and it is 6-7 to adjust pH-value with ammonium hydroxide, is extracted with chloroform, takes chloroform solution；
2. taking chloroform solution, stand, be dehydrated, evaporated under reduced pressure, the absolute ethyl alcohols for being evaporated 2 times of amounts of rear product, stirring is then added
Afterwards, chloroform recovery is added, then is dehydrated with anhydrous sodium sulfate, is evaporated；
3. then using alumina column chromatography, benzene-chloroform (1：2) it elutes, takes back segment, the extract that front end obtains is dissolved in
In absolute ethyl alcohol, stand, you can.
Embodiment 12：Difference lies in the skins of wiper with embodiment 1：Water content of stratum corneum is less than 10%, and sebum
Secrete less crowd (i.e. dry skin).
Performance test：
Suitable subject 50 is selected, is tested for the property according to above-mentioned application method.
1. except mite rate：The grease on skin is scraped using scraping blade before test, mite is observed using the method for micro- sem observation
Borer population amount；After being used continuously for 3 week, mite population is observed again.Then ratio=(number of the preceding acarid of use of except mite is calculated
The quantity of the rear acarid of amount-use)/use the quantity of preceding acarid.
The scar 2. antipruritic, whitening of deoiling is dispelled：The elimination situation of subject's face itch, hair follicle pityriasis, whelk is observed simultaneously.
The symptom resolutions such as its septum reset itch, hair follicle pityriasis, whelk are denoted as effective；The diseases such as facial itch, hair follicle pityriasis, whelk
Shape past release is denoted as effectively；The symptoms such as facial itch, hair follicle pityriasis, whelk are not released and are denoted as in vain.
3. testing the water content of stratum corneum and sebum secretion situation of subjects skin.
Test result：
Example above-mentioned is merely illustrative, some features of the feature for explaining the disclosure.The attached claims
It is intended to the range as wide as possible for requiring to be contemplated that, and embodiments as presented herein is only according to all possible embodiment
Combination selection embodiment explanation.Therefore, the purpose of applicant is that the attached claims are not illustrated the present invention
Feature exemplary selectional restriction.And the progress in science and technology will be formed language express inaccuracy due to and not
The possible equivalent or son being presently considered are replaced, and these variations also should in the conceived case be interpreted by appended
Claim covers.
Claims (10)
1. a kind of composition containing plant extracts, which is characterized in that the composition includes component A and B component, wherein：
The component A is made of liquid component and powdery components；
The liquid component includes Gotu Kola P.E, soapberry extract, Semen Tritici aestivi extract, Fructus Rosae Laevigatae extract, He Ziti
Take object and distilled water；
The powdery components include sodium bicarbonate powder and Semen Cuscutae extract；
The ingredient of the B component includes：Radix Stemonae extract, phellodendron extract, shrubby sophora extract, mulberry bark extract, Radix Glycyrrhizae carry
Take object, green-tea extract and mint extract.
2. a kind of composition containing plant extracts described in claim 1, which is characterized in that in parts by weight, 1 unit quantity
The liquid component include 1-5 part of Gotu Kola P.E, it is 1-5 parts of soapberry extract, 0.1-0.5 parts of Semen Tritici aestivi extract, golden
0.1-0.3 parts of cherry seed extract, 0.01-0.05 parts of Fructus Chebulae extract, 5-10 parts of distilled water.
3. a kind of composition containing plant extracts described in claim 1, which is characterized in that in parts by weight, 1 unit quantity
The ingredient of the B component include：1-3 parts of Radix Stemonae extract, 0.1-0.5 parts of phellodendron extract, 1-3 parts of shrubby sophora extract, mulberry
White 0.1-1 parts of bark extract, 5-10 parts of licorice, 3-15 parts of green-tea extract, 0.1-1 parts of mint extract.
4. a kind of composition containing plant extracts described in claim 1, which is characterized in that the list of the component A and B component
Position amount is than being (1-3)：(0.5-1).
5. a kind of composition containing plant extracts described in claim 1, which is characterized in that the liquid component and powder group
The unit quantity ratio divided is (1-3)：(1-2).
6. a kind of composition containing plant extracts described in claim 2, which is characterized in that in parts by weight, 1 unit quantity
The liquid component include 2 parts of Gotu Kola P.E, 3 parts of soapberry extract, 0.3 part of Semen Tritici aestivi extract, the fruit of Cherokee rose extraction
0.2 part of object, 0.03 part of Fructus Chebulae extract, 8 parts of distilled water.
7. a kind of composition containing plant extracts described in claim 3, which is characterized in that in parts by weight, 1 unit quantity
The ingredient of the B component include：2 parts of Radix Stemonae extract, 0.3 part of phellodendron extract, 2 parts of shrubby sophora extract, root bark of white mulberry extraction
0.6 part of object, 6 parts of licorice, 8 parts of green-tea extract, 0.4 part of mint extract.
8. a kind of composition containing plant extracts described in claim 1, which is characterized in that the Radix Stemonae extract includes climing
Raw Radix Stemonae extract and radix stemonae tuberosae extract.
9. a kind of composition containing plant extracts described in claim 1, which is characterized in that it is used to remove acarid, whitening
It dispels scar.
10. a kind of except mite personal care articles, it includes combination of the claim 1-8 any one of them containing plant extracts
Object.
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| CN109528594A (en) * | 2018-12-29 | 2019-03-29 | 广州睿森生物科技有限公司 | A kind of composite efficacy type anticorrosive composite and its application |
| CN111789786A (en) * | 2020-08-13 | 2020-10-20 | 广州广妆生物科技有限公司 | Mite-killing plant composition and preparation method and application thereof |
| CN111904919A (en) * | 2020-08-13 | 2020-11-10 | 广州广妆生物科技有限公司 | Mite-killing conditioner, shower gel and preparation method thereof |
| CN111920732A (en) * | 2020-08-13 | 2020-11-13 | 广州广妆生物科技有限公司 | Mite-killing conditioner, shampoo and preparation method thereof |
| CN111920733A (en) * | 2020-08-13 | 2020-11-13 | 广州广妆生物科技有限公司 | Mite-removing conditioner, facial cleanser and preparation method of mite-removing conditioner |
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| CN111920732B (en) * | 2020-08-13 | 2023-01-06 | 广州极男化妆品有限公司 | Mite-killing conditioner, shampoo and preparation method thereof |
| CN111920733B (en) * | 2020-08-13 | 2023-01-06 | 广州极男化妆品有限公司 | Mite-removing conditioner, facial cleanser and preparation method of mite-removing conditioner |
| CN111904919B (en) * | 2020-08-13 | 2023-04-07 | 广州极男化妆品有限公司 | Mite-killing conditioner, shower gel and preparation method thereof |
| CN113143781A (en) * | 2021-05-19 | 2021-07-23 | 成都农业科技中心 | Whitening, moisturizing and skin-protecting composition containing lithocarpus litseifolius extract and preparation thereof |
| CN113143781B (en) * | 2021-05-19 | 2022-10-25 | 中国农业科学院都市农业研究所 | Whitening, moisturizing and skin-protecting composition containing lithocarpus litseifolius extract and preparation thereof |
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