CN104825351B - A kind of Lignum Aquilariae Resinatum whitening cleansing facial milk containing and preparation method thereof - Google Patents
A kind of Lignum Aquilariae Resinatum whitening cleansing facial milk containing and preparation method thereof Download PDFInfo
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Abstract
The present invention relates to natural skin care product technical field, particularly relate to a kind of Lignum Aquilariae Resinatum whitening cleansing facial milk containing and preparation method thereof, Lignum Aquilariae Resinatum whitening cleansing facial milk containing, is made up of the raw material of following mass percent: Lignum Aquilariae Resinatum extract 2 8%, Chinese herbal medicine extract 5 18%, Aloe extract 2 10%, lecithin 1 1.5%, TWEEN 80 2 4%, compound vitamin 4 8%, citric acid 1 2%, 2-pyrrolidone-5-carboxylic acid's macrogol ester 7 15%, cocamidopropyl betaine (CAB 35) 25 40% and deionized water surplus.The cleansing milk of the present invention is with pure natural and has fragrance and the Lignum Aquilariae Resinatum of skin care effect and Chinese herbal medicine extract as active ingredient, compound certain emulsified component lecithin and natural complex are made, energy skin whitening, desalination calm pigment, dispelling stain, holding moisture of skin, can kill or suppress to be attached to the antibacterial of skin surface, can also slow down aging, promote epithelial tissue regeneration.
Description
Technical field
The present invention relates to natural skin care product technical field, particularly relate to a kind of Lignum Aquilariae Resinatum whitening cleansing facial milk containing and preparation method thereof.
Background technology
Along with the fast development of society, the raising of people's living standard and the raising of aesthetical standard, increasing people couple
The nursing of skin has had higher requirement.
Cleansing milk is popular widely used facial cleansing agent, but most of cleansing milk in the market are all with each
Plant the clean-up performance that chemical raw material is formulated, the best, also relatively big by the zest of chemical raw material, easily cause skin
Allergy, on the other hand, Nails advocates pale skin, and westerner grows tender of dispelling of various mottle.Chemical raw material be difficult to by
Skin absorption, and natural component is easily absorbed, effect is stable persistently, fundamentally solves the practical problem of whitening and skin-protecting.
Therefore, we are in the urgent need to a kind of novel whitening cleansing milk, both pure natural, have no side effect, nonhazardous, easily absorb,
Give off a strong fragrance, sample pure and fresh uniqueness, there is skin whitening, desalination calm pigment, dispelling stain, effective nursing skin, tender flesh
The effects such as skin.
Summary of the invention
The technical problem to be solved is to provide a kind of Lignum Aquilariae Resinatum whitening cleansing facial milk containing and preparation method thereof, and it has system
Preparation Method is simple, the cleansing milk pure natural for preparing, have no side effect, nonhazardous, non-stimulated, easily absorb, have skin whitening, desalination heavy
The effects such as pigment, dispelling stain, effective nursing skin, tender skin.
For achieving the above object, the technical solution used in the present invention is as follows:
A kind of Lignum Aquilariae Resinatum whitening cleansing facial milk containing, is made up of the raw material of following mass percent: Lignum Aquilariae Resinatum extract 2-8%, Chinese herbal medicine carry
Take thing 5-18%, Aloe extract 2-10%, emulsifier lecithin 1-1.5%, stabilizer T WEEN 80(tween 80) 2-4%,
Synergist compound vitamin 4-8%, preservative citric acid 1-2%, wetting agent 2-pyrrolidone-5-carboxylic acid macrogol ester 7-15%, surface
Activating agent cocamidopropyl betaine (CAB-35) 25-40% and deionized water surplus.
Lignum Aquilariae Resinatum extract mainly has antiinflammatory, antioxidative effect and gives the fragrance that product is pure and fresh, graceful.Chinese herbal medicine carries
Take each component in thing and reached the purpose of whitening, speckle dispelling by different mechanism.Aloe extract mainly provides moisturizing and nursing
The effect of skin care.Emulsifying agent has been mainly emulsifying, decontamination.Stabilizer can improve the stability of product.Synergist is assisted
Help each point of more preferable effect of promotion.Preservative protection product, extends the product shelf phase.Wetting agent is to maintain, supplements skin keratin
Moisture in Ceng.Surfactant have moistening, disperse, foam, decontamination, emulsifying five act on greatly, the emulsifying capacity of oils and fats is reached
To cleaning effect, it it is the chief active thing of face cleaning product.Moisture can go out the secretions of sweat gland and water solublity dirt.
Wherein, the preparation method of described Lignum Aquilariae Resinatum extract is: choose the Lignum Aquilariae Resinatum of high-quality, cuts into Lignum Aquilariae Resinatum thin slice, then will
Lignum Aquilariae Resinatum thin slice is crushed to 30-60 mesh, puts in High-pressure supercritical extraction equipment, is passed through CO2, maintain 40-in a high voltage state
After 60min, moment pressure release, take out, add the mixed solvent of Lignum Aquilariae Resinatum weight 5-8 times, low-temperature extraction after 0.5-1.5 hour from
The heart filters, and filtrate is concentrated into moisture again after Middle hollow fiber membrane and is less than 5%, obtains Lignum Aquilariae Resinatum extract.Described high-quality
Lignum Aquilariae Resinatum refer to resiniferous Lignum Aquilariae Resinatum heartwood.
Wherein, in the preparation method of described Lignum Aquilariae Resinatum extract, high pressure conditions is 40-60MPa；Mixed solvent is hydrogenated castor
Oil, propylene glycol, deionized water are the mixture of 1:3:6 in mass ratio；Middle hollow fiber membrane condition is for using molecular cut off
The pvdf membrane of 100000, operation pressure is 0.05-0.3MPa, and feed velocity is 600ml/min, and operation temperature is 30-35 DEG C.
Lignum Aquilariae Resinatum contains the cellularity of densification, and common extraction means are difficult to the extracts active ingredients in Lignum Aquilariae Resinatum fine, soft fur
Completely.This experiment is at high pressure CO2Unexpected pressure release under process, well can carry out breaking cellular wall to Lignum Aquilariae Resinatum cell, and pollution-free；With
Time add castor oil hydrogenated and propylene glycol, contribute under cryogenic by low pole active principle microcapsules, it is ensured that follow-up
Centrifugation step in active component be present in centrifugal liquid；It addition, mixed solvent also rises for final Lignum Aquilariae Resinatum extract product
Effect to stable system.
Utilizing supercritical extraction to prepare Lignum Aquilariae Resinatum extracting solution, this extracting process is green, the modernization abstraction technique of environmental protection.
Gentle extraction conditions can keep the effective ingredient in Lignum Aquilariae Resinatum and fragrant ingredient activity to greatest extent.Lignum Aquilariae Resinatum: acrid in the mouth, hardship,
Slightly warm in nature, returns the effects such as spleen, stomach, kidney, lung meridian, tool promoting the circulation of QI to relieve pain, warming middle-JIAO to arrest vomiting, helping inspiration to relieve asthma.In addition Lignum Aquilariae Resinatum has antibiotic effect
Immunity, centre of equilibrium can be increased again neural, manage all gas and adjust, help circulation of qi promoting to enter fixed effect.Lignum Aquilariae Resinatum extracting solution contains multiple
Functional components such as flavonoid and agilawood essential oil.In Lignum Aquilariae Resinatum extract, functional components such as flavone etc. have antiinflammatory, antioxidative
Effect, has effect of whitening, slow down aging.Agilawood essential oil is the essential part in Lignum Aquilariae Resinatum extract, not only antibacterium, disease
Poison, mycete, can anti-inflammation, promote cell metabolism and cell regeneration function.And give the fragrance that product is strong, graceful,
Make people's body and mind joyful.
Wherein, described Chinese herbal medicine extract preparation method is: Radix Scutellariae, Radix Glycyrrhizae, Radix Rhodiolae, Flos Matricariae chamomillae, Rhizoma Chuanxiong, Radix Et Rhizoma Rhei are pressed
Mass ratio is the mixture of the ratio composition of 3:1-3:1-3:1-3:1-2:1, is crushed to 150-250 mesh, and adding 4-6 times of concentration is
2 hours post-heating of the alcohol solution dipping of 40% are boiling for 60 minutes decocting, and are filtered to remove filtering residue, collect filtrate and concentrate, dense
Being reduced to 2 times of raw material quality, add weight 1-2% clarifier, centrifugal after clarifying treatment, supernatant adds concentrated solution weight
The polysorbas20 of amount 0.1%-0.5% and the propylene glycol of concentrated solution weight 45%, be Chinese herbal medicine extract after stirring and dissolving.
Radix Scutellariae: bitter, cold, return lung, gallbladder, spleen, large intestine, small intestine meridian, there is heat clearing and damp drying, rush down people's removing toxic substances, hemostasis, antiabortive merit
Effect.Plant sun agent, the baicalin in extract can absorb the ultraviolet of 230 ~ 350nm, suppresses melanocyte proliferation.
Radix Glycyrrhizae: sweet, flat, GUIXIN, lung, spleen, stomach warp, there is invigorating the spleen and replenishing QI, heat-clearing and toxic substances removing, expelling phlegm for arresting cough, relieving spasm to stop pain.Carry
Take the competitive inhibitor that several flavones ingredients in thing are tryrosinases, it is possible to suppress melanic formation, have moisturizing, U.S.
In vain, effect such as light speckle, reparation injured skin.Coordinating the actions of various ingredients in a prescription is had, effect that cushion is strong in this formula.
Radix Rhodiolae: cold, sweet, puckery, returns lung meridian, has QI invigorating lung heat clearing, Fructus Alpiniae Oxyphyllae to nourish heart, effect of hemostasis with astringents, dissipating blood stasis for subsidence of swelling.Carry
Take the coumaric acid in thing and can suppress melanic formation in cell.
Flos Matricariae chamomillae: mildly bitter flavor, Gan Xiang, improving eyesight, moves back liver-fire.Containing endothelin antagonist in extract, in being a kind of antagonism
Pi Su, suppression melanocyte generates.
Rhizoma Chuanxiong: pungent, temperature, return liver, gallbladder meridian.Activating QI to alleviate the depression, method wind-dryness is wet, promoting blood circulation and stopping pain.Microcirculqtory system is had by extract
Good regulation effect, its infusion has stronger restraint to some pathogenic dermatophytes.Extract can also suppress cheese ammonia
The activity of acid enzyme, thus black speck, freckle, senile plaque can be played therapeutical effect.
Radix Et Rhizoma Rhei: bitter, cold.Return spleen, stomach, large intestine, liver, pericardium channel.Purging heat and dredging bowels, removing pathogenic heat from blood and toxic substance from the body, eliminating blood stasis and inducing menstruation.In extract
Containing procyanidin, melanin can be made to fade.
Containing multiple effective efficiency composition in extracts of Chinese herbal medicine, above-mentioned formula is used in conjunction with, mutually coordinated, by having
Imitate sun-proof, effect and suppress melanic formation, the regulation mechanism such as human metabolism, make that human body skin is pale, delicate, mottle is light
Change.
Wherein, in described Chinese herbal medicine extract preparation method, clarifier is chitosan quaternary ammonium salt, and clarification condition is, adds
The clarifier aqueous solution of concentrated solution weight 0.5%-2%, mass concentration is 1%, at normal temperatures after stirring 5-10min, stands 24h.
Chinese herbal medicine through too low alcohol extraction process, a lot of macromole as pectin, starch, cellulose, pigment etc. also can be in the lump
Bring product into.Chitosan quaternary ammonium salt belongs to the natural clarifying agent that a class extracts from marine organisms.This clarifier can be effective
Being removed by these macromolecular substances, and only retain required active component, clarification steps also ensure that Chinese herbal medicine carries simultaneously
The color taking thing is unlikely to too deep, affects outward appearance.
Wherein, the preparation method of described Aloe extract is: by fresh Aloe vulgaris blade peeling, chopping, add
The complex enzyme zymohydrolysis of weight 0.2%-0.6%, enzymolysis solution through enzyme denaturing, centrifugal after obtain the Aloe extract of clear.
Aloe vulgaris be few in number can one of edible health Aloe, safety is higher.Aloe vulgaris blade width
The most abundant, in leaf, spongy tissue (i.e. Aloe gel) is the abundantest, and the molecular weight of its polysaccharide body up to 450,000, is Aloe arborescens var. natalensis
More than 40 times, beauty treatment health care efficacy is the most notable compared with other Aloes.Aloe vulgaris present large area commercialization is planted
Training, material source is more secure.
Wherein, in described Aloe extract preparation method, compound enzyme be liquid cellulase, pectinase in mass ratio
For the mixture of 3:7, enzymatic hydrolysis condition is 37 DEG C, 1 hour.By enzymolysis, can effectively aloe pulp be liquefied, degraded cellulose
And pectin etc., the effective ingredient maintaining Aloe extract to greatest extent does not runs off, and is also convenient for follow-up interpolation and uses.
Aloe: bitter, cold, returns liver, stomach, large intestine channel.Removing heat from the liver, relieving constipation.Containing Aloe gel, barbaloin, many in extract
Plant vitamin, aminoacid and mucopolysaccharide.A kind of extraordinary plant type wetting agent of Aloe, has lubrication, moisturizing, whitening, antiinflammatory
Etc. effect.Aloe also has preferable anti-sunlight function.
Wherein, described centrifugal condition is 4000rpm-8000rpm, and the time is 15-30min.
Wherein, described compound vitamin is that vitamin C, vitamin E, vitamin A, vitamin B2 are in mass ratio for 1-4:1-
The scalemic thereof of 4:1-3:1-3.
Vitamin B2: help Cellular respiration, assists lipid metabolism, prevents acne, hair follicle, acne rosacea.
Vitamin C: the synthesis of stimulation collagen, thus increase skin elasticity, use the spoke that can prevent ultraviolet continuously
Penetrate.There is the effect strengthening leukocytes phagocytic pyogenic baeceria.Melanin can be reduced to melanin antecedent so that melanin quantity reduces
Melanin can be reduced to melanin antecedent so that melanin quantity reduces.
Vitamin A: grow and supplement soma, keeps skin slip, infects from antibacterial.To skin sore, burn, dryness
Skin has the function of auxiliary treatment.
Vitamin E: protection cell.It is mainly used in improving dry skin, moistens tender skin.Antioxidation, strengthening can be promoted
Cell membrane, enhances metabolism, and protection skin resists uv damage.
The major function that Four Vitamins is had nothing in common with each other, compound use can be mutually coordinated, is complementary to one another, and can play more preferably
Effect.
The preparation method of a kind of Lignum Aquilariae Resinatum whitening cleansing facial milk containing, comprises the following steps:
Step 1): in the reactor containing deionized water by proportioning add lecithin, TWEEN 80, compound vitamin and
2-pyrrolidone-5-carboxylic acid's macrogol ester, is slowly stirred uniformly and is warming up to 80-90 DEG C；
Step 2): add cocamidopropyl betaine, after stirring, start cooling；
Step 3): be naturally cooling to 50 DEG C and add continuation cooling after appropriate citric acid stirs；
Step 4): be naturally cooling to 40-45 DEG C and add Lignum Aquilariae Resinatum extract, Chinese herbal medicine extract, Aloe extract, continue to stir
Mix；
Step 5): add deionized water and stir, natural conditions borehole cooling to 35 DEG C discharging, prepare Lignum Aquilariae Resinatum whitening and wash one's face
Milk.
In the preparation method of described Lignum Aquilariae Resinatum whitening cleansing facial milk containing, first the material not readily dissolved is dissolved at relatively high temperatures,
Mixing, the material of non-refractory, as extracted species, due to the composition easily affected by high temperature containing some, destroy, so treating that temperature drops
Add after low, it is ensured that each raw material gives full play to its active ingredient, and prepared Lignum Aquilariae Resinatum whitening cleansing facial milk containing skin effect is good.
The beneficial effects of the present invention is: the present invention, with natural plants, Chinese herbal medicine as raw material, focuses on natural product with modern
The combination of advanced extractive technique, according to pigmentation, the formation mechenism of mottle, selects the formula being suitable for the most.The present invention washes
Face milk pure natural, have no side effect, nonhazardous, non-stimulated, easily absorb；Each effective ingredient can be mutually coordinated, has skin whitening, desalination
The effects such as calm pigment, dispelling stain, effective nursing skin, tender skin.
The Lignum Aquilariae Resinatum whitening cleansing facial milk containing of the present invention is with pure natural and has fragrance and the Lignum Aquilariae Resinatum of skin care effect and Chinese herbal medicine extracting
Thing is active ingredient, and compound certain emulsified component lecithin and natural complex are made, can skin whitening, the calm color of desalination
Element, dispelling stain, holding moisture of skin, can kill or suppress to be attached to the antibacterial of skin surface, moreover it is possible to slow down aging, in promotion
Skin tissue regeneration.Can remove oils and fats and dust on skin, reach the purpose thoroughly cleaned, moisturizing, gentleness are non-stimulated.
Detailed description of the invention
Embodiment 1
A kind of Lignum Aquilariae Resinatum whitening cleansing facial milk containing, is made up of the component of following mass percent [U1]:
Lignum Aquilariae Resinatum extract 5%, Chinese herbal medicine extract 8%, Aloe extract 10%, lecithin 1.5%, TWEEN 80 4%, multiple
Close vitamin 6%, citric acid 1.5%, 2-pyrrolidone-5-carboxylic acid's macrogol ester 10%, cocamidopropyl betaine (CAB-35)
28% and deionized water 26%.
Described compound vitamin, is made up of the component of following mass percent: vitamin C 30%, vitamin E 30%, dimension
Raw element A 20%, vitamin B 20%.
A kind of preparation method of Lignum Aquilariae Resinatum extract:
Choose the Lignum Aquilariae Resinatum 100g of high-quality, cut into Lignum Aquilariae Resinatum thin slice, then Lignum Aquilariae Resinatum thin slice is crushed to 40 mesh, put into high pressure and surpass
In critical extraction equipment, it is passed through CO2, after maintaining 60min under 40 MPa high pressure conditions, moment pressure release.Obtain 10g extract, then
Adding the mixed solvent of 60g, mixed solvent is the mixture of castor oil hydrogenated, propylene glycol, deionized water, and mixed proportion is 1:3:
6.4 DEG C of low-temperature extractions after 1 hour 5000rpm be centrifuged 15min, filter.Filtrate is again through the pvdf membrane of molecular cut off 100,000, behaviour
Being 0.2MPa as pressure, feed velocity is 600ml/min, and operation temperature is 30 DEG C, reduces pressure through Middle hollow fiber membrane final vacuum
It is concentrated into moisture and is less than 5%, obtain 30g Lignum Aquilariae Resinatum extract.
The preparation method of a kind of Chinese herbal medicine extract: by six in Radix Scutellariae, Radix Glycyrrhizae, Radix Rhodiolae, Flos Matricariae chamomillae, Rhizoma Chuanxiong, Radix Et Rhizoma Rhei
Plant mixture (mass ratio is followed successively by 3:1:2:2:1:1) 100g and be crushed to 200 mesh, add 500g 40% alcohol solution dipping 2 hours
Post-heating is boiling for 60 minutes decocting, and is filtered to remove filtering residue, collects filtrate and is concentrated into 200g.Add 3g clarifier, clear
Clear agent is chitosan quaternary ammonium salt, and mass concentration is 1%；After stirring 5-10min under room temperature, stand 24h, 4000rpm after clarifying treatment
Centrifugal 20min, supernatant adds the polysorbas20 of 0.54g and the propylene glycol of 81g, is 260g Chinese herbal medicine extracting after stirring and dissolving
Thing.
A kind of Aloe extract preparation method: by fresh 100g Aloe vulgaris blade peeling, chopping, add 0.4g's
Complex enzyme zymohydrolysis, compound enzyme is the mixture of liquid cellulase, pectinase, and ratio is 3:7；37 DEG C of enzymolysis 1 hour, warp
85 DEG C of water-bath 10min enzyme denaturing are lived, and 4000rpm obtains the Aloe extract of 65g clear after being centrifuged 15min.
The preparation method of a kind of Lignum Aquilariae Resinatum whitening cleansing facial milk containing, sequentially includes the following steps:
Step 1): be proportionally added into lecithin, TWEEN 80, compound dimension life in the reactor containing appropriate amount of deionized water
Element and 2-pyrrolidone-5-carboxylic acid's macrogol ester, be slowly stirred uniformly and be warming up to 90 DEG C；
Step 2): add cocamidopropyl betaine, after stirring, start cooling；
Step 3): be naturally cooling to 50 DEG C and add continuation cooling after citric acid stirs；
Step 4): be naturally cooling to 40 DEG C and add Lignum Aquilariae Resinatum extract, Chinese herbal medicine extract, Aloe extract, continue stirring；
Step 5): add appropriate amount of deionized water stirring to after the most thick, be naturally cooling to 35 DEG C of dischargings, prepare Lignum Aquilariae Resinatum whitening and wash
Face milk.
Embodiment 2
A kind of Lignum Aquilariae Resinatum whitening cleansing facial milk containing, is made up of the component of following mass percent:
Lignum Aquilariae Resinatum extract 6%, Chinese herbal medicine extract 14%, Aloe extract 9%, lecithin 1%, TWEEN 80 2%, compound
Vitamin 5%, citric acid 1.5%, 2-pyrrolidone-5-carboxylic acid's macrogol ester 9%, cocamidopropyl betaine (CAB-35)
26.5% and deionized water 26%.
The matter of six kinds of mixture in Radix Scutellariae, Radix Glycyrrhizae, Radix Rhodiolae, Flos Matricariae chamomillae, Rhizoma Chuanxiong, Radix Et Rhizoma Rhei in described Chinese herbal medicine extract
Amount ratio is followed successively by 3:1:2:2:1:1.
Described compound vitamin, is made up of the component of following mass percent: vitamin C 40%, vitamin E 40%, dimension
Raw element A 10%, vitaminB10 %.
The preparation method of the Lignum Aquilariae Resinatum extract of the present embodiment, Chinese herbal medicine extract and Aloe extract, and Lignum Aquilariae Resinatum whitening
The preparation method of cleansing milk is same as in Example 1, repeats no more here.
Embodiment 3
A kind of Lignum Aquilariae Resinatum whitening cleansing facial milk containing, is made up of the component of following mass percent:
Lignum Aquilariae Resinatum extract 7%, Chinese herbal medicine extract 8%, Aloe extract 4%, lecithin 1%, TWEEN 80 3%, compound
Vitamin 4%, citric acid 2%, 2-pyrrolidone-5-carboxylic acid's macrogol ester 10%, cocamidopropyl betaine (CAB-35) 32% and
Deionized water 29%.
The matter of six kinds of mixture in Radix Scutellariae, Radix Glycyrrhizae, Radix Rhodiolae, Flos Matricariae chamomillae, Rhizoma Chuanxiong, Radix Et Rhizoma Rhei in described Chinese herbal medicine extract
Amount ratio is followed successively by 3:1:3:3:1:1.
Described compound vitamin, is made up of the component of following mass percent: vitamin C 20%, vitamin E 20%, dimension
Raw element A 30%, vitamin B3 0%.
The preparation method of the Lignum Aquilariae Resinatum extract of the present embodiment, Chinese herbal medicine extract and Aloe extract, and Lignum Aquilariae Resinatum whitening
The preparation method of cleansing milk is same as in Example 1, repeats no more here.
Embodiment 4
A kind of Lignum Aquilariae Resinatum whitening cleansing facial milk containing, is made up of the component of following mass percent:
Lignum Aquilariae Resinatum extract 8%, Chinese herbal medicine extract 10%, Aloe extract 7%, lecithin 1%, TWEEN 80 3.5%, multiple
Close vitamin 4.5%, citric acid 2%, 2-pyrrolidone-5-carboxylic acid's macrogol ester 8%, cocamidopropyl betaine (CAB-35)
28% and deionized water 28%.
The matter of six kinds of mixture in Radix Scutellariae, Radix Glycyrrhizae, Radix Rhodiolae, Flos Matricariae chamomillae, Rhizoma Chuanxiong, Radix Et Rhizoma Rhei in described Chinese herbal medicine extract
Amount ratio is followed successively by 3:2:1:1:1:1.
Described compound vitamin, is made up of the component of following mass percent: vitamin C 20%, vitamin E 30%, dimension
Raw element A 20%, vitamin B 30%.
The preparation method of the Lignum Aquilariae Resinatum extract of the present embodiment, Chinese herbal medicine extract and Aloe extract, and Lignum Aquilariae Resinatum whitening
The preparation method of cleansing milk is same as in Example 1, repeats no more here.
Embodiment 5
A kind of Lignum Aquilariae Resinatum whitening cleansing facial milk containing, is made up of the component of following mass percent:
Lignum Aquilariae Resinatum extract 4%, Chinese herbal medicine extract 11%, Aloe extract 10%, lecithin 1%, TWEEN 80 3%, multiple
Close vitamin 5%, citric acid 1%, 2-pyrrolidone-5-carboxylic acid's macrogol ester 7%, cocamidopropyl betaine (CAB-35) 31%
And deionized water 27%.
The matter of six kinds of mixture in Radix Scutellariae, Radix Glycyrrhizae, Radix Rhodiolae, Flos Matricariae chamomillae, Rhizoma Chuanxiong, Radix Et Rhizoma Rhei in described Chinese herbal medicine extract
Amount ratio is followed successively by 3:3:2:1:1:1.
Described compound vitamin, is made up of the component of following mass percent: vitamin C 40%, vitamin E 30%, dimension
Raw element A 20%, vitamin B 10%.
The preparation method of the Lignum Aquilariae Resinatum extract of the present embodiment, Chinese herbal medicine extract and Aloe extract, and Lignum Aquilariae Resinatum whitening
The preparation method of cleansing milk is same as in Example 1, repeats no more here.
The effect of the Lignum Aquilariae Resinatum whitening cleansing facial milk containing of the present invention is described by tests below:
Object of study: choose pachylosis, be dried, dark, have the volunteer of pigmentation, mottle, wrinkle or microgroove altogether
200 people, are randomly divided into 5 groups, often organize 40 people.
The one bottle of about 200g of cleansing milk prepared by embodiment 5-9 respectively, uses 25-45 DEG C after getting up early morning every day and before sleeping
Warm water washes one's face once, washes one's face every time and fully massages face, makes cleansing milk stop about 1 minute in face, cleans, repeat every time with
Upper operation.Test adds up its effective percentage (%) after carrying out 60 days.Criterion of therapeutical effect: (1) is obviously improved: subjective symptoms has largely
Alleviate or disappear.(2) alleviate: subjective symptoms has a certain degree of alleviating but the most obvious.(3) invalid: face's situation is the brightest
Show or do not alleviate.(4) deteriorate: face's situation becomes worse.
Result of the test see table:
| Embodiment 1 | Embodiment 2 | Embodiment 3 | Embodiment 4 | Embodiment 5 | |
| It is obviously improved | 19 | 18 | 22 | 20 | 20 |
| Alleviate | 15 | 20 | 14 | 17 | 15 |
| Invalid | 6 | 2 | 4 | 3 | 5 |
| Deteriorate | 0 | 0 | 0 | 0 | 0 |
| Total effective rate | 85% | 95% | 90% | 92.5% | 87.5% |
Result shows: for pachylosis, be dried, dark, have the personage of pigmentation, mottle, wrinkle or microgroove, for a long time
Use the cleansing milk of the present invention, all have preferable effect, and embodiment 2 effect is better than other embodiments.
A kind of Lignum Aquilariae Resinatum whitening cleansing facial milk containing of the present invention and preparation method thereof, with pure natural and have fragrance and skin care effect
Lignum Aquilariae Resinatum and Chinese herbal medicine extract are active ingredient, and compound certain emulsified component lecithin and natural complex are made, can whitening
Skin, desalination calm pigment, dispelling stain, holding moisture of skin, can kill or suppress to be attached to the antibacterial of skin surface, moreover it is possible to
Slow down aging, promotes epithelial tissue regeneration.Oils and fats and dust on skin can be removed, reach the purpose thoroughly cleaned, moisturizing,
Gentle non-stimulated.
Last it should be noted that, above example is only in order to illustrate technical scheme, rather than the present invention is protected
Protecting the restriction of scope, although having made to explain to the present invention with reference to preferred embodiment, those of ordinary skill in the art should
Work as understanding, technical scheme can be modified or equivalent, without deviating from the reality of technical solution of the present invention
Matter and scope.
Claims (8)
1. a Lignum Aquilariae Resinatum whitening cleansing facial milk containing, it is characterised in that be made up of the raw material of following mass percent: Lignum Aquilariae Resinatum extract 2-
8%, Chinese herbal medicine extract 5-18%, Aloe extract 2-10%, lecithin 1-1.5%, TWEEN 80 2-4%, compound vitamin
4-8%, citric acid 1-2%, 2-pyrrolidone-5-carboxylic acid macrogol ester 7-15%, cocamidopropyl betaine 25-40% and go from
Sub-water surplus；
The preparation method of described Lignum Aquilariae Resinatum extract is: choose Lignum Aquilariae Resinatum, cuts into Lignum Aquilariae Resinatum thin slice, then is crushed to by Lignum Aquilariae Resinatum thin slice
30-60 mesh, puts in High-pressure supercritical extraction equipment, is passed through CO2, after maintaining 40-60min in a high voltage state, moment pressure release,
Taking out, add the mixed solvent of Lignum Aquilariae Resinatum weight 5-8 times, 4 DEG C of low-temperature extraction centrifugal filtrations after 0.5-1.5 hour, filtrate is again
After Middle hollow fiber membrane, it is concentrated into moisture is less than 5%, obtain Lignum Aquilariae Resinatum extract；Described high pressure conditions is 40-
60MPa；
Described mixed solvent is that castor oil hydrogenated, propylene glycol, deionized water are in mass ratio for the mixture of 1:3:6；
Described Chinese herbal medicine extract preparation method is: by Radix Scutellariae, Radix Glycyrrhizae, Radix Rhodiolae, Flos Matricariae chamomillae, Rhizoma Chuanxiong, Radix Et Rhizoma Rhei be in mass ratio
The mixture of the ratio composition of 3:1-3:1-3:1-3:1-2:1, is crushed to 150-250 mesh, adds the ethanol that 4-6 times of concentration is 40%
2 hours post-heating of solution soaking are boiling for 60 minutes decocting, and are filtered to remove filtering residue, collect filtrate and concentrate, be concentrated into former material
2 times of material quality, add 1-2% clarifier, and centrifugal after clarifying treatment, supernatant adds concentrated solution weight 0.1%-0.5%
Polysorbas20 and the propylene glycol of concentrated solution weight 45%, be Chinese herbal medicine extract after stirring and dissolving.
A kind of Lignum Aquilariae Resinatum whitening cleansing facial milk containing the most according to claim 1, it is characterised in that: described Middle hollow fiber membrane condition
For using the pvdf membrane of molecular cut off 100,000, operation pressure is 0.05-0.3MPa, and feed velocity is 600ml/min, operation temperature
Degree is for 30-35 DEG C.
A kind of Lignum Aquilariae Resinatum whitening cleansing facial milk containing the most according to claim 1, it is characterised in that: described Chinese herbal medicine extract preparation side
In method, clarifier is chitosan quaternary ammonium salt, and clarification condition is, adds the clarifier aqueous solution of concentrated solution weight 0.5%-2%, quality
Concentration is 1%, at normal temperatures after stirring 5-10min, stands 24h.
A kind of Lignum Aquilariae Resinatum whitening cleansing facial milk containing the most according to claim 1, it is characterised in that: the preparation side of described Aloe extract
Method is: by fresh Aloe vulgaris blade peeling, chopping, adding the complex enzyme zymohydrolysis of weight 0.2%-0.6%, enzymolysis solution passes through
Enzyme denaturing, centrifugal after obtain the Aloe extract of clear.
A kind of Lignum Aquilariae Resinatum whitening cleansing facial milk containing the most according to claim 4, it is characterised in that: described Aloe extract preparation method
In, compound enzyme be liquid cellulase, pectinase in mass ratio for the mixture of 3:7, enzymatic hydrolysis condition is 37 DEG C, 1 hour.
6. according to a kind of Lignum Aquilariae Resinatum whitening cleansing facial milk containing described in any one in claim 1-4, it is characterised in that: described centrifugal bar
Part is 4000rpm-8000rpm, and the time is 15-30min.
A kind of Lignum Aquilariae Resinatum whitening cleansing facial milk containing the most according to claim 1, it is characterised in that: described compound vitamin is vitamin
C, vitamin E, vitamin A, vitamin B2 are the scalemic thereof of 1-4:1-4:1-3:1-3 in mass ratio.
8. according to the preparation method of a kind of Lignum Aquilariae Resinatum whitening cleansing facial milk containing described in claim 1-7 any one, it is characterised in that: bag
Include following steps:
Step 1): add lecithin, TWEEN 80, compound vitamin and pyrroles by proportioning in the reactor containing deionized water
Alkanone carboxylic acid macrogol ester, is slowly stirred uniformly and is warming up to 80-90 DEG C；
Step 2): add cocamidopropyl betaine, after stirring, start cooling；
Step 3): be naturally cooling to 50 DEG C and add continuation cooling after citric acid stirs；
Step 4): be naturally cooling to 40-45 DEG C and add Lignum Aquilariae Resinatum extract, Chinese herbal medicine extract, Aloe extract, continue stirring；
Step 5): add deionized water and stir, is cooled to 35 DEG C of dischargings, prepares Lignum Aquilariae Resinatum whitening cleansing facial milk containing.
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| CN110772451A (en) * | 2019-11-06 | 2020-02-11 | 茂名市瑜丰沉香创意产业有限公司 | Facial cleanser containing fullerene and agilawood essential oil and preparation method thereof |
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| CN114344213B (en) * | 2021-12-31 | 2024-05-07 | 青海省中医院 | Skin care product and composition containing plant extracts, and preparation method and application thereof |
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| CN101125119B (en) * | 2007-07-18 | 2010-12-22 | 西藏宇妥藏药研究有限公司 | Tibetan materia medica with whitening anti-senility function and application thereof |
| CN104277939A (en) * | 2014-09-11 | 2015-01-14 | 刘峥 | Lily soap |
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Denomination of invention: Eaglewood whitening facial cleanser and preparation method thereof Effective date of registration: 20200727 Granted publication date: 20161123 Pledgee: China Co. truction Bank Corp Dongguan branch Pledgor: DONGGUAN BOTON FLAVORS & FRAGRANCES Co.,Ltd. Registration number: Y2020980004381 |
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Date of cancellation: 20220526 Granted publication date: 20161123 Pledgee: China Co. truction Bank Corp Dongguan branch Pledgor: DONGGUAN BOTON FLAVORS & FRAGRANCES Co.,Ltd. Registration number: Y2020980004381 |
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Address after: No. 8, Xixi Road, Liaobu Town, Dongguan City, Guangdong Province, 523000 Patentee after: Botton Spices Co.,Ltd. Address before: 523401 First Floor, Wealth Building, Liaobu Town, Dongguan City, Guangdong Province Patentee before: DONGGUAN BOTON FLAVORS & FRAGRANCES Co.,Ltd. |