CN108542870B - Mild soothing infant face cream - Google Patents
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/98—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin
- A61K8/981—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin of mammals or bird
- A61K8/986—Milk; Derivatives thereof, e.g. butter
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
- A61K8/42—Amides
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/005—Preparations for sensitive skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/59—Mixtures
- A61K2800/592—Mixtures of compounds complementing their respective functions
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Abstract
The invention discloses mild and soothing infant face cream. The mild soothing infant facial cream comprises the following components in percentage by weight: 5-20% of a humectant; 10-35% of an emollient; 1.0 to 3.5 percent of emulsifier; 0.5 to 3.5 percent of thickening agent; 0.001-5% of milk essence; 0.001-5% of sweet almond oil; 0.001-5% of panthenol; 0.1 to 2.5 percent of other components; 20.5 to 83.4 percent of deionized water. The mild and soothing infant face cream provided by the invention has the advantages of triple nourishing and caring: the panthenol has small molecular weight, can quickly permeate into stratum corneum, stimulate epithelial cell growth and repair skin; the sweet almond oil is quickly absorbed by skin, and various discomforts are effectively relieved; the milk provides closed grease for the skin, a film is formed on the surface of the skin to prevent water loss, the three components have synergistic effect, internal comfort and external protection are realized, the delicate skin of the baby is cared mildly, and the skin of the baby is enabled to be healthy and moist.
Description
Technical Field
The invention relates to a mild and soothing infant face cream, belongs to the technical field of daily skin care products for infants, and particularly relates to a mild and soothing infant face cream and a preparation method thereof.
Background
The skin of infants is different from that of adults, and the skin of infants has incomplete development and little sebum secretion and weak resistance to external adverse factors. The skin discomfort of infants is increased by the increased climatic change and environmental pollution, so the skin of the infants needs to be better nourished and protected, and the skin resistance is enhanced.
The cosmetic field uses transdermal Water Loss (TEWL) to measure skin barrier function. TEWL is closely related to stratum corneum skin permeability and skin hydration, with higher TEWL values indicating more water loss from the skin and poorer skin barrier function, and conversely, better skin barrier function.
At present, most of commercially available infant face creams emphasize mild moistening, and are alleged to be added with natural source components without damaging the skin of a baby. In fact, most of the infant skin care products are added with excessive raw materials and some raw materials which are not suitable for the skin of the infants, so that the damage is not reduced, and the skin burden of the infants is increased. In the prior art, on the premise of ensuring skin moistening, some safe skin care ingredients with efficacy are sought to improve the product value. Patent document CN107412087A provides a plant composition for improving skin barrier function of infants, which mainly aims at the damaged skin of infants, and has mild plant components and no irritation to skin. Patent document CN108066270A provides a multi-effect infant moisturizing cream, which is added with various plant extracts and other moisturizing ingredients, is mild and non-irritant, soothes skin and reduces skin allergy.
In the prior art, the mildness and no stimulation are realized by adding various natural source components, the natural source components are relatively safe, but the natural source components are also added effectively when in use, so that unnecessary raw materials are not introduced. In the prior art, no report has been made on the compounding of milk essence, sweet almond oil and panthenol for preparing the infant face cream, and the three components have synergistic effect, so that the infant face cream can relieve the internal stress and protect the external stress, mildly care the delicate skin of a baby, and make the skin of the baby healthy and moist.
Disclosure of Invention
Aiming at the defects in the prior art, the invention aims to provide mild and soothing infant face cream; the inner layer repairs and relieves the skin, and the outer layer effectively isolates and protects, so that the skin of the baby is healthy and moist.
Through long-term research, researchers of the invention find that the milk essence, the sweet almond oil and the panthenol are compounded to achieve the effects of mildness, relaxation and skin moistening by synergistic interaction, so that the skin of a baby is kept healthy and moist all the time.
According to the invention, the milk essence, the sweet almond oil and the panthenol are innovatively compounded to prepare the infant face cream, and the prepared product has an excellent skin moistening effect and can repair and relieve damaged skin and keep the skin of an infant healthy and moist.
The present invention is realized by the following technical means.
The mild soothing infant facial cream comprises the following components in percentage by weight:
5-20% of a humectant; 10-35% of an emollient; 1.0 to 3.5 percent of emulsifier; 0.5 to 3.5 percent of thickening agent; 0.001-5% of milk essence; 0.001-5% of sweet almond oil; 0.001-5% of panthenol; 0.1 to 2.5 percent of other components; 20.5 to 83.4 percent of deionized water.
Further, the mild soothing infant cream comprises the following components in percentage by weight:
10-15% of a humectant; 15-25% of an emollient; 1.5 to 2.5 percent of emulsifier; 0.8 to 2.4 percent of thickening agent; 0.5-2.5% of milk essence; 1.5 to 3.5 percent of sweet almond oil; 0.5 to 2.5 percent of panthenol; 0.2 to 2.0 percent of other components; 44.6 to 70 percent of deionized water.
The mild and soothing infant face cream provided by the invention is characterized in that the humectant is one or more selected from polyglycerol, glycerol, butanediol, dipropylene glycol, propylene glycol, sorbitol (sugar) alcohol, sodium hyaluronate, polyethylene glycols, luba gum oil, biological sugar gum and pentanediol.
The emollient is one or more selected from caprylic/capric triglyceride, squalane, fatty alcohol, shea butter, meadowfoam seed oil, cetyl palmitate, C10-18 fatty acid triglyceride, silicone oil, vitamin E derivatives, avocado oil, macadamia nut seed oil, grape seed oil, olive oil, rice bran oil, and corn germ oil.
The emulsifier is one or more of alkyl glucosides, polyglycerin, sodium stearyl glutamate, glyceryl stearate and hydrogenated lecithin.
The thickening agent is one or more of acrylic acid (ester)/C10-30 alkanol acrylate cross-linked polymer, carbomer, hydroxyethyl acrylate/sodium acryloyldimethyl taurate copolymer, sodium acrylate/sodium acryloyldimethyl taurate copolymer, ammonium acryloyldimethyl taurate/VP copolymer, polyacrylic acid and acrylamide/ammonium acrylate copolymer.
The mild soothing infant facial cream also contains 0.005-0.5% of pH regulator, wherein the pH regulator is selected from one or more of sodium hydroxide, potassium hydroxide, triethanolamine, aminomethyl propanol and arginine.
The milk serum was purchased from Symrise; the sweet almond oil was purchased from northstar lipids, inc; the panthenol is available from DSM corporation.
Preferably, the mild soothing infant facial cream disclosed by the invention consists of the following components:
4-15% of glycerin, 1-5% of pentanediol, 4-10% of shea butter, 4-15% of caprylic/capric triglyceride, 1-10% of tocopherol acetate, 0.5-2% of monoglyceride, 0.5-1.5% of coco glucoside, 0.2-1.0% of hydroxyethyl acrylate/sodium acryloyldimethyl taurate copolymer, 0.3-1.5% of acrylic acid (ester)/C10-30 alkanol acrylate cross-linked polymer, 0.01-0.08% of sodium hydroxide, 1.5-2.5% of milk essence, 1.5-3% of sweet almond oil, 0.5-2.5% of panthenol, 0.8% of preservative, 0.1% of essence and the balance of deionized water.
In addition, the mild soothing infant facial cream is prepared by the following steps:
1) mixing and heating the water phase raw materials to 75-85 ℃, and stirring for 20 minutes under the condition of heat preservation;
2) mixing the oil phase raw materials, stirring, heating to 75-85 deg.C, and dissolving completely;
3) the oil phase was added to the aqueous phase and stirred at 2000r/min for 10 minutes. Then cooling while stirring;
4) cooling to 50 deg.C, adding pH regulator; continuously stirring and cooling to 40-45 deg.C, adding the rest components, cooling to 38-40 deg.C, testing, and discharging.
Further, in the step 1), the water phase raw material comprises: 4 to 15 percent of glycerin, 1 to 5 percent of pentanediol, 0.2 to 1.0 percent of hydroxyethyl acrylate/sodium acryloyldimethyl taurate copolymer and 0.3 to 1.5 percent of acrylic acid (ester)/C10-30 alkanol acrylate cross-linked polymer;
in the step 2), the oil phase raw materials comprise: 4% -10% of shea butter, 4% -15% of caprylic/capric triglyceride, 1% -10% of tocopheryl acetate, 0.5% -2% of monoglyceride, 0.5% -1.5% of coco glucoside;
in the step 4), the pH adjuster includes: 0.01% -0.08% of sodium hydroxide;
by means of the technical scheme, the invention has the following beneficial effects:
compared with the prior art, the invention creatively adds three skin care ingredients of milk essence, sweet almond oil and panthenol into the infant cream product in a compounding way. The panthenol has small molecular weight, can quickly permeate into stratum corneum, stimulate epithelial cell growth and repair skin; the sweet almond oil is quickly absorbed by skin, and various discomforts are effectively relieved; the milk essence provides closed grease for skin, a film is formed on the surface of the skin to prevent water loss, the three components have synergistic effect, and the milk essence can relieve the inside and protect the outside, mildly care delicate skin of the baby and make the skin of the baby healthy and moist.
Detailed Description
The present invention will be described in further detail below with reference to specific preferred embodiments and effect test examples.
The infant face cream is mainly obtained by mixing a humectant, an emollient, an emulsifier, a thickener, milk essence, sweet almond oil and panthenol, and adding other components.
The humectant is not particularly limited as long as it is a humectant commonly used in the cosmetic field, and examples thereof include polyglycerol, glycerol, butylene glycol, dipropylene glycol, propylene glycol, sorbitol, sodium hyaluronate, polyethylene glycols, luba gum oil, biosaccharide gum, pentanediol, maltitol, seaweed extract, aloe vera extract, trehalose, polyethylene/polypropylene glycol-14/7 dimethyl ether, xylitol, and the like.
The emollient is not particularly limited as long as it is a commonly used emollient in the cosmetic field, particularly vegetable oils and fats, and examples thereof include caprylic/capric triglyceride, squalane, fatty alcohol, shea butter, meadowfoam seed oil, cetyl palmitate, triglycerides of C10-18 fatty acids, silicone oil, vitamin E derivatives, avocado oil, macadamia nut seed oil, grape seed oil, olive oil, rice bran oil, corn germ oil, and silicone oil.
The emulsifier is not particularly limited as long as it can form an oil-in-water emulsion, and in particular, an oil-in-water type emulsifier of natural origin, for example, alkylglucosides, polyglycerols, sodium stearyl glutamate, glyceryl stearate, hydrogenated lecithin, and the like can be used.
Examples of the thickener include acrylic acid (ester)/C10-30 alkanol acrylate crosslinked polymers, carbomer, hydroxyethyl acrylate/sodium acryloyldimethyl taurate copolymer, sodium acrylate/sodium acryloyldimethyl taurate copolymer, ammonium acryloyldimethyl taurate/VP copolymer, polyacrylic acids, acrylamide/ammonium acrylate copolymer, and the like.
Examples of the pH adjuster include arginine, sodium hydroxide, potassium hydroxide, triethanolamine, and aminomethyl propanol.
The milk serum of the present invention was purchased from Symrise; sweet almond oil was purchased from northstar lipids; panthenol was purchased from DSM.
According to the invention, the milk essence, the sweet almond oil and the panthenol are compounded to prepare the infant face cream, and the prepared product has an excellent skin moistening effect, and can repair and relieve damaged skin and keep the skin of a baby healthy and moist.
The technical solutions and effects of the present invention are described below by referring to the test examples through specific preferred embodiments, but the technical solutions of the present invention are not limited thereto.
Examples 1 to 4
The components of the mild soothing infant face cream formula of the present invention are shown in table 1 below.
TABLE 1 infant cream formula Components of examples 1-4 (% by weight)
The preparation process of the infant face cream formula can be expressed as follows:
1) mixing and heating the water phase raw materials to 75-85 ℃, and stirring for 20 minutes under the condition of heat preservation;
2) mixing the oil phase raw materials, stirring, heating to 75-85 deg.C, and dissolving completely;
3) the oil phase was added to the aqueous phase and stirred at 2000r/min for 10 minutes. Then cooling while stirring;
4) cooled to 50 ℃, and added with a pH regulator.
Continuously stirring and cooling to 40-45 deg.C, adding the rest components, cooling to 38-40 deg.C, testing, and discharging.
Comparative examples 1 to 4
The components of an infant face cream formula are shown in the following table 2.
TABLE 2 infant face cream formulation components of comparative examples 1-4 (% by weight)
The preparation process of the infant face cream formula can be expressed as follows:
1) mixing and heating the water phase raw materials to 75-85 ℃, and stirring for 20 minutes under the condition of heat preservation;
2) mixing the oil phase raw materials, stirring, heating to 75-85 deg.C, and dissolving completely;
3) the oil phase was added to the aqueous phase and stirred at 2000r/min for 10 minutes. Then cooling while stirring;
4) cooled to 50 ℃, and added with a pH regulator.
Continuously stirring and cooling to 40-45 deg.C, adding the rest components, cooling to 38-40 deg.C, testing, and discharging.
The contents of the effect test examples are as follows.
1. Evaluation of Using Effect of infant face cream
The mild soothing infant face cream prepared in the examples 1-4 and the comparative examples 1-4 according to the formulas shown in the tables 1 and 2 is used for inspecting the influence of the combination of milk essence, sweet almond oil and panthenol on the using effect of the product.
1.1 evaluation of skin Barrier function
Comparative testing infant creams of comparative examples 1-4 and examples 1-4 were tested for transdermal water loss (TEWL). The lower the TEWL value of the skin, the greater the reduced rate of change, indicating a better barrier function against water loss, when evaluated separately for a healthy 240 subjects 16-25 years old. The rate of change of TEWL values was:
TEWL change rate ═ (measured value-blank control value)/blank control value · 100%
Using a Tewameter TThe M300 is tested by a skin moisture loss tester. 3cm of each forearm of the subject2The area of the size is the test area, and the test area of the arm should be washed with clean water and sit still in a constant temperature and humidity environment for 30 minutes before the test of the subject. Then 2.0mg of sample/cm2The samples were evenly spread in the test area using latex gloves, tested for 4 hours TEWL values, and the TEWL rate was calculated as shown in tables 3 and 4 below:
TABLE 3 test group transdermal moisture loss (TEWL) Rate of change
TABLE 4 Change rate of percutaneous Water loss (TEWL) in control group
As can be seen from tables 3 and 4, the test group had a significantly higher rate of change in the reduction of TEWL values than the control group, i.e., the test group had significantly better skin barrier function than the control group, and the effect was most optimal when the three components were added at a ratio of 1:1: 1. The using effect of the infant face cream added with the milk essence, the sweet almond oil and the panthenol is better than the effect of adding the milk essence, the sweet almond oil or the panthenol alone.
1.2 evaluation of safety of infant face cream
The safety of the face cream is evaluated by adopting a human body skin patch experiment. The safety of the infant face creams of the comparative examples 1 to 4 and the example 1 is tested, and the influence of the addition of the milk essence, the sweet almond oil or the panthenol single component and the compound components of the milk essence, the sweet almond oil or the panthenol single component on the safety of the face cream is examined.
The test method comprises the following steps: the test method of the patch for human skin is as follows: technical Specifications for cosmetic safety (2015 edition). Selecting a proper spot test device, selecting at least 60 qualified volunteers to test by a closed spot test method, and adding a test sample and a blank control (without any substance) sample into the spot test device according to a random distribution table. The spot test device with the test object is applied to the inner side of the forearm of the subject, the test device is lightly pressed with the palm to be uniformly applied to the skin for 24 hours, the skin reaction is observed according to the standard of the table 5 after 30min (after the indentation disappears), 24 hours and 48 hours of removing the spot test device of the test object respectively, and the observation result is recorded. The results are shown in tables 6 and 7 below.
TABLE 5 skin closed Patch test skin response grading Standard
TABLE 6 test group Patch test results
TABLE 7 test results of control patch
As can be seen from tables 6 and 7, neither the test group nor the control group exhibited adverse reactions. The fact that the added milk essence, the sweet almond oil or the panthenol single component and the compounded components of the milk essence, the sweet almond oil or the panthenol single component have no influence on the safety of the cream is proved, and the components are safe and mild and are suitable for being added into infant products.
The above description is only a preferred embodiment of the present invention, and is not intended to limit the present invention in any way, so that any simple modification, equivalent change and modification made to the above embodiment according to the technical spirit of the present invention are within the scope of the technical solution of the present invention.
Claims (4)
1. A mild soothing infant facial cream is characterized by comprising the following components:
4-15% of glycerin, 1-5% of pentanediol, 4-10% of shea butter, 4-15% of caprylic/capric triglyceride, 1-10% of tocopherol acetate, 0.5-2% of monoglyceride, 0.5-1.5% of coco glucoside, 0.2-1.0% of hydroxyethyl acrylate/sodium acryloyldimethyl taurate copolymer, 0.3-1.5% of acrylic acid (ester)/C10-30 alkanol acrylate cross-linked polymer, 0.01-0.08% of sodium hydroxide, 1.5% of milk essence, 1.5% of sweet almond oil, 1.5% of panthenol, 0.8% of preservative, 0.1% of essence and the balance of deionized water.
2. The mild soothing infant facial cream of claim 1, wherein: the milk serum was purchased from Symrise; the sweet almond oil was purchased from northstar lipids, inc; the panthenol is available from DSM corporation.
3. The mild soothing infant facial cream of claim 1, wherein: is prepared by the following process steps:
1) mixing and heating the water phase raw materials to 75-85 ℃, and stirring for 20 minutes under the condition of heat preservation;
2) mixing the oil phase raw materials, stirring, heating to 75-85 deg.C, and dissolving completely;
3) adding the oil phase into the water phase, stirring at 2000r/min for 10 minutes, and then cooling while stirring;
4) cooling to 50 deg.C, adding pH regulator;
continuously stirring and cooling to 40-45 deg.C, adding the rest components, cooling to 38-40 deg.C, testing, and discharging.
4. The mild soothing infant facial cream of claim 3, wherein: in the step 1), the water phase raw material comprises: 4 to 15 percent of glycerin, 1 to 5 percent of pentanediol, 0.2 to 1.0 percent of hydroxyethyl acrylate/sodium acryloyldimethyl taurate copolymer and 0.3 to 1.5 percent of acrylic acid (ester)/C10-30 alkanol acrylate cross-linked polymer;
in the step 2), the oil phase raw materials comprise: 4% -10% of shea butter, 4% -15% of caprylic/capric triglyceride, 1% -10% of tocopheryl acetate, 0.5% -2% of monoglyceride, 0.5% -1.5% of coco glucoside;
in the step 4), the pH adjuster includes: 0.01% -0.08% of sodium hydroxide.
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| CN109091411A (en) * | 2018-11-13 | 2018-12-28 | 王亚平 | A kind of infant's lotion and preparation method thereof |
| CN111228154A (en) * | 2020-03-12 | 2020-06-05 | 广东袋鼠妈妈生物科技有限公司 | Fresh wheat extract protoplasm milk for infants and preparation method thereof |
| CN111603433B (en) * | 2020-05-29 | 2022-11-18 | 杭州心悦化妆品有限公司 | Mild washing and protecting article for infants and preparation method thereof |
| CN112999143B (en) * | 2021-03-02 | 2022-06-24 | 山东艾益典生物技术有限公司 | Repairing and relieving skin care product containing metazoan components and preparation method thereof |
| CN113712894B (en) * | 2021-09-26 | 2023-04-11 | 湖北省麦诗特生物科技有限公司 | Essence emulsion composition with moisturizing and relieving effects and preparation method and application thereof |
| CN114557935A (en) * | 2022-03-19 | 2022-05-31 | 康柏利科技（苏州）有限公司 | Milk protein-containing face cream and preparation method thereof |
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