CN108498353A - A kind of tooth-cleaning powder and preparation method thereof - Google Patents
A kind of tooth-cleaning powder and preparation method thereof Download PDFInfo
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- CN108498353A CN108498353A CN201810519676.XA CN201810519676A CN108498353A CN 108498353 A CN108498353 A CN 108498353A CN 201810519676 A CN201810519676 A CN 201810519676A CN 108498353 A CN108498353 A CN 108498353A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9789—Magnoliopsida [dicotyledons]
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- A61K8/00—Cosmetics or similar toiletry preparations
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- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
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- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
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- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
- A61K8/44—Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
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- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
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- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/965—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of inanimate origin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q11/00—Preparations for care of the teeth, of the oral cavity or of dentures; Dentifrices, e.g. toothpastes; Mouth rinses
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Abstract
The invention discloses a kind of tooth-cleaning powders and preparation method thereof, wherein the tooth-cleaning powder is made of the raw material of following parts by weight：8~10 parts of Sculellaria barbata, 4~9 parts of oldenlandia diffusa, 2~6 parts of feverfew, 2~5 parts of mung bean, 2.5~4 parts of lemon polysaccharide, 0.8~1.8 part of jade powder, 2~5 parts of calcium monohydrogen phosphate, 0.2~0.5 part of sodium N-lauroyl sarcosinate, 0.05~0.1 part of menthol, 0.01~0.02 part of saccharin.The tooth-cleaning powder of the present invention while functions of whitening teeth, and can antibacterial, anti-inflammatory, reduce internal heat, play the role of protecting oral cavity, gum, safeguard dental health, improve the type of tooth-cleaning powder technology content and abundant tooth-cleaning powder to meet consumer demand.
Description
Technical field
The invention belongs to daily necessities preparing technical fields, and in particular to a kind of tooth-cleaning powder and preparation method thereof.
Background technology
Tooth powder is common cleaning supplies in daily life, with the continuous development of science and technology, technological equipment it is continuous
Improve and perfect, various types of tooth powder are come out one after another, and the quality and grade of product is continuously improved, and present kind is by single
Clean type tooth powder develops into great variety of goods, tooth powder vdiverse in function.The aesthetic quality to tooth powder and effect quality with people
Requirement it is also higher and higher, for consumers with medicinal property tooth-cleaning powder, can tooth-whitening and insecticidal and antibacterial
Dentifrice, it will push tooth powder technology content be continuously improved and it is perfect, it is higher that consumer is met with better product
It is required that.
Invention content
The present invention provides a kind of tooth-cleaning powders, while having functions of whitening teeth, and energy antibacterial anti-inflammatory, protection gum is played,
It safeguards the effect of dental health, improves the type of tooth-cleaning powder technology content and abundant tooth-cleaning powder to meet consumer demand.
To achieve the goals above, the present invention proposes following technical scheme：
A kind of tooth-cleaning powder is made of the raw material of following parts by weight：It is 8~10 parts of Sculellaria barbata, 4~9 parts of oldenlandia diffusa, white
2~6 parts of chrysanthemum, 2~5 parts of mung bean, 2.5~4 parts of lemon polysaccharide, 0.8~1.8 part of jade powder, 2~5 parts of calcium monohydrogen phosphate, lauroyl
0.2~0.5 part of base sodium sarcosinate, 0.05~0.1 part of menthol, 0.01~0.02 part of saccharin.
Preferably, a kind of tooth-cleaning powder of the present invention, is made of the raw material of following parts by weight：It is 8.5~9.5 parts of Sculellaria barbata, white
5.25~7.75 parts of HERBA HEDYOTIS DIFFUSAE of flower, 3~5 parts of feverfew, 2.75~4.25 parts of mung bean, 2.875~3.625 parts of lemon polysaccharide, jade
1.05~1.55 parts of mountain flour, 2.75~4.25 parts of calcium monohydrogen phosphate, 0.275~0.425 part of sodium N-lauroyl sarcosinate, menthol
0.063~0.088 part, 0.013~0.018 part of saccharin.
It is highly preferred that a kind of tooth-cleaning powder of the present invention, is made of the raw material of following parts by weight：9 parts of Sculellaria barbata, oldenlandia
6.5 parts of grass, 4 parts of feverfew, 3.5 parts of mung bean, 3.25 parts of lemon polysaccharide, 1.3 parts of jade powder, 3.5 parts of calcium monohydrogen phosphate, lauroyl
0.35 part of sodium sarcosinate, 0.075 part of menthol, 0.015 part of saccharin.
The preparation method of above-mentioned lemon polysaccharide is：
A. boiling 1~3 time is heated after lemon being sliced, filtered after degreasing, decoloration and is dried at 35~65 DEG C, then powder
Broken and 40~80 sieves excessively, it is dry, obtain lemon powder；
B. it is 1 to press solid-liquid ratio:30~50 are added alkaline solution, and 0.5~1h is extracted at 70~80 DEG C, and extraction is closed afterwards twice
And extracting solution；
C. it is being centrifuged after the Sevage reagents for merging extracting solution addition extracting liquid volume 1/6~1/2 shake 18~22min
18~22min, the albuminate of Polysaccharide removing solution layer and organic solution layer intersection are centrifuged with 3500~4500r/min in machine
Matter, repetitive operation 3~4 times remove the protein and partial pigment in solution, until solution is in colorless and transparent；
D. above-mentioned colourless transparent solution is pipetted, freeze-drying just obtains lemon polysaccharide.
The pH of above-mentioned alkaline solution is 8~9, is allocated with the NaOH of 0.1mol/L.
A kind of tooth-cleaning powder of the present invention, which is characterized in that the jade powder is Khotan jade, dushan diopside, Xiuyan Jade and turquoise
One or more, be crushed to particle size be 1~100nm.
A kind of application method of tooth-cleaning powder of the present invention is to glue some tooth-cleaning powders with toothbrush before brushing teeth sooner or later daily, as brushing teeth one
Sample carrys out backwash several times, with clear water rinse it is clean after can normal use toothpaste continue to brush teeth.
A kind of preparation method of tooth-cleaning powder of the present invention, includes the following steps：By weight by Sculellaria barbata, oldenlandia
Grass, feverfew, mung bean are cleaned with clear water, and it is more than that 2~5cm of solid matter impregnates 1~1.5h that pure water, which is added, is added more than solid
The pure water of 2~5cm of body substance, after being boiled by fire, then small fire is decocted to 1/2 that solution is original volume, and well-done solution is fallen
Go out, be repeated 2 times decoction in the same way, 3 solution are filtered, up to dry powder after concentrate drying, be then added lemon polysaccharide,
Jade powder, calcium monohydrogen phosphate, sodium N-lauroyl sarcosinate, menthol, saccharin, stirring evenly can obtain.
Raw material related introduction needed for tooth-cleaning powder of the present invention is as follows：
Sculellaria barbata is the drying herb of labiate Sculellaria barbata, and acrid flavour, hardship are cold in nature, clearing heat and detoxicating；Oldenlandia diffusa,
It is bitter, light, it is cold in nature.Primary efficacy is clearing heat and detoxicating, medicinal powder for relieving pain knot, promoting urination and removing dampness.Outstanding kind treatment various types inflammation；Feverfew
Also known as camomile, Hang Ju, FLOS CHRYSANTHEMI ALBA from Haizhou of China, tea chrysanthemum, medicine chrysanthemum, chrysanthemum glucoside, amino acid, flavonoids and multivitamin and trace element are included,
It wets one's whistle and antibacterial and other effects with nourishing the liver to improve visual acuity, clearing away heart-fire；Contain a kind of globulin and polysaccharide in mung bean, has suppression to staphylococcus
It makes and uses.
Jade powder and calcium monohydrogen phosphate are rubbing agent, and the friction effect with the flank of tooth achievees the purpose that clean tooth, and jade powder is also
More than the 30 kinds of trace element beneficial to human body, these elements such as selenium, zinc, nickel, cobalt, manganese, magnesium, calcium containing needed by human body can promote
Gingival cell blood follows bad, enhancing metabolism, plays a part of to conserve gum.
Sodium N-lauroyl sarcosinate is that surfactant is also foaming agent, can fast foaming foam but also clear fine purifiation dental
Dirt in tooth, the tension for mainly reducing hydration cleaning dental surface promotes dirt to leave, while dirt being wrapped up with dampening
It flows and walks.
Menthol is aromatic, and aromatic is incorporated in tooth powder, and powder can not only be made to have certain fragrance, lasting mouth
Chamber eliminates halitosis, and also certain sterilizing function.
Lemon polysaccharide is gum protectant can alleviate containing organic acid, lipid, carotenoid, minerals, flavonoids etc.
Calcium ion promotes Blood coagulation, prevention hypertension and cardiac muscle to obstruct, have contraction to improve coagulation function, can mainly prevent gum from going out
Mass formed by blood stasis shape.
Saccharin is sweetener, mainly eliminates the peculiar smell of other raw materials in powder.
Beneficial effects of the present invention are：Tooth-cleaning powder while functions of whitening teeth, and can antibacterial, anti-inflammatory, reduce internal heat, play protection
Oral cavity, gum safeguard the effect of dental health, improve the type of tooth-cleaning powder technology content and abundant tooth-cleaning powder to meet consumer
Demand.
Specific implementation mode
In order to make the technical means, the creative features, the aims and the efficiencies achieved by the present invention be easy to understand, tie below
Specific embodiment is closed, the present invention is further explained.
Embodiment 1
A kind of tooth-cleaning powder is made of the raw material of following parts by weight：9 parts of Sculellaria barbata, 6.5 parts of oldenlandia diffusa, feverfew 4
Part, 3.5 parts of mung bean, 3.25 parts of lemon polysaccharide, 1.3 parts of jade powder, 3.5 parts of calcium monohydrogen phosphate, 0.35 part of sodium N-lauroyl sarcosinate,
0.075 part of menthol, 0.015 part of saccharin.
The preparation method of above-mentioned lemon polysaccharide is：
A. boiling 2 times is heated after lemon being sliced, filtered after degreasing, decoloration and is dried at 50 DEG C, then crushing and mistake
60 sieves, it is dry, obtain lemon powder；
B. it is 1 to press solid-liquid ratio:40 are added alkaline solution, and 0.75h is extracted at 75 DEG C, and extraction merges extracting solution afterwards twice；
C. the Sevage reagents for merging extracting solution and being added extracting liquid volume 1/3 shake after 20min in centrifuge with
4000r/min centrifugation 20min, the denatured protein of Polysaccharide removing solution layer and organic solution layer intersection, repetitive operation 3 times,
The protein and partial pigment in solution are removed, until solution is in colorless and transparent；
D. above-mentioned colourless transparent solution is pipetted, freeze-drying just obtains lemon polysaccharide.
The pH of above-mentioned alkaline solution is 8.5, is allocated with the NaOH of 0.1mol/L.
A kind of tooth-cleaning powder of the present embodiment, which is characterized in that the jade powder is Khotan jade, dushan diopside, Xiuyan Jade and green pine
The one or more of stone, it is 50nm to be crushed to particle size.
A kind of application method of tooth-cleaning powder of the present embodiment is to glue some tooth-cleaning powders with toothbrush before brushing teeth sooner or later daily, as brushing teeth
Equally carry out backwash several times, with clear water rinse it is clean after can normal use toothpaste continue to brush teeth.
A kind of preparation method of tooth-cleaning powder of the present embodiment, includes the following steps：By weight by Sculellaria barbata, oldenlandia
Grass, feverfew, mung bean are cleaned with clear water, and it is more than that solid matter 3.5cm impregnates 1.25h that pure water, which is added, is added more than solid
The pure water of substance 3.5cm, after being boiled by fire, then small fire is decocted to 1/2 that solution is original volume, and well-done solution is poured out,
It is repeated 2 times decoction in the same way, 3 solution are filtered, up to dry powder after concentrate drying, lemon polysaccharide, jade is then added
Mountain flour, calcium monohydrogen phosphate, sodium N-lauroyl sarcosinate, menthol, saccharin, stirring evenly can obtain.
Embodiment 2
A kind of tooth-cleaning powder is made of the raw material of following parts by weight：8 parts of Sculellaria barbata, 4 parts of oldenlandia diffusa, feverfew 2
Part, 2 parts of mung bean, 2.5 parts of lemon polysaccharide, 0.8 part of jade powder, 2 parts of calcium monohydrogen phosphate, 0.2 part of sodium N-lauroyl sarcosinate, menthol
0.05 part, 0.01 part of saccharin.
The preparation method of above-mentioned lemon polysaccharide is：
A. boiling 1 time is heated after lemon being sliced, filtered after degreasing, decoloration and is dried at 35 DEG C, then crushing and mistake
40 sieves, it is dry, obtain lemon powder；
B. it is 1 to press solid-liquid ratio:30 are added alkaline solution, and 0.5h is extracted at 70 DEG C, and extraction merges extracting solution afterwards twice；
C. the Sevage reagents for merging extracting solution and being added extracting liquid volume 1/6 shake after 18min in centrifuge with
3500r/min centrifugation 18min, the denatured protein of Polysaccharide removing solution layer and organic solution layer intersection, repetitive operation 3 times,
The protein and partial pigment in solution are removed, until solution is in colorless and transparent；
D. above-mentioned colourless transparent solution is pipetted, freeze-drying just obtains lemon polysaccharide.
The pH of above-mentioned alkaline solution is 8, is allocated with the NaOH of 0.1mol/L.
A kind of tooth-cleaning powder of the present embodiment, which is characterized in that the jade powder is Khotan jade, dushan diopside, Xiuyan Jade and green pine
The one or more of stone, it is 1nm to be crushed to particle size.
A kind of application method of tooth-cleaning powder of the present embodiment is to glue some tooth-cleaning powders with toothbrush before brushing teeth sooner or later daily, as brushing teeth
Equally carry out backwash several times, with clear water rinse it is clean after can normal use toothpaste continue to brush teeth.
A kind of preparation method of tooth-cleaning powder of the present embodiment, includes the following steps：By weight by Sculellaria barbata, oldenlandia
Grass, feverfew, mung bean are cleaned with clear water, and it is more than that solid matter 2cm impregnates 1h that pure water, which is added, is added more than solid matter
The pure water of 2cm, after being boiled by fire, then small fire is decocted to 1/2 that solution is original volume, well-done solution is poured out, with same
Mode be repeated 2 times decoction, 3 solution are filtered, up to dry powder after concentrate drying, lemon polysaccharide, jade powder, phosphorus is then added
Sour hydrogen calcium, sodium N-lauroyl sarcosinate, menthol, saccharin, stirring evenly can obtain.
Embodiment 3
A kind of tooth-cleaning powder is made of the raw material of following parts by weight：10 parts of Sculellaria barbata, 9 parts of oldenlandia diffusa, feverfew 6
Part, 5 parts of mung bean, 4 parts of lemon polysaccharide, 1.8 parts of jade powder, 5 parts of calcium monohydrogen phosphate, 0.5 part of sodium N-lauroyl sarcosinate, menthol
0.1 part, 0.02 part of saccharin.
The preparation method of above-mentioned lemon polysaccharide is：
A. boiling 3 times is heated after lemon being sliced, filtered after degreasing, decoloration and is dried at 65 DEG C, then crushing and mistake
80 sieves, it is dry, obtain lemon powder；
B. it is 1 to press solid-liquid ratio:50 are added alkaline solution, and 1h is extracted at 80 DEG C, and extraction merges extracting solution afterwards twice；
C. the Sevage reagents for merging extracting solution and being added extracting liquid volume 1/2 shake after 22min in centrifuge with
4500r/min centrifugation 22min, the denatured protein of Polysaccharide removing solution layer and organic solution layer intersection, repetitive operation 4 times,
The protein and partial pigment in solution are removed, until solution is in colorless and transparent；
D. above-mentioned colourless transparent solution is pipetted, freeze-drying just obtains lemon polysaccharide.
The pH of above-mentioned alkaline solution is 9, is allocated with the NaOH of 0.1mol/L.
A kind of tooth-cleaning powder of the present embodiment, which is characterized in that the jade powder is Khotan jade, dushan diopside, Xiuyan Jade and green pine
The one or more of stone, it is 100nm to be crushed to particle size.
A kind of application method of tooth-cleaning powder of the present embodiment is to glue some tooth-cleaning powders with toothbrush before brushing teeth sooner or later daily, as brushing teeth
Equally carry out backwash several times, with clear water rinse it is clean after can normal use toothpaste continue to brush teeth.
A kind of preparation method of tooth-cleaning powder of the present embodiment, includes the following steps：By weight by Sculellaria barbata, oldenlandia
Grass, feverfew, mung bean are cleaned with clear water, and it is more than that solid matter 5cm impregnates 1.5h that pure water, which is added, is added more than solid matter
The pure water of 5cm, after being boiled by fire, then small fire is decocted to 1/2 that solution is original volume, well-done solution is poured out, with same
Mode be repeated 2 times decoction, 3 solution are filtered, up to dry powder after concentrate drying, lemon polysaccharide, jade powder, phosphorus is then added
Sour hydrogen calcium, sodium N-lauroyl sarcosinate, menthol, saccharin, stirring evenly can obtain.
Embodiment 4
A kind of tooth-cleaning powder is made of the raw material of following parts by weight：8.5 parts of Sculellaria barbata, 5.25 parts of oldenlandia diffusa, feverfew
Spend 3 parts, 2.75 parts of mung bean, 2.875 parts of lemon polysaccharide, 1.05 parts of jade powder, 2.75 parts of calcium monohydrogen phosphate, sodium N-lauroyl sarcosinate
0.275 part, 0.063 part of menthol, 0.013 part of saccharin.
The preparation method of above-mentioned lemon polysaccharide is：
A. boiling 2 times is heated after lemon being sliced, filtered after degreasing, decoloration and is dried at 40 DEG C, then crushing and mistake
50 sieves, it is dry, obtain lemon powder；
B. it is 1 to press solid-liquid ratio:35 are added alkaline solution, and 0.8h is extracted at 73 DEG C, and extraction merges extracting solution afterwards twice；
C. the Sevage reagents for merging extracting solution and being added extracting liquid volume 1/3 shake after 19min in centrifuge with
3750r/min centrifugation 19min, the denatured protein of Polysaccharide removing solution layer and organic solution layer intersection, repetitive operation 3 times,
The protein and partial pigment in solution are removed, until solution is in colorless and transparent；
D. above-mentioned colourless transparent solution is pipetted, freeze-drying just obtains lemon polysaccharide.
The pH of above-mentioned alkaline solution is 8.5, is allocated with the NaOH of 0.1mol/L.
A kind of tooth-cleaning powder of the present embodiment, which is characterized in that the jade powder is Khotan jade, dushan diopside, Xiuyan Jade and green pine
The one or more of stone, it is 25nm to be crushed to particle size.
A kind of application method of tooth-cleaning powder of the present embodiment is to glue some tooth-cleaning powders with toothbrush before brushing teeth sooner or later daily, as brushing teeth
Equally carry out backwash several times, with clear water rinse it is clean after can normal use toothpaste continue to brush teeth.
A kind of preparation method of tooth-cleaning powder of the present embodiment, includes the following steps：By weight by Sculellaria barbata, oldenlandia
Grass, feverfew, mung bean are cleaned with clear water, and it is more than that solid matter 3cm impregnates 1.2h that pure water, which is added, is added more than solid matter
The pure water of 3cm, after being boiled by fire, then small fire is decocted to 1/2 that solution is original volume, well-done solution is poured out, with same
Mode be repeated 2 times decoction, 3 solution are filtered, up to dry powder after concentrate drying, lemon polysaccharide, jade powder, phosphorus is then added
Sour hydrogen calcium, sodium N-lauroyl sarcosinate, menthol, saccharin, stirring evenly can obtain.
Embodiment 5
A kind of tooth-cleaning powder is made of the raw material of following parts by weight：9.5 parts of Sculellaria barbata, 7.75 parts of oldenlandia diffusa, feverfew
Spend 5 parts, 4.25 parts of mung bean, 3.625 parts of lemon polysaccharide, 1.55 parts of jade powder, 4.25 parts of calcium monohydrogen phosphate, sodium N-lauroyl sarcosinate
0.425 part, 0.088 part of menthol, 0.018 part of saccharin.
The preparation method of above-mentioned lemon polysaccharide is：
A. boiling 2 times is heated after lemon being sliced, filtered after degreasing, decoloration and is dried at 60 DEG C, then crushing and mistake
70 sieves, it is dry, obtain lemon powder；
B. it is 1 to press solid-liquid ratio:45 are added alkaline solution, and 0.8h is extracted at 78 DEG C, and extraction merges extracting solution afterwards twice；
C. the Sevage reagents for merging extracting solution and being added extracting liquid volume 1/3 shake after 21min in centrifuge with
4250r/min centrifugation 21min, the denatured protein of Polysaccharide removing solution layer and organic solution layer intersection, repetitive operation 4 times,
The protein and partial pigment in solution are removed, until solution is in colorless and transparent；
D. above-mentioned colourless transparent solution is pipetted, freeze-drying just obtains lemon polysaccharide.
The pH of above-mentioned alkaline solution is 8.5, is allocated with the NaOH of 0.1mol/L.
A kind of tooth-cleaning powder of the present embodiment, which is characterized in that the jade powder is Khotan jade, dushan diopside, Xiuyan Jade and green pine
The one or more of stone, it is 75nm to be crushed to particle size.
A kind of application method of tooth-cleaning powder of the present embodiment is to glue some tooth-cleaning powders with toothbrush before brushing teeth sooner or later daily, as brushing teeth
Equally carry out backwash several times, with clear water rinse it is clean after can normal use toothpaste continue to brush teeth.
A kind of preparation method of tooth-cleaning powder of the present embodiment, includes the following steps：By weight by Sculellaria barbata, oldenlandia
Grass, feverfew, mung bean are cleaned with clear water, and it is more than that solid matter 4cm impregnates 1.4h that pure water, which is added, is added more than solid matter
The pure water of 4cm, after being boiled by fire, then small fire is decocted to 1/2 that solution is original volume, well-done solution is poured out, with same
Mode be repeated 2 times decoction, 3 solution are filtered, up to dry powder after concentrate drying, lemon polysaccharide, jade powder, phosphorus is then added
Sour hydrogen calcium, sodium N-lauroyl sarcosinate, menthol, saccharin, stirring evenly can obtain.
Comparative example 1
Difference lies in it does not include Sculellaria barbata ingredient to prepare in the raw material of tooth-cleaning powder with embodiment 1.
Comparative example 2
Difference lies in it does not include jade meal component to prepare in the raw material of tooth-cleaning powder with embodiment 1.
Comparative example 3
Difference lies in it does not include lemon polysaccharide component to prepare in the raw material of tooth-cleaning powder with embodiment 1.
Compliance test result
The volunteer that 80 teeth are partially yellow, have oral cavity excessive internal heat symptom is found, is divided into 8 groups, every group respectively using above-mentioned
The tooth-cleaning powder of Examples 1 to 5 and comparative example 1~3 glues some tooth-cleaning powders before brushing teeth sooner or later daily with toothbrush, comes as brushing teeth
Several times of backwash, with clear water rinse it is clean after can normal use toothpaste continue to brush teeth.
After continuous use one month, the suggestion feedback of their one month used is recorded with table 1, as follows：
Table 1
As can be known from the above table, data are not much different between Examples 1 to 5, and are better than comparative example 1~3.Analyze 1 He of embodiment
The oral cavity excessive internal heat rate of descent of comparative example 1~3, comparative example 1 is minimum, and the bleeding gums symptom reduction number of comparative example 3 is minimum, comparison
The cleaning of teeth situation of example 2 is least ideal, illustrates that Scutellaria barbata, which is added, can effectively reduce oral cavity excessive internal heat, jade powder is added can be with
Tartar, tooth spot and the dark yellow phenomenon of tooth are reduced, lemon polysaccharide, which is added, can significantly reduce bleeding gums, tooth-cleaning powder of the present invention
Each ingredient is indispensable, otherwise can weaken whole effect.
Several embodiments of the invention above described embodiment only expresses, the description thereof is more specific and detailed, but simultaneously
Cannot the limitation to the scope of the claims of the present invention therefore be interpreted as.It should be pointed out that for those of ordinary skill in the art
For, without departing from the inventive concept of the premise, various modifications and improvements can be made, these belong to the guarantor of the present invention
Protect range.
Claims (8)
1. a kind of tooth-cleaning powder, which is characterized in that be made of the raw material of following parts by weight：8~10 parts of Sculellaria barbata, oldenlandia diffusa
4~9 parts, 2~6 parts of feverfew, 2~5 parts of mung bean, 2.5~4 parts of lemon polysaccharide, 0.8~1.8 part of jade powder, calcium monohydrogen phosphate 2~5
Part, 0.2~0.5 part of sodium N-lauroyl sarcosinate, 0.05~0.1 part of menthol, 0.01~0.02 part of saccharin.
2. a kind of tooth-cleaning powder according to claim 1, which is characterized in that be made of the raw material of following parts by weight：Half
8.5~9.5 parts of lotus, 5.25~7.75 parts of oldenlandia diffusa, 3~5 parts of feverfew, 2.75~4.25 parts of mung bean, lemon polysaccharide
2.875~3.625 parts, 1.05~1.55 parts of jade powder, 2.75~4.25 parts of calcium monohydrogen phosphate, sodium N-lauroyl sarcosinate 0.275
~0.425 part, 0.063~0.088 part of menthol, 0.013~0.018 part of saccharin.
3. a kind of tooth-cleaning powder according to claim 2, which is characterized in that be made of the raw material of following parts by weight：Half
9 parts of lotus, 6.5 parts of oldenlandia diffusa, 4 parts of feverfew, 3.5 parts of mung bean, 3.25 parts of lemon polysaccharide, 1.3 parts of jade powder, calcium monohydrogen phosphate
3.5 parts, 0.35 part of sodium N-lauroyl sarcosinate, 0.075 part of menthol, 0.015 part of saccharin.
4. according to a kind of tooth-cleaning powder of claims 1 to 3 any one of them, which is characterized in that the preparation side of the lemon polysaccharide
Method is：
A. boiling 1~3 time is heated after lemon being sliced, filtered after degreasing, decoloration and is dried at 35~65 DEG C, is then crushed simultaneously
40~80 sieves are crossed, it is dry, obtain lemon powder；
B. it is 1 to press solid-liquid ratio:30~50 are added alkaline solution, and 0.5~1h is extracted at 70~80 DEG C, and extraction merges afterwards twice to be carried
Take liquid；
C. after the Sevage reagents for merging extracting solution addition extracting liquid volume 1/6~1/2 shake 18~22min in centrifuge
With 3500~4500r/min centrifuge 18~22min, the denatured protein of Polysaccharide removing solution layer and organic solution layer intersection,
Repetitive operation 3~4 times removes protein and partial pigment in solution, until solution is in colorless and transparent；
D. above-mentioned colourless transparent solution is pipetted, freeze-drying just obtains lemon polysaccharide.
5. a kind of tooth-cleaning powder according to claim 4, which is characterized in that the pH of the alkaline solution is 8~9, is used
The NaOH of 0.1mol/L is allocated.
6. according to a kind of tooth-cleaning powder of claims 1 to 3 any one of them, which is characterized in that the jade powder is Khotan jade, solely
The one or more of mountain jade, Xiuyan Jade and turquoise, it is 1~100nm to be crushed to particle size.
7. according to a kind of tooth-cleaning powder of claims 1 to 3 any one of them, which is characterized in that the application method of the tooth-cleaning powder
To glue some tooth-cleaning powders with toothbrush before brushing teeth sooner or later daily, backwash is carried out as brushing teeth several times, with clear water rinse it is clean after
Continue to brush teeth with normal use toothpaste.
8. a kind of prepare such as a kind of method of tooth-cleaning powder of claim 1~7 any one of them, which is characterized in that including following
Step：Sculellaria barbata, oldenlandia diffusa, feverfew, mung bean are cleaned with clear water by weight, it is more than solids that pure water, which is added,
Matter about 2~5cm impregnates 1~1.5h, adds the pure water more than 2~5cm of solid matter, and after being boiled by fire, then small fire decocts
To 1/2 that solution is original volume, well-done solution is poured out, is repeated 2 times decoction in the same way, 3 solution are filtered, it is dense
Up to dry powder after contracting is dry, lemon polysaccharide, jade powder, calcium monohydrogen phosphate, sodium N-lauroyl sarcosinate, menthol, sugar is then added
Essence stirs evenly, you can obtains tooth-cleaning powder of the present invention.
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| CN201810519676.XA CN108498353A (en) | 2018-05-25 | 2018-05-25 | A kind of tooth-cleaning powder and preparation method thereof |
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| Application Number | Priority Date | Filing Date | Title |
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| CN201810519676.XA CN108498353A (en) | 2018-05-25 | 2018-05-25 | A kind of tooth-cleaning powder and preparation method thereof |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112641668A (en) * | 2020-09-14 | 2021-04-13 | 浙江昆能新材料科技有限公司 | Toothpaste capable of efficiently removing oral odor |
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| CN1915212A (en) * | 2006-08-24 | 2007-02-21 | 王灿留 | Toothpaste prepared from natural jade mineral |
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|---|---|---|---|---|
| CN1915212A (en) * | 2006-08-24 | 2007-02-21 | 王灿留 | Toothpaste prepared from natural jade mineral |
| CN101744939A (en) * | 2010-01-31 | 2010-06-23 | 张敏洁 | Chinese medicinal herb compound and preparation method with health care effect for preventing mouth disease |
| CN107281090A (en) * | 2017-08-01 | 2017-10-24 | 何家平 | A kind of compound alum Chinese traditional medicine tooth powder technique |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN112641668A (en) * | 2020-09-14 | 2021-04-13 | 浙江昆能新材料科技有限公司 | Toothpaste capable of efficiently removing oral odor |
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