CN108359531A - The quick-fried pearl essence of lily odor type and its application in cigarette - Google Patents
The quick-fried pearl essence of lily odor type and its application in cigarette Download PDFInfo
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- CN108359531A CN108359531A CN201810237418.2A CN201810237418A CN108359531A CN 108359531 A CN108359531 A CN 108359531A CN 201810237418 A CN201810237418 A CN 201810237418A CN 108359531 A CN108359531 A CN 108359531A
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- Prior art keywords
- quick
- lily
- fried pearl
- cigarette
- odor type
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Classifications
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24D—CIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
- A24D3/00—Tobacco smoke filters, e.g. filter-tips, filtering inserts; Filters specially adapted for simulated smoking devices; Mouthpieces for cigars or cigarettes
- A24D3/06—Use of materials for tobacco smoke filters
- A24D3/061—Use of materials for tobacco smoke filters containing additives entrapped within capsules, sponge-like material or the like, for further release upon smoking
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/02—Recovery or refining of essential oils from raw materials
- C11B9/025—Recovery by solvent extraction
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- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Life Sciences & Earth Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Materials Engineering (AREA)
- Fats And Perfumes (AREA)
Abstract
The present invention relates to cigarette filter rod production technical fields, and in particular to a kind of quick-fried pearl essence of lily odor type and its application in cigarette；The quick-fried pearl essence of lily odor type, consists of the following mass percentage components：4 ~ 8%, 2 ethyl hexanol of Flos Lilii viriduli extract, 1 ~ 3%, 1,8 Cineole 0.6 ~ 1.5%, β carypohyllenes 0.2 ~ 1.5%, enanthic acid 0.6 ~ 1%, caproic acid 1 ~ 1.8%, terpenes of orange oil 0.4 ~ 0.5%, acetic acid 2.5 ~ 3.5%, butyl acetate 0.3 ~ 0.5%, Glycerin, mixed triester with caprylic acid capric acid 80 ~ 88%；The quick-fried pearl prepared with essence of the present invention can assign cigarette lily fragrance and effect, make quick-fried pearl while having lily simple and elegant and the fragrance of a flower of faint scent, also have effects that moistening lung simultaneously, relieve inflammation or internal heat, calm the nerves, quick-fried pearl formula is unique, it can improve and enrich cigarette flavor, it is obviously improved promote the production of body fluid sense and time sweet tea sense of cigarette, dry sensation is reduced, improves the harmony of fragrance and flue gas.
Description
Technical field
The present invention relates to cigarette filter rod production technical fields, and in particular to a kind of quick-fried pearl essence of lily odor type and its is rolling up
Application in cigarette.
Background technology
Lily is the cultivation population that bulb can be formed in Liliaceae lilium, perennial herb plant, also known as open country hundred
Conjunction, cone, BULBUS LILII, medicine lily, family lily etc..Lily in European and American countries mainly as flower culture, and China's cultivation hundred
Its bulb of master recovery is closed as edible or medicinal." lanzhou lily " is Lanzhou specialty, and taste is extremely sweet, fiber is seldom and has no
Bitter taste, it is not only well-known throughout the country, it can also claim the first in the world.Liliaceous primary efficacy is moistening lung, relieves inflammation or internal heat, calms the nerves.Lily has
The features such as simple and elegant and faint scent, is rich in protein, sugar, phosphorus, iron and various trace elements, has high medical value and edible
Value.
" quick-fried pearl addition " assigns fragrant innovative technology as a kind of cigarette, and the category structure to be modelled as core with odor type provides
It is new, more specifically perceive supporting method, quick-fried pearl due to its content special delivery mode, in supplement, improvement, coordination
Smoking property of cigarette quality and the function of promotion, change cigarette product style etc. are more and more prominent, improve the interest of cigarette smoking
Taste and aesthetic quality.
Although and currently on the market there are a certain number of quick-fried pearl cigarette, the fragrance in this quick-fried pearl, which is lack of pertinence, to be set
Meter, thus it is relatively poor with flue gas harmony, and be affected to the odor characteristic of cigarette itself, affect the suction of quick-fried pearl cigarette
Sense of food by.
Invention content
The present invention is that the fragrance solved in existing quick-fried pearl is lack of pertinence design, and poor technology is asked with flue gas harmony
Topic provides a kind of quick-fried pearl essence of lily odor type and the application in cigarette, quick-fried pearl is made to assign cigarette lily fragrance, improves and rich
Rich cigarette flavor is obviously improved promote the production of body fluid sense and time sweet tea sense of cigarette, reduces dry sensation, and then improve the coordination of fragrance and flue gas
Property.
In order to solve the above technical problems, the technical solution adopted in the present invention is：A kind of quick-fried pearl essence of lily odor type, by
The group of following mass percent is grouped as：Flos Lilii viriduli extract 4~8%, 2-Ethylhexyl Alcohol 1~3%, 1, 8-Cineole 0.6~
1.5%, β-carypohyllenes 0.2~1.5%, enanthic acid 0.6~1%, caproic acid 1~1.8%, terpenes of orange oil 0.4~0.5%, acetic acid
2.5~3.5%, butyl acetate 0.3~0.5%, Glycerin, mixed triester with caprylic acid capric acid 80~88%.
Flos Lilii viriduli extract：The lily fragrance of a flower makes one excited, has effects that moistening lung, relieves inflammation or internal heat, calms the nerves.
2-Ethylhexyl Alcohol：There is mild, salted cake fried in sesame oil, happy rose style light floral odor gas, it is sweet tea, with fruit aromatic
Fat-fragrance of a flower taste.
1, 8-Cineole：Refrigerant fragrance, some are like camphor breath.
β-carypohyllene：For improving and the natural flavor of promoting or transferring cigarette perfume.
Enanthic acid：Improve and inhales taste.
Caproic acid：Fruity flavor can be enhanced.
Terpenes of orange oil：There are fresh orange fragrance and lemon sample fragrance, can increase pure and fresh elegant on news perfume.
Acetic acid：For pungent smoke can be mitigated in tobacco, undesirable miscellaneous gas is covered.
Butyl acetate：For enhancing fruit-like flavour.
The quick-fried pearl essence of preferred lily odor type, consists of the following mass percentage components：Flos Lilii viriduli extract
6%, 2-Ethylhexyl Alcohol 2%, 1, 8-Cineole 1%, β-carypohyllene 1%, enanthic acid 0.8%, caproic acid 1.4%, terpenes of orange oil
0.4%, acetic acid 3%, butyl acetate 0.4%, Glycerin, mixed triester with caprylic acid capric acid 84%.
Above-mentioned Flos Lilii viriduli extract of stating is by supercritical CO2Prepared by extracting process, specifically include following steps：1) by hundred
The sieving of flower bud crushed after being dried is closed, the lily powder between 20~40 mesh is obtained；2) gained lily powder is packed into and is extracted
It takes and sets 40~50 DEG C of furnace box temperature in kettle, collects 100 DEG C of valve temperature, adjust 200~300bar of pressure, absolute ethyl alcohol is added and does
Entrainer；3) lily is extracted in such a way that static extracting and dynamic extraction combine；4) Flos Lilii viriduli extract is collected.
The adding proportion of lily powder and absolute ethyl alcohol is 100g in step 2)：4~20mL.
A diameter of 2.5~4mm of the quick-fried pearl of lily odor type prepared by the above-mentioned quick-fried pearl essence of lily odor type, essence in quick-fried pearl
Content is 18~25uL/.
The preferred quick-fried a diameter of 3.4mm of pearl, weight 21mg/, essence content are 20 μ L/.
The present invention's also provides application of the quick-fried pearl of lily odor type in cigarette, and quick-fried pearl is located in the middle part of cigarette filter rod, every volume
A quick-fried pearl is added in cigarette filter.
Compared with prior art the invention has the advantages that：
The quick-fried pearl prepared with essence of the present invention can assign cigarette lily fragrance and effect, make quick-fried pearl while having lily
Simple and elegant and faint scent the fragrance of a flower, while also having effects that have moistening lung, relieve inflammation or internal heat, calm the nerves, quick-fried pearl formula is unique, can improve and enrich
Cigarette flavor is obviously improved promote the production of body fluid sense and time sweet tea sense of cigarette, reduces dry sensation, improve the harmony of fragrance and flue gas.Hundred
Close flower extract and combine other essence, by " quick-fried pearl add " technology make cigarette category style characteristic can perceptibility rise to one
A new step.
Specific implementation mode
Below in conjunction with specific embodiment, the invention will be further described.
1~example of example 3 is that quick-fried pearl is respectively prepared with composition in three kinds of determining quick-fried pearls of lily odor type of multiple adjustment
It is tested afterwards in same vehicle by same test level.
Example 1：
Essence used in the quick-fried pearl of lily odor type, consists of the following mass percentage components：Flos Lilii viriduli extract 8%, 2- second
Base hexanol 3%, 1, 8-Cineole 1.5%, β-carypohyllene 0.2%, enanthic acid 1%, caproic acid 1.8%, terpenes of orange oil 0.5%, second
Acid 3.5%, butyl acetate 0.5%, Glycerin, mixed triester with caprylic acid capric acid 80%.
A diameter of 3.4mm is made, the quick-fried pearl of cigarette that weight is 21mg/, quick-fried pearl essence content is 20uL/.
According to filter stick production technology, quick-fried pearl is transferred to by filter stick center by filter-stick forming device, it is 24.3mm to make an addition to circumference
Cigarette filter rod in, quick-fried pearl position is apart from the 12.5mm of lip end at, and every cigarette one quick-fried pearl of addition is made containing the quick-fried of quick-fried pearl
Pearl filter stick, for producing the quick-fried pearl cigarette of lily.
For the prepared quick-fried pearl cigarette of lily, by 9 professional sensory evaluation personnel to the sample and control blank cigarette
Sample (not adding quick-fried pearl) is detected and compares suction evaluation.
Flue gas inspection result and suction evaluation score value etc. are shown in Table 3 and table 4.
Cigarette smoking result is in the present embodiment：Lily fragrance is with cigarette perfume compared with harmony, and miscellaneous gas is reduced, and irritation reduces, remaining
Taste improves.
Example 2：
Essence used in the quick-fried pearl of lily odor type, consists of the following mass percentage components：Flos Lilii viriduli extract 6%, 2- second
Base hexanol 2%, 1, 8-Cineole 1%, β-carypohyllene 1%, enanthic acid 0.8%, caproic acid 1.4%, terpenes of orange oil 0.4%, acetic acid
3%, butyl acetate 0.4%, Glycerin, mixed triester with caprylic acid capric acid 84%.
A diameter of 3.4mm is made, the quick-fried pearl of cigarette that weight is 21mg/, quick-fried pearl essence content is 20uL/.
According to filter stick production technology, quick-fried pearl is transferred to by filter stick center by filter-stick forming device, it is 24.3mm to make an addition to circumference
Cigarette filter rod in, quick-fried pearl position is apart from the 12.5mm of lip end at, and every cigarette one quick-fried pearl of addition is made containing the quick-fried of quick-fried pearl
Pearl filter stick, for producing the quick-fried pearl cigarette of lily.
For the prepared quick-fried pearl cigarette of lily, by 9 professional sensory evaluation personnel to the sample and control blank cigarette
Sample (not adding quick-fried pearl) is detected and compares suction evaluation.
Flue gas inspection result and suction evaluation score value etc. are shown in Table 3 and table 4.
Cigarette smoking result is in the present embodiment：Cigarette perfume is full, and concentration is denseer, jealous alcohol and clean, sense of promoting the production of body fluid, time sweet tea sense
Obviously, hamony is good.
Example 3：
Essence used in the quick-fried pearl of lily odor type, consists of the following mass percentage components：Flos Lilii viriduli extract 4%, 2- second
Base hexanol 1%, 1, 8-Cineole 0.6%, β-carypohyllene 1.5%, enanthic acid 0.6%, caproic acid 1%, terpenes of orange oil 0.5%, second
Acid 2.5%, butyl acetate 0.3%, Glycerin, mixed triester with caprylic acid capric acid 88%.
A diameter of 3.4mm is made, the quick-fried pearl of cigarette that weight is 21mg/, quick-fried pearl essence content is 20uL/.
According to filter stick production technology, quick-fried pearl is transferred to by filter stick center by filter-stick forming device, it is 24.3mm to make an addition to circumference
Cigarette filter rod in, quick-fried pearl position is apart from the 12.5mm of lip end at, and every cigarette one quick-fried pearl of addition is made containing the quick-fried of quick-fried pearl
Pearl filter stick, for producing the quick-fried pearl cigarette of lily.
For the prepared quick-fried pearl cigarette of lily, by 9 professional sensory evaluation personnel to the sample and control blank cigarette
Sample (not adding quick-fried pearl) is detected and compares suction evaluation.
Flue gas inspection result and suction evaluation score value etc. are shown in Table 3 and table 4.
3 cigarette smoking result of example is：Fragrance is promoted, lily fragrance and flue gas harmony, the miscellaneous more normal cigarette (control sample of gas
Cigarette) there are increase, irritation slightly to reduce, pleasant impression slightly improves.
Quick-fried pearl product prepared by above-described embodiment is detected, while to prepared by the quick-fried pearl of above-described embodiment
Cigarette and existing quick-fried pearl cigarette carry out conventional detection as a contrast, and testing result is shown in Tables 1 and 2.
The testing result of prepared quick-fried pearl in the different embodiments of table 1
The different implementations of table 2 are obtained to contain quick-fried pearl filter stick testing result
| Sample | Length (mm) | Circumference (mm) | Circularity (mm) | Pressure drop (Pa) | Hardness (%) |
| Technical standard | 100±0.50 | 24.25±0.20 | ≤0.35 | 3100±300 | ≥84 |
| Example 1 | 100.1 | 24.2 | 0.16 | 3160 | 88.6 |
| Example 2 | 100 | 24.1 | 0.18 | 3110 | 89.1 |
| Example 3 | 99.9 | 24.2 | 0.17 | 3130 | 88.9 |
| Control | 100.1 | 24.1 | 0.18 | 3105 | 90.2 |
Without significant difference, filter stick pressure drop is increased the physical index of the quick-fried pearl cigarette of the present invention it can be seen from Tables 1 and 2
Add.
The physical index and main flume testing result of 3 kinds of cigarettes sample of table
4 kinds of cigarettes sample sensory quality assessment result of table
| Sample | Gloss (5) | Fragrance (32) | Harmony (6) | Miscellaneous gas (12) | Irritation (20) | Pleasant impression (25) | Total (100) |
| Example 1 | 4.5 | 27.83 | 4.83 | 10.06 | 17.22 | 21.11 | 85.55 |
| Example 2 | 4.5 | 27.89 | 4.89 | 10.06 | 17.22 | 21.17 | 85.73 |
| Example 3 | 4.5 | 28 | 4.94 | 9.11 | 17.17 | 21.0 | 84.72 |
| Control | 4.5 | 27.5 | 4.89 | 9.33 | 17.06 | 20.94 | 84.77 |
The cigarette sample of 1~example of example 3 is smoked panel test through 9 professions personnel that smoke panel test, and smoking result is as follows：7 personnel that smoke panel test
Think that 2 lily style of example highlights the most, with cigarette perfume compared with harmony, cigarette perfume is full, and concentration is denseer, jealous alcohol and clean, sense of promoting the production of body fluid,
Return sweet tea sense it is apparent, hamony is good；It is best that 6 personnel that smoke panel test think that 2 lily fragrance of example is combined with cigarette perfume, and 1 personnel that smoke panel test recognizes
It is sent out thoroughly slightly to influence cigarette perfume；2 personnel that smoke panel test think that 3 style of example is unique, and lily fragrance is apparent, and 1 personnel that smoke panel test thinks
Example 3 influences cigarette perfume and sends out thoroughly；1 personnel that smoke panel test thinks example 1 compared with harmony, and comfort is good, and 1 personnel that smoke panel test thinks to influence cigarette perfume
Hair thoroughly.
The present invention prepares quick-fried pearl by the essence of design lily odor type and applied to after cigarette, is obviously improved promoting the production of body fluid for cigarette
Sense and time sweet tea sense, reduce dry sensation, improve the harmony of fragrance and flue gas.The special efficacy that lily has can also reduce
The harm of cigarette improves smoking property of cigarette quality.
Claims (7)
1. a kind of quick-fried pearl essence of lily odor type, which is characterized in that consist of the following mass percentage components：Lily is extracted
Object 4 ~ 8%, 2-Ethylhexyl Alcohol 1 ~ 3%, 1, 8-Cineole 0.6 ~ 1.5%, β-carypohyllene 0.2 ~ 1.5%, enanthic acid 0.6 ~ 1%, caproic acid 1 ~
1.8%, terpenes of orange oil 0.4 ~ 0.5%, acetic acid 2.5 ~ 3.5%, butyl acetate 0.3 ~ 0.5%, Glycerin, mixed triester with caprylic acid capric acid 80 ~ 88%.
2. the quick-fried pearl essence of lily odor type according to claim 1, which is characterized in that by the component of following mass percent
Composition：Flos Lilii viriduli extract 6%, 2-Ethylhexyl Alcohol 2%, 1, 8-Cineole 1%, β-carypohyllene 1%, 0.8 % of enanthic acid, caproic acid 1.4
%, 0.4 % of terpenes of orange oil, acetic acid 3%, 0.4 % of butyl acetate, Glycerin, mixed triester with caprylic acid capric acid 84%.
3. the quick-fried pearl essence of lily odor type according to claim 1 or 2, which is characterized in that the Flos Lilii viriduli extract is
By supercritical CO2Prepared by extracting process, specifically include following steps：1）Lily flower bud crushed after being dried is sieved, is obtained
Lily powder between 20 ~ 40 mesh；2）Gained lily powder is fitted into extraction kettle and sets 40 ~ 50 DEG C of furnace box temperature, is received
Collect 100 DEG C of valve temperature, adjust 200 ~ 300bar of pressure, absolute ethyl alcohol is added and does entrainer；3）Extracted using static extracting and dynamic
The mode of combination is taken to extract lily；4）Collect Flos Lilii viriduli extract.
4. the quick-fried pearl essence of lily odor type according to claim 3, which is characterized in that step 2）Middle lily powder and nothing
The adding proportion of water-ethanol is 100g：4~20mL.
5. a kind of quick-fried pearl of lily odor type prepared by lily odor type quick-fried pearl essence as claimed in claim 1 or 2, feature exist
Essence content is 18 ~ 25uL/ in, a diameter of 2.5 ~ 4 mm of prepared quick-fried pearl, quick-fried pearl.
6. the quick-fried pearl of lily odor type according to claim 5, which is characterized in that quick-fried a diameter of 3.4 mm of pearl, weight 21
Mg/, essence content is 20 μ L/.
7. a kind of application of quick-fried pearl of lily odor type as claimed in claim 6 in cigarette, which is characterized in that quick-fried pearl is located at cigarette
In the middle part of filter stick, a quick-fried pearl is added in every cigarette filter rod.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810237418.2A CN108359531A (en) | 2018-03-22 | 2018-03-22 | The quick-fried pearl essence of lily odor type and its application in cigarette |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810237418.2A CN108359531A (en) | 2018-03-22 | 2018-03-22 | The quick-fried pearl essence of lily odor type and its application in cigarette |
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| Publication Number | Publication Date |
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| CN108359531A true CN108359531A (en) | 2018-08-03 |
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ID=63001332
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| CN201810237418.2A Pending CN108359531A (en) | 2018-03-22 | 2018-03-22 | The quick-fried pearl essence of lily odor type and its application in cigarette |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110819457A (en) * | 2019-12-09 | 2020-02-21 | 将军烟草集团有限公司 | Sweet tea flavor and preparation method and application thereof |
| CN112175732A (en) * | 2020-09-23 | 2021-01-05 | 甘肃烟草工业有限责任公司 | Rose fragrance type essence for blasting beads and application thereof in cigarettes |
Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107034021A (en) * | 2017-04-27 | 2017-08-11 | 河南中烟工业有限责任公司 | A kind of cigarette quick-fried pearl savory essence of lily and its application in cigarette |
-
2018
- 2018-03-22 CN CN201810237418.2A patent/CN108359531A/en active Pending
Patent Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107034021A (en) * | 2017-04-27 | 2017-08-11 | 河南中烟工业有限责任公司 | A kind of cigarette quick-fried pearl savory essence of lily and its application in cigarette |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110819457A (en) * | 2019-12-09 | 2020-02-21 | 将军烟草集团有限公司 | Sweet tea flavor and preparation method and application thereof |
| CN112175732A (en) * | 2020-09-23 | 2021-01-05 | 甘肃烟草工业有限责任公司 | Rose fragrance type essence for blasting beads and application thereof in cigarettes |
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Application publication date: 20180803 |