CN106987314B - Citrus reticulata flavor essence for bead blasting of cigarettes and application of citrus reticulata flavor essence in cigarettes - Google Patents
Citrus reticulata flavor essence for bead blasting of cigarettes and application of citrus reticulata flavor essence in cigarettes Download PDFInfo
- Publication number
- CN106987314B CN106987314B CN201710288573.2A CN201710288573A CN106987314B CN 106987314 B CN106987314 B CN 106987314B CN 201710288573 A CN201710288573 A CN 201710288573A CN 106987314 B CN106987314 B CN 106987314B
- Authority
- CN
- China
- Prior art keywords
- cigarette
- blasting
- bead blasting
- bead
- ponkan
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/0007—Aliphatic compounds
- C11B9/0015—Aliphatic compounds containing oxygen as the only heteroatom
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/28—Treatment of tobacco products or tobacco substitutes by chemical substances
- A24B15/30—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances
- A24B15/301—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances by aromatic compounds
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/28—Treatment of tobacco products or tobacco substitutes by chemical substances
- A24B15/30—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances
- A24B15/302—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances by natural substances obtained from animals or plants
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/28—Treatment of tobacco products or tobacco substitutes by chemical substances
- A24B15/30—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances
- A24B15/32—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances by acyclic compounds
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/0061—Essential oils; Perfumes compounds containing a six-membered aromatic ring not condensed with another ring
Landscapes
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- General Health & Medical Sciences (AREA)
- Toxicology (AREA)
- General Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Agronomy & Crop Science (AREA)
- Botany (AREA)
- Cigarettes, Filters, And Manufacturing Of Filters (AREA)
Abstract
The invention belongs to the technical field of cigarette filter stick production, and particularly relates to a small green citrus flavor essence for cigarette bead blasting and application thereof in cigarettes. The ponkan essence consists of a ponkan extract, butanedione, ethyl vanillin, methyl cinnamate, geraniol, sweet orange oil and caprylic capric glyceride. The essence can be used for preparing small green citrus flavor cigarette blasting beads, and the blasting beads can be added into a filter stick and used for preparing cigarette blasting bead cigarettes. The application can prepare and obtain a cigarette bead blasting product with stable and uniform forming quality by providing the minor green orange flavor specially used for cigarette bead blasting and combining a relatively perfect bead blasting production process, and after the bead blasting is placed into a cigarette filter, the irritation of the cigarette can be better weakened, the aroma of the cigarette can be improved and enriched, the aroma richness, the sensory quality and the smoking interest of the cigarette can be obviously improved, so that the minor green orange flavor has relatively good application value and popularization and application significance in design, development, production and sale of the bead blasting cigarette.
Description
Technical Field
The invention belongs to the technical field of cigarette filter stick production, and particularly relates to a small green citrus flavor essence for cigarette bead blasting and application thereof in cigarettes.
Background
In the traditional cigarette flavoring technology, the flavoring liquid is mainly added into tobacco shreds, the added flavoring liquid is partially lost in the cigarette combustion process, and meanwhile, as the reaction of a complex material system at high temperature is difficult to expect, part of the flavoring liquid can generate some undesirable sensory effects. As a novel cigarette flavoring mode, the bead blasting flavoring can overcome the defects of the existing flavoring mode to a certain extent, and the main reasons are as follows: the exploded beads contain spices, before smoking cigarettes, consumers preferably crush the exploded beads contained in the filter rods and then smoke the cigarettes, and smoke gas passes through the filter tips and acts on the consumers together with the exploded bead feed liquid, so that the flavoring and fragrance supplementing process is completed; the mode can effectively avoid the loss of the spice liquid in the combustion process of the tobacco on one hand, and on the other hand, the spice is arranged in the sealed exploding bead, so that the loss can not occur during the storage of the cigarette, and the stability of the quality of the cigarette is ensured.
The bead blasting cigarette is used as a new material in cigarettes, and due to the special release mode of the content of the bead blasting cigarette, the bead blasting cigarette has more and more outstanding functions in the aspects of supplementing, improving and coordinating the smoking quality of the cigarettes, improving, changing, cigarette product style and the like, and improves the interestingness and sensory quality of cigarette smoking, so that the bead blasting cigarette is increasingly applied to Chinese cigarette production in recent years and is also popular with consumers.
In the prior art, although a certain number of bead-exploded cigarettes exist in the market at present, the fragrance in the bead-exploded cigarettes is poor in coordination with smoke due to lack of targeted design, and the smoking feeling of the bead-exploded cigarettes is influenced due to large influence on the fragrance characteristics of the cigarettes.
Although the 'bead-popping' cigarette appears like a bamboo shoot in spring after rain, the 'bead-popping' cigarette has a plurality of new problems in the aspects of addition and use due to the fact that the product is relatively novel and the current production standard and specification are relatively lacked. Particularly, for the particularity of cigarette products, the influence of the 'bead blasting' filter stick on physical indexes, chemical indexes, hazard indexes and the like of cigarettes is rarely reported in the aspects of the design of a 'bead blasting' inclusion formula, the stable release of the inclusion and the like. Therefore, the 'bead blasting' inclusion with different components is designed, the special inclusion release rule of the 'bead blasting' is systematically researched, and the 'bead blasting' inclusion has important theoretical and application significance on the aspects of the influence of physical indexes, smoke indexes, hazard indexes and the like of cigarettes.
Disclosure of Invention
The invention aims to provide a targeted ponkan essence for a cigarette filter stick, so that the types of cigarette products are enriched, and the cigarette products with different style characteristics are provided.
The technical solution adopted in the present application is detailed as follows.
The ponkan essence for bead blasting of cigarettes comprises the following components in percentage by mass:
10.0-15.0% of small green orange extract,
1.0 to 2.0% of butanedione,
0.3 to 0.6% of ethyl vanillin,
0.5 to 1.0% of methyl cinnamate,
0.2 to 0.5% of geraniol,
1.0 to 2.0 percent of sweet orange oil,
78.9-87.0% of caprylic/capric glyceride.
The ponkan extract is an ethanol extract of the ponkan;
the caprylic capric glyceride (MCT) is the product of esterification of fatty acid containing 8-12 carbon chains with glycerol.
The ponkan extract can be prepared by the following steps:
(1) crushing the dried small green oranges, and sieving the crushed small green oranges by a sieve of 40-60 meshes to prepare small green orange powder;
(2) adding an ethanol solution with the volume fraction of 60-90% into the small green citrus powder obtained in the step (1), and carrying out hot reflux for 3-5 h in water bath at the temperature of 60-80 ℃; the material-liquid ratio of the minor green tangerine powder to the ethanol solution is as follows: ethanol =1 g: 4-6 mL;
(3) and (3) concentrating the hot reflux liquid in the step (2) under reduced pressure at 55-65 ℃ and 60-80 Kpa until the volume is unchanged, and obtaining the extract, namely the ponkan extract.
The green orange flavor essence for bead blasting of cigarettes comprises the following specific formula: 12% of ponkan extract, 1.5% of butanedione, 0.4% of ethyl vanillin, 0.7% of methyl cinnamate, 0.35% of geraniol, 1.5% of sweet orange oil and 83.55% of caprylic capric glyceride.
It needs to be explained that different essences are different according to purposes, the formula of the essence is generally specially designed, in the application, the citrus reticulata blanco essence is specially designed according to the purposes in the final cigarette by combining the production process characteristics of the bead blasting of the cigarette, so that the results of adjusting the smoke quality and improving the smoking quality of the cigarette can be better realized on the basis of ensuring the bead blasting quality.
The small green orange flavor cigarette bead blasting is prepared by using the small green orange flavor essence for cigarette bead blasting, the cigarette bead blasting is to wrap essence and spice in a closed bead blasting by using a natural polymer material or a synthetic polymer material to form a round sealed bead blasting with different colors, the diameter of the bead blasting is 2.0-4.0 mm, and the essence content in the bead blasting is 20-25 mu L/particle; specific examples thereof include: the diameter of the blasting beads is 3.65mm, and the weight is 23 mg/granule; the content of essence in the exploded bead is 23 muL/granule, in a word, the specific specification can be adjusted according to different machine equipment and different specifications of used filter sticks.
The application of the small green citrus flavor cigarette bead blasting in cigarettes is characterized in that the cigarette bead blasting is added into a common (circumference 24.3 mm) cigarette filter stick, the bead blasting position is 12.5mm away from the lip end, and one bead blasting is added to each cigarette.
The ponkan essence for bead blasting of cigarettes provided by the application has obvious herbal fragrance, and the fragrance is the most important aroma characteristic in cigarette smoke; after the cigarette is prepared into a product form of 'bead blasting' and applied to cigarettes, the result of cigarette smoking shows that: compared with a comparison sample, after the small green citrus flavored cigarette is smoked, the smoke aroma richness can be obviously improved on the premise of not changing the smoke aroma style of the cigarette, the full feeling and richness of smoke are enhanced, the compatibility of aroma and the sensory quality of products is further improved, and the smoking interestingness of the cigarette is increased; meanwhile, the small green tangerine has the effects of regulating qi, invigorating stomach, eliminating phlegm, moistening throat, restoring consciousness, refreshing and the like, so that the application has the effect of reducing the smoking harm of cigarettes to a certain degree.
In general, the minor green citrus flavor essence adopted in the application is obtained by extracting from natural minor green citrus, so that after the aroma substances enter cigarette smoke, the irritation of the smoke can be reduced, the soft roundness, aroma fullness and plumpness of the cigarette smoke are improved, and the smoking quality and the sensory comfort degree of the cigarette smoke are further improved.
In a word, the application can prepare and obtain a cigarette bead blasting product with stable and uniform forming quality by providing the small green orange flavor specially used for cigarette bead blasting and combining a relatively perfect bead blasting production process, the stimulation of cigarettes can be better weakened after the bead blasting is placed into a cigarette filter, the fragrance of the cigarettes is improved and enriched, the fragrance richness, the sensory quality and the smoking interestingness of the cigarettes are remarkably improved, and the small green orange flavor has the effects of regulating qi, invigorating stomach, eliminating phlegm, moistening throat, refreshing, reducing cigarette harm and the like, so that the small green orange flavor has relatively good application value and popularization and application significance for design, development, production and sale of the bead blasting cigarettes.
Detailed Description
The present invention is further illustrated by the following examples. Before describing the specific embodiments, the process for preparing the cigarette blasting beads described in the following embodiments will be briefly described as follows.
The main preparation process of the cigarette blasting bead in the prior art is as follows:
the mainstream technology of the bead blasting production mainly adopts a split-flow method-liquid mid-point drop method preparation process to carry out production, namely, a rubber column is cut off by utilizing the shearing force of the counter punching of cooling oil, and the bead blasting and drop preparation is finished; specifically, the method comprises the following steps: firstly, utilizing two cooling oils with different incident angles to form shearing force in a solenoid, cutting off wall materials and core liquid in the dripping process, finally condensing the wall materials and the core liquid into balls in the cooling oil under the action of surface tension, and then preparing the final finished product blasting balls after procedures of deoiling, drying, screening and the like; the method is adopted to finish the processing of the bead blasting prepared in the following embodiments by Shanghai Huabao Biotech Co., Ltd;
it should also be noted that the materials used in the following examples: butanedione, ethyl vanillin, methyl cinnamate, geraniol, sweet orange oil, caprylic capric glyceride and the like are also products of Shanghai Huabao Biotech Co., Ltd;
the small green citrus is a tea prepared by selecting immature citrus young fruits and Yunnan Pu' er tea as raw materials, and the small green citrus is randomly purchased by a company of Xinhui, Guangdong.
The extract of ponkan used in the following examples was prepared as follows:
(1) crushing the dried small green oranges, and sieving the crushed small green oranges by a 50-mesh sieve to prepare small green orange powder;
(2) adding an ethanol solution with the volume fraction of 75% into the small green tangerine powder obtained in the step (1), and carrying out hot reflux for 4h in water bath at 70 ℃; the material-liquid ratio of the minor green tangerine powder to the ethanol solution is as follows: ethanol =1 g: 5 mL;
(3) and (3) concentrating the hot reflux liquid in the step (2) under reduced pressure at 60 ℃ and 70Kpa until the volume is unchanged, and obtaining the extract, namely the ponkan extract.
Example 1
The ponkan essence for cigarette bead blasting in the embodiment comprises the following components in percentage by mass:
10% of ponkan extract, 1.0% of butanedione, 0.3% of ethyl vanillin, 0.5% of methyl cinnamate, 0.2% of geraniol, 1.0% of sweet orange oil and 87.0% of caprylic/capric glyceride.
The small green citrus flavor essence is prepared into cigarette bead blasting with the diameter of 3.65mm and the weight of 23 mg/bead, and the content of the essence in the bead blasting is 23 mu L/bead, namely the small green citrus flavor cigarette bead blasting.
According to the existing filter stick production process, the bead blasting machine is used for placing the bead blasting machine in the center of a filter stick and adding the bead blasting machine into a cigarette filter stick with a common circumference (24.3 mm), the bead blasting position is 12.5mm away from the lip end, one bead blasting machine is added to each cigarette to obtain a bead blasting filter stick, and the filter stick is rolled and connected with a cigarette sample to obtain the minor green citrus flavor bead blasting cigarette.
For the prepared small green citrus flavor bead-exploded cigarettes, 7 professional sensory evaluation personnel perform detection and comparative smoking evaluation on the samples and the blank cigarette samples (blank bead-exploded samples are added at the same positions) of the control example.
Smoke detection and specific puff score see subsequent tables.
The smoking evaluation results show that 7 cigarette evaluation personnel consistently think that after the bead blasting of the citrus reticulata blanco flavored cigarette is added, the aroma of the citrus reticulata blanco flavor of the cigarette sample is obvious, the aroma richness of the smoke is improved to a certain extent, the feeling of fresh sweet aroma and scorched sweet aroma is enhanced, the sweet return feeling is realized, the irritation is reduced, the miscellaneous gas is reduced, the smoke fineness is improved, and the aftertaste is improved.
Example 2
The ponkan essence for cigarette bead blasting in the embodiment comprises the following components in percentage by mass:
12% of ponkan extract, 1.5% of butanedione, 0.4% of ethyl vanillin, 0.7% of methyl cinnamate, 0.35% of geraniol, 1.5% of sweet orange oil and 83.55% of caprylic capric glyceride.
The small green citrus flavor essence is prepared into cigarette bead blasting with the diameter of 3.65mm and the weight of 23 mg/bead, and the content of the essence in the bead blasting is 23 mu L/bead, namely the small green citrus flavor cigarette bead blasting.
According to the existing filter stick production process, the bead blasting machine is used for placing the bead blasting machine in the center of a filter stick and adding the bead blasting machine into a common (circumference 24.3 mm) cigarette filter stick, the bead blasting position is 12.5mm away from the lip end, one bead blasting machine is added to each cigarette to obtain a bead blasting filter stick, and the filter stick is rolled and connected with a cigarette sample to obtain the minor green citrus flavor bead blasting cigarette.
For the prepared small green citrus flavor bead-exploded cigarettes, 7 professional sensory evaluation personnel perform detection and comparative smoking evaluation on the samples and the blank cigarette samples (blank bead-exploded samples are added at the same positions) of the control example.
Smoke detection and specific puff score see subsequent tables.
The smoking evaluation results show that 7 cigarette evaluation personnel consistently think that after the bead blasting of the citrus reticulata blanco flavored cigarette is added, the 'citrus reticulata flavor' of the cigarette sample is obvious, the richness of the smoke is obviously increased, the feeling of sweet and fresh taste and burnt sweet taste is obviously enhanced, the back sweet feeling is obvious, the irritation is obviously reduced, the offensive odor is reduced, the fineness of the smoke is obviously improved, and the aftertaste is obviously improved.
Example 3
The ponkan essence for cigarette bead blasting in the embodiment comprises the following components in percentage by mass:
15% of ponkan extract, 2.0% of butanedione, 0.6% of ethyl vanillin, 1.0% of methyl cinnamate, 0.5% of geraniol, 2.0% of sweet orange oil and 78.9% of caprylic capric glyceride.
The small green citrus flavor essence is prepared into cigarette bead blasting with the diameter of 3.65mm and the weight of 23 mg/bead, and the content of the essence in the bead blasting is 23 mu L/bead, namely the small green citrus flavor cigarette bead blasting.
According to the existing filter stick production process, the bead blasting machine is used for placing the bead blasting machine in the center of a filter stick and adding the bead blasting machine into a common (circumference 24.3 mm) cigarette filter stick, the bead blasting position is 12.5mm away from the lip end, one bead blasting machine is added to each cigarette to obtain a bead blasting filter stick, and the filter stick is rolled and connected with a cigarette sample to obtain the minor green citrus flavor bead blasting cigarette.
For the prepared small green citrus flavor bead-exploded cigarettes, 7 professional sensory evaluation personnel perform detection and comparative smoking evaluation on the samples and the blank cigarette samples (blank bead-exploded samples are added at the same positions) of the control example.
Smoke detection and specific puff score see subsequent tables.
The smoking evaluation results show that 7 cigarette evaluation personnel consistently think that after the bead blasting of the citrus reticulata blanco cigarette is added, the 'citrus reticulata blanco' fragrance of the cigarette sample is very obvious, the coordination of the smoke fragrance is reduced, the irritation is increased, the offensive odor is reduced, the smoke coordination is poor, the cigarette has uncomfortable sweet and greasy feeling, and the aftertaste is inferior to that of a normal cigarette (a control cigarette).
The bead blasting products prepared in different embodiments are detected, meanwhile, the cigarettes prepared in the embodiments are subjected to conventional detection, so that the physicochemical indexes of an acetate fiber tow sample, the physical indexes of a filter stick sample and the physicochemical indexes of the cigarette sample in the cigarette sample are measured, in addition, the indexes of total particulate matter, tar, nicotine, moisture and the like in the main stream smoke of the cigarettes are measured according to the method of measuring the total particulate matter and the tar by a smoking machine for conventional analysis of GB/T19609-2004 cigarettes, and the specific results are shown in the following table.
Table 1, test results of the exploded beads prepared in the different examples:
table 2, test results of filter rods containing exploded beads prepared in different examples:
table 3, physical indexes and mainstream smoke detection results for different cigarette samples:
as can be seen from the data in the table 2, compared with the normal acetate fiber tow filter stick, the physical indexes of the filter stick for placing the small green orange exploded beads have no obvious difference, and the pressure drop of the filter stick is obviously changed. As can be seen from the data in Table 3, the mainstream smoke of the small green orange flavor bead-exploded cigarette is changed compared with the normal cigarette of the control example, but after bead-explosion and pinching, the key indexes of tar and nicotine which influence the cigarette sense are not obviously changed.
Table 4, sensory quality evaluation results for different cigarette samples:
as can be seen from the results in Table 4, the sensory quality of the cigarettes can be remarkably improved by using the small green citrus blasting beads, the sensory score can be improved by 1.15 minutes to the maximum, the aroma is remarkably improved, the aftertaste is improved, and the irritation and the offensive odor are also greatly reduced.
In conclusion, after the formula of the bead blasting with specific fragrance is designed in a targeted manner and applied to cigarettes, the fragrance characteristics of the cigarettes during smoking can be obviously improved, smoking feeling is enriched and improved, and meanwhile, the harm of the cigarettes can be reduced due to the special effect of the small green oranges. Therefore, the puffed bead of the small green orange can highlight the fragrance of the small green orange in the cigarette, improve the smoking quality and reduce the harm of the cigarette, and has certain popularization and application values in the industry.
It should be emphasized that the above formula of popping beads is designed for improving cigarettes with conventional formula, and has good application effect when applied to fine cigarettes, but the specification of popping beads and the addition amount in the filter stick need to be properly adjusted according to the specific tobacco formula and design requirements, and will not be described in detail herein.
Claims (6)
1. The ponkan essence for bead blasting of cigarettes is characterized by comprising the following components in percentage by mass:
10.0-15.0% of an extract of ponkan, 1.0-2.0% of butanedione, 0.3-0.6% of ethyl vanillin, 0.5-1.0% of methyl cinnamate, 0.2-0.5% of geraniol, 1.0-2.0% of sweet orange oil and 78.9-87.0% of caprylic capric glyceride;
the ponkan extract is an ethanol extract of the ponkan; the preparation method specifically comprises the following steps:
(1) crushing the dried small green oranges, and sieving the crushed small green oranges by a sieve of 40-60 meshes to prepare small green orange powder;
the small green citrus is tea prepared from immature citrus young fruits and Yunnan Pu' er tea serving as raw materials in the Xinhui area of Guangdong;
(2) adding an ethanol solution with the volume fraction of 60-90% into the small green citrus powder obtained in the step (1), and carrying out hot reflux for 3-5 h in water bath at the temperature of 60-80 ℃; the material-liquid ratio of the minor green tangerine powder to the ethanol solution is as follows: ethanol =1 g: 4-6 mL;
(3) and (3) concentrating the hot reflux liquid in the step (2) under reduced pressure at 55-65 ℃ and 60-80 Kpa until the volume is unchanged, and obtaining the extract, namely the ponkan extract.
2. The ponkan flavor for cigarette blasting according to claim 1, which comprises the following components in percentage by mass:
12% of ponkan extract, 1.5% of butanedione, 0.4% of ethyl vanillin, 0.7% of methyl cinnamate, 0.35% of geraniol, 1.5% of sweet orange oil and 83.55% of caprylic capric glyceride;
or the following steps:
10% of ponkan extract, 1.0% of butanedione, 0.3% of ethyl vanillin, 0.5% of methyl cinnamate, 0.2% of geraniol, 1.0% of sweet orange oil and 87.0% of caprylic capric glyceride;
or the following steps:
15% of ponkan extract, 2.0% of butanedione, 0.6% of ethyl vanillin, 1.0% of methyl cinnamate, 0.5% of geraniol, 2.0% of sweet orange oil and 78.9% of caprylic capric glyceride.
3. The minor green citrus flavor cigarette bead blasting for cigarette bead blasting according to claim 1, wherein the diameter of the bead blasting is 2.0-4.0 mm, and the content of the flavor in the bead blasting is 20-25 μ L/bead.
4. The accelerated beading of Citrus reticulata blanco flavor cigarette of claim 3, wherein the diameter of the accelerated beading is 3.65mm, the weight of the accelerated beading is 23 mg/grain, and the content of the essence in the accelerated beading is 23 μ L/grain.
5. The use of the ponkan-flavored cigarette bead blasting of claim 3 in a cigarette, wherein the cigarette bead blasting is added to a filter rod.
6. The use of the ponkan flavor cigarette blasting beads in cigarettes according to claim 5, wherein the cigarette blasting beads are located in the middle of a filter rod, and one blasting bead is added to each cigarette filter rod.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710288573.2A CN106987314B (en) | 2017-04-27 | 2017-04-27 | Citrus reticulata flavor essence for bead blasting of cigarettes and application of citrus reticulata flavor essence in cigarettes |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710288573.2A CN106987314B (en) | 2017-04-27 | 2017-04-27 | Citrus reticulata flavor essence for bead blasting of cigarettes and application of citrus reticulata flavor essence in cigarettes |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN106987314A CN106987314A (en) | 2017-07-28 |
| CN106987314B true CN106987314B (en) | 2021-01-08 |
Family
ID=59418813
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201710288573.2A Active CN106987314B (en) | 2017-04-27 | 2017-04-27 | Citrus reticulata flavor essence for bead blasting of cigarettes and application of citrus reticulata flavor essence in cigarettes |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN106987314B (en) |
Families Citing this family (11)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110574962B (en) * | 2018-06-08 | 2023-06-13 | 湖南中烟工业有限责任公司 | Preparation method of tea-flavored essence for cigarettes and cigarette explosion beads and explosion bead cigarettes |
| CN109043755A (en) * | 2018-08-29 | 2018-12-21 | 台山市精工源木制品有限公司 | A kind of preparation method and applications of the portable small green mandarin orange of arousing brain, raising spirit |
| CN109393571A (en) * | 2018-11-14 | 2019-03-01 | 湖北中烟工业有限责任公司 | Orange sweet wine taste essence and preparation method thereof for electric heating low temperature cigarette filter stick |
| CN109602081A (en) * | 2019-01-11 | 2019-04-12 | 广西中烟工业有限责任公司 | A kind of shatian pomelo cigarette quick-fried pearl essence and its application in cigarette |
| CN109868185A (en) * | 2019-01-31 | 2019-06-11 | 广西中烟工业有限责任公司 | A kind of faenum graecum cigarette quick-fried pearl essence and its application in cigarette |
| CN109868184A (en) * | 2019-01-31 | 2019-06-11 | 广西中烟工业有限责任公司 | A kind of Radix Glycyrrhizae cigarette quick-fried pearl essence and its application in cigarette |
| CN109965045A (en) * | 2019-03-20 | 2019-07-05 | 福建绿色黄金生物科技有限公司 | One grows tea and green mandarin orange composition, preparation method and applications |
| CN110819457B (en) * | 2019-12-09 | 2023-03-31 | 将军烟草集团有限公司 | Sweet tea flavor with blasting beads and preparation method and application thereof |
| CN110819456A (en) * | 2019-12-09 | 2020-02-21 | 将军烟草集团有限公司 | Green lemon essence for bead blasting and application of green lemon essence in cigarettes |
| CN111254015A (en) * | 2020-03-20 | 2020-06-09 | 云南中烟工业有限责任公司 | Pu' er tea essence bead for cigarettes and preparation method thereof |
| CN111961531B (en) * | 2020-09-10 | 2023-09-29 | 将军烟草集团有限公司济南包装材料分公司 | Bead-explosion essence for citrus parviflora and preparation method and application thereof |
Family Cites Families (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US8671951B2 (en) * | 2010-03-26 | 2014-03-18 | Philip Morris Usa Inc. | Methods of manufacturing cigarettes and filter subassemblies with squeezable flavor capsule |
| WO2014005614A1 (en) * | 2012-07-02 | 2014-01-09 | Symrise Ag | A method of flavouring a smoking product |
| CN103584276B (en) * | 2013-11-13 | 2015-05-20 | 川渝中烟工业有限责任公司 | Ambergris cigarette and ambergris spices |
| GB2534210B (en) * | 2015-01-19 | 2017-07-19 | Ngip Res Ltd | Aerosol-generating article |
| CN104804871A (en) * | 2015-04-27 | 2015-07-29 | 湖北中烟工业有限责任公司 | Spicy spice for kretek blasting bead, preparation method and application thereof |
| CN105925376B (en) * | 2016-07-06 | 2019-11-19 | 红塔辽宁烟草有限责任公司 | The essence of the quick-fried pearl of cigarette and its application |
-
2017
- 2017-04-27 CN CN201710288573.2A patent/CN106987314B/en active Active
Also Published As
| Publication number | Publication date |
|---|---|
| CN106987314A (en) | 2017-07-28 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN106987314B (en) | Citrus reticulata flavor essence for bead blasting of cigarettes and application of citrus reticulata flavor essence in cigarettes | |
| CN112656024B (en) | Preparation method of cooling and aroma-enhancing particles for HNB (household Natural gas) cigarettes and cooling and aroma-enhancing particles for HNB cigarettes | |
| CN103054180B (en) | Aromatized composite particle filter stick and production method thereof | |
| CN107034017A (en) | A kind of cigarette quick-fried pearl savory essence of dried orange peel and its application in cigarette | |
| CN103054186B (en) | Chinese medicinal composite particle filter stick and preparation method thereof | |
| CN108576932B (en) | Raw material formula of mixed type flavor cooling and blending section, preparation method thereof and base rod of cigarette without burning during heating | |
| CN108576931B (en) | Raw material formula of flue-cured tobacco flavor cooling and blending section, preparation method thereof and base rod of cigarette without burning during heating | |
| CN110819457B (en) | Sweet tea flavor with blasting beads and preparation method and application thereof | |
| CN109953366B (en) | Cordyceps sinensis extracting solution and preparation method, composition and application thereof | |
| CN106947597B (en) | Pine pollen essence for cigarette bead blasting and application of pine pollen essence in cigarettes | |
| CN115948197B (en) | Preparation method and application of sesame oil | |
| CN107022415B (en) | Semen Scaphii Lychnophori essence for cigarette bead blasting and application thereof in cigarette | |
| CN107177419A (en) | A kind of cigarette quick-fried pearl Momordica grosvenori essence and its application in cigarette | |
| CN103054181A (en) | Coffee or cocoa composite particle filtering bar and manufacturing method thereof | |
| CN111418892A (en) | Cigarette filter stick additive and application thereof | |
| CN107034021A (en) | A kind of cigarette quick-fried pearl savory essence of lily and its application in cigarette | |
| CN106947599A (en) | A kind of cigarette quick-fried pearl HERBA DENDROBII essence and its application in cigarette | |
| CN107418730B (en) | Kumquat flavor essence for bead blasting of cigarettes and application of kumquat flavor essence in cigarettes | |
| CN107822200A (en) | A kind of herbal tea essence for cigarette with quick-fried pearl | |
| CN103054187B (en) | Spice composite particle filter stick and preparation method thereof | |
| CN110982625A (en) | Licorice-flavored dried beads for cigarette filter tips and preparation method thereof | |
| CN110122921B (en) | Preparation method of black tea puffed beads | |
| CN108542000B (en) | Raw material formula of tobacco shred flavor cooling and flavoring section, preparation method thereof and heating non-combustion cigarette base rod | |
| CN114634841B (en) | Vitamin milk tea essence, preparation method thereof and cigarette | |
| CN107034016B (en) | Raspberry essence for cigarette bead blasting and application of raspberry essence in cigarettes |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| GR01 | Patent grant | ||
| GR01 | Patent grant |